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Manufacture and research of TPS/PE biocomposites properties
PublikacjaIn this paper the process of native starch preparing for modification by extrusion and manufacture of biocomposites is presented. The first aim of this study was to determine the mixing and granulating condition of native starch to obtain granulated native starch. For mixing and granulation of native starch Intensive Mixer manufactured by Maschinenfabrik Gustav Eirich was used. Mixing and granulation in a single process is a new...
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Commonly Accessible Web Service Platform - Wiki-WS
PublikacjaWeb Service technology on the basis had to supply complete and reliable system components. Nowadays this technology is commonly used by companies providing results of their work to end users and hiding implementation details. This paper presents a SOA-enabled platform - Wiki-WS - that empowers users to deploy, modify, discover and invoke web services. Moreover it discusses concepts and functionalities of this open source management...
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Optimization algorithm and filtration using the adaptive TIN model at the stage of initial processing of the ALS point cloud
PublikacjaAirborne laser scanning (ALS) provides survey results in the form of a point cloud. The ALS point cloud is a source of data used primarily for constructing a digital terrain model (DTM). To generate a DTM, the set of ALS observations must be first subjected to the point cloud processing methodology. A standard methodology is composed of the following stages: acquisition of the ALS data, initial processing (including filtration),...
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Cooperative Word Net Editor for Lexical Semantic Acquisition
PublikacjaThe article describes an approach for building Word Net semantic dictionary in a collaborative approach paradigm. The presented system system enables functionality for gathering lexical data in a Wikipedia-like style. The core of the system is a user-friendly interface based on component for interactive graph navigation. The component has been used for Word Net semantic network presentation on web page, and it brings functionalities...
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High temperature corrosion and corrosion protection of porous Ni22Cr alloys
PublikacjaIn this work corrosion kinetics of the porous IN625 alloy is studied in the temperature range of 700 °C – 800 °C in air and humidified hydrogen for up to 1000 hours. Moreover, an effective and simple method of reducing corrosion rates of porous alloys by the infiltration of the rare earths elements is shown. Modification by the yttrium containing precursor reduces the corrosion rate by a factor of 50 in air at 700 °C so that the...
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THE POSSIBILITY OF USE OF LASER-MODIFIED Ti6Al4V ALLOY IN FRICTION PAIRS IN ENDOPROSTHESES
PublikacjaThe purpose of this paper is to show results of laser treatment at cryogenic conditions of the Ti6Al4V alloy used for orthopedic applications. That modification process ought to bring beneficial changes of microstructure and residual stresses in the surface layer. The paper presents the abrasive wear of the base and laser remelted material in association with ceramics Al2O3. Despite the surface cracking after laser treatment the...
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Modelling of cutting by means of fracture mechanics
PublikacjaThe suitability of modern fracture mechanic theory was proved for the estimation of the cutting force and the cutting specific resistance. This paper shows modification of Ernst-Merchant theory and its application for determination some other properties of wood sample. This theory is acceptable for evaluation of shear yield stresses and shear plane angle. Sawing by gang saw machine was used as a process similar to the orthogonal...
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MODELLING OF CUTTING BY MEANS OF FRACTURE MECHANICS
PublikacjaThe suitability of modern fracture mechanic theory was proved for the estimation of the cutting force and the cutting specific resistance. This paper shows modification of Ernst-Merchant theory and its application for determination some other properties of wood sample. This theory is acceptable for evaluation of shear yield stresses and shear plane angle. Sawing by gang saw machine was used as a process similar to the orthogonal...
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Historical crane on the redesigned original trestle bridge as a memorial of Gdansk Shipyard
PublikacjaThe paper includes selected aspects of the study, whose goal is to hold the historical crane 642-24 in its current location after the modification of trestle bridge static scheme. The scope of the paper includes the assessment of current technical condition of the object, a presentation of FEM analyses, a description of the assumed load cases, results of the static calculations, checking the effort of construction elements, global...
