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Wyniki wyszukiwania dla: zirconium alloys
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The Influence of Microstructure on the Passive Layer Chemistry and Corrosion Resistance for Some Titanium-Based Alloys
PublikacjaThe effect of microstructure and chemistry on the kinetics of passive layer growth and passivity breakdown of some Ti-based alloys, namely Ti-6Al-4V, Ti-6Al-7Nb and TC21 alloys, was studied. The rate of pitting corrosion was evaluated using cyclic polarization measurements. Chronoamperometry was applied to assess the passive layer growth kinetics and breakdown. Microstructure influence on the uniform corrosion rate of these alloys...
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Identification of Bodner-Partom Viscoplastic Model Parameters for Some Aluminum Alloys at Elevated Temperature
PublikacjaThe paper presents the identification process of inelastic (viscoplastic) properties for two aluminum alloys at a temperature of 120°C. The material parameters are calculated on the basis of uniaxial tension tests. Twelve tests at elevated temperature for each alloy have been performed—three tests for four different strain rates. The main purpose of the paper is to identify the Bodner-Partom viscoplastic model parameters for two...
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Environmental degradation of titanium alloy in artificial saliva
PublikacjaThe titanium and its alloys are potentially prone to hydrogen embrittlement, including those proposed for dental implants. The research has been aimed to assess a susceptibility to environment-enhanced degradation of the Ti-13Zr-13Nb alloy in artificial saliva with or without hydrofluoric acid, subject or not to cathodic polarisation. The results have shown that even if artificial saliva is safe environment, both cathodic polarization...
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Elasto-viscoplastic properties of AA2017 aluminium alloy
PublikacjaArtykuł opisuje procedurę identyfikacji parmetrów materiałowych dla sprężysto-lepkoplastycznego modelu Bodnera-Partoma. Prezentowane są symulacje numeryczne testów jednoosiowego rozciągania z różnymi prędkościmi odkształcenia, które porównane są z wynikami eksperymantalnymi.
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Tracking of the Multimodal Ordering Process in FePd Alloy
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Internal friction in FePd alloy during ordering
PublikacjaStwierdzono występowanie wysokiego poziomu tarcia wewnętrznego w zahartowanym stopie FePd (50% at. Pd). Zbadano proces uporządkowania atomowego w korelacji ze zmianami tarcia wewnętrznego defektu modułu i relaksacji magnetycznej stopu porządkującego się podczas nagrzewania do 900 K. Zaobserwowano efekt prędkości nagrzewania na punkt Curie.
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Oxidation and hydrogen behavior in Zr-2Mn alloy
PublikacjaThe purpose of the present research was to determine the oxidation and hydrogenation behavior in the new Zr-2Mn alloy. The oxidation of alloy was performed at temperatures between 350°C and 900°C for 30 minutes. The hydrogen charging was made for 72 h at a current density 80 mA/cm2. The charged samples were heat treated at 400°C for 4 h to obtain a uniform hydrogen profile content across the sample. The oxidation resulted in an...
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Elctrochemical oxidation and corrosion resistance of the Ti13Nb13Zr alloy
PublikacjaThis paper presents the results of oxidation and corrosion tests carried out on titanium alloy Ti13Nb13Zr. The oxide film was prepared by electrochemical environment 2M H3PO4 for 30 min and 1 h, at a constant voltage 40V. The tests of corrosion resistance were performed by potentiostatic method in Ringer's solution at different pH values: 7, 5 and 3. The change in an appearance of surface and the increase in corrosion resistance...
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Hydroxyapatite deposition on the laser modified Ti13Nb13Zr alloy
PublikacjaThe Ti13Nb13Zr alloy was subjected to laser modification with the Nd:YAG laser provided that such treatment would increase the surface roughness followed improved adhesion of hydroxyapatite (HAp) coatings The hydroxyapatite was deposited by electrophoretic method in suspension of 0.5 g HA powder and 100 ml ethyl alcohol. The deposition was carried out for 10 min at 10 V voltage followed by drying at room temperature for 24 h and...
