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Photophysics of electrophosphorescent platinum (II) porphyrin in solid films
PublikacjaW pracy badano elektronowe procesy w porfirynowym kompleksie platyny (PtOEP) umieszczonej w matrycy polimerowej lub w postaci warstw uzyskanych przez próżniowe naparowanie. Mierzono widma absorpcji i emisji oraz wykonano pomiary elektromodulowanej luminescencji i fotoprzewodnictwa. Przeprowadzono wszechstronną dyskusję własności stanów wzbudzenia elektronowego w PtOEP w kontekscie zastosowania tego związku w organicznych diodach...
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Frontispiece: Tuning of High Spin Ground State and Slow Magnetic Relaxation within Trimetallic Cyanide‐Bridged {Ni II x Co II 9− x [W V (CN) 8 ] 6 } and {Mn II x Co II 9− x [W V (CN) 8 ] 6 } Clusters
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On the Role of Polarimetric Decomposition and Speckle Filtering Methods for C-Band SAR Wetland Classification Purposes
PublikacjaPrevious wetlands studies have thoroughly verified the usefulness of data from synthetic aperture radar (SAR) sensors in various acquisition modes. However, the effect of the processing parameters in wetland classification remains poorly explored. In this study, we investigated the influence of speckle filters and decomposition methods with different combinations of filter and decomposition windows sizes on classification accuracy....
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Projektowanie i analiza rekursywnych cyfrowych oscylatorów sygnałów sinusoidalnych i świergotowych
PublikacjaPrzedmiotem badań w rozprawie są rzeczywiste liniowe filtry cyfrowe rekursywne stacjonarne rzędu drugiego i wyższych, o dwu, trzech i więcej wyjściach - generujące, po pobudzeniu ich warunkami początkowymi, drgania niegasnące sinusoidalne lub przebiegi świergotowe na każdym wyjściu. Informacja o parametrach generowanych sygnałów jest zadawana w postaci warunków początkowych i współczynników struktury filtru. W rozprawie dokonano...
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Spectroscopic and cytotoxic characteristics of (p-cymene)Ru(II) complexes with bidentate coumarins and density functional theory comparison with selected Pd(II) complexes
PublikacjaThis paper presents the synthesis of two new (p-cymene)-ruthenium(II) complexes with the bidentate coumarin ligands. Both complexes were characterized by FTIR spectroscopy, 1H NMR, 13C NMR, MS, elemental analysis and DFT calculations. The X-ray structure of complex 3a was also solved. The cytotoxic properties of both complexes were examined on human leukemia NALM-6 and HL-60 cells and melanoma WM-115 cells. The complexes possess...
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Zero phase shift digital filtering for assessment of exposure to non-sinusoidal magnetic fields
PublikacjaAccuracy of assessment of human body exposure to magnetic fields is affected by several uncertainty sources. One of them is estimation of the total exposure to non-sinusoidal fields. Standard methods can be implemented using analogue or digital filters that introduce a phase shift that affect the result of total exposure level estimation. The paper presents a new method that allows performing more precise assessment of exposure...
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Series Passive Compensation of Common Mode Voltage in Multilevel Inverter Drives
PublikacjaThis paper presents an approach to the problem of a magnetic saturation of CM chokes that accompanies the method of passive compensation of a common mode (CM) voltage in an inverter drive system. Measurements have been provided in a drive system including multilevel inverters and the filter having sinusoidal output voltages and zero CM voltage. The theoretical analysis and experimental results show that the problem with magnetic...
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Układy napędowe z silnikami indukcyjnymi i filtrami wyjściowymi falowników : Zagadnienia wybrane. - J. Guziński.
PublikacjaMonografia przedstawia zagadnienia związane z układami napędowymi z silnikami indukcyjnymi i filtrami wyjściowymi falowników. Pokazano problemy składowej zerowej, prądów łożyskowych oraz układów do ograniczania niekorzystnych efektów zasilania falownikowego. Omówiono wybrane struktury filtrów wraz z zaleceniami projektowymi. Skupiono się na estymacji zmiennych stanu oraz metodach sterowania przy uwzględnieniu modelu filtru sinusoidalnego....
