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Study of Integer Spin S = 1 in the Polar Magnet β-Ni(IO3)2
PublicationPolar magnetic materials exhibiting appreciable asymmetric exchange interactions can potentially host new topological states of matter such as vortex-like spin textures; however, realizations have been mostly limited to half-integer spins due to rare numbers of integer spin systems with broken spatial inversion lattice symmetries. Here, we studied the structure and magnetic properties of the S = 1 integer spin polar magnet β-Ni(IO3)2...
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Modeling of Passive and Forced Convection Heat Transfer in Channels with Rib Turbulators
PublicationThe main goal of the research presented in this paper was the experimental and numerical analysis of heat enhancement and aerodynamic phenomena during air flow in a channel equipped with flow turbulators in the form of properly configured ribs. The use of ribs intensifies the heat transfer and at the same time increases not only the flow resistance but also the energy costs. Therefore, designing modern heat exchangers with optimal...
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Adenocarcinoma, metastatic, NOS - Female, 76 - Tissue image [4080730010648401]
Open Research DataThis is the histopathological image of BRONCHUS AND LUNG tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: VS200 Olympus slide scanner (20x magnification) and saved to DICOM format.
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Adenocarcinoma, metastatic, NOS - Female, 76 - Tissue image [4080730010644561]
Open Research DataThis is the histopathological image of BRONCHUS AND LUNG tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: VS200 Olympus slide scanner (20x magnification) and saved to DICOM format.
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Adenocarcinoma, metastatic, NOS - Female, 76 - Tissue image [4080730010642231]
Open Research DataThis is the histopathological image of BRONCHUS AND LUNG tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: VS200 Olympus slide scanner (20x magnification) and saved to DICOM format.
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Adenocarcinoma, metastatic, NOS - Female, 76 - Tissue image [4080730010642141]
Open Research DataThis is the histopathological image of BRONCHUS AND LUNG tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: VS200 Olympus slide scanner (20x magnification) and saved to DICOM format.
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Adenocarcinoma, metastatic, NOS - Female, 76 - Tissue image [4080730010647871]
Open Research DataThis is the histopathological image of BRONCHUS AND LUNG tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: VS200 Olympus slide scanner (20x magnification) and saved to DICOM format.
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Adenocarcinoma, metastatic, NOS - Female, 76 - Tissue image [4080730010646921]
Open Research DataThis is the histopathological image of BRONCHUS AND LUNG tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: VS200 Olympus slide scanner (20x magnification) and saved to DICOM format.
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Measurements of ultrasonic bulk and guided wave propagation in additively manufactured cubes and plates obtained by ultrasonic pulse velocity analyzer and scanning laser vibrometry
Open Research DataThe DataSet contains the results of measurements of ultrasonic wave propagation in additively manufactured samples made of polylactic acid (PLA). Three types of raster angles in two consecutive layers were assumed: 0°/90° (#1), 45°/-45° (#2) and 90°/90° (#3) with respect to the x-axis. For each printing variants a cubic sample (#C1-3) with dimensions...
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Enantiomeric Resolution of N,N'-Dimethyldithiodianthranilide through Diastereomeric silver(I) complex. Chiroptical spectra, racemization barrier and molecular self-assembly
PublicationN,N'-dimetyloditiodiantranilid, związek o chiralności płaszczyznowej, rozdzielono na enancjomery. Optycznie czynne molekuły uzyskano w wyniku tworzenia chiralnego kompleksu N,N'-dimetyloditiodiantranilidu z solą srebrową kwasu (1S)-kamforosulfonowego. W oparciu o badania rentgenostrukturalne monokryształu uzyskanego kompleksu określono absolutną konfigurację przykoordynowanego ligandu jako (R). Enancjomery N,N'-dimetyloditiodiantranilid...
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Piotr Konieczka prof. dr hab. inż.
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Zastosowanie nowatorskich materiałów geosyntetycznych w konstrukcjach oporowych z gruntu zbrojonego
PublicationArtykuł prezentuje metodę projektowania stromych skarp wznoszonych z gruntów słabo przepuszczalnych, zbrojonych geosiatkami drenującymi. Z analiz przeprowadzonych dla różnej wodoprzepuszczalności gruntu i różnej geometrii skarpy wynika, że pionowy rozstaw i długość zbrojenia mają istotne znaczenie dla stateczności skarpy. Dla gruntów słabo przepuszczalnych, o typowych wartościach współczynników ściśliwości objętościowej oraz konsolidacji,...
