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Preparation of environmental samples for gas chromatographic determination of selected organic pollutants
PublikacjaOpisano różne metody izolacji i wzbogacania zanieczyszczeń organicznych z ciekłych, gazowych i stałych próbek środowiskowych. Opisano konstrukcję i testowanie nowych systemów do przygotowania próbek oraz ich zastosowanie w połączeniu z chromatografią gazową do oznaczania zanieczyszczeń organicznych w póbkach rzeczywistych.
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OPTIMIZATION OF THE LAST STAGE OF GAS-STEAM TURBINE USING A HYBRID METHOD
PublikacjaThis paper relates to the CFD calculation of a new turbine type which is in the phase of theoretical analysis, because the working fluid is a mixture of steam and gas generated in wet combustion chamber. At first, this article concentrates on a possibility of streamlining the flow efficiency of a last stage of axial turbine working on gas-steam mixture using a hybrid of the particle swarm optimization algorithm with the Nelder-Mead...
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Band Gap Engineering toward Semimetallic Character of Quinone-Rich Polydopamine
PublikacjaSemiconductor|melanin interfaces have received increasingly more attention in the fields of photocatalysis and applied electrochemistry because of their facile synthesis, unique electrical properties, and strong capability toward photosensitization. In this work, we describe the electropolymerization of quinone-rich polydopamine (PDA) on the surface of hydrogenated TiO2 nanotubes with enhanced photoactivity in the visible spectrum....
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Special Issue on “Advanced Liquid Waste and Gas Waste Treatment Processes”
PublikacjaThe editorial contains a short review of the content of the Special Issue on waste gas and liquid streams treatment strategies.
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From flow to jamming: Lattice Gas Automaton simulations in granular materials
PublikacjaWe introduce the first extension of a Lattice Gas Automaton (LGA) model to accurately replicate observed emergent phenomena in granular materials with a special focus on previously unexplored jamming transitions by incorporating gravitational effects, energy dissipation in particle collisions, and wall friction. We successfully reproduce flow rate evolution, density wave formation, and jamming transition observed in experiments....
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Electrochemical investigations of stainless steels used in flue‐gas desulphurization units
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Low and high energy explosive materials used in shale gas recovery
PublikacjaNowadays the explosives are widely used in many areas of life, including industry and mining. A wide range of explosive materials is used in the petroleum industry - from low to high explosives. Recently, as the unconventional oil and gas production became possible, explosives are also found to be used in perforators during the pre-completion stage of the fracturing process. This paper presents literature on theoretical and practical...
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Gender Gap in Parental Leave Intentions: Evidence from 37 Countries
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Residual K1 and K2 Oscillations in Precise GPS Solutions: Case Study
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Application of acoustic emission metod for measurement of joint gap and cartilage surfaces
PublikacjaW artykule przedstawiono zastosowanie emisji akustycznej do lokalizacji wczesnych uszkodzeń stawu biodrowego lub kolanowego człowieka. Ponadto metoda ta służy do pomiaru wysokości szczeliny stawu oraz struktury geometrycznej powierzchni chrząstki stawowej. Jest to metoda nieinwazyjna. Pomiary metodą emisji akustycznej stosujemy na ogół w materiałach, w których energia sprężysta zmienia się nagle. Takie zmiany energii mogą być...
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Modern techniques of sample preparation for determination of organic analytes by gas chromatography
PublikacjaW pracy dokonano przeglądu szerokiego spektrum technik przygotowania próbki, ze szczególnym uwzględnieniem technik o charakterze prośrodowiskowym. Opisu technik dokonano pod kątem wykorzystywanych mechanizmów izolacji analitów oraz stosowanych rozwiązań aparaturowych. Przegląd rozwiązań aparaturowych uzupełniono o podstawy teoretyczne izolacji bazującej na zjawisku podziału analitów.
