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Search results for: Sampling/extraction techniques
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Plasma-Based Deposition and Processing Techniques for Optical Fiber Sensing
PublicationPlasma-based techniques are widely applied for well-controlled deposition, etching or surface functionalization of a number of materials. It is difficult to imagine fabrication of novel microelectronic and optoelectronic devices without using plasma-enhanced deposition of thin films, their selective etching or functionalization of their surfaces for subsequent selective binding of chemical or biological molecules. Depending on...
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Magnetic deep eutectic solvents as efficient media for extraction of furfural and 5-hydroxymethylfurfural from aqueous samples
PublicationThe extraction of furfural (FF) and 5-hydroxymethylfurfural (HMF) from hydrolysates is currently one of the main challenges in bio-refinery. In this work, the separation of FF and HMF from the aqueous phase was carried out using a new type of green solvents – Magnetic Deep Eutectic Solvents (MDES). A conductor-like screening model for realistic solvents (COSMO-RS) was used for the preselection of 400 MDES. MDES which exhibit the...
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A Review: Structural Shape and Stress Control Techniques and their Applications
PublicationThis review article presents prior studies on controlling shape and stress in flexible structures. The study offers a comprehensive survey of literature concerning the adjustment and regulation of shape, stress, or both in structures and emphasizes such control’s importance. The control of systems is classified into three primary classes: nodal movement control, axial force control, and controlling the two classes concurrently....
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Comparison of the measurement techniques employed for evaluation of ambient air odour quality
PublicationThe paper presents the results of investigation on ambient air odour quality in a vicinity of the industrial sewage treatment plant being a part of the crude oil processing plant. The investigation was performed during spring-winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type sensor. The field...
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The dispersive micro-solid phase extraction method for MS-based lipidomics of human breast milk*
PublicationA simple and rapid microextraction method ensuring high lipidome coverage was developed for liquid chromatography mass spectrometry (LC-MS)-based lipidomics of human breast milk. The dispersive microsolid phase extraction (D-µ-SPE) technique, coupled with the design of experiment (DoE) method, enabled the study of the influence of several conditions (desorption solvent, stationary phase ratio, and sorption and desorption time)...
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Green aspects of techniques for the determination of currently used pesticides in environmental samples
PublicationPesticides are among the most dangerous environmental pollutants because of their stability, mobility and long-term effects on living organisms. Their presence in the environment is a particular danger. It is therefore crucial to monitor pesticide residues using all available analytical methods. The analysis of environmental samples for the presence of pesticides is very difficult: the processes involved in sample preparation are...
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Experience-Based Cognition for Driving Behavioral Fingerprint Extraction
PublicationABSTRACT With the rapid progress of information technologies, cars have been made increasingly intelligent. This allows cars to act as cognitive agents, i.e., to acquire knowledge and understanding of the driving habits and behavioral characteristics of drivers (i.e., driving behavioral fingerprint) through experience. Such knowledge can be then reused to facilitate the interaction between a car and its driver, and to develop better and...
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New Trends in Sample Preparation Techniques for the Analysis of the Residues of Pharmaceuticals in Environmental Samples
PublicationPharmaceutical residues in the environment is a field of special interest due to the adverse effects to either human health or aquatic and soil environment. Pharmaceuticals have been already detected in underground, surface and wastewaters, soils, manure and sediments. The growing awareness of environmental pollution arising from human activity forces the need for their comprehensive determination. Environmental samples are complex...
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Development of SPME fiber coatings with tunable porosity for physical confinement of ionic liquids as an extraction media
PublicationExtending the use of ionic liquids in sample preparation techniques remains a challenge. This paper presents procedures enabling the easy application of ionic liquids to the SPME technique. For this purpose, two approaches for producing a porous silica coating on a metal rod were investigated. Two silica precursor and porogen systems were used in the research: K2SiO3 + Formamide and Tetramethyl-orthosilicate + Polyethylene oxide....
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Using Continuous Integration Techniques in Open Source Projects – An Exploratory Study
PublicationFor a growing number of software projects, continuous integration (CI) techniques are becoming an essential part of the process. However, the maturity of their adoption in open source projects varies. In this paper, we present an empirical study on GitHub repositories to explore the use of continuous integration techniques in open source projects. Following the Goal-Question-Metric (GQM) approach, 3 research questions and 7 metrics...
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Molecularly imprinted polymers applied in capillary electrochromatography and electrophoresis techniques
PublicationMolecularly imprinted polymers (MIPs) are synthetic materials with predetermined selectivity for a particular analyte or group of structure-linked chemicals which make them an ideal separation component. The process of developing and applying new types of MIPs in the field of environmental analytical chemistry has been broadly discussedi n many scientific studies in recent years. The use of new types of MIP sorbents as unique sorption...