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Interactions of selected mono- and disaccharides with precipitated calcium carbonate particles
PublikacjaCalcium carbonate is a widespread compound in nature and it can be produced by living organisms in the biomineralization process. Calcite, aragonite and vaterite are anhydrous polymorphic forms of calcium carbonate, wherein the calcite is the most thermodynamically stable. Vaterite is the metastable crystalline phase, which can be a precursor of calcite and aragonite, because it can easily transformed by dissolution and re crystallization...
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DETERMINATION OF SURFACTANTS IN ENVIRONMENTAL SAMPLES. PART II. ANIONIC COMPOUNDS
PublikacjaSurfactants (SAA) with negative charge of polar group are named as anionic compounds. They are main constituent of most products containing synthetic surfactants. The linear alkylbenzene sulfonates (LAS), alkyl ethoxysulfates (AES) and alkyl sulfates (AS) are typically applied from this class of compounds. Those surfactants are ingredients of household detergents and cleaners, laundry detergents, cosmetic. Moreover they can be...
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How thermal stability of ionic liquids leads to more efficient TiO2-based nanophotocatalysts: Theoretical and experimental studies
PublikacjaIonic liquids (ILs) containing distinct nitrogen-bearing organic cations (pyridinium, pyrrolidinium, imidazolium, ammonium, morpholinium) were first used for the preparation of 23 IL-TiO2 types of composites by ionic liquid assisted solvothermal synthesis. These 23 optimal ILs structures (i.e. compounds exhibiting an optimal combination of specific properties, functionality, and safety) for synthesis and experimental validation...
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The dispersive micro-solid phase extraction method for MS-based lipidomics of human breast milk*
PublikacjaA simple and rapid microextraction method ensuring high lipidome coverage was developed for liquid chromatography mass spectrometry (LC-MS)-based lipidomics of human breast milk. The dispersive microsolid phase extraction (D-µ-SPE) technique, coupled with the design of experiment (DoE) method, enabled the study of the influence of several conditions (desorption solvent, stationary phase ratio, and sorption and desorption time)...
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New approach for e-cigarette aerosol collection by an original automatic aerosol generator utilizing melt-blown non-woven fabric
PublikacjaCurrently, there is lack of standardized conditions for the collection and analysis of e-cigarette (EC) aerosol. Considering the urgent need for the development of these guidelines, a procedure for EC aerosol analysis was developed. A novel automatic e-cigarette aerosol generator was designed. For the first time, melt-blown non-woven fabric was applied for the effective uptake of compounds released from vaporized e-liquid. The...
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Processing of Biomass Prior to Hydrogen Fermentation and Post-Fermentative Broth Management
PublikacjaUsing bioconversion and simultaneous value-added product generation requires purifica- tion of the gaseous and the liquid streams before, during, and after the bioconversion process. The effect of diversified process parameters on the efficiency of biohydrogen generation via biological pro- cesses is a broad object of research. Biomass-based raw materials are often applied in investigations regarding biohydrogen generation using...
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Ni-WC/Al2O3 and Ni-WC/MgWO4/MgAl2O4 catalysts for resource recovery via pyrolysis combined with the dry reforming of plastics (PCDR)
PublikacjaPlastic waste (PW) is currently one of an environmental threat. Despite the increasing share of recycled plastics, their disposal remains high. Therefore, there is a high demand for new PW management systems. Among them, pyrolysis combined with dry reforming (PCDR) is an advantageous solution because it allows for resource recovery in the form of gas and liquid fuels, with simultaneous utilization of CO2. To date, catalysts based...
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XRD pattern of Mo2Ga2C, Mo2CTx/Mo2GaC and Ni-Mo2CTx/Mo2Ga2C materials
Dane BadawczeIn the dataset are included raw data for the preparation of XRD pattern of Mo2Ga2C, Mo2CTx/Mo2GaC and Ni-Mo2CTx/Mo2Ga2C materials.
