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Fe-modified Mn2CuO4 spinel oxides: coatings based on abundant elements for solid oxide cell interconnects
PublikacjaThe current state of the art steel interconnect coating materials are based on critical raw material - Co-oxide spinels. Replacing Co-oxide spinels with alternative, abundant materials can reduce the dependence on the critical raw materials. Cobalt-free coatings with the general formula Mn2-xCuFexO4, where x = 0, 0.1, 0.3, were electrophoretically deposited on a ferritic stainless-steel support and evaluated. Prior to deposition,...
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Multilayer coatings based on cerium oxide and manganese cobaltite spinel for Crofer22APU SOC interconnects
PublikacjaThe current state of the art steel interconnect coating materials are based on critical raw material - Co-oxide spinels. Replacing Co-oxide spinels with alternative, abundant materials can reduce the dependence on the critical raw materials. Cobalt-free coatings with the general formula Mn2-xCuFexO4, where x = 0, 0.1, 0.3, were electrophoretically deposited on a ferritic stainless-steel support and evaluated. Prior to deposition,...
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Enhanced electrochemical performance of partially amorphous La0.6Sr0.4CoO3-δ oxygen electrode materials for low-temperature solid oxide cells operating at 400 °C
PublikacjaThis work evaluates partially amorphous La0.6Sr0.4CoO3-δ (LSC) as a potential oxygen electrode for lowtemperature solid oxide cells. LSC was deposited using the spin-coating technique onto Ce0.8Gd0.2O2-δ (CGO) substrates. The optimal oxygen electrode thickness was determined as 500 nm. The electrochemical impedance spectroscopy (EIS) study showed a significant improvement in oxygen reduction/oxidation reaction kinetics when annealing...
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Microscopic examination of CuNiFeR pipeline
Dane BadawczeCopper and nickel alloys called cunifers (Cu, Ni, Fe and R – rest of alloy elements) have found wide application in the production of ship pipeline components in contact with sea water, such as, for example, the main engine cooling system. These alloys are characterized by a very high corrosion resistance, which is ensured by appropriately carried out...
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Macroscopic examination of CuNiFeR pipeline
Dane BadawczeCopper and nickel alloys called cunifers (Cu, Ni, Fe and R – rest of alloy elements) have found wide application in the production of ship pipeline components in contact with sea water, such as, for example, the main engine cooling system. These alloys are characterized by a very high corrosion resistance, which is ensured by appropriately carried out...
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Formation of High Corrosion Resistant Nanotubular Layers on TitaniumAlloy Ti13Nb13Zr
PublikacjaThis paper presents results of oxidation tests and corrosion investigations of titanium alloy Ti13Nb13Zr performed at different conditions. The oxide layers have been formed by electrochemical method in 2M H3PO4 + 0.3% HF solution for 30 min. and 1 h at 20 V constantvoltage. The corrosion tests have been made by potentiodynamic method in Ringer`s solution at pH ranged between 3 and 7. It has been shown that the nano-oxide films,...
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Formation of High Corrosion Resistant Nanotubular Layers on TitaniumAlloy Ti13Nb13Zr
PublikacjaThis paper presents results of oxidation tests and corrosion investigations of titanium alloy Ti13Nb13Zr performed at different conditions. The oxide layers have been formed by electrochemical method in 2M H3PO4 + 0.3% HF solution for 30 min. and 1 h at 20 V constantvoltage. The corrosion tests have been made by potentiodynamic method in Ringer`s solution at pH ranged between 3 and 7. It has been shown that the nano-oxide films,...
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Possible quadrupole-order-driven commensurate-incommensurate phase transition in B20 CoGe
PublikacjaThe B20-type cobalt germanide CoGe was investigated by measuring the specific heat, resistivity, and 59Co nuclear magnetic resonance (NMR).We observed a phase transition at TQ = 13.7 K, evidenced by a very narrow peak of the specific heat and sharp changes of the nuclear spin-spin (T −1 2 ) and spin-lattice (T −1 1 ) relaxation rates. The fact that the entropy release is extremely small and the Knight shift is almost independent...
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Pre-oxidation of porous ferritic Fe22Cr alloys for lifespan extension at high-temperature
PublikacjaPre-oxidation of porous ferritic Fe22Cr alloys was extensively studied in this paper. Weight gain measurements and SEM analysis revealed that pre-oxidation performed at 900◦C for 40 min increased the lifespan of the alloy. A Cr evaporation study did not disclose any significant influence of the pre-oxidation process on the Cr content in the alloy. For a more detailed assessment, TEM imaging and X-ray tomography measurements of...
