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Influence of the preparation method and aluminum ion substitution on the structure and electrical properties of lithium–iron ferrites
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New Method for Photoactive Cement Preparation—Selected Mechanical Properties and Photocatalytic Activity of New Materials
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Microwave-Reactor-Based Preparation of Red Iron Oxide Pigment from Waste Iron Sulfate
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Esterification kinetics of glycerol with fatty acids in the presence of zinc carboxylates: Preparation of modified acylglycerol emulsifiers.
PublikacjaZbadano zależności kinetyczne estryfikacji glicerolu kwasami tłuszczowymi (C12:0 - C18:0), prowadzonych w obecności soli cynku tych kwasów tłuszczowych. Przeanalizowano wpływ temperatury, stężenia karboksylanu oraz budowy części hydrofobowej kwasu tłuszczowego i karboksylanu, na postęp reakcji estryfikacji. Wyznaczono wartości odpowiednich stałych szybkości reakcji, energii aktywacji oraz maksymalnej zawartości monoestru glicerolu,...
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Preparation of Pseudopeptides Building Blocks with Retro-Thioamide Bond Mediated via Thiocarbamoyl Meldrum's Acid
PublikacjaAn easy and efficient synthesis of pseudo tripeptide containing a thiomalonamide moiety was developed. Isothiocyanate derivatives of amino acids react smoothly with 2,2-dimethyl-1,3-dioxane-4,6-dione yielding new thiocarbamoyl Meldrum's acids. Thermal decomposition of this new Meldrum's acid derivatives generate thiocarbamoyl ketenes, which acylate amino acid esters to give pseudo tripeptides.
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Eu3+ doped tellurite glass ceramics containing SrF2 nanocrystals: Preparation, structure and luminescence properties
PublikacjaEu3+ doped tellurite glass ceramics containing SrF2 nanocrystals were prepared using melt quenching technique and subsequent heat treatment of glass in 370 °C for different time periods. Thermal properties of glass matrix have been determined based on DSC measurements. XRD and XPS results confirmed formation of SrF2 nanocrystals in glass matrices after annealing at 370 °C. FTIR studies revealed absorption bands in the range of...
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High-performance method of carbon nanotubes modification by microwave plasma for thin composite films preparation
PublikacjaIn this work we present a simple and efficient method of nitrogen plasma modification of carbon nanotubes (CNTs). The process allows for treatment of the nanotubes in the form of powder with quite a high yield (65 mg of CNTs per hour). The modified carbon nanotubes contain approx. 3.8% of nitrogen, mostly in the pyridinic form. Plasma treated CNTs exhibit better dispersibility in water and higher electric capacitance than pristine...
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Implementing SP4CE Learning Rooms concept and AUTODESK online certification in the preparation of a new generation of engineers.
PublikacjaIn academia, educators do not always cope with rapidly changing technologies. Yet keeping up with new trends is essential to graduates’ success in a competitive job market. In the article, the author will answer the question of how Autodesk University Open Educational Resources and Certiport exams including GMetrix can enhance students’ academic progress and prepare them for future career. The concept of co-operation between Authorized...
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Chitin and derivative chitosan-based structures — Preparation strategies aided by deep eutectic solvents: A review
PublikacjaThe high molecular weight of chitin, as a biopolymer, challenges its extraction due to its insolubility in the solvents. Also, chitosan, as the N-deacetylated form of chitin, can be employed as a primary material for different industries. The low mechanical stability and poor plasticity of chitosan films, as a result of incompatible interaction between chitosan and the used solvent, have limited its industrialization. Deep eutectic...
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Preparation and Characterization of Microsphere ZnO ALD Coating Dedicated for the Fiber-Optic Refractive Index Sensor
PublikacjaWe report the fabrication of a novel fiber-optic sensor device, based on the use of a microsphere conformally coated with a thin layer of zinc oxide (ZnO) by atomic layer deposition (ALD), and its use as a refractive index sensor. The microsphere was prepared on the tip of a single-mode optical fiber, on which a conformal ZnO thin film of 200 nm was deposited using an ALD process based on diethyl zinc (DEZ) and water at 100 °C....