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Ocena możliwości zautomatyzowanej analizy obrazów z badań endoskopowych do wspomagania diagnostyki gastropatii wrotnej
PublikacjaAnaliza obrazów z powszechnie wykonywanych badań endoskopowych jest jedną z możliwych metod wykrywania wczesnego stadium gastropatii wrotnej fragmentów przewodu pokarmowego człowieka. W artykule przedstawiono opis eksperymentów związanych z utworzeniem autorskiego algorytmu wykrywania gastropatii na obrazach z nagrań badań endoskopowych w celu wspomagania procesu diagnostycznego. Przedstawiono cechy charakterystyczne schorzenia....
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Lithium tetrakis(tri-tert-butoxysilanethiolato)gallate(III). Acta Cryst.Sect. E Struct. Rep. [online]**2002 vol. 58 s. m728-m729, 1 rys. 1 tab. bibliogr. 13 poz. Tetrakis(tri-tert-butoksysilanotiolano)gallan(III) litu.
PublikacjaPraca opisuje syntezę oraz strukturę krystaliczną i cząsteczkową tetrakis(tri-tert-butoksysilanotiolano)gallanu(III) litu. Kation litu jest koordynowany wewnątrz cząsteczki przez dwa atomy tlenu z dwóch grup tert-butoksylo-wych. Strukturę wyznaczono stosując rentgenowską analizę strukturalną mono-kryształu.
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Interactions of fish gelatin and chitosan in uncrosslinked and crosslinked with EDC films: FT-IR study
PublikacjaFilms based on fish gelatin, chitosan and blend of fish gelatin and chitosan before and after cross-linking with EDC have been characterized by FT-IR spectroscopy. The FT-IR spectrum of fish gelatin film showed the characteristic amide I, amide II and amide III bands, and the FT-IR spectrum of chitosan film confirmed that the polymer was only a partially deacetylated product, and included CH3-C=O and NH2 groups, the latter both...
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Monitoring Lead Concentration in the Surrounding Environmental Components of a Lead Battery Company: Plants, Air and Effluents—Case Study, Kenya
PublikacjaLead (Pb) pollution from smelters and lead–acid battery has become a serious problem worldwide owing to its toxic nature as a heavy metal. Stricter regulations and monitoring strategies have been formulated, legislated and implemented in various parts of the world on heavy metal usage. Developed countries such as the USA and in Europe largely operate within the set standards, however, developing countries such as Kenya, Nigeria...
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Influence of Thermal Decomposition of Wood and Wood-Based Materials on the State of the Atmospheric Air. Emissions of Toxic Compounds and Greenhouse Gases
PublikacjaThis paper presents the energy characteristics of wood and wood-based materials in the form of commercially available pellets, furniture board (MDF) and OSB. Toxicometric indices were determined for gaseous destructs arising from thermal decomposition and combustion of the materials studied. The paper proves that combustion conditions are crucial in terms of toxic destructive emissions. It has been shown that the combustion of...
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The impact of air humidity on the operation of proton exchange membrane fuel cells determined using dynamic electrochemical impedance spectroscopy
PublikacjaThis paper describes the changes in the fuel cell impedance across a range of current loads and humidity changes. The changes of each equivalent circuit parameters representing specific processes occurring in fuel cells, as a function of humidity and current changes, were determined. Within the combined scope of current and humidity, the optimal working conditions of the cells were determined, corresponding to the lowest impedance...
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A framework for Air Quality Management Zones - Useful GIS-based tool for urban planning: Case studies in Antwerp and Gdańsk
PublikacjaThere is a growing recognition of the importance of proper urban design in the improvement of air flow and pollution dispersion and in reducing human exposure to air pollution. However, a limited number of studies have been published so far focusing on the development of standard procedures which could be applied by urban planners to effectively evaluate urban conditions with respect to air quality. To fill this gap, a new approach...