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Properties of Composite Oxide Layers on The Ti13Nb13Zr Alloy
PublikacjaThe development of composite oxide layers on the Ti13Nb13Zr alloy, their structure and properties have been demonstrated. Two subsequent methods were applied to prepare the composite layers. During the first stage gas oxidation produced a solid oxide layer, and subsequently oxide nanotubes were produced by using an electrochemical method. Scanning electron microscopy (SEM), chemical analysis, energy dispersive X-ray spectroscopy...
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Phase investigations of copper based CuZn38Al2MnFe alloy
PublikacjaW pracy przedstawiono analizę fazową mosiądzu CuZn38Al2MnFe. Wykazano, że obecność fazy Fe4Mn77Si19 powoduje kruchość stopu w teście zginania próbek.
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Zirconia-based mixed potential sensor with Pt electrode prepared by spin-coating of polymeric precursor
PublikacjaMany types of yttria-stabilized zirconia (YSZ) based gas sensors have been explored extensively in recent years. Great attention have been directed to mixed-potential-type gas sensors. It is due to growing concerns with environmental issues. Not without a significance is the fact of very attractive performance of this type of sensor allowing to detect low concentration of pollutant gases. In this paper two types of YSZ based mixed-potential...
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π-Indenyl substituted zirconium compounds containing terminal bondedphosphanylphosphido ligands [Ind2Zr(Cl){(Me3Si)P-PR2-jP1}]. Synthesis,X-ray analysis and NMR studies
PublikacjaPraca prezentuję reakcję kompleksów indenylowych cyrkonu z solami litowymi difosfanów o ogólnym wzorze R2P-P(SiMe3)Li, gdzie R = tBu, Et2N, iPr2N. W wyniku tych reakcji otrzymano 3 nowe kompleksy fosfanylofosfidowe.Otrzymane nowe kompleksy zbadano przy pomocy technik rentgenowskiej analizy strukturalnej i NMR.Dichloro-bis(indenyl)zirconium(IV) reacts with lithium derivatives of diphosphanes R2P-P(SiMe3)Li (R = tBu, Et2N, iPr2N)...
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The influence of microstructure on the corrosion resistance for some titanium-based alloys
Dane BadawczeThis dataset contains scanning electron microscopy (SEM) micrographs revealing the microstructure of some Ti-based alloys, namely: Ti-6Al-4V (file name: TiV), Ti-6Al-7Nb (file name: TiNb) and TC21 (file name: TiAlSnZrMoCrNbSi) alloys and their localized corrosion as a result of passive layer breakdown in a corrosive environment, ie. 0.9% NaCl solution...
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Fabrication, Microstructure and High Temperature Corrosion Resistance of Porous Alloys for Solid Oxide Fuel Cells
PublikacjaPorous alloys find use in modern Solid Oxide Fuel Cells as the supporting structures. As they are exposed to high temperatures (> 500°C) an oxide scale forms on their surface due to high temperature corrosion phenomena. Since the ratio between the surface area and volume is much higher than for planar samples, formation of the oxide can lead to a breakaway oxidation after relatively short times. Therefore corrosion properties of...
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Durability evaluation of Ni‐Cr‐Mo super alloys in a simulated scrubbed flue gas environment
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Evaluation of drawability of tailor-welded blanks made of titanium alloys Grade 2 || Grade 5
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Microstructure and corrosion properties of the (Mn-N-O-P) type layers created on aluminium alloys
PublikacjaPrzedstawiono mikrostrukturę i właściwości korozyjne warstw powierzchniowych typu (Mn-N-O-P) wytworzonych na stopach aluminium. Wykazano, iż warstwy (Mn-N-O-P) podwyższają wielokrotnie odporność korozyjną stopów aluminium i mogą być stosowane jako warstwy ochronne na tych materiałach.