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The theoretical description of friction force in bio-joints as function of cartilage roughness
PublicationWartości sił tarcia w naturalnych stawach człowieka a szczególnie w endoprotezach stawu biodrowego rzutują na proces zużywania się powierzchni stawowych. Dlatego problem wyznaczania sił tarcia w biołożyskach jest bardzo istotny. W trakcie chodzenia mamy co najmniej ruch sferycznej powierzchni głowy w dwóch różnych kierunkach dla naturalnych i sztucznych stawów biodrowych człowieka. Dlatego też siły tarcia występują co najmniej...
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Paid work activity and entrepreneurial cognitions of students – evidence from European emerging economies
PublicationPurpose – This paper aims to investigate whether paid work activity (PWA) experience of students from five emerging economies is related to academic results and self-assessment of possessed entrepreneurial traits. Additionally, the authors verify the relationship between obtaining work experience and the willingness to start own business among students. Design/methodology/approach – Participants included 3,631 students of the first...
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Synthesis, structural and spectroscopic properties of asymmetric schiff bases derived from 2,3-diaminopyridine
PublicationTwo Schiff base derivatives, 4-(2-amino-3-pyridyliminomethyl)phenol (I) and 3-(2-amino-3- pyridyliminomethyl)nitrobenzene (II ), were synthesised and characterised by spectroscopy. The structure of I was determined by single crystal X-ray diffraction studies. The asymmetric Schiff base derived from 2,3-diaminopyridine selectively recognise transition and heavy metal cations, and some anion. Ligands I and II form stable complexes...
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The effect of morphology and crystalline structure of Mo/MoO3 layers on photocatalytic degradation of water organic pollutants
PublicationMolybdenum oxide layers were formed by anodization of the Mo metallic foil in a water/ethylene glycol-based electrolyte containing fluoride ions. The as-prepared, amorphous samples were annealed in air at different temperatures in a range from 100 �C to 700 �C. The crystal phase and morphology of anodized and annealed MoO3 layers were investigated using X-ray diffraction, Raman spectroscopy, and scanning electron microscopy. The...
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The Quaternization Reaction of 5-O-Sulfonates of Methyl 2,3-o-Isopropylidene-β-D-Ribofuranoside with Selected Heterocyclic and Aliphatic Amines
PublicationThe synthesis of N-((methyl 5-deoxy-2,3-O-isopropylidene-β-D-ribofuranoside)-5-yl) ammonium salts are presented. To determine the effect of the nucleophile type and outgoing group on the quaternization reaction, selected aliphatic and heterocyclic aromatic amines reacted with: methyl 2,3-O-isopropylidene-5-O-tosyl-β-D-ribofuranoside or methyl 2,3-O-isopropylidene-5-O-mesyl-β-D -ribofuranoside or methyl 2,3-O-isopropylidene-5-O-triflyl-β-D-ribofuranoside...
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Atom-economic thiophosphoroselenenylations of C–H acid esters and amides
PublicationThree improved thiophosphoroselenenylation procedures of CHacids, including derivatives of malonic and acetyl-, phosphono-, 4-nitrophenyl- and 3-pyridylacetic acids, have been described and compared to previously reported thiophosphoroselenylation of diethyl malonate using bis(disopropoxyphosphinothioyl)diselenide alone or with the aid of methyl iodide. The use of iodine makes it possible to utilize both equivalents of the selenenylating...
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Production and Properties of the Porous Layer Obtained by the Electrochemical Method on the Surface of Austenitic Steel
Publication: The growing demand for implants has seen increasing interest in the introduction of new technologies and surface modification methods of metal biomaterials. This research aimed to produce and characterize a porous layer grown on austenitic stainless steel 316L, obtained via the anodization process near the micro-arc oxidation, i.e., low voltage micro-arc oxidation (LVMAO). The discussed layer significantly influences the properties...
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MgPdSb─An Electron-Deficient Half-Heusler Phase
PublicationThe half-Heusler family consists of many semiconducting intermetallic compounds, virtually all of them having a valence electron count (VEC) of 18. We have studied an electron-deficient (VEC = 17) phase MgPdSb and its Pd-stuffed variant MgPd1.25Sb. The cubic F4̅3m crystal structure was confirmed by the Rietveld refinement of powder X-ray diffraction (XRD) data. The lattice parameter is a = 6.284 and 6.335 Å for MgPdSb and MgPd1.25Sb,...
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Nutrient recovery from deammonification effluent in a pilot study using two-step reject water treatment technology
PublicationThe aim of this study was to assess the possibility of phosphorus and nitrogen recovery from the liquid fraction of digestates (reject water) pilot study using a two-step technology, where the precipitation of biogenic compounds in the form of magnesium ammonium phosphate (struvite) will be preceded by a deammonification process. The tests confirmed the possibility of nutrient recovery from deammonification effluent. A removal...