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Solvent Impact on the Diversity of Products in the Reaction of Lithium Diphenylphosphide and a Ti(III) Complex Supported by a tBu2P–P(SiMe3) Ligand
PublikacjaWe present two important trends in the reactivity ofthe titanium complex [MeNacNacTi(Cl){η2-P(SiMe3)-PtBu2}](MeNacNac− = [Ar]NC(Me)CHC(Me)N[Ar]; Ar = 2,6-iPr2Ph)with nucleophilic reagents RLi (R = Ph2P,tBuO, (Me3Si)2N, andtBu2N) depending on the reaction medium. Reaction in nonpolarsolvent (toluene) leads to three main products: via an autoredoxprocess and nucleophilic substitution at the Ti-atom to afford theTi(IV) complex [MeNacNacTi(R){η2-P-PtBu2}]...
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Bimodal Nd-Doped LuVO4 Nanoprobes Functionalized with Polyacrilic Acid for X-Ray Computed Tomography and NIR Luminescent Imaging
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High Cu content LaNi1-xCuxO3-δ perovskites as candidate air electrode materials for Reversible Solid Oxide Cells
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Air Pollution Research Based on Spider Web and Parallel Continuous Particulate Monitoring—A Comparison Study Coupled with Identification of Sources
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A compartment model of alveolar–capillary oxygen diffusion with ventilation–perfusion gradient and dynamics of air transport through the respiratory tract
PublikacjaThis paper presents a model of alveolar–capillary oxygen diffusion with dynamics of air transport through the respiratory tract. For this purpose electrical model representing the respiratory tract mechanics and differentia equations representing oxygen membrane diffusion are combined. Relevant thermodynamic relations describing the mass of oxygen transported into the human body are proposed as the connection between these models,...
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Euro III / Euro IV Emissions - A Study of Cold Start and Warm Up Phases with a SI (Spark Ignition) Engine
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Occurrence of fungi and cytotoxicity of the species: Aspergillus ochraceus, Aspergillus niger and Aspergillus flavus isolated from the air of hospital wards
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Weryfikacja i aktualizacja "Katalogu typowych konstrukcji nawierzchni podatnych i półsztywnych" z 1997 roku - Etap III
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Nanosized carbon black as synergist in PP/POE-MA/IFR system for simultaneously improving thermal, electrical and mechanical properties
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Exhaust gas temperature measurements in diagnostic examination of naval gas turbine engines. Part III. Diagnostic and operating tolerances
PublikacjaThe third part of the article presents a method for detecting failures of the automatic engine control system with the aid of an exhaust gas temperature setter, specially designed and machined for this purpose. It also presents a procedure of identifying the operating tolerances and determining the diagnostic tolerances for the exhaust gas temperature recorded in the naval turbine engine during the start-up and acceleration processes....
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Preliminary study of possible relationships between exposure to PCDD/Fs and dl-PCBs in ambient air and the length of life of people
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Air pollution in the places of Betula pendula growth and development changes the physicochemical properties and the main allergen content of its pollen
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Physicochemical profile of Os (III) complexes with pyrazine derivatives: From solution behavior to DNA binding studies and biological assay
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Application of passive sampling technique for monitoring of BTEX concentration in urban air: Field comparison of different types of passive samplers
PublikacjaW efekcie przeprowadzonych badań potwierdzono przydatności techniki dozymetrii pasywnej wykorzystywanej na etapie izolacji i wzbogacania analitów do uzyskania informacji o poziomie stężeń zanieczyszczeń z grupy BTEX w powietrzu atmosferycznym na terenie aglomeracji Trójmiejskiej. Dodatkowo, porównano wyniki oznaczeń uzyskanych z wykorzystaniem dwóch typów dozymetrów pasywnych.
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Determination of volatile aliphatic amines in air by solid phase microex traction coupled with gas chromatography with flame ionization detection.
PublikacjaOpisano nową metodę oznaczania lotnych amin alifatycznych w powietrzu. Metodyka oparta jest na zastosowaniu techniki mikroekstrakcji do fazy stacjonarnej na etapie pobierania próbek oraz zestawu GC-FID do rozdzielania i oznaczania poszczególnych analitów.Badaniom poddano nowe typy faz stacjonarnych.Zbadano wpływ wilgotności powietrza na proces pobierania próbek analitów z powietrza.