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Improvement of machinability of Ti and its alloys using cooling-lubrication techniques: a review and future prospect
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Structure and thermoelectric properties of Bi–Te alloys obtained by novel method of oxide substrates reduction
PublikacjaA novel method of thermoelectric materials fabrication has been developed. Oxide reagents have been melted at high temperature in air, quenched, milled to powder and reduced in hydrogen to form Bi–Te alloys. Structural and thermoelectric properties of samples have been investigated depending on initial composition and temperature of reduction process. Sample 25Bi2O3–75TeO2 reduced at 340 °C for 10 h has been found to be a p-type...
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Investigation of corrosion behavior of 6060 and 6082 aluminum alloys under simulated acid rain conditions
PublikacjaInstantaneous impedance changes of 6060 and 6082 type aluminum alloys in pure water, and simulated acid rain poured into the pure water was investigated by dynamic electrochemical impedance spectroscopy (DEIS). In this way, the influence of aluminum content on the corrosion behavior of 6060 and 6082 type aluminum alloys immersed in simulated acid rain was determined. The corrosion rate of the alloy decreased with increasing Al...
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Influence of High Temperature Oxidation on Hydrogen Absorption and Degradation of Zircaloy-2 and Zr 700 Alloys
PublikacjaThe present research was aimed at determining the effects of the oxide layers on hydrogen absorption, microstructure and mechanical properties of the Zircaloy- 2 and Zr 702 alloys. The oxidation was made at 350 °C, 700 °C and 900 °C for 10 to 30 min in laboratory air, followed by hydrogen cathodic charging for 72 h and annealing at 400 °C for 4 h. The slow strain rate tests were carried out on oxidized, charged and annealed specimens. The...
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Mateusz Kopec Dr hab. inż.
OsobyHead of the Materials and Structural Testing Laboratory in Institute of Fundamental Technological Research PAS and Academic visitor in Imperial College London. Lecturer and Master/PhD students supervisor in Doctoral School of IPPT PAN and TIB PAN, and Imperial College London. Member of Polish Materials Science Society, Member of the Board of Polish Society of Theoretical and Applied Mechanics, and Council Member of the European...
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π-Indenyl substituted zirconium compounds containing terminal bonded phosphanylphosphido ligands [Ind2Zr(Cl){(Me3Si)P–PR2-κP1}]. Synthesis, X-ray analysis and NMR studies
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The Mesoporous Porphyrinic Zirconium Metal-Organic Framework for Pipette-Tip Solid-Phase Extraction of Mercury from Fish Samples Followed by Cold Vapor Atomic Absorption Spectrometric Determination
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Laser Welding of UNS S33207 Hyper-Duplex Stainless Steel to 6061 Aluminum Alloy Using High Entropy Alloy as a Filler Material
PublikacjaThe high entropy alloy (HEA) filler used during the fabrication method determines the reliability of HEAs for steel-aluminum dissimilar alloy configuration. HEAs have a direct impact on the formation of intermetallic compounds (IMC) formed by the interaction of iron (Fe) and aluminum (Al), and influence the size of the joint’s interaction zone. A novel welding process for Fe-Al alloy joints was developed to prevent the development...
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High temperature corrosion resistance of porous hastelloy alloy
PublikacjaTo further understand the suitability of Ni-Cr-base alloy for solid oxide fuel cell (SOFC), a commercial Ni-Cr-Fe-Mo alloy, Hastelloy X was selected and evaluated for oxidation behaviour under high temperature conditions. HastelloyX was chosen due to its unusual resistance to oxidizing, reducing and neutral atmospheres. For long term stability of metal supported fuel cell, the corrosion resistance plays a vital role and must be...
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EXPERIMENTAL EVALUATION OF THE EMISSIVITY OF A NITI SHAPE MEMORY ALLOY
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Influence of the heat treatment on corrosion characteristics of the Superston alloy
PublikacjaW artykule przedstawiono wpływ hartowania i odpuszczania na twardość i właściwości korozyjne stopu Superston, stosowanego na śruby okrętowe. Stwierdzono, iż hartowanie z temperatury 900 st.C i odpuszczanie w temperaturze 550 st.C znacząco podwyższa odporność na korozję stopu Superston w 3% roztworze NaCl w porownaniu ze stanem odlanym.