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Positron Scattering and Annihilation in Organic Molecules
PublikacjaIn this paper, we address the problem of connecting positron lifetimes in liquids with collision cross sections in gases. We present the analyses of annihilation lifetime spectra of positrons in the liquid benzene, c-hexane, n-hexane, methanol and ethanol and calculations of scattering cross sections of positrons with benzene and c-hexane in the gas phase.
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Synchronic digital stereophotography and photogrammetric analyses in monitoring the flow of liquids in open channels
PublikacjaThe authors present the results of their research into photogrammetric documents based on synchronic digital images. Examples presented in the paper indicate the value of synchronic stereophotography in registering phenomena connected with liquids. Combining synchronic stereophotography with photogrammetric methods has allowed the authors to develop an application useful for monitoring the flow of a liquid in an open channel.
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Energy and valuable organic products recovery from anaerobic processes
PublikacjaChapter 8 contains: Introduction, Energy balance in wastewater treatment plants and potential energy recovery, Potential valuable products recovery, Anaerobic processes focused on liquid products recovery; Anaerobic digestion (AD) processes focused on gaseous products recovery, Processes enhancing energy and valuable organic products recovery, Conclusions and perspectives. Anaerobic processes offer different pathways for the recovery...
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Thermodynamic study of binary mixtures of toluene with ionic liquids, 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide, 1-hexyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide and 1-butylpyridinium bis(trifluoromethylsulfonyl)imide
PublikacjaDensities, refractive indices and viscosities at 293.15, 298.15, 303.15, 308.15 and 313.15 K of binary mixtures of toluene with 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide, 1-hexyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide and 1-butylpyridinium bis(trifluoromethylsulfonyl)imide have been measured over the miscible region at p = 0.1 MPa. From the experimental data, values of excess molar volume,...
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Use of pyridinium and pyrrolidinium ionic liquids for removal of toluene from gas streams
PublikacjaSeparation of toluene from a toluene/N2 gas mixture using supported liquid membranes based on a series of pyridinium (1-butylpyridinium- bis(trifluoromethylsulfonyl)imide - [C4Py][Tf2N], 1-hexylpyridinium trifluoromethanesulfone [C6Py][Tf2N]) and pyrrolidinium (1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide - [C4Pyrr][Tf2N], 1-hexyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide - [C6Pyrr][Tf2N], 1-butyl-1-methylpyrrolidinium...
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Prediction of the Biogenic Amines Index of Poultry Meat Using an Electronic Nose
PublikacjaThe biogenic amines index of fresh chicken meat samples during refrigerated storage was predicted based on the headspace analysis using an electronic nose equipped with an array of electrochemical sensors. The reference biogenic amines index values were obtained using dispersive liquid–liquid microextraction–gas chromatography–mass spectrometry. A prototype electronic nose with modular construction and a dedicated sample chamber...
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SURFACTANTS IN KLODNICA RIVER (KATOWICE, POLAND). PART I. LINEAR ALKYLBENZENE SULPHONATES (LAS)
PublikacjaSurfactants are a group of compounds with specific physico-chemical properties and therefore they are used in many spheres of human activity. Surface-active substances undergo various physico-chemical transformations, what enables their migration between different elements of the environment and may lead to its pollution. Selected anionic surfactants were determined in samples of water from the Klodnica river (25 samples) and bottom...
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Direct determination of cadaverine in the volatile fraction of aerobically stored chicken breast samples
PublikacjaTo supplement the currently used methods for poultry meat shelf life assessment, it might be necessary to develop a technique for rapid headspace analysis of volatiles with no prior sample preparation step. Biogenic amines, in particular cadaverine, are considered meat spoilage indicators. Described in this article are the results of a preliminary investigation of the applicability of proton transfer reaction mass spectrometry...