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Experimental and numerical study of thermal and electrical potential of BIPV/T collector in the form of air-cooled photovoltaic roof tile
PublikacjaAmong renewable energy sources, Building-Integrated Photovoltaic/Thermal (BIPV/T) systems are gaining increasing interest. To improve their economic competitiveness, technologies that increase their efficiency are searched for. The paper is devoted to evaluating the impact of various air-cooling configurations on the thermal and electrical performance of a photovoltaic roof tile. A numerical model of the own experimental system...
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Technical foundations for noninvasive assessment of changes in the width of the subarachnoid space with near-infrared transillumination-backscattering sounding (NIR-TBSS)
PublikacjaPraca opisuje metodę transiluminacji w bliskiej podczerwieni umożliwiającą nieinwazyjne monitorowanie zmian szerokości przestrzeni podpajęczynówkowej oraz amplitudy tętnienia naczyń powierzchniowych mózgu.
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Investigation of RH effect on uncommon limonene ozonolysis products and SOA formation in indoor air with real time measurement techniques
PublikacjaScientific interest in SOA influence on indoor air quality increases since last 20 years. It is well known, that particles of nano-sized diameter pose a threat for human health causing, among others: eye, upper airway irritation, inflammatory response in cells, worsening asthma, hypertension, diabetes, and central nervous dysfunction. Terpenes are reactive VOCs, commonly emitted in indoor air and considered to be SOA precursors...
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A new approach in the calibration of passive samplersA new approach on the calibration of passive dosimeters for studies of indoor air (....--------ROZBIEŻNOŚĆ TYTUŁÓW-------------------------------------
PublikacjaPrzedstawiono problematykę kalibracji próbników pasywnych wykorzystywanych w Katedrze Chemii Analitycznej Wydz. Chemicznego PG do monitoringu jakości powietrza wewnętrznego. Proponowane podejście pozwala na oszacowanie wartości stałych kalibracyjnych, a tym samym oznaczenia stężeń związków od heksanu do dodekanu. Tak więc permeacyjne dozymetry pasywne mogą być wykorzystane w analogicznym zakresie jak próbniki aktywne.
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High-temperature Corrosion of ~ 30 Pct Porous FeCr Stainless Steels in Air: Long-Term Evaluation Up to Breakaway
PublikacjaIn this work, a long-term (up to 6000 hours) corrosion evaluation of three porous (~ 30 pct of initial porosity) ferritic iron-chromium alloys with different Cr contents (20, 22, and 27 wt pct of Cr) was carried out at 600 C, 700 C, 800 C, and 900 C in air. Mass gain measurements and SEM analyses revealed that at temperatures above 600 C, all alloys exhibit breakaway corrosion, whereas at 600 C, none of the alloys were heavily...
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Application of Electronic Nose to Ambient Air Quality Evaluation With Respect to Odour Nuisance in Vicinity of Municipal Landfills and Sewage Treatment
PublikacjaThis chapter contains information about application of the electronic nose type instruments to evaluation of ambient air odour quality connected with such sectors of human activity as municipal landfills or sewage treatment plants. The authors present potential sources of emission from these sectors, characterize the chemical compounds responsible for presence of unpleasant odours, describe the influence of those compounds on human...
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Comparison of the Measurement Techniques Employed for Evaluation of Ambient Air Odour Quality Influenced by Operation of Industrial Sewage Treatment Plant
PublikacjaThe paper presents the results of investigation on ambient air quality evaluation with respect to concentration of odorants in a vicinity of a sewage treatment plant of the LOTOS Group S.A. petroleum plant. The investigation was performed during winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type...
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Structure of solvation water around the active and inactive regions of a type III antifreeze protein and its mutants of lowered activity
PublikacjaWater molecules from the solvation shell of the ice-binding surface are considered important for the antifreeze proteins to perform their function properly. Herein, we discuss the problem whether the extent of changes of the mean properties of solvation water can be connected with the antifreeze activity of the protein. To this aim, the structure of solvation water of a type III antifreeze protein from Macrozoarces americanus (eel...
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Experimental and comparative study on the two-phase pressure drop of air-water mixture in U-bend and straight pipe annuli
PublikacjaIn this paper, the experimental and theoretical analysis of pressure drop in singlephase and two phase-flow were presented for straight and U-bend smooth tube annulus and tube annulus with wire coil insert. Experiments for various boundary conditions were performed. In case of U-tube and straight tube with and without turbulator, tests were made for the water-water and air-water systems. The study covered a wide measuring range,...