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Morphology control via dual solvent crystallization for high-mobility functionalized pentacene-blend thin film transistors
PublicationWe present an approach to improving the performance of solution processed organic semiconductor transistors based on a dual solvent system. We here apply this to a blend containing the π-conjugated small molecule 6,13 bis(triisopropylsilylethynyl) pentacene (TIPS-pentacene) and polystyrene, which acts as an inert binder. Using a semiconductor-binder solution of two solvents, where the main solvent is a better solvent of the small...
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Syntheses and structures of the first terminal phosphanylphosphido complex of hafnium [cp2hf(cl){η1-(me3si)p-p(net2)2}] and the firstzirconocene-phosphanylphosphinidene dimer [cp2zr{μ2-p-p(net2)2}2zrcp2]
PublicationReactions of (Et2N)2P-P(SiMe3)Li with [Cp2MCl2] (M= Zr, Hf) in toluene or pentane yield the related terminal phosphanylphosphido complexes [Cp2M(Cl){η1-(Me3Si)P-P(NEt2)2}]. The solid statestructure of [Cp2Hf(Cl){η1-(Me3Si)P-P(NEt2)2}] was established by single crystal X-ray diffraction. The reaction of (Et2N)2P-P(SiMe3)Li with [Cp2ZrCl2] in THF or DME solutions leads to the formationof deep red crystals of the first neutral diamagnetic...
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Bis(ammonium) Zoledronate Dihydrate
PublicationNeutralization of 2-(1-imidazole)-1-hydroxyl-1,1`-ethylidenediphosphonic acid (zoledronic acid) by an excess of ammonia yielded bis(ammonium) zoledronate dihydrate, {C5H8N2O7P2 2−, 2(H4N+), 2(H2O)}. The product is readily soluble in water and forms monocrystals for which the X-ray structural analysis was carried out. The zoledronic anion is of double negative charge due to deprotonation of three P–OH groups and protonation of the...
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Superconductivity and itinerant ferromagnetism of Y9Co7 probed by ac susceptibility
PublicationThe ac magnetic susceptibility of a single crystal sample of the compound Y9Co7 has been measured in applied dc fields ranging from 0–6.7 kOe by utilizing a tunnel diode resonator circuit. In agreement with previous measurements on this material, a superconducting transition has been observed to occur at TSC ≈ 2.5 K. A broad maximum has been observed in the zero field susceptibility measurements from 2.5 K < T < 8 K and its behavior...
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Copper-based 2D-coordination polymer as catalyst for allylation of aldehydes
PublicationA copper-tartrate, [Cu2(Tart)2(H2O)2]·4H2O, was synthesized at room temperature in aqueous media using copper chloride and D-tartaric acid. The compound crystallizes in the monoclinic system P21 space group and was characterized by infrared spectroscopy, thermogravimetry, X-ray powder diffraction and the results are in good agreement with the single crystal...
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Influence of controlled crystallization and SrF2 content on the structure and properties of Eu3+ doped phosphate glasses
PublicationNew phosphate glasses and glass-ceramics P2O5–Bi2O3–K2O–Nb2O5-SrF2 doped with Eu were synthesized and studied in this work. The influence of the SrF2 content (0–15 mol%) and the parameters of the heat treatment on their structural and optical properties were investigated. For the above purpose, the structural characterization by FTIR spectroscopy and XRD measurements was carried out, which showed a significant effect of SrF2 on...
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Present state of sewage and wastewater treatment plants in the polish coast of Baltic sea.
PublicationW pracy przedstawiono stan gospodarki ściekowej w czterech strefach polskiego wybrzeża Bałtyku: Zalewu Wiślanego, Zatoki Gdańskiej z Zatoką Pucką, strefy otwartego morza oraz Zalewu Szczecińskiego. Wymienione strefy scharakteryzowano pod względem hydrologicznym oraz przedstawiono charakterystykę i efektywność pracy oczyszczalni ścieków zlokalizowanych na terenie każdej z nich. Ponadto, oszacowano inne, istotnie ważne źródła zanieczyszczeń...
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Zespół Fizyki Ciała Stałego
Research TeamsTematyka badawcza Katedry Fizyki Ciała Stałego obejmuje wytwarzanie i badanie materiałów dla energetyki (m.in. nanostruktury, sensory) o innowacyjnych właściwościach fizyko-chemicznych, tj: * kryształy, polikryształy, ceramika, szkło * materiały objętościowe, cienkie warstwy, nanomateriały * materiały metaliczne, półprzewodnikowe, nadprzewodnikowe, izolatory Tematyka badawcza obejmuje również badania symulacyjne i obliczeniowe...
