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Wyniki wyszukiwania dla: 5-PHASE MOTOR
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Stereoselective Alkylation of Indole with 5-Arylidene-Meldrum’s Acids in the Presence of Organocatalysts
PublikacjaBackground: Indole motif is frequently present in biologically active compounds. Enantiomerically pure or enriched 2,2-dimethyl-5-(aryl(1H-indol-3-yl)methyl)-1,3-dioxane-4,6-diones can be considered as a convenient starting point for the synthesis of a indole ring fused with cyclic ketones with biological activity. Preparation of chiral 2,2-dimethyl-5-(aryl(1H-indol-3-yl)methyl)-1,3-dioxane- 4,6-diones requires the reaction of...
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[Rozdział] 5. Niepewność
PublikacjaPrzedstawiono podstawowe informacje dotyczące szacowania niepewności wyników pomiarów analitycznych. Opisano sposoby szacowania niepewności oraz podano przykłady praktycznego tworzenia budżetu niepewności.
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Asynchronous phase-location system
PublikacjaThis paper presents concept and implementation of digital phase-location system, designed as a navigational aid for marine applications. The main feature of the proposed system is the ability to work in both synchronous mode, with one master station and set of slave stations synchronised with master, and in asynchronous mode with independent clocking of all stations.
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Energy losses in the hydraulic rotational motor - definitions and relations for evaluation of the efficiency of motor and hydrostatic drive
PublikacjaStosowane dotychczas w badaniach naukowych i w praktyce przemysłowej metody oceny strat i sprawności energetycznej obrotowych silników hydraulicznych stosowanych w napędach hydrostatycznych dają błędne rezultaty, ponieważ obarczone są wpływem samych strat na parametry, w funkcji których straty i sprawności są oceniane.Celem pracy było zdefiniowanie w silniku parametrów pracy, rozwijanych mocy, występujących strat i sprawności energetycznej...
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FLUID PHASE EQUILIBRIA
Czasopisma -
The unstable thermoelectric effect in non-stoichiometric Cu2Se during the non-equilibrium phase transition
PublikacjaThe superionic α ↔ β phase transition in Cu1.96Se thermoelectric material is investigated by means of thermal analysis (DSC) and measurements of Seebeck coefficient and electrical conductivity. Results of the DSC measurements with 1–10 K/min heating and cooling rates show that the material is close to the equilibrium phase composition during the transformation. However, the kinetic limitation of the process exists, which is indicated...
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Electric shock hazard in circuits with variable-speed drives
PublikacjaThe conventional approach to electrical safety under fault condition in typical power systems considers earth fault currents of sinusoidal waveform and frequency of 50/60 Hz. However, in circuits with variable-speed drives, there is earth fault current flow with harmonics, and these harmonics influence the threshold of ventricular fibrillation. The paper presents earth fault current waveforms in circuits with variable-speed drives...
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Automatic Watercraft Recognition and Identification on Water Areas Covered by Video Monitoring as Extension for Sea and River Traffic Supervision Systems
PublikacjaThe article presents the watercraft recognition and identification system as an extension for the presently used visual water area monitoring systems, such as VTS (Vessel Traffic Service) or RIS (River Information Service). The watercraft identification systems (AIS - Automatic Identification Systems) which are presently used in both sea and inland navigation require purchase and installation of relatively expensive transceivers...
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The Origins of the Concept of Ideology
PublikacjaThe concept of "ideology" as, firstly, a term that points at non-epistemological conditioning of cognitive processes, and, secondly, as a term which aimed at disclosing the ancillary role of given ideas in regard to specific political interests of certain groups, has long history. Since Francis Bacon's theory of idols modern philosophy endavoured to create a comprehensive classification of systematic cognitive errors which divert...
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Electron-Induced Decomposition of 5-Bromo-4-thiouracil and 5-Bromo-4-thio-2′-deoxyuridine: The Effect of the Deoxyribose Moiety on Dissociative Electron Attachment
PublikacjaWhen modified uridine derivatives are incorporated into DNA, radical species may form that cause DNA damage. This category of molecules has been proposed as radiosensitizers and is currently being researched. Here, we study electron attachment to 5-bromo-4-thiouracil (BrSU), a uracil derivative, and 5-bromo-4-thio-20 -deoxyuridine (BrSdU), with an attached deoxyribose moiety via the N-glycosidic (N1-C) bond. Quadrupole mass spectrometry...