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Superconducting Energy Gap in Hole-Doped Graphene Beyond the Migdal's Theory
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Method and system for disciplining a local reference oscillator by GPS 1PPS signal
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Dissociative electron attachment to gas phase thiothymine: experimental and theoretical approaches
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Standard gas mixtures- indispensable reference materials in the analysis of gaseous media
PublikacjaIn recent years the need for the quality control and assurance of analytical measurement results has been particularly strongly emphasised. Certified reference materials play an invaluable role in this process. The article characterises the basic types of reference materials, focusing in particular on those in the gaseous state. It also reviews the literature on the techniques of preparing standard gas mixtures over the last ten...
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Accelerated solvent extraction-gas chromatographic determination of acidic herbicides in soil
PublikacjaPrzyspieszona ekstrakcja rozpuszczalnikiem z wykorzystaniem wody jako ekstraktanta okazała się skutecznym sposobem izolacji herbicydów kwasowych (MCPP, MCPA, 2,4-D, 2,4,5-T, PCP, dinoseb, dinoterb) z próbek gleby. Wysoka zawartość substancji iłowych powodowała problemy techniczne, które udało się pokonać poprzez zwiększenie stosunku piasku do gleby w celce ekstrakcyjnej. Anality przenoszono z ekstraktu wodnego do rozpuszczalnika...
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A low-band gap, nitrogen-modified titania visible-light photocatalyst
PublikacjaFotokatalizatory tlenku tytanu(IV) zmodyfikowanego azotem zostały zsyntetyzowane poprzez ogrzewanie wodorotlenku tytanu i mocznika w temperaturze 400ºC. Otrzymane fotokatalizatory charakteryzują się silną absorpcją w zakresie promieniowania widzialnego (400-500 nm) odznaczając się niskimi wartościami energii pasma wzbronionego (2,20 i 2,46 eV). Aktywność fotokatalityczną w świetle widzialnym potwierdzono przeprowadzając reakcję...
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Liquid circulation in the agitated airlift reactor with the high gas disengagement zone
PublikacjaPrzedstawiono doświadczalne zależności stopnia zatrzymania gazu i prędkości cyrkulacji cieczy od prędkości przepływu gazu i częstości obrotów mieszadła. Obserwowano wzrost prędkości cyrkulacji cieczy ze wzrostem wysokości strefy napowietrzania. Dla niskich częstości obrotów mieszadła prędkość cyrkulacji cieczy wzrastała wraz ze wzrostem prędkości przepływu gazu, natomiast dla wysokich cząstości obrotów mieszadła prędkość cyrkulacji...
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Weakly nonlinear dynamics of short acoustic waves in exponentially stratified gas
PublikacjaRozpatruje się dynamika krótkich (w porównywaniu z charakterystyczną skalą zmiany gęstości gazu atmosferycznego) fal akustycznych. Wyprowadzone nowe równanie ewolucyjne, które uwzględnia dyspersję i nieliniowy charakter propagacji tych fal. Porównuje sie liniowa i nieliniowa dynamika. Ilustracje propagacji, numeryczne wyliczione na podstawie nowych wzorów, są przedstawione. Indexed and abstracted (from vol. 32(1) 2007) in Science...
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Projektowanie układów geometrycznych toru w dostosowaniu do systemu GPS
PublikacjaW pracy zwrócono uwagę na fakt, że zastosowanie satelitarnej techniki pomiarowej (w wariancie pomiarów ciągłych) powoduje konieczność opracowania nowej metody projektowania układów geometrycznych toru. Ponieważ kształtowanie kierunków prostych trasy na podstawie pomiarów satelitarnych nie sprawia żadnych trudności, skupiono się na kwestii projektowania odcinków położonych w łuku. Założono, że projektowanie układu geometrycznego...
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Badania odbioru sygnałów systemu GPS w obecności sygnałów zakłócających
PublikacjaNiniejszy artykuł poświęcono opisowi badań możliwości odbioru - w obecności zakłóceń - sygnałów transmitowanych w systemie nawigacji satelitarnej GPS. Tytułem wstępu dokonano ogólnej charakterystyki tego systemu. W części drugiej wymieniono rodzaje zagrożeń stojących przed użytkownikami usługi lokalizacji. Następnie, przedstawiono schemat stanowiska badawczego do oceny wpływu zakłóceń na odbiór sygnałów nawigacyjnych. W punkcie...
