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Size Exclusion Coupled to Reversed Phase Liquid Chromatography for the Characterization of Cranberry Products
PublikacjaA combination of solvent extraction, size exclusion purification, and reversed-phase liquid chromatography with UV absorption and fluorescence detection was here used for the determination of flavan-3-ols and related oligomeric compounds in cranberry products. The method relied on robust, simple, and inexpensive instrumental equipment present in most of routine analytical laboratories. Sample extracts in methanol/water/hydrochloric...
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Balance of pesticides mass in gas, liquid and solid phase after their chemical degradation.
PublikacjaOpisano metodę usuwania pestycydów z wody przy zastosowaniu fotodegradacji (UV) i katalizatora (TiO2). Efektywność procesu usuwania pestycydów była kontrolowana przy zastosowaniu chromatografu gazowego z detektorem wychwytu elektronów. Oznaczano zawartość pestycydów w wodzie, a także zaadsorbowanych na powierzchni stałej, oraz w fazie gazowej. Największa zawartość pestycydów znajdowała się na fazie stałej, następnie w cieczy i...
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Socioemotional Wealth (SEW) of Family Firms and CEO Behavioral Biases in the Implementation of Sustainable Development Goals (SDGs)
PublikacjaAgreed upon by the UN member states, Agenda 2030 assumes joint action for long- term sustainable development. These actions are focused on the implementation of 17 Sustainable Development Goals (SDGs), where actions are assumed to lead to the suppression of negative externalities of human activity. It is stressed that the objectives of sustainable development can only be achieved through deep institutional changes in most dimensions...
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Electrochemical and biological characterization of lyotropic liquid crystalline phases – retardation of drug release from hexagonal mesophases
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X-ray diffractometry results of the SrTi0.50Fe0.50O3-d powder
Dane BadawczeThis dataset contains results of X-ray diffractometry mesurement (XRD) of the SrTi0.50Fe0.50O3-d (STF50) powder after ball milling. The phase composition of the investigated STF50 powder was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder. Measurements...
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X-ray diffractometry results of the SrTi0.35Fe0.65O3-d powder
Dane BadawczeThis dataset contains results of X-ray diffractometry mesurement (XRD) of the SrTi0.35Fe0.65O3-d (STF35) powder after ball milling. The phase composition of the investigated STF35 powder was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder. Measurements...
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X-ray diffractometry results of the SrTi0.30Fe0.70O3-d powder
Dane BadawczeThis dataset contains results of X-ray diffractometry mesurement (XRD) of the SrTi0.30Fe0.70O3-d (STF70) powder after ball milling. The phase composition of the investigated STF70 powder was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder. Measurements...
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Influence of e-beam irradiation on the dynamic creep and fatigue properties of poly(aliphatic/aromatic-ester) copolymers for biomedical applications
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Analysis of the unique structural and physicochemical properties of the DraD/AfaD invasin in the context of its belonging to the family of chaperone/usher type fimbrial subunits
PublikacjaInwazyna DraD kodowana przez operon dra posiada strukturę charakterystyczną dla białek podjednostkowych fimbrii typu chaperone-usher. Fold-Ig białka DraD posiada dwie charakterystyczne cechy wyróżniające je z pośród rodziny fimbrialnych białek podjednostkowych: 1) zaburzenie struktury beta-beczki w rejonie szczeliny akceptorowej objawiające się układem wiązań wodorowych głównego łańcucha polipeptydowego oraz 2) nietypowo usytuowany...
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X-ray diffractometry results of the Sr0.90Ti0.30Fe0.70O3-d material before and after H2-TPR measurement
Dane BadawczeThis dataset contains results of X-ray diffractometry mesurement (XRD) of the Sr0.90Ti0.30Fe0.70O3-d material. The phase composition of the investigated powders was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder and powder after H2-TPR (temperature programmed...
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X-ray diffractometry results of the Sr0.95Ti0.30Fe0.70O3-d material before and after H2-TPR measurement
Dane BadawczeThis dataset contains results of X-ray diffractometry mesurement (XRD) of the Sr0.95Ti0.30Fe0.70O3-d material. The phase composition of the investigated powders was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder and powder after H2-TPR (temperature programmed...
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Images of topography and mechanical properties (phase imaging) of cast iron samples from water installations
Dane BadawczeMeasurements in contact and semi-contact mode. NTEGRA Prima (NT-MDT) device. CSG 10.