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Synthesis and structure of selected quaternary N-(1,4-anhydro-5-deoxy-2,3-O-isopropylidene-D,L-ribitol-5-yl)ammonium salts.
PublikacjaOpracowano metody otrzymywania czwartorzędowych soli amoniowych, pochodnych rybitolu, zawierających reszty: pirydyny, 2-metylopirydyny, 3-karbamoilopirydyny, 4-(N,N-dimetyloamino)pirydyny, chinoliny oraz dwóch amin alifatycznych trimetyloaminy i trietyloaminy. Związki te powstają w reakcji 1,4-anhydro-2,3-O-izopropylideno-5-O-tozylo-D,L-rybitolu z odpowiednimi zasadami azotowymi.
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Miniaturized solid-phase extraction techniques
PublikacjaMore than 80% of analysis time is spent on sample collection and sample preparation, so sample preparation is a critical part of the analytical process. Traditionally, liquid-liquid extraction was developed and employed to screen for general unknowns. However, solid-phase extraction (SPE) is becoming highly popular as an alternative, due to its simplicity and economy in terms of time and solvent. This review summarizes the current...
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Halogen bonded polypseudorotaxanes based on a pillar[5]arene host
PublikacjaTwo crystalline supramolecular polypseudorotaxanes were obtained by combining permethylated pillar[5]arene as a macrocyclic wheel with 1,4-bis(1-imidazolyl)butane and 1,4-bis(iodoethynyl)benzene or 1,4-diiodo-1,3-butadiyne linked by C–I⋯N halogen bonds and creating a polyrotaxane axis. The resulting highly ordered supramolecular arrays were characterized by X-ray crystallography.
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New Polymeric Materials for Solid Phase Extraction
PublikacjaSolid phase extraction (SPE) is a popular sample preparation technique, which can be applied directly in gas–solid phase and liquid–solid phase, or indirectly to solid samples by using, e.g., thermodesorption with subsequent chromatographic analysis. Although SPE can be described as a physical extraction process involving a liquid phase and a solid phase, the increased use of packed sorbent formats seems to have led to a bias toward...
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5-Bromo-2′-deoxycytidine—a potential DNA photosensitizer
PublikacjaA double-stranded oligonucleotide, 80 base pairs in length, was multiply labeled with 5-bromo-2′-deoxycytidine (BrdC) using polymerase chain reaction (PCR). The modified oligonucleotide was irradiated with 300 nm photons and its damage was assayed by employing DHPLC, LC-MS and denaturing polyacrylamide gel electrophoresis (PAGE). Two types of damage were demonstrated, namely, single strand breaks (SSBs) and intrastrand cross-links...
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THE PHASE SHIFTERS INFLUENCE ON THE POWER SYSTEM STABILITY
PublikacjaThe paper presents the effect of phase shifters as FACTS devices on the possibility of improving the angle stability. Presented results obtained by the dynamic simulation performed on the mathematical model of the three machine system cooperating with the 400 kV network. The generative blocks models include turbine models with their controllers and models of synchronous generators with their excitation systems and voltage regulation....
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Critical behaviour of the smectic A*–C* phase transition and electroclinic effect of ferroelectric liquid crystals with terphenyl rigid core
Publikacja -
Vestnik Volgogradskogo gosudarstvennogo universiteta. Serija 5. Jurisprudencija
Czasopisma -
Phase transition of a dimorphic fungus Penicillium marneffei
PublikacjaPenicillium marneffei is a pathogenic fungus that afflicts immunocompromised individuals who live or travel in Southeast Asia. This species is unique, because it is the only dimorphic member of the genus Penicillium. Dimorphism results from a process, termed phase transition, which is regulated by temperature of incubation. At room temperature, the fungus grows filamentously (mould phase), but at body temperature (37°C), a uninucleate...
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Automated Design of Linear Phase Filters
PublikacjaThis paper presents a fast technique for an automated design of microwave filters with linear phase. The proposed method exploits the cost function defined using the location of complex zeros and poles of the filter’s transfer and reflection function. The effectiveness of the proposed technique is presented with two illustrative examples.