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Comparative evaluation of different methods for determining phytochemicals and antioxidant activity in products containing betalains - Verification of beetroot samples
PublikacjaThis study presents methods that can be used to assess the health quality of products containing betalains. The paper compares and verifies data on the phytochemical composition of three different pigmented beetroot cultivars using spectrophotometric, HPLC-DAD, HPTLC and LC-Q-Orbitrap-HRMS techniques. Additionally, we compared the total antioxidant activity in both the cell-free and cellular systems. Betalain contribution to antioxidant...
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Smartphone-based digital image colorimetry for the determination of total capsaicinoid content in chili pepper extracts
PublikacjaA simple smartphone-based digital image colorimetry was proposed for the determination of total capsaicinoid content and the assessment of chili pepper pungency. The biobased solvent D-limonene was used for the first time to isolate analytes. Capsaicinoids were efficiently separated from chili pepper by solid-liquid extraction with D-limonene followed by partitioning of the analytes into the ammonium hydroxide solution to eliminate...
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A new construction of shell-and-tube heat exchanger with impinging jets and minichannels technologies for heat recovery from gases – experimental analysis
PublikacjaA dynamic development of technologies allowing waste heat utilization is observed in a correspondence with a pro-ecological approach of the zero waste idea. Such approach becomes the most demanding in the area of low-temperature was heat sources, especially gaseous media. Till now, they were usually not utilized due to unfavorable thermal conditions and high costs. Therefore, the zero waste approach directs research on techniques...
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Dynamics of a simplified HPT model in relation to 24h TSH profiles
PublikacjaWe propose a simplified mathematical model of the hypothalamus-pituitary-thyroid (HPT) axis in an endocrine system. The considered model is a modification of the model proposed by Mukhopadhyay and Bhattacharyya in [10]. Our system of delay differential equations reconstructs the HPT axis in relation to 24h profiles of human in physiological conditions. Homeostatic control of the thyroid-pituitary axis is considered by using...
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Absence of superconductivity in fluorine-doped neptunium pnictide NpFeAsO
PublikacjaX-ray diffraction, specific heat, magnetic susceptibility and inelastic x-ray scattering measurements on the transurarium oxypnictides NpFeAsO and NpFeAsO0.85F0.15 are presented. No superconductivity down to 2 K was observed upon fluorine doping, contrary to the structurally analogous rare-earth pnictides. No modification of the phonon density of states was observed upon doping with fluorine. We discuss our results in light of...
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Flow visualization and heat transfer investigations on the flat plate with streamwise pressure gradient
PublikacjaPaper presents experimental investigations results for film cooling on a flat plate. The main objective of the design is the streamwise pressure distribution on the flat plate as in the blade cascade. The transient and steady-state technique with liquid crystals for the surface temperature distribution with film cooling has been used in experiments in a low speed wind tunnel.
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RP-HPLC WITH DETECTION BY MEANS OF ESI-MS AND UV FOR IDENTIFICATION OF CHROMATOGRAPHIC PEAKS OF SOME HYDROXY DERIVATIVES OF EPOXY RESIN
PublikacjaThe composition of products synthesized on the basis of ED-24 epoxy resin has been studied using a reversed phase high-performance liquid chromatography followed by an electrospray ionization mass spectrometry (RP-HPLC/ESI-MS). The synthesized products contain free hydroxy groups and such groups, as epoxy, peroxy, carboxy or acrylate.
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Catalysts for advanced oxidation processes: Deep eutectic solvents-assisted synthesis – A review
PublikacjaNew catalyst synthesis techniques, including green materials, are extensively studied for heterogeneous photocatalytic advanced oxidation processes (AOPs) on spotlight of sustainable development. Deep eutectic solvents (DESs) started to be used in this field as environmentally friendly alternative to ionic liquids (ILs). During the catalyst synthesis, DESs can act as stabilizers, capping agents, structure directing agents, templates,...