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The unstable thermoelectric effect in non-stoichiometric Cu2Se during the non-equilibrium phase transition
PublikacjaThe superionic α ↔ β phase transition in Cu1.96Se thermoelectric material is investigated by means of thermal analysis (DSC) and measurements of Seebeck coefficient and electrical conductivity. Results of the DSC measurements with 1–10 K/min heating and cooling rates show that the material is close to the equilibrium phase composition during the transformation. However, the kinetic limitation of the process exists, which is indicated...
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Compact 4 × 4 butler matrix with non‐standard phase differences for IoT applications
PublikacjaButler matrices represent a popular class of feeding networks for antenna arrays. Large dimensions and the lack of flexibility in terms of achievable output phase difference make conventional Butler structures of limited use for modern communication devices. In this work, a compact planar 4 × 4 matrix with non-standard relative phase shifts of –30º, 150º, –120º, and 60º has been proposed. The structure is designed to operate at...
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Mathematical modeling of hydrogen production performance in thermocatalytic reactor based on the intermetallic phase of Ni3Al
PublikacjaThe main goal of the following work is to adjust mathematical modelling for mass transfer, to specific conditions resulting from presence of chemical surface reactions in the flow of the mixture consisting of helium and methanol. The thermocatalytic devices used for decomposition of organic compounds incorporate microchannels coupled at the ends and heated to 500 oC at the walls regions. The results of the experiment were compared...
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Post-Pyrolytic Carbon as a Phase Change Materials (PCMs) Carrier for Application in Building Materials
PublikacjaThis article covers new application for char as a carrier of phase-change materials (PCM) that could be used as an additive to building materials. Being composed of bio-char and PCM, the granulate successfully competes with more expensive commercial materials of this type, such as Micronal® PCM. As a PCM carrier, char that was obtained from the pyrolysis of chestnut fruit (Aesculus hippocastanum) with different absorbances of the...
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Dynamic fracture of brittle shells in a space-time adaptive isogeometric phase field framework
PublikacjaPhase field models for fracture prediction gained popularity as the formulation does not require the specification of ad-hoc criteria and no discontinuities are inserted in the body. This work focuses on dynamic crack evolution of brittle shell structures considering large deformations. The energy contributions from in-plane and out-of-plane deformations are separately split into tensile and compressive components and the resulting...
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Low-Loss Mechanically Tunable Resonator and Phase Shifters in Groove Gap Waveguide Technology
PublikacjaThis research is focused on the design and realization of high-performance high-power variable phase shifters in groove gap waveguide technology. Specifically, it is shown that the unique characteristic of groove gap waveguides, which is its proper operation without the need for electrical connection between the top and bottom sections of the waveguide, can be used to design mechanically tunable devices. Using the proposed method,...
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Testing Stability of Digital Filters Using Multimodal Particle Swarm Optimization with Phase Analysis
PublikacjaIn this paper, a novel meta-heuristic method for evaluation of digital filter stability is presented. The proposed method is very general because it allows one to evaluate stability of systems whose characteristic equations are not based on polynomials. The method combines an efficient evolutionary algorithm represented by the particle swarm optimization and the phase analysis of a complex function in the characteristic equation....
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Multimodal Particle Swarm Optimization with Phase Analysis to Solve Complex Equations of Electromagnetic Analysis
PublikacjaIn this paper, a new meta-heuristic method of finding roots and poles of a complex function of a complex variable is presented. The algorithm combines an efficient space exploration provided by the particle swarm optimization (PSO) and the classification of root and pole occurrences based on the phase analysis of the complex function. The method initially generates two uniformly distributed populations of particles on the complex...