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Predicting the critical micelle concentration of aqueous solutions of ionic liquids and other ionic surfactants
PublicationNiektóre ciecze jonowe, szczególnie te będące kombinacją organicznego i nieorganicznego jonu, wykazują strukturalne podobieństwo do surfaktantów. Krytyczne stężenie micelizacji jest podstawowym parametrem w chemii powierzchni i nauce o koloidach. Parametr ten został zmierzony dla wielu cieczy jonowych, jednakże ze względu na ogromną ilość możliwych kombinacji anionów i kationów jego eksperymentalny pomiar dla wszystkich struktur...
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Współczesne problemy i i kierunki rozwoju elastycznych systemów produkcyjnych
PublicationPrzedstawione opracowanie monograficzne poświęcone jest współczesnej problematyce elastycznych systemów produkcyjnych, a w szczególności ich zagadnieniom sterowania i wytwarzania. Zawarto w nim także charakterystykę najbardziej zaawansowanych technologii informatycznych; dokonano klasyfikacji ich metod oraz podstawowych problemów metodologicznych ich projektowania w zakresie planowania, sterowania i wytwarzania. Praca obejmuje...
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Modelowanie procesu wysychania filmu cieczowego na ściance
PublicationZaprezentowany w pracy teoretyczny model kryzysu wrzenia przy wysokich stopniach suchości jest modyfikacją wcześniejszej wersji przedstawionej przez Sedlera i Mikielewicza (1981). Model używany do analizy procesu wysychania filmu cieczowego na ściance, pozwala także na sformułowanie równań bilansu masy cieczy w filmie i w rdzeniu. Rozwiązanie układu równań zawiera parametry, które wyznaczane są eksperymentalnie. W niniejszej pracy...
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Strontium-based nanosized phosphates as anticorrosive fi llers of epoxy and polyurethane coating compositions
PublicationAnticorrosive epoxy and polyurethane coatings were compounded using zinc-free nanosized phosphates of strontium (SP) or strontium and aluminum (SAP). For comparison, a nanosized calcium aluminum ammonium phosphate (CAP) and a microsized zinc phosphate (ZP) were tested. Results of salts spray and cyclic corrosion tests revealed better anticorrosive properties of the SAP-based coatings...
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The mechanical properties and bactericidal degradation effectiveness of tannic acid-based thin films for wound care
PublicationThe surface area is the most important aspect when considering the interactions between a material and the surrounding environment. Chitosan (CTS) and tannic acid (TA) were previously successfully tested by us to obtain thin films to serve as wound dressings or food packaging materials. However, surface properties as well as the antimicrobial activity of the material were not considered. They are important if the material is likely...
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Peptide dendrimers as antifungal agents and carriers for potential antifungal agent—N3‐(4‐methoxyfumaroyl)‐(S)‐2,3‐ diaminopropanoic acid—synthesis and antimicrobial activity
PublicationA series of peptide dendrimers and their conjugates with antimicrobial agent FMDP (N3‐(4‐methoxyfumaroyl)‐(S)‐2,3‐diamino‐propanoic acid) were synthesized. The obtained compounds were tested for the antibacterial and antifungal activity. All novel dendrimers displayed much better activity against the tested strains than FMDP itself. Moreover, their conjugates with FMDP also exhibited antimicrobial activity. The most promising molecules...
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New Tetragonal ReGa5(M) (M = Sn, Pb, Bi) Single Crystals Grown from Delicate Electrons Changing
PublicationSingle crystals of the new Ga-rich phases ReGa~5(Sn), ReGa~5(Pb) and ReGa~5(Bi) were successfully obtained from the flux method. The new tetragonal phases crystallize in the space group P4/mnc (No. 128) with vertex-sharing capped Re2@Ga14 oblong chains. Vacancies were discovered on the Ga4 and Ga5 sites, which can be understood as the direct inclusion of elemental Sn, Pb and Bi into the structure. Heat capacity measurements were...
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Biomasa
PublicationPraca przedstawia aktualny stan prawny w Polsce dotyczący biomasy, w szczególności jej prawne definicje zawarte w różnych aktach prawnych. Przedstawiono również właściwości opałowe biomasy. Zgodnie z danymi GUS w roku 2011 ze źródeł odnawialnych pozyskano 312.828 TJ (1012J), co stanowi 10,9% ogólnej ilości wyprodukowanej energii, a w 2012 r. 356.070 TJ co stanowi 11,7% ogólnej ilości pozyskanej energii. Najwięcej energii odnawialnej...