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Influence of the internal electrolyte composition on amperometric sulphur dioxide sensor properties
PublikacjaIn this work amperometric sulphur dioxide sensor with a liquid electrolyte, a mercury sulphate reference electrode and solid polymer electrolyte (Nafion) covered with gold as a working electrode will be presented. The main goal of this research is to determine the influence of internal electrolyte composition on the sensor properties. Sensor filled with 1M and 5M sulphuric acid has been investigated.
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Injectable poloxamer/graphene oxide hydrogels with well‐controlled mechanical and rheological properties
PublikacjaAlthough significant progress has been made in the design and application of injectable hydrogels for biomedical applications, concurrent control of rheological and mechanical properties of injectable hydrogels has remained as an open challenge to the researchers. In this work, we introduce and put into practice a photo‐curable poloxamer (also known as Pluronic)/graphene oxide (Plu/GO) injectable hydrogel with well‐controlled rheological...
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Highly effective asphaltene-derived adsorbents for gas phase removal of volatile organic compounds
PublikacjaA novel nitrated asphaltene-derived adsorbent (Asf-Nitro) was prepared using facile isolation and modification procedures. The successful modification was confirmed by Fourier-transform infrared spectroscopy (FTIR). The nitrated adsorbent was evaluated in terms of dispersive and specific interactions, Lewis acid-base properties and adsorption isotherms by means of inverse gas chromatography (IGC). Nitration was found to be extremely...
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Tailoring a low-energy ball milled MnCo2O4 spinel catalyst to boost oxygen evolution reaction performance
PublikacjaThe development of cost-efficient oxygen evolution reaction (OER) catalysts is one of the most important tasks facing modern techniques for hydrogen production. In this work, for the first time, a low-energy ball milling process of MnCo2O4 (MCO) spinel powders, with a mechanical modification time exceeding 1 day was used. After 6 days of ball-milling, the obtained overpotential of the electrocatalyst reached the value of 375 mV...
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Novel microstrip low-pass filters with fractal defected ground structures
PublikacjaIn this study, three microstrip low-pass filters (LPFs) containing fractal-shaped defected ground structures have been designed and manufactured. To improve the performance of microstrip LPF, cascades of inductively coupled fractal resonators have been applied. Simultaneously, to achieve relatively constant microstrip impedance resulting in essentially low reflection losses, a modification of the strip geometry has been introduced....
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Matrix Strengthening the Identification of Observations with Split Functional Models in the Squared Msplit(q) Estimation Process
PublikacjaThis article addresses the issue of raising the level of identification of observations with either single or more split functional models in the squared Msplit(q) estimation process. The theoretical part of the study presents the theoretical grounds for the classical method for estimating parameters in a split functional model and proposes a modification of the computational algorithm to increase the quality of the determinations...
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Analiza wpływu transmisji danych na jakość działania rozproszonych systemów sterowania
PublikacjaW artykule przedstawiono zagadnienia związane z transmisją danych w rozproszonych systemach sterowania. Opisano cechy charakterystyczne przemysłowych sieci i protokołów informatycznych. Utworzono model rozproszonego systemu sterowania poziomem cieczy w zbiorniku, w którym komunikacja oparta została na protokole Modbus RTU. Na podstawie zmian parametrów transmisji danych wykazano, że poprawna komunikacja pomiędzy elementami systemu...
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Influence of the internal electrolyte composition on amperometric sulphur dioxide sensor properties
PublikacjaIn this work investigation of an amperometric sulphur dioxide sensor with a liquid electrolyte, a mercury sulphate reference electrode and solid polymer electrolyte (Nafion) covered with gold as a working electrode properties is presented. The main goal of this research is to determine the influence of internal electrolyte composition on the sensor properties. Sensor filled with 1M and 5M sulphuric acid has been studied.