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Evaluation the environmental fate of pharmaceuticals using a level III model based on poly-parameter linear free energy relationships
PublikacjaOpisano możliwości zastosowania modelu ''Level III Model'' do opisu losu środowiskowego pozostałości farmaceutyków w środowisku. Zastosowany model umożliwia oszacowanie trwałości, stężeń oraz transportu poszczególnych zanieczyszczeń pomiędzy poszczególnymi elementami składowymi środowiska (powietrze, woda, gleba i osady denne).
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Wykorzystanie analogowych filtrów aktywnych w diagnostyce łożysk silników indukcyjnych. Zastosowanie Komputerów w Nauce i Technice. XIII cykl seminariów zorganizowanych przez PTETiS, Oddział Gdańsk.
PublikacjaDziedziną zainteresowań autorów referatu jest diagnostyka silników indukcyjnych a szczególnie diagnostyka przy wykorzystaniu prądu zasilającego silnik.
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The comparison of the removal of copper(II) and zinc(II) ions from aqueous solution using 2,6-diaminopyridine in a polymer inclusion membrane and in a classic solvent extraction
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Pozorne objętości molowe oraz ściśliwości adiabatyczne nadchloranów i chlorków metali szeregu Mn(II) - Zn(II) w N,N-dimetyloacetamidzie
Publikacja.
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Novel Diazocrowns with Pyrrole Residue as Lead(II) Colorimetric Probes
PublikacjaNovel 18- and 23-membered diazomacrocycles were obtained with satisfactory yields by diazocoupling of aromatic diamines with pyrrole in reactions carried under high dilution conditions. X-ray structure of macrocycle bearing five carbon atoms linkage was determined and described. Compounds were characterized as chromogenic heavy metal ions receptors. Selective color and spectral response for lead(II) was found in acetonitrile and...
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The Reactivity of the Imine Bond within Polynuclear Nickel(II) Complexes
PublikacjaThree novel Ni complexes with the Schiff base ligand 2-methoxy-6-(E-2-pyridyliminomethyl)-phenol (L1) are described. In comparison with the similar 2-(pyridine-2-ylimino-methyl)phenol (pymp), the mode of coordination of L1 is altered due to the presence of methoxy substituent introducing the sterical hindrance. During the synthesis of the complexes, partial hydrolysis of the ligand was observed. Since such immediate hydrolysis...
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Sulfurization of phosphanylphosphinidene ligand: Access to phosphinothioyltrithiophosphonato platinum(II) complexes
PublikacjaThe reactivity of phosphanylphosphinidene Pt(0) complexes [DppePt(η2-P–PtBu2)] (1) and [(pTol3P)2Pt(η2-P–PtBu2)] (2) toward sulfur was studied. Reactions of 1 and 2 with an excess of sulfur led to the formation of the first transition metal complexes 3 and 4 with phosphinothioyltrithiophosphonato ligands with the formula [tBu2P(=S)–P(=S)S2]2-. In contrast to previous reports on the phosphanylphosphinidene moiety sulfurization,...
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Lead(II)-selective ionophores for ion-selective electrodes: A review
PublikacjaIn potentiometry, high selectivity of the ion-selective membranes must be assured in order to reliably measure various analytes in clinical, industrial and environmental samples. Due to the toxic nature of lead(II) it is important to monitor Pb2+ distribution in natural waters. This may be achieved by implementation of ion-selective electrodes (ISEs) with high selectivity towards lead(II) and low detection limit. A great number...
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Modulation and multiplexing in ultra-broadband photonic internet: Part II
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An excess electron bound to urea oligomers. II. Chains and ribbons
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Concept of Compatibility Region for the Evaluation of IR UWB Electromagnetic Compatibility
PublikacjaThis paper presents a new proposal for the unified evaluation of ultra wideband and narrowband radio communication systems electromagnetic compatibility, called “compatibility region”. The idea of compatibility region is based on the relation between the ratio of narrowband to ultra wideband signal power in a receiver and some transmission quality indicators (bit error rate, effective data rate).