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Surface treatment of porous Ti13Nb13Zr alloy for biomedical applications
PublikacjaPrzeprowadzono badania materiału porowatego, przeznaczonego na implanty ortopedyczne, wytworzonego metodą metalurgii proszków ze stopu Ti13Nb13Zr. Proszki z badanego stopu uzyskano metodą rozpylania plazmowego. Otrzymano próbki o otwartej porowatej strukturze, stopniu porowatości do 68% i średniej wielkości porów w przedziale 30-150 mikrometrów. Obróbka próbek porowatych - utlenianie termiczne, chemiczne i/lub elektrochemiczne...
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High temperature corrosion resistance of porous hastelloy alloy
PublikacjaW pracy przedstawiono badania korozyjne stopu Hastelloy w wysokich temperaturach.
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Special Issue “Corrosion Resistance of Alloy and Coating Materials”
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Cavitation behavior of the SUPERSTON alloy after laser treatment
PublikacjaResults of laser treatment at cryogenic conditions and its influence on microstructure, microhardness and cavitation resistance of the SUPERSTON alloy are presented in this paper. Obtained results point at possibility of the increase hardness and cavitation resistance of the parts worked in cavitation conditions.
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Porous biomaterial for orthopaedic implants based on titanium alloy
PublikacjaTytan i jego stopy są szeroko stosowane jako biomateriały dla zastosowań ortopedycznych. Badania związane z ich najlepszą odpornością na korozję i ścieranie, biozgodnością i bioaktywnością są stale prowadzone. Obecne badania koncentrują się również na projektowaniu i produkcji materiałów porowatych w oparciu o stopy np. Ti-13Nb-13Zr, które mogą być stosowane do wytwarzania implantów. Jedną z najbardziej efektywnych metod wytwarzania...
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Underwater robot actuated by shape memory alloy wires
PublikacjaW pracy przedstawiono koncepcję projektu robota podwodnego z napędem wykorzystującym materiały SMA ze stopów z pamięcią kształtu. Rozpatrywany układ ma budowę modułową złożoną z segmentów na podobieństwo do anatomicznej budowy dżdżownicy. Pojedyńczy segment składa się z dwóch okrągłych tarcz, pomiędzy którymi umieszczono balon wypełniony wodą. Wielkość balonu jest dopasowana w taki sposób do rozmiarów tarcz oraz długości sprężyn...
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Influence of Staphylloccoccus bacteria adhesion on the degradation of the Ti6Al4V alloy
PublikacjaThe paper deals with bacteria adhesion and the degradation of the Ti6Al4V alloy
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Morphology and properties of nanotubular oxide layer on the Ti13Zr13Nb alloy
PublikacjaThe Ti13Zr13Nb alloy in solid and porous form was oxidised. The constant voltage 20 V, oxidation time 0.5 and 1 h, and 1 M H3PO4 (orthophosphoric acid) with addition of HF (hydrofluoric acid) as a test solution were applied. SEM (Scanning Electron Microscope) examinations of surface, EDS (Energy Dispersive X-ray Spectroscopy) chemical analysis, nanohardness and nano-scratch tests, and corrosion potentiokinetic tests at various...
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THE PROPERTIES OF NANOSILVER – DOPED NANOHYDROXYAPATITE COATING ON THE Ti13Zr13Nb ALLOY
PublikacjaThe aim of this research was to study the properties of nanohydroxyapatite (nanoHAp) and nanohydroxyapatite, doped with nanosilver (nanoHAp/nanoAg), coatings obtained by an electrophoretic deposition process. The suspensions was prepared by dispersing 0.1 g of HAp nanopowder for nanoHAp coatings and 0.1 g of nanoHAp and 0.025 g nanoAg for nanoHAp/nanoAg coatings. The deposition was carried out for 1 min at 50 V voltage followed...