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Control of mass concentration of reagents by sound in a gas with nonequilibrium chemical reactions
PublikacjaThe weakly nonlinear dynamics of a chemically reacting gas is studied. Nonlinear interaction of acoustic and nonacoustic types of motion are considered. We decompose the base equations using the relationships of the gas-dynamic perturbations specific for every type of motion. The governing equation for the mass fraction of a reagent influenced by dominating sound is derived and discussed. The conclusions concern the equilibrium...
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Operational causes of fatigue failures within the passages of gas turbine engines
PublikacjaThe short profile of a fatigue wear process of gas turbine engine's constructional elements has been introduced in the article. The primary causes of a fatigue cracks formation within the mechanical system as well as within the passages of the engine have been showed. Especial attention was devoted to the low-cycle fatigue, what is associated with unsteady thermal-flow processes being worked out in the passages.The selected damages...
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Enantioselective comprehensive two-dimensional gas chromatography of lavender essential oil
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Effects of a rotating magnetic field on gas-liquid mass transfer coefficient
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The Effect of CO2 Gas Emissions on the Market Value, Price and Shares Returns
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Thermal failure of a second rotor stage in heavy duty gas turbine
PublikacjaThe impulse mode of operation and the supply of various types of fuels causes frequent failures even in the heavy duty gas turbines. The paper presents the ravages of second rotor stage failure in a gas turbine. The excessive thermal elongation rise caused by fuel change was indicated as the main cause. We applied nonlinear numerical analysis, preceded by thermodynamic calculations of the turbine and visual inspection of the effects...
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On design and analysis of flow characteristics of the last stage of gas-steam turbine
PublikacjaResearch regarding blade design and analysis of flow have been conducted for over a century. Meanwhile new concepts and design approaches were created and improved. Advancements in information technologies allowed to introduce computational fluid dynamics (CFD) and computational flow mechanics (CFM). Currently a combination of mentioned methods is used for design of turbine blades. These methods enabled us to improve flow efficiency...
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Degradation of protective coatings in steel chimneys of flue gas desulfurisation system
PublikacjaThis paper presents problems associated with corrosion of steel stacks and changes in philosophy of corrosion protection when implemented into flue gas desulphurization systems. In-situ tests were taken by means of electrochemical impedance spectroscopy at the stack which discharges flue gas before wet lime/limestone desulphurization. A very quick electrolyte absorption by the spherical infill vinylester coating was found using...
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Mobile Gas Chromatographs Coupled with Mass and Ion Mobility Spectrometers and their Applications
PublikacjaThe articles describes the developments un combining of mass and ion mobility spectrometers (MS, IMS0 with miniature gas chromatographs (GC). The examples of applications of miniaturised GC-MS and GC-IMS devices are presented.
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Investigation of long-range dependencies in the stochastic part of daily GPS solutions
PublikacjaThe long-range dependence (LRD) of the stochastic part of GPS-derived topocentric coordinates change (North, East, Up) results with relatively high autocorrelation values with a focus on self-similarity. One of the reasons for such self-similarity in the GPS time series are noises that are commonly recognised to prevail in the form of the flicker noise model. To prove the self-similarity of the stochastic part of GPS time series...
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Detection of apple in orange juice using ultra-fast gas chromatography
PublikacjaThe determination of authenticity is an increasingly important issue for food quality and safety. The use of an electronic nose based on ultra-fast gas chromatography technique ensures rapid analysis of the volatile compounds from food products. Due to the fact that this technique enables chemical profiling of agricultural products, it can be an effective tool for authentication when combined with chemometrics. In this article...