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Matrix Metalloproteinase-9 Is Required for Hippocampal Late-Phase Long-Term Potentiation and Memory
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pH Gradient as a Tool for the Separation of Ionizable Analytes in Reversed-Phase High-Performance Chromatography
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Structural phase transitions and photoluminescence properties of oxonitridosilicate phosphors under high hydrostatic pressure
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Development and validation of urinary nucleosides and creatinine assay by capillary electrophoresis with solid phase extraction
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Headspace Liquid-Phase Microextraction of Chlorobenzenes in Soil with Gas Chromatography-Electron Capture Detection
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Solid Phase Photocatalytic Reaction on the Soot/TiO2 Interface: The Role of Migrating OH Radicals
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Nickel loaded zeolites FAU and MFI: Characterization and activity in water-phase hydrodehalogenation of TCE
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Distinguishing between polymorphic forms of linezolid by solid-phase electronic and vibrational circular dichroism
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Dielectric response of electric-field distortions of the twist-bend nematic phase for LC dimers
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Origin of the liquid-liquid phase transition for trans-1,2-dichloroethylene observed by IR spectroscopy
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Thermophysical properties of the phase change material mixtures – preliminary studies on macromolecular hydrocarbons example.
PublikacjaThe aim of this work is a theoretical and experimental analysis of the macromolecular hydrocarbon mixtures composition and the impact on thermophysical parameters of the phase change materials (PCM) made from these mixtures. The analysis of the current state of knowledge extended by the author’s own studies have been presented. Thermophysical characteristics of the hydrocarbons and their mixtures have been specified, in such a...
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Chapter 13 : The influence of dispersion phase on composite coating properties after cold working
PublikacjaW pracy określono wpływ fazy dyspersyjnej Al2O3 na wybrane potencjalne właściwości powłok kompozytowych o osnowie niklowej. Powłoki Ni-Al-Al2O3 zostały nałożone na próbki stalowe przy użyciu technologii poddźwiękowego płomieniowego natryskiwania cieplnego. Następnie poddane zostały obróbce plastycznej na zimno i na gorąco poprzez walcowanie, a także prasowania na zimno na prasie hydraulicznej. Obróbka plastyczna jest metodą alternatywną...
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Assessment of phase stability and in vitro biological properties of hydroxyapatite coatings composed of hexagonal rods
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High temperature monoclinic-to-tetragonal phase transition in magnesium doped lanthanum ortho-niobate
PublikacjaMagnesium doped lanthanum ortho-niobate (La0.98Mg0.02NbO4) was prepared by the molten salt synthesis method. X-ray diffraction and dilatometry methods were used to study high temperature behavior of the ceramic material. Special attention was paid to the phase transition between the monoclinic and tetragonal phases. The values of spontaneous strain on the basis of unit cell parameter, obtained by Rietveld refinement, have been...
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STUDYING THE PROCESS OF OBTAINING PHOSPHATES OF METALS BASED ON THE PHASE EQUILIBRIA OF FOUR COMPONENT SYSTEMS
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Synthesis, structure and application of a new class of Tr-podands derived in phase-transfer catalysis
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Sensorless IPMSM drive with rotor position estimator based on analysis of phase current derivatives
PublikacjaThis paper describes a sensorless Interior Permanent Magnet Synchronous Motor (IPMSM) drive designed for traction applications. Wide-speed sensorless operation is provided with the use of three methods of rotor position estimation designed for: a standstill, low- and high-speed range. The paper focuses on the high-speed estimation algorithm. The estimator uses the derivatives of motor phase currentsresulting from PWM modulation...
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Studies on applicability of new solid-phase microextraction and determination of short - chain monocarboxylic acids
PublikacjaA convenient approach to monitor the short-chain monocaroboksylic acids (SCAMs) in different samples is gas chromatography (GC) preceded by sample preparation based on solid-phase microextraction (SPME). The fiber with polar coatings were used to extract the SCAMs from headspace of liquid and solid samples. Recently polimeric ionic liquid (PIL) fiber coatings have been proposed to extract volatile organic compounds, minly polar...
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Polyethylene glycol-coated solid-phase microextraction fibres for the extraction of polar analytes-A review
PublikacjaThe article discusses the merits and limitations of commercially available solid-phase microextraction (SPME) fibres and compares them with the new type of extraction coatings, in particular those containing polyethylene glycol as sorbent, as well as the methods of the preparation of the latter. It also analyses their possible application for the extraction of a broad spectrum of analytes, with particular emphasis on the sampling...
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Applications of metal organic framework adsorbents for pipette-tip micro solid-phase extraction
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Comparison the Accuracy of the Extrapolation Methods of the Time Phase Coincidence in Synchronization of Power Generating Units
PublikacjaW artykule opisano metody ekstrapolacji chwili zgodności fazowej napięć łączonych obiektów elektroenergetycznych. Przeprowadzono analizę porównawczą wybranych metod ekstrapolacji w równych warunkach pracy oraz przedstawiono najistotniejsze wyniki badań.