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Comparison of oil yield and quality obtained by different extraction procedures from salmon (Salmo salar) processing byproducts
PublicationThe content and composition of lipids in different byproducts (skins, heads, and backbones) from mechanically processed farmed Atlantic salmon were determined and compared with that obtained from wild salmon. Three different procedures were used to establish the optimal conditions of oil extraction (at high temperature −95°C, “cold” extraction at temperature not exceeding 15°C and enzyme assisted with Alcalase). “Cold” extraction...
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Effect of Water Content in Extraction Mixture on the Pressurized Liquid Extraction Efficiency—Stability of Quercetin 4′-Glucoside During Extraction from Onions
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Sławomir Jerzy Ambroziak dr hab. inż.
PeopleSławomir J. Ambroziak was born in Poland, in 1982. He received the M.Sc., Ph.D. and D.Sc. degrees in radio communication from Gdańsk University of Technology (Gdańsk Tech), Poland, in 2008, 2013, and 2020 respectively. Since 2008 he is with the Department of Radiocommunication Systems and Networks of the Gdańsk Tech: 2008-2013 as Research Assistant, 2013-2020 as Assistant Professor, and since 2020 as Associate Professor. He is...
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Techniques of acquiring additional features of the responses of individual gas sensors
PublicationGas sensors usually exhibit lack of selectivity, require fre quent calibration, exhibit drift of the response and a lot of factors, such as humidity or ambient temperature, influen ce their performance. Different approaches can be used to overcome this shortcomings. Building arrays of different sensors and usage of pattern recognition methods to analyze responses of elements...
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Is mesh fixation necessary in laparoendoscopic techniques for M3 inguinal defects? An experimental study.
Publicationrepairs, in case of large direct hernias (M3) mesh fixation is recommended to reduce recurrence risk. Despite lack of highquality evidence, the recommendation was upgraded to strong by expert panel. The authors conducted a research experiment to verify the hypothesis that it is possible to preserve the mesh in the operating field in large direct hernias (M3) without the need to use fixing materials. Method The authors conducted...
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Extraction and evaluation of gas-flow-dependent features from dynamic measurements of gas sensors array
PublicationGas analyzers based on gas sensors are the devices which enable recognition of various kinds of volatile compounds. They have continuously been developed and investigated for over three decades, however there are still limitations which slow down the implementation of those devices in many applications. For example, the main drawbacks are the lack of selectivity, sensitivity...
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Investigation of solid polymer electrolyte gas sensor with different electrochemical techniques
PublicationIn this work solid polymer electrolyte (SPE) amperometric sulphur dioxide sensor is investigated. Nafion was used as a membrane electrode and 1M sulphuric acid as an internal electrolyte. Sensor response to sulphur dioxide was measured. Besides traditional constant voltage amperometry also different electrochemical techniques were used. Results obtained by these methods are compared.
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GIS three-dimensional Modelling with geo-informatics techniques
PublicationThe integration issue of virtual models and geo-referenced database have a very broad spectrum of potential applications. Before the integration issue was on the cusp, it was quite problematic to combine three-dimensional models with the geo-referenced database. An integrated database contains a variety of data including such as object orientated data model and raster data. Within this paper, authors present an integration process...
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High Efficiency Configuration Space Sampling -- probing the distribution of available states
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Data Sampling-Based Feature Selection Framework for Software Defect Prediction
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Efficient sampling of high-energy states by machine learning force fields
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Calibration of Passive Samplers for the Monitoring of Pharmaceuticals in Water-Sampling Rate Variation
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The influence of sampling parameters on accuracy of capacitance measurement in the method based on DSP.
PublicationW artykule przedstawiono metodę pomiaru parametrów impedancyjnych bazującą na próbkowaniu sygnałów pomiarowych i DSP. Przeanalizowano wpływ głównych źródeł niepewności i błędów na dokładność pomiaru pojemności. Zawarto analizę dla następujących parametrów: niesynchroniczne próbkowanie sygnałów pomiarowych (napięciowego i prądowego), rozdzielczość przetwornika a/c i ilość zbieranych próbek. Załączono wyniki symulacji.
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Constrained aerodynamic shape optimization using neural networks and sequential sampling
PublicationAerodynamic shape optimization (ASO) involves computational fluid dynamics (CFD)-based search for an optimal aerodynamic shape such as airfoils and wings. Gradient-based optimization (GBO) with adjoints can be used efficiently to solve ASO problems with many design variables, but problems with many constraints can still be challenging. The recently created efficient global optimization algorithm with neural network (NN)-based prediction...