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The recovery and the separation of metal ions from galvanic wastewaters
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The application of membrane extraction in the separation of zinc and cadmium ions
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Techniques of preparing plant material for chromatographic separation and analysis
PublikacjaArtykuł przedstawia dyskusję na temat technik wykorzystywanych podczas przygotowywania próbek materiału roślinnego do rozdzielania chromatograficznego i analizy. Opisane techniki to: suszenie, homogenizacja, ługowanie, ekstrakcja. Przedstawiono także techniki ekstrakcyjne tj. ekstrakcja z wykorzystaniem ultradźwięków, przyśpieszona ekstrakcja rozpuszczalnikiem, ekstrakcja z wykorzystaniem mikrofal, ekstrakcja z wykorzystaniem rozpuszczalnika...
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The application of ultrafiltration for separation of glycerol solution fermented by bacteria
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A study of separation by the direct-contact membrane distillation process
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Inorganic membrane: a game changer for gas separation and purification
PublikacjaThis review explores the advancements and remaining challenges in inorganic membrane science, particularly focusing on their potential for industrial applications. It delves into the fundamental principles of inorganic membrane design, fabrication, and characterization techniques. The review also critically analyzes key challenges faced by inorganic membranes, such as physical aging, plasticization, defective formation, and fouling....
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Deep Eutectic Solvents: Properties and Applications in CO2 Separation
PublikacjaNowadays, many researchers are focused on finding a solution to the problem of global warming. Carbon dioxide is considered to be responsible for the “greenhouse” effect. The largest global emission of industrial CO2 comes from fossil fuel combustion, which makes power plants the perfect point source targets for immediate CO2 emission reductions. A state-of-the-art method for capturing carbon dioxide is chemical absorption using...
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Separation of CO2 from biogas using absorption columns
PublikacjaBiogaz zawiera ok. 50-70% metanu, 30-40% di tlenku węgla oraz niewielkie ilości innych związków jak siarkowodór czy amoniaku. Dla uzyskania wysokokalorycznego gazu konieczne jest usunięcie ze strumienia di tlenku węgla. Praca opisuje potencjał użycia do tego celu kolumn absorpcyjnych oraz cieczy jonowych jako absorbenta
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Liquid chromatography techniques for separation of flavonoids from Droseraceae
PublikacjaFlavonoids which are presented in insectivorous plants of the Droseraceae family have wide range of advantageous properties i.e. an antioxidant, anti-inflammatory and antimicrobial activities, antitumor activity was reported as well.The purpose of the research was to develop the most favourable conditions for liquid chromatographic separation and identification of myricetin and quercetin in extracts of insectivorous plants. In...
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Phase Separation and Electrical Properties of Manganese Borosilicate Glasses
PublikacjaThe structure and electrical properties of manganese borosilicate glasses of a composition of xMnO-(0.8-x)SiO2-(0.2)B2O3 (x=0.4, 0.5 and 0.6 in mol) were investigated by impedance spectroscopy, SEM, XRD and confocal microscopy methods. The influence of composition on the glass structure and electrical properties was discussed. A separation of two amorphous phases was observed and it was concluded that one phase is SiO2-rich and...
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Action of an Antiserum to a-Tocoquinone on Photosystem II-Particle Preparations of N icotiana tabacum
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Biologically Active Preparations from the Leaves of Wild Plant Species of the Genus Rubus
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Propagation analysis of the point-to-point radio links operating in the band
PublikacjaThe theoretical possibilities of utilizing the EHF-band frequencies for point-to-point short range communications have been discussed. The most important factors that affect propagation attenuation in this band have been briefly described, as well as relevant mathematical formulas that allow for numerical analysis of these phenomena. After that, a research have been carried out in which the authors have analyzed propagation losses...
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Radio wave propagation conditions for terrestrial radiocommunications in the EHF band
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Numerical analysis of the finite amplitude plane wave propagation problem
PublikacjaRozważano zagadnienie propagacji fali płaskiej o skończonej amplitudzie w środowisku wodnym. Przedstawiono model matematyczny i przykładowe wyniki obliczeń numerycznych. Model matematyczny zbudowano w oparciu o równanie akustyki nieliniowej. Do rozwiązania zagadnienia zastosowano metodę różnic skończonych. Badano wpływ wartości parametrów numerycznych na dokładność obliczeń oraz analizowano wpływ wartości parametrów fizycznych...