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Effect of native air-formed oxidation on the corrosion behavior of AA7075 aluminum alloys
PublikacjaThe microstructure of aluminum alloys plays a key role in their corrosion resistance. In particular, the presence of intermetallic precipitates differing in the potential from the alloy matrix induces local corrosion. The study presents the effect of native air-formed oxidation on the corrosion behavior of AA 7075 aluminum alloy. Various microscopic and spectroscopic techniques were used to examine the changes occurring in the...
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Tensile test of part of CuNiFeR pipeline
Dane BadawczeCopper and nickel alloys called cunifers (Cu, Ni, Fe and R – rest of alloy elements) have found wide application in the production of ship pipeline components in contact with sea water, such as, for example, the main engine cooling system. These alloys are characterized by a very high corrosion resistance, which is ensured by appropriately carried out...
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Scaling of numbers in residue arithmetic with the flexible selection of scaling factor
PublikacjaA scaling technique of numbers in resudue arithmetic with the flexible selection of the scaling factor is presented. The required scaling factor can be selected from the set of moduli products of the Residue Number System (RNS) base. By permutation of moduli of the number system base it is possible to create many auxilliary Mixed-Radix Systems associated with the given RNS with respect to the base, but they have different sets...
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Nonlinear impedance of as-quenched Bi2VO5.5 glass-ceramic was measured with impedance spectroscopy method at low temperature region
Dane BadawczeThe nonlinear electrical properties of as-quenched Bi2VO5.5 glass-ceramic was measured by impedance spectroscopy method.
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Valence state of Manganium in a MnCoO ceramics
Dane BadawczeManganium -cobalt based ceramics materials were produced by solid state reaction and sintred in a furnance in air atmosphere for 20h. Annealing temperature was 600 Celsius degree. For investigations a series of samples, with a various composition was chosen: MnCoO, Mn, Co2O and Mn2CoO. In order to determine valence states of the Mn, X-Ray photoemission...
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Experimental Study on Effectiveness of a Prototype Seismic Isolation System Made of Polymeric Bearings
PublikacjaSeismic isolation is identified as one of the most popular and effective methods of protecting structures under strong dynamic excitations. Base isolators, such as Lead Rubber Bearings, High Damping Rubber Bearings, and Friction Pendulum Bearings, are widely used in practice in many earthquake-prone regions of the world to mitigate structural vibrations, and therefore minimize loss of life and property damage during seismic events....
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Wpływ zawartości grafitu na właściwości mechaniczne warstw hybrydowych Ni-P/Si3N4/grafit osadzonych na stopie AW-7075 metodą redukcji chemicznej.
PublikacjaPrzedstawiono wpływ obecności grafitu jako fazy dyspersyjnej na właściwości mechaniczne warstw hybrydowych Ni-P/Si3N4/grafit, które osadzono metodą redukcji chemicznej na stopie glinu AW-7075. Wykonano badania morfologii powierzchni warstw metodą mikroskopii świetlnej i skaningowej. Dalszą część pracy stanowiły badania mechaniczne, czyli pomiary mikrotwardości warstw oraz ich adhezji do aluminiowego podłoża, a także analizy wpływu...
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Ocena odporności na zużycie ścierne stopów Ti na elementy pary trącej endoprotez stawu kolanowego
PublikacjaNajczęściej stosowanym biomateriałem tytanowym na elementy endoprotez stawu kolanowego jest stop Ti6Al4V. Z uwagi na zawartość wanadu, zaliczanego do pierwiastków o dużej toksyczności podejmowane są działania w kierunku zastąpienia wskazanego stopu - stopami bezwanadowymi. Jednym z najbardziej obiecujących jest stop Ti13Nb13Zr zawierający w swoim składzie jedynie pierwiastki witalne, niewywołujące stanów zapalnych i odczynów...
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Effect of microstructure on mechanical properties of BA1055 bronze castings
PublikacjaThe article presents research results performed on aluminum bronze CuAl10Fe5Ni5 (BA1032) castings used for marine propellers. Metallographic studies were made on light microscope and a scanning electron microscope to assess quantitatively and qualitatively the alloy microstructure. It has been shown that the shape, size and distribution of the iron-rich phase precipitates in bronze microstructure significantly affect its mechanical...
