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Wyniki wyszukiwania dla: SMS
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The potential role of fatty acids in prostate cancer determined by GC–MS analysis of formalin-fixed paraffin-embedded tissue samples
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Dynamics of hepatitis B virus quasispecies heterogeneity in association with nucleos(t)ide analogue treatment determined by MALDI-TOF MS
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Recenzja książki ks. Tadeusza Zadykowicza, pt. Zasady dobrej turystyki, Lublin, Wydawnictwo KUL, Lublin 2019, ss. 172.
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Electrochemistry/mass spectrometry (EC/MS) for fast generation and identification of novel reactive metabolites of two unsymmetrical bisacridines with anticancer activity.
PublikacjaThe development of a new drug requires knowledge about its metabolic fate in a living organism, regarding the comprehensive assessment of both drug therapeutic activity and toxicity profiles. Electrochemistry (EC) coupled with mass spectrometry (MS) is an efficient tool for predicting the phase I metabolism of redox-sensitive drugs. In particular, EC/MS represents a clear advantage for the generation of reactive drug transformation...
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Method for the simultaneous determination of monoaromatic and polycyclic aromatic hydrocarbons in industrial effluents using dispersive liquid-liquid microextraction with GC-MS
PublikacjaWe present a new method for simultaneous determination of 22 monoaromatic and polycyclic aromatic hydrocarbons in postoxidative effluents from the production of petroleum bitumen using dispersive liquid-liquid microextraction coupled to gas chromatography and mass spectrometry. The eight extraction parameters including the type and volume of extraction and disperser solvent, pH, salting out effect, extraction and centrifugation...
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Miniaturized, green salting-out liquid–liquid microextraction coupled with GC–MS used to evaluate biogenic amines in wine samples
PublikacjaMonitoring of the biogenic amines (BAs) content in food products, including wine, is important due to the health and safety of consumers and from the quality control point of view. In a given study, simultaneous derivatization and salting-out liquid–liquid microextraction (SALLME) coupled with GC–MS for BAs determination from wine samples was developed. For the optimization the Box-Behnken design was applied, where three independent...
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Training Services in Small and Medium-sized Enterprises: Evidence from Poland
PublikacjaIn the knowledge-based economy knowledge and skills are becoming more and more significant for the success of companies. This applies also to firms from small and medium-sized enterprises (SMEs) sector. As large companies in many cases posses special divisions devoted to trainings, they normally have no problems with updating the knowledge and skills of their employees. The situation is different with regard to SMEs, which often...
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Mechanochemically synthesized Mn3O4@β-cyclodextrin mediates efficient electron transfer process for peroxymonosulfate activation
PublikacjaThe rational surface engineering of heterogeneous catalysts is of great significance in advanced oxidation processes (AOPs) for eliminating refractory contaminants but remains challenging. In this study, β-cyclodextrin modified Mn3O4 (Mn3O4@β-CD) was prepared through a mechanochemical approach for peroxymonosulfate (PMS) activation, which achieved efficient bisphenol A (BPA) removal via electron transfer process (ETP). The reactive...
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Performance of Vector-valued Intensity Measures for Estimating Residual Drift of Steel MRFs with Viscous Dampers
PublikacjaViscous Dampers (VDs) are widely used as passive energy dissipation system for improving seismic performance levels especially in retrofitting of buildings. Residual Inter-story Drift Ratio (R-IDR) is another important factor that specifies the condition of building after earthquake. The values of R-IDR illustrates the possibility of retrofitting and repairing of a building. Therefore, this study aims to explore the vector-valued...
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Impact of slow breathing on the blood pressure and subarachnoid space width oscillations in humans
PublikacjaThe aim of the study was to assess cardiac and respiratory blood pressure (BP) and subarachnoid space (SAS) width oscillations during the resting state for slow and fast breathing and breathing against inspiratory resistance. Experiments were performed on a group of 20 healthy volunteers (8 males and 12 females; age 25.3 ± 7.9 years; BMI = 22.1 ± 3.2 kg/m2). BP and heart rate (HR) were measured using continuous finger-pulse photoplethysmography....
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Combination of hydrodynamic cavitation and SR-AOPs for simultaneous degradation of BTEX in water
PublikacjaHydrodynamic cavitation (HC) is an emerging technology gaining interest in water treatment for use in elimination of a wide range of organic pollutants. The energy released during cavitation phenomenon has number of applications and, particularly, it can be utilized for activation of persulfate (PS) and peroxymonosulfate (PMS). In the present study, hybrid techniques: HC combined with persulfates – HC-PS and HC-PMS were tested...