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Analysis of odor interactions in ternary gas mixtures using electronic nose
PublikacjaIn recent years there has been a noticeable increase in interest in the use of electronic noses in analytical chemistry. These devices perform a holistic analysis of the gas mixtures composition, without the separation and identification of its individual components. For this reason e-noses are increasingly replacing the conventional olfactometers, due to the significantly shorter analysis time and possible automation. In the work...
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Nonlinear Interaction of Modes in a Planar Flow of a Gas with Viscous and Thermal Attenuation
PublikacjaThe nonlinear interaction of wave and non-wave modes in a gas planar flow are considered. Attention is mainly paid to the case when one sound mode is dominant and excites the counter-propagating sound mode and the entropy mode. The modes are determined by links between perturbations of pressure, density, and fluid velocity. This definition follows from the linear conservation equations in the differential form and thermodynamic...
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Non-matrix reference materials-the challenges in the preparation of standard gas mixtures
PublikacjaIn the last few years particularly great pressure is exerted on quality control and assurance of analytical measurement results. An invaluable role in this process is played by reference materials. The paper presents the characteristics of basic types of reference materials, with particular attention to gaseous reference materials.
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Preparation and characterization of asphaltene based adsorbents for gas-solid adsorption systems
PublikacjaThe dissertation presents results of the experimental research on asphaltene-based adsorbents (support coated with asphaltene layer) for gas-solid adsorption systems, with special reference to volatile organic compounds (VOCs) removal from gas streams. Analysis of gas adsorption properties revealed that asphaltenes isolated from oxidized bitumen have strong affinity toward VOCs. Interactions with target gas molecules, and selectivity...
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GVC involvement and the gender wage gap: Micro -evidence on European countries
PublikacjaWe examine linkages between involvement in global value chains (GVCs) and gender wage inequalities. We use merged data from Structure of Earnings Survey and the World Input Output Database covering 18 European countries. We employ information on employees’ personal and company characteristics and a sectoral involvement in GVCs. In general, the wages of workers from sectors more involved in GVCs are lower. However, the relationship...
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CLAY MINERALS – MINERALOGY AND PHENOMENON OF CLAY SWELLING IN OIL & GAS INDUSTRY
PublikacjaAmong the minerals found in the earth's crust, clay minerals are of the widest interest. Due to the specific properties such as plasticity, absorbing and catalytic properties clay minerals are used in many industries (oil & gas, chemistry, pharmacy, refractory technology, ceramics etc.). In drilling, a phenomenon of swelling clays is frequently observed. It has an important impact on the cementing quality. During the last few decades...
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Control system for contactless electrical energy transfer with varying air gap
PublikacjaInductive power transfer (IPT) is a system by which electrical energy may be transmitted without electrical connection through a large air gap between coils. Systems usually considered in the literature are the ones with a constant air gap. The paper describes the analysis of IPT, which allows for supplying an electrical load in the conditions of slow, in relation to the dynamics of power supply, changes in the dimensions of the...
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Thermal self-action effects of acoustic beam in a vibrationally relaxing gas
PublikacjaThermal self-action of acoustic beam in a molecular gas with excited internal degrees of molecules’ freedom, is studied. This kind of thermal self-action differs from that in a Newtonian fluid. Heating or cooling of a medium takes place due to transfer of internal vibrational energy. Equilibrium and non-equilibrium gases, which may be acoustically active, are considered. A beam in an acoustically active gas is self-focusing unlike...
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A commercial gas boiler fitted with the ORC module as perspective solution for households
PublikacjaIn this paper the applicability of the commercial gas boiler (De Dietrich DTG X23N) coupled with the laboratory prototype micro ORC setup was experimentally studied. The main objective was to determine the working fluid capability to obtain required temperatures of vapour prior to the turbine, attainable heat rates and efficiencies of the whole system. The boiler thermal power was 25 kW. Tests were carried out with a single stage...