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A remark on singular sets of vector bundle morphisms
PublikacjaIf characteristic classes for two vector bundles over the same base space do not coincide, then the bundles are not isomorphic. We give under rather common assumptions a lower bound on the topological dimension of the set of all points in the base over which a morphism between such bundles is not bijective. Moreover, we show that this set is topologically non-trivial.
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Nonlinear impedance of vanadate glasses containing BaTiO3
Dane BadawczeThe nonlinear impedance of vanadate glasses doped with BaTiO3 was measured. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on a preheated (573...
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Nonlinear impedance of Bi2VO5.5 glass-ceramic annealed at 423 K was measured with impedance spectroscopy method at high temperature region
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic annealed at 423 K was measured by impedance spectroscopy method.
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Non-linear impedance of V2O5 nanorods obtained at 923K
Dane BadawczeThe DataSet contains the non-linear electrical properties of V2O5 nanorods which were measured by the impedance spectroscopy method. V2O5 nanorods were obtained by the sol-gel method. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The precursor powder was pressed into the disk-shaped pellets (12mm in diameter...
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Nonlinear impedance of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured with impedance spectroscopy method at high temperature region
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured by impedance spectroscopy method.
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Nonlinear impedance of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured with impedance spectroscopy method at low temperature region
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured by impedance spectroscopy method.
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3D point cloud as a representation of silo / tank
Dane BadawczeThe product presents a point cloud in the set of coordinates X Y Z. The data was obtained by terrestrial laser scanning and its processing for the analysis of tanks geometry. The development process indicates the possibility to obtain the reliable results useful for the evaluation of the tank side surfaces geometry.
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Reduction of vibrations of steel structure models with Polymeric Bearings - experimental study
PublikacjaEarthquake-induced ground motions are the most severe and unpredictable threats to the structures all around the world. Therefore, designing earthquake protective systems has become an extremely challenging problem in civil engineering. Base isolation is one of the most popular and widely adopted methods of protecting structures against earthquake forces. The present paper reports the results obtained from the shaking table experimental...
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Playback detection using machine learning with spectrogram features approach
PublikacjaThis paper presents 2D image processing approach to playback detection in automatic speaker verification (ASV) systems using spectrograms as speech signal representation. Three feature extraction and classification methods: histograms of oriented gradients (HOG) with support vector machines (SVM), HAAR wavelets with AdaBoost classifier and deep convolutional neural networks (CNN) were compared on different data partitions in respect...
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Experimental investigation of thermal energy storage in shell-and-multi-tube unit with nano-enhanced phase change material
PublikacjaThis paper deals with thermal energy storage with use of nanoparticle enhanced phase change material in shell-and-multitube unit. The experiments are conducted under atmospheric pressure. Paraffin wax and two different fatty acids are used as base phase change material. Graphite and multi-walled carbon nanotubes serve as nanoparticles. Graphite nanoparticles are tested at the concentrations of 0.1%, 1% and 5% by weight, while multi-walled...
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X-ray Photoelectron Spectroscopy of Carboxylic Acids as Corrosion Inhibitors of Aluminium Alloys
PublikacjaThe datasets, titled X-ray Photoelectron Spectroscopy studies of citric acid adsorption on aluminium alloy 5754 in alkaline media and X-ray Photoelectron Spectroscopy studies of various carboxylic acids adsorption on aluminium alloys in alkaline media, contain XPS studies of the corrosion inhibitory action of selected dicarboxylic acids towards commercially available aluminium alloy 5754 in alkaline media at pH=11. These datasets...
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The effect of preliminary creep-strain on material behavior under LCF tension/compression and pure torsion regimes
PublikacjaThis paper presents the results of experimental tests of monotonic tension and torsion, creep-rupture and preliminary creep at 200C and 300C, as well as low-cycle fatigue of 2024 T3511 aluminum alloy. The fatigue process was conducted at room temperature for uniaxial tension/compression and torsion. The as-received material and pre-deformed material were also investigated during creep at elevated temperature. Basic monotonic,...
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Nonlinear impedance of vanadate glass-ceramics containing BaTiO3
Dane BadawczeThe nonlinear impedance of vanadate glasses doped with BaTiO3 was measured. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on a preheated (573...