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On phase equilibrium of an elastic liquid shell with wedge disclination
PublikacjaBased on the six-parameter shell theory we consider the phase equilibrium of a two-phase liquid membrane containing a wedge disclination. The considered problems are related to modelling of phase transitions in biological or lipid membranes. In order to capture the membrane behaviour we consider a special case of elastic shells which energy is invariant under major transformations of a reference configuration and can be treated...
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Liquid–phase microextraction: A review of reviews
PublikacjaSample preparation is an important step in chemical analysis. It is generally done to deal with problems associated with the nature of the matrix, low analyte concentrations in real samples or analyte features incompatible with the instrumentation. Classical methods of extraction consume large volumes of hazardous solvents and other reagents and are not in line with the recent emergence of green analytical chemistry. Liquid-phase...
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Stability and phase transition investigation of olanzapine polymorphs
PublikacjaWe use electrical embedded-fragment QM method with both DFT/ωB97XD/6-31G* and MP2/6-31G* to investigate the phase transformations of olanzapine. Gibbs free energy calculations predict that form I is always the most stable structure and form II is the least stable one, while form IV is more stable than form III below about 200 K but less stable above this temperature, implying a polymorphic phase transformation. This may account...
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Timed rolling and rising tests in Duchenne muscular dystrophy ambulant boys: a feasibility study
PublikacjaBACKGROUND: Functional activities are extensively used in motor assessments of patients with Duchenne muscular dystrophy. The role of timed items has been reported as an early prognostic factor for disease progression. However, there are two functional activities that are not widely assessed in clinical practice among Duchenne muscular dystrophy patients: rolling and bed rising. This study aimed to investigate whether the 360-degree...
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Testing sensitivity of A-type residual current devices to earth fault currents with harmonics
PublikacjaIn many applications, modern current-using equipment utilizes power electronic converters to control the consumed power and to adjust the motor speed. Such equipment is used both in industrial and domestic installations. A characteristic feature of the converters is producing distorted earth fault currents, which contain a wide spectrum of harmonics, including high-order harmonics. Nowadays, protection against electric shock in...
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Selection of an artificial pre-training neural network for the classification of inland vessels based on their images
PublikacjaArtificial neural networks (ANN) are the most commonly used algorithms for image classification problems. An image classifier takes an image or video as input and classifies it into one of the possible categories that it was trained to identify. They are applied in various areas such as security, defense, healthcare, biology, forensics, communication, etc. There is no need to create one’s own ANN because there are several pre-trained...
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Mobile satellite measurements in designing and exploitation of rail roads
PublikacjaThe article presents a summary of several years (2009-2015) of studies on the application of mobile satellite Global Navigation Satellite Systems (GNSS) measurements in the field of designing and operation of railways. These studies have been conducted by an interdisciplinary research team from the Gdansk University of Technology and the Gdynia Maritime University. Mobile satellite GNSS measurements are taken during a ride (through...
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Synthesis and molecular structure of novel 2-(alkylthio)-4-chloro-N-(4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-yl)-5-methylbenzenesulfonamideswith potential anticancer activity
PublikacjaOtrzymano 15 nowych związków: 2-(alkilotio)-4-chloro-N-(4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-yl)-5-metylobenzenosulfonamidów, dla których opracowano nową metodę syntezy. Dla jednej pochodnej wyznaczono strukturę rentgenowską. Związek nr 36 wykazuje wysoką aktywność przeciwnowotworową w stosunku do 13 linii komórek nowotworowych o poziomie GI_50 w zakresie stężeń 1,9-3,0 μM.
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Ekspertyza przyczyn awarii turbozespołu nr 5 w Elektrowni Turów
PublikacjaGłównym celem pracy było określenie przyczyn awarii łożysk nr 4 oraz generatora 50WT20H-100 turbozespołu nr 5 Elektrowni Turów. Opisano przebieg zdarzenia oraz opracowano wnioski zawierające przyczyny zaistniałej awarii łożysk.
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Phase-difference positioning in asynchronous system
PublikacjaThis paper presents concept and implementation of digital positioning system based on phase difference measurements, designed as a navigational aid for marine applications. Main feature of proposed system is the ability to work in both synchronous mode, with one master station and set of slave stations synchronized with master, and in asynchronous mode with independent clocking of all stations.