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Zastosowanie filtracji przestrzennej do eliminacji spoofingu w systemie GPS
PublikacjaArtykuł podejmuje problematykę przeciwdziałania atakowi elektronicznemu typu spoofing w systemie GPS, polegającemu na niepowołanej transmisji imitacji sygnałów odbieranych z satelitów nawigacyjnych tego systemu. Odbiór sygnałów imitujących powoduje wyznaczenie nieprawidłowych wskazań czasu, położenia i prędkości odbiornika GPS. Proponowaną w artykule metodą ochrony odbiornika przed działaniem sygnałów imitujących jest adaptacyjna...
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Method of selecting the LS-SVM algorithm parameters in gas detection process
PublikacjaIn this paper we showed the method of resistive gas sensors data processing. The UV irradiation and temperature modulation was applied to improve gas sensors’ selectivity and sensitivity. Noise voltage across the sensor’s terminals (proportional to its resistance fluctuations) was recorded to estimate power spectral density. This function was an input data vector for LS-SVM (least squares – support vector machine) algorithm, which...
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Investigation of solid polymer electrolyte gas sensor with different electrochemical techniques
PublikacjaIn this work solid polymer electrolyte (SPE) amperometric sulphur dioxide sensor is investigated. Nafion was used as a membrane electrode and 1M sulphuric acid as an internal electrolyte. Sensor response to sulphur dioxide was measured. Besides traditional constant voltage amperometry also different electrochemical techniques were used. Results obtained by these methods are compared.
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Bridging the gap between business process models and use-case models
PublikacjaToday's software development methodologies are equipped with a plethora of methods and techniques for business process engineering and Requirements Engineering. However, heavy investments in IT have not brought forth expected results. What seems to be lacking is a systematic approach that consolidates both disciplines to gain a synergistic effect. To address this challenge we extend Use-Case Driven Approach (UCDA) by binding use...
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Ag/Pt-modified TiO2 nanoparticles for toluene photooxidation in the gas phase
PublikacjaAg/Pt-modified TiO2nanocomposites were synthesized using the sol–gel method. The effect of metal typeand amount as well as synthesis route on the photocatalytic activity in reaction of toluene removal, usedas a model volatile organic compound, was investigated. Toluene, at the concentration of about 200 ppm,was irradiated over modified TiO2using light-emitting diodes (LEDs, max= 415 nm). The results showedthat toluene could be...
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Standard gas mixtures- indispensable reference materials in the analysis of gaseous media
PublikacjaIn recent years the need for the quality control and assurance of analytical measurement results has been particularly strongly emphasised. Certified reference materials play an invaluable role in this process. The article characterises the basic types of reference materials, focusing in particular on those in the gaseous state. It also reviews the literature on the techniques of preparing standard gas mixtures over the last ten...
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On the Nonlinear Effects of Magnetoacoustic Perturbations in a Perfectly Conducting Viscous and Thermoconducting Gas
PublikacjaNonlinear effects of planar and quasi-planar magnetosound perturbations are discussed. The plasma is as- sumed to be a Newtonian thermoconducting gas with infinite electrical conductivity permeated by a magnetic field orthogonal to the trajectories of gas particles. Generation of the non-wave modes (magnetoacoustic heating and streaming) in the field of periodic and aperiodic magnetoacoustic perturbations is discussed. The results...
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Implementing Sustainable Development Goals with Digital Government – Aspiration-capacity gap
PublikacjaSustainable Development Goals (SDGs) represent a commitment by all United Nations Member States to pursue development efforts, including ending poverty and hunger, promoting well-being and education, reducing inequalities, fostering peace, and protecting the planet. Member States and their governments are supposed to take ownership of the SDGs, strengthen the implementation means, and improve public governance as both the means...
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Two-Dimensional Gas Chromatography Coupled With Mass Spectrometry in Food Analysis
PublikacjaThe development of instrumental analytical techniques provided the opportunity for in-depth characterization of many food matrices. In particular, the use of gas chromatography coupled with mass spectrometry gives impressive results in terms of quality and authenticity testing, conducting food freshness evaluations and contamination assessments. A new variant of gas chromatography, namely two-dimensional gas chromatography (GC...