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EXPERIMENTAL EVALUATION OF DLC/STEEL SLIDING CONTACTS’ OPERATIONAL ENVELOPE
PublikacjaIn an industrial project concerning sliding bearings, a sliding pair was selected of high alloy steel vs. industrial grade DLC coated high alloy steel as a basis for an innovative design of high performance sliding bearings lubricated with a synthetic oil for use in geared transmission units. The development process required credible data on the ultimate resistance of the sliding pair to very high contact stress. An experimental...
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Ferromagnetic nanoparticles imaging by means of Magnetic Force Microscopy
Dane BadawczeFerromagnetic nanoparticles can be used as building blocks for advanced thin film magnets, and can also be used in data storage and biomedical technologies. Nano-crystalline ferrites with the chemical formula NixZn (1 - x) Fe2O4, where x = 0, 0.2, 0.4, 0.6, 0.8, 1.0 show anti-corrosion properties and suppress electromagnetic interference, in the case...
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Impact of Temperature and Nanoparticle Concentration on Turbulent Forced Convective Heat Transfer of Nanofluids
PublikacjaTheoretical analysis of the influence of nanoparticles and temperature on the average Nusselt (Nu) number and the average heat transfer coefficient (HTC) during the turbulent flow of nanofluid in a horizontal, round tube was carried out. The Nu number is a function of the Reynolds (Re) number and the Prandtl (Pr) number, which in turn are functions of the thermophysical properties of the liquid and the flow conditions. On the other...
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Allergic Reactions as a Defense of the Organism to the Influence of Implants Components Made of Stainless Steel
PublikacjaDue to the increasing number of cases of hypersensitivity caused by direct contact with metals, as well as the increasing demand for implants in humans all ages numerous studies on the effects of the impact of implant components are being carried out. The paper presents the phenomenon of etiology of allergy in general terms and in relation to the biomaterials used in medicine. There have been characterized in terms of impact on...
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Allergic reactions as a defense of the organism to the influence of implants components made of stainless steel
PublikacjaDue to the increasing number of cases of hypersensitivity caused by direct contact with metals, as well as the increasing demand for implants in humans all ages numerous studies on the effects of the impact of implant components are being carried out. The paper presents the phenomenon of etiology of allergy in general terms and in relation to the biomaterials used in medicine. There have been characterized in terms of impact on...
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Low temperature deposition of dense MnCo 2 O 4 protective coatings for steel interconnects of solid oxide cells
PublikacjaIn this work manganese cobalt spinel (MnCo2O4) coatings were deposited on steel substrates by spray pyrolysis at 390 °C. This is at much lower temperatures than previously reported (typically in excess of 900 °C). It was possible to produce coatings with well controlled thickness (2-5-10 μm). The as-deposited coatings were evaluated for their microstructural changes and electrical conductivity up to 800 °C. Results confirm the...
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Tetrahedrally modified MnMe0.1Co1.9O4 (Me = Zn, Mg, Li) spinels for non-enzymatic glucose sensing
PublikacjaIn this work, tetrahedrally modified MnMe0.1Co1.9O4 (Me = Zn, Mg, Li) spinels were prepared via the sol–gel synthesis method with subsequent ball-milling fragmentation. The prepared samples were evaluated as glucose–sensing catalyst. The reference MnCo2O4 spinel exhibited a sensitivity of 49 µA mM−1 cm−2 and a nonlinearity error of 5.2% in the response range from 0.02 to 1 mM. The partial substitution of cobalt in the reference...
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Electrophoretic co-deposition of Fe2O3 and Mn1,5Co1,5O4: Processing and oxidation performance of Fe-doped Mn-Co coatings for solid oxide cell interconnects
PublikacjaThe “in-situ” Fe-doping of the manganese cobalt spinel was achieved by electrophoretic co-deposition of Mn1,5Co1,5O4 and Fe2O3 powders followed by a two-step reactive sintering treatment. The effects on the coating properties of two different Fe-doping levels (5 and 10 wt.% respectively) and two different temperatures of the reducing treatment (900 and 1000 °C) are discussed. Samples with Fe-doped coatings demonstrated a lower...
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Nonlinear high temperature impedance of 35P2O5-30Fe2O3-35Nb2O5 glass
Dane BadawczeThe nonlinear high temperature impedance of iron- phosphate glasses doped with niobium oxide was measured. Glass samples of the composition of 35P2O5-30Fe2O3-35Nb2O5 (in %mol) were prepared by the conventional melt quenching technique. Appropriate amounts of reagents ((NH4)2HPO4 (≥99.9%, POCH), Fe2O3 (≥99.9%, POCH) and Nb2O5 (≥99.9%, PLUKA AG) were...