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Adipokine and cytokine levels in patients with adrenocortical cancer, subclinical Cushing's syndrome and healthy controls
PublikacjaIntroduction In recent years researchers have focused at hormonal activity in Cushing’s syndrome (CS) in connection with metabolic disorders and the role of adipokines and cytokines secreted by the adipose tissue. The aim of the study was to investigate levels of adipokines and cytokines in patients with: subclinical CS (SCS) – in relation to hormonal parameters of hypercortisolemia, and, adrenocortical cancer (ACC). Materials...
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Usługi IP Multimedia Subsystem
PublikacjaW artykule przedstawiono usługi IP Multimedia Subsystem. Omówiono usługi "tradycyjne": obecności, usługę PoC i komunikatora oraz nowe, jak: konferencja HD, telewizja IP na platformie IMS, scentralizowane usługi IMS oraz szeroko dyskutowana zunifikowana komunikacja.
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A New Fuzzy Sliding Mode Controller with PID Sliding Surface for Underwater Manipulators
PublikacjaDesign of an accurate and robust controller is challenging topic in underwater manipulator control. This is due to hydrodynamic disturbances in underwater environment. In this paper a sliding mode control (SMC) included a PID sliding surface and fuzzy tunable gain is designed. In this proposed controller robustness property of SMC and fast response of PID are incorporated with fuzzy rules to reduce error tracking. In the control...
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Crucial factors for improving the ISO 14001 environmental management system
PublikacjaThe practice of using environmental management systems (EMS) ISO 14001 at the organisational level indicates that the efficacy of such solutions depends on many factors, both endogenous and exogenous in nature. This article aims to identify the fac- tors that determine the opportunities for the improvement of EMS in organisations, the analysis of the relationship between the factors and the classification of the factors due to...
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Can sodium 1-alkylsulfonates participate in the sodium dodecyl sulfate micelle formation?
PublikacjaThe aggregation behavior of sodium dodecyl sulfate (SDS) was studied in an aqueous solution in the presence of increasing concentrations of selected sodium 1-alkylsulfonates, namely sodium 1-octanesulfonate, sodium 1-decanesulfonate, and sodium 1-dodecanesufonate. The critical micelle concentration (CMC) of SDS was determined by conductivity and fluorescence intensity measurements. The steady-state fluorescence quenching experiments...
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Centralny serwer w multimedialnym systemie dyspozytorsko-teleinformatycznym STRADAR
PublikacjaPrzedstawiono architekturę i najnowsze funkcje centralnego serwera (Centrum) w rozproszonym systemie monitorowania akwenów morskich opracowanym dla straży granicznej. System umożliwia prezentację bieżącej i archiwalnej sytuacji na mapie, obrazu z kamer, rozmów telefonicznych oraz plików i wiadomości tekstowych (SMS) wymienianych przez funkcjonariuszy straży granicznej. W artykule skupiono się na nowych funkcjonalnościach centrum,...
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Conditions of Best Practice Transfer - Results of the Quick IGA Project
PublikacjaThe Quick IGA project supports the development of working and organizational structures in SMEs in order to increase the employment rate of women and elderly and concurrently increases innovation capacities. One of the main project’s tasks was to find best practices from SMEs in Nordic countries in that field (in the first step) and identify (in second step) possibilities and conditions of their implementation in SMEs in other...
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An optimal sliding mode control based on immune-wavelet algorithm for underwater robotic manipulator
PublikacjaIn this paper, a robust optimal Sliding Mode Controller (SMC) based on new algorithm of Artificial Immune System (AIS) is proposed for trajectory tracking of underwater manipulators. A new AIS algorithm is used to derive optimal values of surface parameters and boundary layer thickness in SMC with considering minimum torques and error. Surface parameters and boundary layer thickness are considered as antibody in AIS and Morlet...
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Quality Assurance of Educational Processes as the Foundation of the Quality Management System in Gdansk University of Technology
PublikacjaThe paper presents a model of quality management system (QMS) developed by the author in Gdansk University of Technology (GUT). The core of the model is internal quality assurance system of educational processes based on the ENQA guidelines. Next described in the paper steps of GUT QMS development are the implementation of one of the normative QMS models (e.g. ISO 9001, ISO/IEC 17025) in selected organizational units of GUT and...