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Urban noise propagation modeling in the Multimedia Noise Monitoring System
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Statistical adjustment of selected propagation models for applications in container terminal
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Longitudinal wave propagation. Part I—Comparison of rod theories
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Longitudinal wave propagation. Part II—Analysis of crack influence
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Diagnostics of bolted lap joint using guided wave propagation
PublikacjaThe paper presents numerical and experimental analyses of elastic waves propagation in a bolted lap joint. In experimental investigations condition assessment of the joint was performed with the use of symmetric waves excited by a piezoactuator. Numerical calculations were conducted in commercial finite element method software Abaqus. The influence of number of bolts and the value of the initial stress on recorded signals was examined....
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Application of guided wave propagation in diagnostics of steel bridge components
PublikacjaEarly detection of potential defects and identification of their location are necessary to ensure safe, reliable and long-term use of engineering structures. Non-destructive diagnostic tests based on guided wave propagation are becoming more popular because of the possibility to inspect large areas during a single measurement with a small number of sensors. The aim of this study is the application of guided wave propagation in...
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Spectral plate element for crach detection with use of propagation wares.
PublikacjaW pracy przedstawiono model płyty oparty na metodzie elementów spectralnych. Przedstawiono wyniki analizy interakcji pęknięcia zmęczeniowego i propagującej się fali.
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Propagation Characteristics of Partial Discharges in an Oil-Filled Power Transformer
PublikacjaPower transformers are among the most important assets in the power transmission and distribution grid. However, they suffer from degradation and possible faults causing major electrical and financial losses. Partial discharges (PDs) are used to identify the insulation health status and their degradation level. PDs are incipient, low-magnitude faults caused by localized dielectric breakdown. Those activities emit signals in many...
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Square-wave propagation along coupled coplanar transmission line.
PublikacjaW pracy przedstawiono wyniki modelowania propagacji fali prostokątnej w układzie sprzężonych linii koplanarnych z uziemionym centralnym paskiem. Przeanalizowano napięcia przesłuchów na bliskim i dalekim końcu linii sprzężonych wykazując poprawę zgodności wyników modelowania i eksperymentu przy uwzględnieniu propagacji wielomodowej.
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Non-Perfect Propagation of Information to a Noisy Environment with Self-Evolution
PublikacjaWe study the non-perfect propagation of information for evolving a low-dimensional environment that includes self-evolution as well as noisy initial states and analyse the interrelations between the degree of objectivization and environment parameters. In particular, we consider an analytical model of three interacting qubits and derive its objectivity parameters. The numerical analysis shows that the quality of the spectrum broadcast...
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Nonlinear Properties of Seawater as a Factor Determining Nonlinear Wave Propagation
PublikacjaTaking practical advantage of nonlinear acoustical interactions occurring in seawater [1, 2] requires knowledge of the parameter of nonlinearity B=A of this medium. The literature does not offer much reports on B=A parameter value for seawater. In the few papers concerning that address the issue, results concerning ocean waters with high salinity and at large depths are given [3], while studies concerning seawater with low salinity...
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Efficient Complex Root Tracing Algorithm for Propagation and Radiation Problems
PublikacjaAn efficient complex root tracing algorithm for propagation and radiation problems is presented. The proposed approach is based on a discretization of Cauchy’s Argument Principle and its generalization to the C × R space. Moreover, an engagement of the tracing process with a global root finding algorithm recently presented in the literature is performed. In order to confirm a validity and efficiency of the proposed technique, a...
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Shipping Low Frequency Noise and Its Propagation in Shallow Water
PublikacjaOne of the most significant factor influencing acoustical climate of the sea is underwater noise generated by moving ships. If the considered sea area has features of the shallow water, namely the wave frequency fulfils relation f < 10c/h, where c denotes phase speed of sound, and h is depths of the sea, then in certain distance from the wave source specific image of sound pressure distribution in the mean of wave modes appears....
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Damage detection strategies based on propagation of guided elastic waves
PublikacjaW pracy przedstawiono wyniki symulacji numerycznych oraz badań eksperymentalnych nad wykorzystaniemprowadzonych falsprężystych do wykrywania ilokalizacji uszkodzeń w dwu i trójwymiarowych elementach konstrukcyjnych wykonanych z materiałów izotropowych i kompozytowych.