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Investigations of hydraulic jump configured by a two phase air water jetimpinging on a flat plate.
PublikacjaPrzedstawiono wyniki badań eksperymentalnych uskoku hydraulicznego powstającego przy napływie strugi uderzającej na powierzchnię płaskiej płyty.
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Evaluation of Linkers’ Influence on Peptide-Based Piezoelectric Biosensors’ Sensitivity to Aldehydes in the Gas Phase
PublikacjaRecent findings qualified aldehydes as potential biomarkers for disease diagnosis. One of the possibilities is to use electrochemical biosensors in point-of-care (PoC), but these need further development to overcome some limitations. Currently, the primary goal is to enhance their metrological parameters in terms of sensitivity and selectivity. Previous findings indicate that peptide OBPP4 (KLLFDSLTDLKKKMSEC-NH2) is a promising...
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Dead time effects compensation strategy by third harmonic injection for a five-phase inverter
PublikacjaThis paper proposes a method for compensation of dead-time effects for a fivephase inverter. In the proposed method an additional control subsystem was added to the field-oriented control (FOC) scheme in the coordinate system mapped to the third harmonic. The additional control loop operates in the fixed, orthogonal reference frame ( α - β coordinates) without the need for additional Park transformations. The purpose of this method...
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Kinetics of Intermetallic Phase Precipitation in Manual Metal Arc Welded Duplex Stainless Steels
PublikacjaThe article presents the influence of heat treatment on the kinetics of transformations in lean duplex LDX2101 steel and a weld made of standard duplex 2209 material, which was welded by manual metal arc welding. Changes in the microstructure, hardness, and magnetic phase content were analyzed after heat treatment was conducted at a temperature of 800 °C for a period ranging from 15 to 1440 min. Light and scanning microscopy, Vickers...
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Phenomenon of hydraulic jump formed on liquid layer by single-phase impinging liquid jet
PublikacjaPrzedstawiono analizę teoretyczną zjawiska uskoku hydraulicznego tworzonego przez uderzającą strugę. rezultaty analizy teoretycznej porównano z wynikami badań eksperymentalnych.
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On the mechanism of oscillations in three-phase system containing coationc surfactant and nitrobenzene liquid membrane
PublikacjaObserwuje się oscylacje różnicy potencjału elektochemicznego między fazami wodnymi oscylatora zawierającego bromek heksadecylotrimetyloamoniowy. Ta różnica potencjału składa sie z potencjałów na granicach faz między membraną a fazą wodną donorową oraz membraną a fazą wodną akceptorową. Wykazano, że oscylacje zachodzą na granicy fazy akceptorowej i membrany. Są one spowodowane procesami adsorpcji/desorpcji pary jonowej surfaktantu...
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Phase separation in poly(butylene terephthalate)-based materials prepared by solid-state modification
PublikacjaThe morphology of a series of poly(butylene terephthalate) (PBT)/fatty acid dimer diol (FADD)-based copolyesters prepared by solid-state modi fi cation (SSM) was studied. It was shown that in copolyesters containing less than 10 wt% FADD two different phases, i.e. a PBT crystalline phase and a PBT-rich amorphous phase, are present. The FADD residues were more or less homogeneously distributed throughout the interlamellar regions....
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Nonlinear control of five phase induction motor with synchronized third harmonic flux injection
PublikacjaThe paper deals with the novel control system for five phase induction motor (IM) that enables the injection of the rotor flux 3rd harmonic component. Two multiscalar models are transformed from the 1-1 and 2-2 vector models developed in the 1st and 3rd harmonic planes. Based on the obtained multiscalar models the synthesis of dual multiscalar control is established. The obtained two multiscalar control systems can independently...
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Thermophysical Properties of the Phase Change Material Mixtures – Preliminary Studies on Macromolecular Hydrocarbons Example.
PublikacjaThe aim of this work is a theoretical and experimental analysis of the macromolecular hydrocarbons mixtures composition and the impact on thermophysical parameters of the phase change materials (PCM) made from these mixtures. The analysis of the current state of knowledge extended by the author's own studies have been presented. Thermophysical characteristics of the hydrocarbons and their mixtures have been specified, in such a...