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Enzo Di Natali, Bioetica e Magistero. Da Pio XII a Papa Francesco, Edizioni Medinova, Favara 2015, ss. 944
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Refleksja homonimistki po lekturze: Radosław Kaleta, „Białorusko-polska homonimia międzyjęzykowa”, Warszawa: Slawistyczny Ośrodek Wydawniczy, 2014, ss. 169
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Study of effect of phosphate and uranium ions on the thermal properties of surfactant-modified natural red clay using TG–FTIR–MS techniques
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Simultaneous determination of ibuprofen and its metabolites in complex equine urine matrices by GC-EI-MS in excretion study in view of doping control
PublikacjaA novel assay for the simultaneous determination of ibuprofen (IBU) and its four probable metabolites, 1-hydroxyibuprofen (1-OH IBU), 2-hydroxyibuprofen (2-OH IBU), 3-hydroxyibuprofen (3-OH IBU) and carboxyibuprofen (CBX IBU) in equine urine samples with the application of Gas Chromatography-Electron Ionization-Mass Spectrometry (GC-EI-MS) has been developed and elaborated. The new approach for sample preparation including minimizing...
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SLIDING MODE-PID FUZZY CONTROLLER WITH A NEW REACHING MODE FOR UNDERWATER ROBOTIC MANIPULATORS
PublikacjaDesign of an accurate and robust controller is a challenging topic in an underwater manipulator control. This is due to hydrodynamic disturbances in underwater environment. In this paper a sliding mode control (SMC) included a PID sliding surface and fuzzy tunable gain is designed. In this proposed controller robustness property of SMC and fast response of PID are incorporated with fuzzy rules to reduce error tracking. In the...
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MRAS-Based Switching Linear Feedback Strategy for Sensorless Speed Control of Induction Motor Drives
PublikacjaThis paper presents a newly designed switching linear feedback structure of sliding mode control (SLF-SMC) plugged with an model reference adaptive system (MRAS) based sensorless fieldoriented control (SFOC) for induction motor (IM). Indeed, the performance of the MRAS depends mainly on the operating point and the parametric variation of the IM. Hence, the sliding mode control (SMC) could be considered a good control alternative...
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Female entrepreneurship in Kazakhstan
PublikacjaWomen constitute the majority of the Kazakh population and, even though they live almost 10 years longer than men on average, they are far less economically active. Less than half of the female population take up employment. Women’s wages are often as much as 30% lower than men’s. The subjective reasons for undertaking economic activity as mentioned by women included: independence from the husband, low earnings of the husband and...
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Determination of non-steroidal anti-inflammatory drugs in natural waters using off-line and on-line SPE followed by LC coupled with DAD-MS
PublikacjaOpisano dwie metody pozwalające na jednoczesne oznaczanie zawartości niesterydowych leków przeciwzapalnych (difluisal, diklofenak, naproksen, tolmetin, fenoprofen, ibuprofen) w próbkach wodnych. Próbki przygotowywano do analizy z użyciem techniki ekstrakcji do fazy stałej (off-line i on-line). Natomiast oznaczeń końcowych dokonano z użyciem LC-DAD-MS. Sprawdzono kilka różnych kolumienek ekstrakcyjnych i wybrano RP-18 jako najlepsze...
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Ultrasound-assisted heterogeneous activation of persulfate and peroxymonosulfate by asphaltenes for the degradation of BTEX in water
PublikacjaThis study investigated – for the first time - the simultaneous degradation of benzene, toluene, ethylbenzene and o-xylene (BTEX) by persulfate (PS) and peroxymonosulfate (PMS) activated by asphaltenes (Asph) under ultrasound (US) irradiation. Advantageous properties such as high thermal stability, low production cost and extensive availability make asphaltenes as an appealing carbonaceous material for heterogeneous catalysis....
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Zastosowanie metody studium przypadku w kształceniu menedżerów
PublikacjaKształcenie z wykorzystaniem metod rozwiązywania problemów (problem-based learning) staje się coraz bardziej popularne na wszystkich poziomach kształcenia, również w edukacji biznesowej. Przykładem takiej metody jest studium przypadku (case study). Metoda studium przypadku pozwala na rozwijanie umiejętności i kompetencji wykorzystywanych przez menedżerów w ich pracy, np. umiejętności syntezy, identyfikacji problemów, czy podejmowania...
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Increased inspiratory resistance affects the dynamic relationship between blood pressure changes and subarachnoid space width oscillations
PublikacjaBackground and objective Respiration is known to affect cerebrospinal fluid (CSF) movement. We hypothesised that increased inspiratory resistance would affect the dynamic relationship between blood pressure (BP) changes and subarachnoid space width (SAS) oscillations. Methods Experiments were performed in a group of 20 healthy volunteers undergoing controlled intermittent Mueller Manoeuvres (the key characteristic of the procedure...