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Analysis of guided wave propagation in adhesive joints of steel rods
PublikacjaThe aim of the study is the elastic wave propagation in adhesive joints of metal rods that are one of the simplest kind of glue connections. They are consisted of two metal members and an adhesive layer joining two parts together. The analysis is directed to technical diagnostics of such type of connections. Longitudinal and transversal guided waves were excited in prepared joints. Signals of propagating waves were registered in...
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Detection of debonding in adhesive joints using Lamb wave propagation
PublikacjaAdhesively bonded joints are widely used in many branches of industry. Mechanical degradation of this type of connections does not have significant symptoms that can be noticed during visual assessment, so non-destructive testing becomes a very important issue. The paper deals with experimental investigations of adhesively bonded steel plates with different defects. Five samples (an intact one and four with damages in the form...
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Simulation of Signal Propagation Along Fractional-Order Transmission Lines
PublikacjaIn this paper, the simulation method of signal propagation along fractional-order (FO) transmission lines is presented. Initially, fractional calculus and the model of FO transmission line are introduced. Then, the algorithm allowing for simulation of the nonmonochromatic wave propagation along FO transmission lines is presented. It employs computations in the frequency domain, i.e., an analytical excitation is transformed to the...
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Simulation of Wave Propagation in Media Described by Fractional-Order Models
PublikacjaIn this paper, algorithms for simulation of the wave propagation in electromagnetic media described by fractional-order (FO) models (FOMs) are presented. Initially, fractional calculus and FO Maxwell's equations are introduced. The problem of the wave propagation is formulated for media described by FOMs. Then, algorithms for simulation of the non-monochromatic wave propagation are presented which employ computations in the time...
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Bandwidth Dependence of the Propagation Channel in Circular Metallic BAN Environments
PublikacjaIn this paper, the bandwidth dependence of the propagation channel for Body Area Networks (BANs) in circular metallic environments is addressed and models are proposed to evaluate the appropriate short-term fading margins that should be considered as a function of the system bandwidth. The deployment of BANs in metallic indoor environments, such as ships, factories, warehouses and other similar environments, involves additional...
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Numerical Study of Concrete Mesostructure Effect on Lamb Wave Propagation
PublikacjaThe article presents the results of the numerical investigation of Lamb wave propagation in concrete plates while taking into account the complex concrete mesostructure. Several concrete models with randomly distributed aggregates were generated with the use of the Monte Carlo method. The influence of aggregate ratio and particle size on dispersion curves representing Lamb wave modes was analyzed. The results obtained for heterogeneous...
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Hazardous material-related propagation of the effects of train accidents in the subgrade
PublikacjaA large part of the transport of hazardous materials is carried out by rail. Therefore, the security of these transports is becoming increasingly important. Every catastrophe involving dangerous materials has a negative impact on the participants of the incident and the surrounding environment, because its range is generally not local. It follows that in the event of a catastrophe, its effects should be minimized and remediation...
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Signal propagation in electromagnetic media described by fractional-order models
PublikacjaIn this paper, signal propagation is analysed in electromagnetic media described by fractional-order (FO) models (FOMs). Maxwell’s equations with FO constitutive relations are introduced in the time domain. Then, their phasor representation is derived for one-dimensional case of the plane wave propagation. With the use of the Fourier transformation, the algorithm for simulation of the non-monochromatic wave propagation is introduced....
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Longitudinal wave propagation. Part II, Analysis of crack influence
PublikacjaW pracy analizowano wpływ pęknięć zmęczeniowych na propagacje fali wzdłużnej w prętach. Opracowano nowe typy element ów spektralnych oparte na teorii elementarnej, Love'a, Mindlina i trójpostaciowej.
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Longitudinal wave propagation. Part I - Comparison of rod theories
PublikacjaW pracy przedstawiono modele spektralnych elementów skończonych do analizy propagacji fali wzdłuznej w pretach. Opracowano modele wykorzystujace teorię elementarną, teorie Love'a, teorie Mindlina oraz teorię trójpostaciową.
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Damage detection in elements of strutures by the elastic wave propagation method.
PublikacjaW pracy przedstawiono wyniki badań dotyczace wykorzystania fal sprężystych do detekcji uszkodzeń i jedno i dwu wymiarowych elementach konstrukcyjnych.