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Nonlinear impedance of 58(2Bi2O3-V2O5)-42SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Dane BadawczeThe nonlinear electrcial properties of 58(2Bi2O3-V2O5)-42SrB4O7 glass was measured by impedance spectroscopy method.
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A Comparison of Empirical Correlations of Viscosity and Thermal Conductivity of Water-Ethylene Glycol-Al2O3 Nanofluids
PublikacjaBecause of their superb thermal conductivity, nanofluids are seen as new generation of cooling mediums in many engineering applications. It is well established that even a small amount of nanoparticles mixed with a base fluid may result in distinct thermal conductivity enhancement. On the other hand, addition of nanoparticles to the base fluid results in its substantial viscosity increase. Therefore, it is very dicult to evaluate...
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Wykorzystanie środowiska ekspertowego do projektowania wybranych podsystemów energetycznych statków
PublikacjaW artykule przedstawiono koncepcję wykorzystania badań symulacyjnych oraz systemu ekspertowego z bazą wiedzy do wspomagania projektowania podsystemów energetycznych statków. Opisano przykładową strukturą steru strumieniowego oraz poszczególne jej elementy składowe.This paper presents a concept of application of simulation investigations and an expert system with a knowledge-base and data-base to improve design procedures of a ship...
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Selection of Electrode Material for Inconel 617/P92 Steel SMAW Dissimilar Welds
PublikacjaThe present work aimed to investigate the microstructure and mechanical properties of the dissimilar shielded metal arc welded (SMAW) joint of Alloy 617 and P92 steel for advanced ultrasupercritical boilers. The SMAW joint was produced using three different types of electrodes, namely, ENiCrFe-3, ENiCrMo-3, and ENiCrCoMo-1. During microstructural observation of the welded joints, no possible cracking was detected in the weldments....
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Fabrication, Microstructure and High Temperature Corrosion Resistance of Porous Alloys for Solid Oxide Fuel Cells
PublikacjaPorous alloys find use in modern Solid Oxide Fuel Cells as the supporting structures. As they are exposed to high temperatures (> 500°C) an oxide scale forms on their surface due to high temperature corrosion phenomena. Since the ratio between the surface area and volume is much higher than for planar samples, formation of the oxide can lead to a breakaway oxidation after relatively short times. Therefore corrosion properties of...
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Influence of High Temperature Oxidation on Hydrogen Absorption and Degradation of Zircaloy-2 and Zr 700 Alloys
PublikacjaThe present research was aimed at determining the effects of the oxide layers on hydrogen absorption, microstructure and mechanical properties of the Zircaloy- 2 and Zr 702 alloys. The oxidation was made at 350 °C, 700 °C and 900 °C for 10 to 30 min in laboratory air, followed by hydrogen cathodic charging for 72 h and annealing at 400 °C for 4 h. The slow strain rate tests were carried out on oxidized, charged and annealed specimens. The...
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Scaling of signed residue numbers with mixed-radix conversion in FPGA with extended scaling factor selection
PublikacjaA scaling technique of signed residue numbers in FPGA is proposed. The technique is based on conversion of residue numbers to the Mixed-Radix System (MRS). The scaling factor is assumed to be a moduli product from the Residue Number System (RNS) base. Scaling is performed by scaling of MRS terms, the subsequent generation of residue representations of scaled terms, binary addition of these representations and generation of residues...
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Nonlinear high temperature impedance of 35P2O5-30Fe2O3-27.5Nb2O5-7.5TiO2 glass
Dane BadawczeThe nonlinear high temperature impedance of iron- phosphate glasses doped with niobium oxide was measured. Glass samples of the composition of 35P2O5-30Fe2O3-27.5Nb2O5-7.5TiO2 (in %mol) were prepared by the conventional melt quenching technique. Appropriate amounts of reagents ((NH4)2HPO4 (≥99.9%, POCH), Fe2O3 (≥99.9%, POCH), Nb2O5 (≥99.9%, PLUKA AG)...
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Nonlinear impedance as a function of A.C. voltage of Bi2VO5.5 ceramic of thickness 2.88 mm was measured at 693 K with impedance spectroscopy method
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.88 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of temperature and frequency for Bi2VO5.5 ceramic of thickness 2.52 mm was measured at different A.C. voltage with impedance spectroscopy method
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm was measured by impedance spectroscopy method.