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Pressure drop and heat transfer during boiling and condensation at subcritical region
PublikacjaMost of the data presented in the literature relate to saturation temperatures in the range - 20°C to 40°C due to the application in refrigeration technology. There is necessity to extend databases to higher values of saturation temperature due to new applications such as Organic Rankine Cycle and high temperature heat pumps. Only few papers contain data for high reduced pressure for low boiling point liquids. This paper focus...
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Direct-Ultrasonic Assisted Microextraction Coupled with RTL-GC-FID/GC-MS as a Future Standard Procedure for Monitoring 26 potentially Allergenic Fragrances in Water Samples
PublikacjaThis research topic grew up as a result of awareness of constant anthropogenic and natural input to the environment constituents of personal care products (PCPs) residues. This group of emerging pollutants encompasses a wide range of chemicals, including potentially allergenic fragrance compounds. The aim of the present study was to investigate presence of 26 fragrance allergens in water samples. Simple and rapid methodology based...
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Study of Icosahedral Clusters in Close-packed Simple Liquids
PublikacjaThe local structure of liquid copper was determined using Steinhardt order parameters, with particular attention paid to icosahedral clusters. The positions of atoms were obtained from three sets of molecular dynamics simulations, with the forces obtained from: the Sutton-Chen (SC) potential, the Naval Research Laboratory total energy tight-binding (NRL-TB) method and the divide-and-conquer learn-on-the-fly (DCLOTF) method, respectively....
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Deep eutectic solvents in analytical sample preconcentration Part B: Solid-phase (micro)extraction
PublikacjaOne of the key challenges of modern analytical chemistry is the monitoring of trace amounts of contaminants using sensitive and selective instrumental techniques. Due to the variety and complexity of some samples, it is often necessary to properly prepare a sample and to perform a preconcentration of trace amounts of analytes. In line with the principles of Green Analytical Chemistry (GAC), it is important for an analytical procedure...
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Review of the Application of Graphene-Based Coatings as Anticorrosion Layers
PublikacjaDue to the excellent properties of graphene, including flexibility that allows it to adjust to the curvature of the substrate surface, chemical inertness, and impermeability, graphene is used as an anticorrosion layer. In this review, we present the current state-of-the-art in the application of graphene in the field of protective coatings. This review provides detailed discussions about the protective properties of graphene coatings...
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Statistical significance of displacements in heterogeneous control networks
PublikacjaThis paper proposes a modification of the classical process for evaluating the statistical significance of displacements in the case of heterogeneous (e.g. linear-angular) control networks established to deformation measurements and analysis. The basis for the proposed solution is the idea of local variance factors. The theoretical discussion was complemented with an example of its application on a simulated horizontal control...
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Topology Discovery of Hierarchical Ethernet LANs without SNMP support
PublikacjaThis paper presents an algorithm that allows for discovery of layer-2 hierarchical Ethernet network topology using agents running on selected end nodes. No SNMP, MIB, hardware, firmware, or operating system-level software modification is required. The method is based on transmission of customized Ethernet frames among installed software agents. It can be used to discover the topology of LAN or one VLAN segment as long as no MAC...
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Millimeter Wave Retrodirective Van Atta Arrays in LTCC Technology
PublikacjaThe millimeter wave Van Atta arrays, intended for chipless RFID applications and fabricated in LTCC technology, are presented in this paper. The arrays are designed for 24 GHz and 60 GHz bands. The method for an easy modification of the RCS characteristic by increasing the number of single-dimensional arrays, intended for increasing the RCS level, is also presented. The LTCC manufacturing process is described in detail. The fabricated...
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Investigation of the Aerodynamics of an Innovative Vertical-Axis Wind Turbine
PublikacjaThe paper presents the results of an experimental investigation and a three dimensional numerical analysis of the transient aerodynamic phenomena occurring in the innovative modification of classic Savonius wind turbine. An attempt to explain the increased efficiency of the innovative design a comparison with the traditional solution is undertaken. A vorticity measure based on the integral of the velocity gradient tensor second...