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Microstructure and corrosion properties of the laser treated SUPERSTON alloy
PublikacjaPrzedstwiono wyniki laserowego nadtapiania powierzchni stopu SUPERSTON w warunkach kriogenicznych. Zaprezentowano obraz powierzchni stopu po badaniach korozyjnych oraz wyniki pomiarów mikrotwardości i odporności korozyjnej.
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Synthesis, characterization and application of a zirconium-based MOF-808 functionalized with isonicotinic acid for fast and efficient solid phase extraction of uranium(VI) from wastewater prior to its spectrophotometric determination
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Optimization of Self-Organized TiO2 Nanotube Geometry on Ti and Ti Alloys Using Fuzzy Logic Reasoning
PublikacjaThe geometry of self-organized TiO2 nanotubes, obtained by electrochemicalanodization, has been determined by using fuzzy reasoning approach. The efficiency of TiO2nanotubular layer in biomedical applications depends on geometry and available surface area ofnanotubes, which can be determined by their diameter and length. The structure of nanotubesdepends on processing parameters of electrochemical anodization, like applied potential,anodization...
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Evaluation of Surface Topography after Face Turning of CoCr Alloys Fabricated by Casting and Selective Laser Melting
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Multisine impedimetric monitoring with an in-depth distribution of relaxation times analysis of WE43 and AZ31 magnesium alloys corrosion
PublikacjaThis research aims to develop and utilize an impedance-based tool for monitoring non-stationary electrochemical processes, coupling the multisinusoidal perturbation signal approach and distribution of relaxation times (DRT) analysis for the first time. The approach was used to distinguish independent processes occurring at the surface of AZ31 and WE43 Mg alloys undergoing corrosion in Hank’s Balanced Salt Solution at 37 °C. We...
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Analysis of chemical composition and hardness of copper alloys = Badania składu chemicznego oraz twardości stopów miedzi
PublikacjaWykonano analizę składu chemicznego oraz badania twardości stopów miedzi zastosowanych na elementy łożyskowe. Sformułowano wnioski.
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Structure and thermoelectric properties of Cs-Bi-Te alloys fabricated by different routes of reduction of oxide reagents
PublikacjaCesium-bismuth-telluride polycrystalline materials were fabricated using a cost-effective method based on a reduction of oxide reagents, leading to a production of a material with good thermoelectric properties. Several samples with various initial stoichiometry were prepared by melting of oxide powders at 1050 °C, quenching, milling to powders and then reducing in pure hydrogen at 400 °C. Another concept was to obtain the CsBi4Te6...
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Understanding the origin of high corrosion inhibition efficiency of bee products towards aluminium alloys in alkaline environments
PublikacjaVarious bee products were found to be efficient corrosion inhibitors of aluminium in different environments. In particular, bee pollen was found to be highly effective in alkaline electrolytes, yet its highly complex composition and possible synergistic interactions hinder determination of the compounds acting as active corrosion inhibitors. The main purpose of the following work is to investigate the effect of solvents used for...
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Evaluation of adhesive forces and the specific surface energy of zirconia stabilized by yttria with alumina additions ceramic by AFM method
PublikacjaThe adhesive forces and the specific surface energy of ceramic material surfaces are very important for further tribological and biomedical applications of ceramics. Partially stabilized zirconia (zirconium oxide) is popular for manufacturing various medical products. ZrO2 stabilized by Y2O3 with additions of 5 wt% alumina was produced by slip casting method with a subsequent sintering. Structure and chemical composition of ceramic...
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PA32 aluminum alloy - tensile properties
Dane BadawczeIn addition to steel, aluminium alloys are the main building material used in the shipbuilding industry. Due to its undoubted advantages, such as low density (nearly three times lower than in the case of steel for shipbuilding) and high corrosion resistance, it is often used for hulls of yachts and small vessels as well as superstructures. For safety...
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Electrochemical investigations of Al–Mg alloy subjected to tensile test
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Impedance analysis of Portevin-Le Chatelier effect on aluminium alloy
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