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Niepewność dopasowania funkcji liniowej i logarytmicznej do punktów pomiarowych przy wyznaczaniu przewodności cieplnej materiałów
PublicationWyznaczanie właściwości cieplnych różnych materiałów budowlanych stanowią dziedzinę wiedzy ważną do analizy problemów związanych z wymianą ciepła w technice. Dla cenienia wielkości przewodzenia ciepła bardzo istotne znaczenie mają badania pozwalające na doświadczalne wyznaczenie wartości współczynnika przewodności cieplnej Znajomość tego współczynnika dla różnego rodzaju materiałów jest ważna w praktyce inżynierskiej, a także...
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Dzieła inżynierii w krajobrazie delty Wisły
PublicationOmówiono przeobrażenia historyczne układu hydrologicznego delty Wisły od Cypla Mątowskiego do kolejnych ujść: pierwotnie naturalnego w Wisłoujściu później w Gdańsku - Nowym Porcie, naturalnego w Gdańsku Górkach z 1840 r. oraz sztucznego w Gdańsku - Świbnie z 1895 r. Zaprezentowano budowle hydrotechniczne w Białej Górze, Piekle (relikt), Gdańskiej Głowie, Gdańsku-Przegalinie oraz przepompownie i przepusty wałowe na Nizinie Walichnowskiej....
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A review on electrospun membranes for potential air filtration application
PublicationAir pollution is one of the major environmental concerns in most highly populated cities, which is typically caused by particulate (PM2.5 and PM0.1) or gaseous pollutants that can be removed using electrospun membranes. These membranes are characterized by different features in terms of uniform and controllable structure, tuneable porosity, and high surface area, where their separation efficiency strongly depends on their properties....
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A structural study of the hydrated and the dimethylsulfoxide, N, N´-dimet-hylpropyleneurea, acetonitryle, pyridine and N,N-dimethylthioformamide solvated nickel(II) ion in solution and solid state.
PublicationOznaczono strukturę w stanie stałym i ciekłym solwatowanego jonu niklu(II) w rozpuszczalnikach o różnych właściwościach donorowych: w wodzie, dimetylo-sulfotlenku, N,N`-dimetylopropylomoczniku, acetonitrylu, pirydynie i N,N-di-metylotioformamidzie. Stwierdzono, że nikiel(II) tworzy przede wszystkim sześciokoordynacyjne solwaty (woda, acetonitryl, DMTF). Jako solwat pięciokoordynacyjny istnieje tylko w dimetylopropylomoczniku....
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Wymiana Ciepła,W,Energetyka,sem.04, letni 22/23
e-Learning CoursesKurs elerning do wykładu z Wymiany i Wymienników Ciepła.
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Wymiana Ciepła,L,Energetyka,sem.04, letni 22/23
e-Learning CoursesKurs elerningowy do Laboratorium z Wymiany Ciepła.
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Wymiana ciepła, W, E, sem.4, letni 23/24
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Wymiana ciepła, L, MiBM, sem.5, zimowy 23/24
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Wymiana ciepła, W, MiBM, sem.5, zimowy 23/24
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Wymiana ciepła, L, E, sem.4, letni 23/24
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Non-enzymatic glutathione-mediated conjugation of unsymmetrical bisacridine C-2028 with anticancer activity
Open Research DataThe presented data complement the studies on the interplay between C-2028 (anticancer-active unsymmetrical bisacridine) and the glutathione S-transferase/glutathione (GST/GSH) system.
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Structural features responsible for control of the eukaryotic GlcN-6-P synthase activity
PublicationGlucosamine-6-phosphate (GlcN-6-P) synthase is responsible for catalysis of the first and practically irreversible step in hexosamine metabolism. As UDP-GlcNAc, the final product of the hexosamine path, constitutes one of the essential substrates for assembly of bacterial and fungal cell walls, the enzyme is an interesting target for antimicrobial therapy.The structure of E. coli enzyme, known since 2001, forms a dimer of two identical...
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Zasada działania i charakterystyka impulsów prototypowego lasera femtosekundowego
PublicationW niniejszym artykule zaprezentowano ideę działania prototypowego lasera femtosekundowego przeznaczonego do mikroobróbki materiałów. Laser ten stanowi połączenie oscylatora femtosekundowego na ciele stałym oraz wzmacniacza impulsów femtosekundowych na fotonicznych włóknach światłowodowych o rdzeniu domieszkowanym iterbem. Wykorzystanie femtosekundowych impulsów laserowych w mikroobróbce materiałów oferuje szereg korzyści w stosunku...