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Nanosorbents as Materials for Extraction Processes of Environmental Contaminants and Others
PublikacjaThe aim of this work focuses on the application of nanomaterials (NMs) in different sorp- tive extraction techniques for the analysis of organic contaminants from environmental samples of distinct matrix compositions. Without any doubt, the integration of specific NMs such as carbona- ceous nanomaterials, magnetic nanoparticles (MNPs), metal–organic frameworks (MOFs), silica na- noparticles, and ion-imprinted NPs with so lid-phase...
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Influence of low-temperature physical hardening on stiffness and tensile strength of asphalt concrete and stone mastic asphalt
PublikacjaThis paper presents laboratory testing of stiffness modulus and indirect tensile strength of three asphalt concrete (AC) and three stone mastic asphalt (SMA) mixes after isothermal storage at temperature of -20oC, at different time intervals up to 16 days. The tests under repeated dynamic loading showed physical hardening of all tested mixes which was manifested by an evident increase of their stiffness moduli after isothermal...
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Performance of Passive and Active Balancing Systems of Lithium Batteries in Onerous Mine Environment
PublikacjaTo use lithium-iron-phosphate battery packs in the supply systems of any electric mining equipment and/or machines, the required conditions of work safety must be met. This applies in particular to coal mines endangered by fire and/or explosion. To meet the spark-safety conditions, the cells (together with the battery management system—BMS) must be isolated from the influence of the environment, and therefore placed in special...
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Coupling of Blood Pressure and Subarachnoid Space Oscillations at Cardiac Frequency Evoked by Handgrip and Cold Tests: A Bispectral Analysis
PublikacjaThe aim of the study was to assess blood pressure–subarachnoid space (BP–SAS) width coupling properties using time–frequency bispectral analysis based on wavelet transforms during handgrip and cold tests. The experiments were performed on a group of 16 healthy subjects (F/M; 7/9) of the mean age 27.2 ± 6.8 years and body mass index of 23.8 ± 4.1 kg/m². The sequence of challenges was first handgrip and then cold test. The handgrip...
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Bezpieczeństwo w IP Multimedia Subsystem
PublikacjaAbstrakt Artykuł jest trzecim w cyklu prac poświęconych IP Multimedia Subsystem (IMS) - po przedstawieniu architektury i usług IMS, odpowiednio w zeszytach 12/2009 oraz 2-3/2011 Przeglądu Telekomunikacyjnego i Wiadomości Telekomunikacyjnych. W obecnym artykule przedstawiono sposoby zapewnienia bezpieczeństwa przy realizacji tych usług.Artykuł został podzielony został na trzy części w których omówiono ogólne wyzwania bezpieczeństwa...
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Sterowanie poziomami napięć i rozpływem mocy biernej na szczeblu operatora systemu przesyłowego. Systemy elektroenergetyczne:eksploatacja, stabilność, niezawodność, awarie i restytucje, modelowanie i symulacje.
PublikacjaPrzedstawiono docelową strukturę hierarchicznego systemu sterowania poziomami napięć i rozpływem mocy biernej w systemie elektroenergetycznym realizowana na szczeblu operatora systemu przesyłowego. Omówiono zadania z operatora systemu w tym zakresie, wymagana strukturę sprzętową EMS oraz strukturę programową EMS w zakresie sterowania napięciami i rozpływem mocy biernej.
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Small and Medium-sized Enterprises in Visegrad Countries towards Internationalisation Challenges in the European Union
PublikacjaThe chapter characterises and compares SMEs in Visegrad Countries and their international behaviours.
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Application of dynamic headspace and gas chromatography coupled to mass spectrometry (DHS-GC-MS) for the determination of oxygenated volatile organic compounds in refinery effluents
PublikacjaThe paper presents a new procedure for the determination of oxygenated volatile organic compounds (O-VOCs) in postoxidative effluents from the production of petroleum asphalt using dynamic headspace coupled to gas chromatography-mass spectrometry in the selected ion monitoring (SIM) mode (DHSGC-MS). Among the GC capillary columns tested, a polar SLB-IL111 column with the ionic liquid stationary phase was found to be superior due...
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Identyfikacja lotnych składników ścieków z instalacji oksydacji asfaltów z wykorzystaniem chromatografii gazowej sprzężonej ze spektrometrią mas (GC-MS)
PublikacjaW pracy przedstawiono wyniki badań nad identyfikacją lotnych związków organicznych występujących w ściekach z instalacji oksydacji asfaltów. Ścieki poddano deemulgacji, w celu usunięcia fazy organicznej, a następnie ekstrakcji dichlorometanem, w celu wyizolowania pozostałych w ściekach związków organicznych. Zidentyfikowano 30 związków organicznych oraz szereg n-alkanów, które pozostały w ściekach pomimo zastosowanej deemulgacji....