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5 urodziny sztuki Trójmiasta
Publikacja -
Superconductivity in the Nb-Ru-Ge σ phase
PublikacjaWe show that the previously unreported ternary σ-phase material Nb20.4Ru5.7Ge3.9 (Nb0.68Ru0.19Ge0.13) is a superconductor with a critical temperature of 2.2 K. Temperature-dependent magnetic susceptibility, resistance, and specific-heat measurements were used to characterize the superconducting transition. The Sommerfeld constant γ for Nb20.4Ru5.7Ge3.9 is 91 mJ mol f.u. −1K−2 (∼3 mJ mol atom−1 K−2) and the specific-heat anomaly at...
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Influence of Phase Composition on Dielectric Properties of Bismuth-Based Ceramics with Scheelite-Type Structure
PublikacjaGoal of the present research was to study dielectric properties of BiNbO4 ceramics fabricated by solid state reaction route followed with pressureless sintering. The samples were fabricated from the mixture of oxides, viz. Nb2O5 and Bi2O3. Apart from stoichiometric amount an excess of 3%, 5% and 10% by mole of Bi2O3 was used. It was found that an excess amount of Bi2O3 oxide caused formation of Bi5Nb3O15 minor phase in amount of...
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Magnetic deep eutectic solvents as efficient media for extraction of furfural and 5-hydroxymethylfurfural from aqueous samples
PublikacjaThe extraction of furfural (FF) and 5-hydroxymethylfurfural (HMF) from hydrolysates is currently one of the main challenges in bio-refinery. In this work, the separation of FF and HMF from the aqueous phase was carried out using a new type of green solvents – Magnetic Deep Eutectic Solvents (MDES). A conductor-like screening model for realistic solvents (COSMO-RS) was used for the preselection of 400 MDES. MDES which exhibit the...
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An Overview of Treatment Approaches for Octahydro-1, 3, 5, 7-tetranitro-1, 3, 5, 7-tetrazocine (HMX) Explosive in Soil, Groundwater, and Wastewater
PublikacjaOctahydro-1, 3, 5, 7-tetranitro-1, 3, 5, 7-tetrazocine (HMX) is extensively exploited in the manufacturing of explosives; therefore, a significant level of HMX contamination can be encountered near explosive production plants. For instance, up to 12 ppm HMX concentrations have been observed in the wastewater effluent of a munitions manufacturing facility, while up to 45,000 mg/kg of HMX has been found in a soil sample taken from...
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Effects of liquid phase modification on the performance of biotrickling filters
Dane BadawczeDataset presents the effects of liquid phase modification on the biotrickling filtration (BTF) performance of air polluted with toluene, ethylbenzene, xylene and styrene.
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Determination of t8/5 cooling times for underwater local dry welding of steel
PublikacjaKnowledge of thermal history is the basic condition for studying the structure - properties of welded joints. The determinant of thermal history is the thermal cycle, whose in-situ measurements are still a big challenge. Water as the welding environment complicates this issue even more. The article presents a method to determine an equation for calculating t8/5 cooling times for underwater gas metal arc welding of unalloyed steels...
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Electron-Induced Decomposition of Uracil-5-yl O-(N,N-dimethylsulfamate): Role of Methylation in Molecular Stability
PublikacjaThe incorporation of modified uracil derivatives into DNA leads to the formation of radical species that induce DNA damage. Molecules of this class have been suggested as radiosensitizers and are still under investigation. In this study, we present the results of dissociative electron attachment to uracil-5-yl O-(N,N-dimethylsulfamate) in the gas phase. We observed the formation of 10 fragment anions in the studied range of electron...
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Synthesis and structure of Bi 5 FeTi 3 O 15 ceramics
PublikacjaAim of the present research was to fabricate and study crystal structure and phase composition of Bi5FeTi3O15 (BTFO) ceramics exhibiting Aurivillius - type structure. By means of simultaneous thermal analysis and X-ray diffraction analysis the process of synthesis of BTFO ceramics has been studied. Mixed oxide method followed by pressureless sintering was used for ceramics preparation. Three endothermic thermal effects have been...
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Experimental investigation of thermal energy storage in shell-and-multi-tube unit with nano-enhanced phase change material
PublikacjaThis paper deals with thermal energy storage with use of nanoparticle enhanced phase change material in shell-and-multitube unit. The experiments are conducted under atmospheric pressure. Paraffin wax and two different fatty acids are used as base phase change material. Graphite and multi-walled carbon nanotubes serve as nanoparticles. Graphite nanoparticles are tested at the concentrations of 0.1%, 1% and 5% by weight, while multi-walled...
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Układ sterowania 5-fazową maszyną synchroniczną z magnesami trwałymi (PMSM)
PublikacjaW pracy przedstawiono nowy układ sterowania bezczujnikowego 5-fazową maszyną synchroniczną z magnesami trwałymi zagłębionymi (IPMSM) . Zaproponowany układ wykorzystuje obserwator stanu dla zmiennych w pierwszym układzie współrzędnych (1 harmoniczna), jak i drugim (3 harmoniczna), w celu zwiększenia gęstości momentu elektromagnetycznego. Zaprezentowano schemat kompletnego układu sterowania, przebiegi zmiennych w stanie ustalonym,...
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Phase Transition in a Sequence-Structure Channel
PublikacjaWe study an interesting channel which maps binary sequences to self-avoiding walks in the two-dimensional grid, inspired by a model of protein folding from statistical physics. The channel is characterized by a Boltzmann/Gibbs distribution with a free parameter corresponding to temperature. We estimate the conditional entropy between the input sequence and the output fold, giving an upper bound which exhibits an unusual phase transition...
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CALPHAD-COMPUTER COUPLING OF PHASE DIAGRAMS AND THERMOCHEMISTRY
Czasopisma -
5-formylcytosine and 5-hydroxymethyluracil as surrogate markers of TET2 and SF3B1 mutations in myelodysplastic syndrome, respectively
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Cycling as a Sustainable Transport Alternative in Polish Cittaslow Towns
PublikacjaIt is well known that growing motor traffic in urban areas causes air pollution and noise which affects the environment and public health. It is hardly surprising then that cycling should be used as an alternative mode of transport, not just in major cities but also in smaller ones including those that are members of the Cittaslow network. Their approach is based on sustainable development, care for the environment and transport...
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Human memory enhancement through electrical stimulation in the temporal cortex
PublikacjaDirect electrical stimulation of the human brain can elicit sensory and motor perceptions as well as recall of memories. Stimulating higher order association areas of the lateral temporal cortex in particular was reported to activate visual and auditory memory representations of past experiences (Penfield and Perot, 1963). We hypothesized that this effect could be used to modulate memory processing. Recent attempts at memory enhancement...
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ROAD SAFETY FOR CYCLISTS BASED ON THE CALORIES NEEDED
PublikacjaCyclists are a vulnerable group of road users, especially when no separate infrastructure for cyclists is provided. Then, road factors such as distance and altitude differences can indirectly affect cyclists' safety. Therefore, the authors proposed a procedure based on the geometric characteristics of the road that can determine riding difficulties for cyclists. The proposed procedure can be used both by the public authorities who...
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MgPdSb─An Electron-Deficient Half-Heusler Phase
PublikacjaThe half-Heusler family consists of many semiconducting intermetallic compounds, virtually all of them having a valence electron count (VEC) of 18. We have studied an electron-deficient (VEC = 17) phase MgPdSb and its Pd-stuffed variant MgPd1.25Sb. The cubic F4̅3m crystal structure was confirmed by the Rietveld refinement of powder X-ray diffraction (XRD) data. The lattice parameter is a = 6.284 and 6.335 Å for MgPdSb and MgPd1.25Sb,...
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Application of the Anammox Process for Treatment of Liquid Phase Digestate
PublikacjaThe liquid phase of the digestate (LPD) contains a relatively high concentration of nitrogen, with total ammonium nitrogen being the dominant form of nitrogen, as well as other essential nutrients such as phosphorus and potassium. Consequently, it must be treated before it is released into the environment. However, there are no reports of co-purification of LPD in the anammox process in sequencing batch reactor with granular sludge,...
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Digital phase-location system for marine applications
PublikacjaThis paper presents concept and implementation of digital phase-location system, designed as a navigational aid for marine applications. Main feature of proposed system is the ability to work in both synchronous mode, with one master station and set of slave stations synchronized with master, and in asynchronous mode with independent clocking of all stations.