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Natalia Ejtminowicz, Katarzyna Urban, Antoni Zięba (red.), Ekologia prokreacji. Vademecum, Polskie Stowarzyszenie Obrońców Życia, Kraków 2016, ss. 360
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A comprehensive lipidomic analysis of oilseeds using LC-Q-TOF-MS and dispersive micro-solid phase (D-μ-SPE) extraction techniques
PublikacjaGrowing public health awareness increased the demand for natural products with positive health benefits. Vegetable oils containing omega-3 fatty acids (FA) such as alpha-linolenic acid (ALA) has been proposed as a possible source of eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA). In this work, a comprehensive lipidome analysis and comparison of seven oilseeds, including flaxseed, chia, hemp, black cumin, white sesame,...
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A method for a comprehensive lipidomic analysis of flaxseed (Linum usitatissimum) with the use of LC–Q-TOF-MS and dispersive micro-solid-phase (μDSPE) extraction
PublikacjaFlaxseed (FS) is one of the richest sources of α-linolenic acid oil and lignans, and it is suggested that the consumption of flaxseed may contribute to the prevention of certain chronic diseases such as many types of cancer, diabetes, cardiovascular diseases and cerebrovascular stroke. Here, we demonstrate a new method for comprehensive FS lipidome profiling with the use of LC–Q-TOF-MS and dispersive micro-solid-phase extraction....
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The use of RP-HPLC–Q-TOF–MS as a powerful tool for wastewater composition profiling and selection of water pollution marker specific to wastewater contamination
PublikacjaLimited drinking water resources and water pollution are one of the main worldwide problems. To reduce the consumption of fresh water resources, the use of treated wastewater has been proposed. The farmlands have been irrigated with wastewater for centuries, but the composition of used sewage has changed over the years. Recent research has revealed the presence of hundreds of new organic contaminants in many environmental waters,...
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Non-volatile molecular composition and discrimination of single grape white of chardonnay, riesling, sauvignon blanc and silvaner using untargeted GC–MS analysis
PublikacjaThis study developed and applied a GC–MS method aiming at molecular fingerprinting of 120 commercial single grape white wines (Chardonnay, Riesling, Sauvignon Blanc and Silvaner) for possible authentication according to grape variety. The method allowed detection of 372 peaks and tentative identification of 146 metabolites including alcohols, organic acids, esters, amino acids and sugars. The grape variety effect explained 8.3%...
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Concentration of Potentially Bioactive Compounds in Italian Extra Virgin Olive Oils from Various Sources by Using LC-MS and Multivariate Data Analysis
PublikacjaHigh quality extra virgin olive oils represent an optimal source of nutraceuticals. The European Union (EU) is the world’s leading olive oil producer, with the Mediterranean region as the main contributor. This makes the EU the greatest exporter and consumer of olive oil in the world. However, small olive oil producers also contribute to olive oil production. Beneficial effects on human health of extra virgin olive oil are well...
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Multimedialny system nadzoru dla straży granicznej – projekt STRADAR
PublikacjaSTRADAR jest systemem nadzoru przeznaczonym do wspierania działań operacyjnych morskiej straży granicznej, umożliwiającym zbieranie, przetwarzanie i udostępnianie informacji i danych pochodzących z takich sensorów, jak radary, kamery wideo, AIS, GPS, aparaty fotograficzne oraz z połączeń audio, wiadomości SMS, plików i notatek. Informacje te mogą być udostępniane na bieżąco oraz archiwalnie z synchronizacją zdarzeń lub bez synchronizacji....
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Environmental impact assessment of municipal biogas plants – case study
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Impact of Urbanization on Stormwater Runoff from a Small Urban Catchment: Gdańsk Małomiejska Basin Case Study
PublikacjaThis paper deals with the impact of different forms of urbanization on the basin outflow. The influence of changes in land cover/use, drainage system development, reservoirs, and alternative ways of stormwater management (green roofs, permeable pavements) on basin runoff was presented in the case of a small urban basin in Gdańsk (Poland. Seven variants of area development (in the period of 2000-2012) – three historical and four...
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Core loss resistance impact on sensorless speed control of an induction motor using hybrid adaptive sliding mode observer
PublikacjaInduction motors (IMs) experience power losses when a portion of the input power is converted to heat instead of driving the load. The combined effect of copper losses, core losses, and mechanical losses results in IM power losses. Unfortunately, the core losses in the motor, which have a considerable impact on its energy efficiency, are not taken into account by the generally employed dynamic model in the majority of the studies. Due...