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Passive sampling as a tool for obtaining reliable analyticalinformation in environmental quality monitoring
PublicationSpośród technik pobierania próbek analitów technika dozymetrii pasywnej wydaje się być interesującą alternatywą w stosunku do powszechnie stosowanych technik dynamicznych. Dozymetria pasywna łączy w sobie etap pobierania próbki z etapem izolacji i wzbogacania analitów, które są zatrzymywane w odpowiednim medium zatrzymującym. Prowadzi to do znacznego uproszczenia operacji analitycznych wykonywanych in situ. W odróżnieniu od aktywnych...
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An Approach to Imbalanced Data Classification Based on Instance Selection and Over-Sampling
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Learning from Imbalanced Data Using Over-Sampling and the Firefly Algorithm
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Validation and Regulatory Issues for Sample Preparation in: Comprehensive Sampling and Sample Preparation
PublicationW rozdziale opisano podstawowe terminy związane z walidacja procedury analitycznej. Szczególnie zwrócono uwagę na etapy pobierania i przygotowania próbek do analizy. Podano także rolę i znaczenie poszczególnych składowych procesu kontroli i zapewnienia jakości wyników pomiarów analitycznych.
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Characterization of PLZT Thin Films for Fast Electro-Optical Sampling Circuits
PublicationW artykule omówiono technologię wytwarzania cienkich warstw wybranych kompozycji ceramik ołowiowo-lantanowo-cyrkonowo-tytanowych, nazywanych ceramikami PLZT. Przedstawiono wyniki badań jakości warstw za pomocą techniki XRD. wyniki pomiaru grubości warstw, ich względnej przenikalności dielektrycznej i współczynnika załamania. Omówiono kierunki dalszych prac.
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Probabilistic Analysis of Structure Models using Target Random Sampling (TRS)
PublicationThe work presents testing methods of sensitivity and reliability of mechanical or structural systems. All computations concerned the case of Zigler column, a simple model of a compressed column involving two random variables only. A conclusion was drawn that the standard Monte Carlo method, its reduction variants and the response surface method allow to assess the sensitivity of structural response to the variation of random structural...
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Azo dyes: Sources, occurrence, toxicity, sampling, analysis, and their removal methods
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The Use of Sensory Analysis Techniques to Assess the Quality of Indoor Air
PublicationThe quality of indoor air is one of the significant elements that influences people's well-being and health inside buildings. Emissions of pollutants, which may cause odor nuisance, are the main reason for people's complaints regarding the quality of indoor air. As a result, it is necessary to perform tests aimed at identifying the sources of odors inside buildings. The article contains basic information on the characteristics...
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Determination of Selected Metals in Fruit Wines by Spectroscopic Techniques
PublicationThe determination of metals in different types of food and beverages samples has drawn significant attention due to several reasons with the most important one being the nutritional and toxic effects of these elements or their compounds. The knowledge of certain elements content in wines/fruit wines is of special interest due to their toxicity in case of excessive intake and also the effect they seem to have on the organoleptic...
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PTR-MS and GC-MS as complementary techniques for analysis of volatiles: A tutorial review
PublicationThis tutorial review is a critical commentary on the combined use of two instrumental analytical techniques, namely GC-MS and PTR-MS. The first mention of such an analytical approach likely appeared after the year 2000 and despite many advantages, it has not been applied very often. Therefore, the aim of this article is to elaborate on the concept of their combined use and to provide a curse tutorial for those considering taking...
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EPJ Techniques and Instrumentation
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Journal of Analytical Techniques
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Journal of Biomolecular Techniques
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Surgical Techniques Development
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Techniques in Gastrointestinal Endoscopy
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Operative Techniques in Orthopaedics
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INSTRUMENTS AND EXPERIMENTAL TECHNIQUES
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Techniques - Sciences - Methodes
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Nuclear Science and Techniques
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Phenolic compounds from Nerium oleander leaves: microwave assisted extraction, characterization, antiproliferative and cytotoxic activities
PublicationA microwave-assisted extraction (MAE) method was used for the extraction of phenolic compounds from Nerium oleander leaves. The influence of variables such as ethanol concentration, microwave power, irradiation time and liquid/solid ratio on polyphenol extraction was modelled using a second-order regression equation based on response surface methodology (RSM). The optimal conditions for MAE were: extraction solvent 35% ethanol...
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2023/2024_LATO Modern Techniques in Control Theory
e-Learning CoursesWykład i ćwiczenia z przedmiotu Nowoczesne metody teorii sterowania
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2021/2022_LATO Modern Techniques in Control Theory
e-Learning CoursesWykład i ćwiczenia z przedmiotu Nowoczesne metody teorii sterowania
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A simplified behavioral MOSFET model based on parameters extraction for circuit simulations.
PublicationThe paper presents results on behavior modeling of general purpose Metal-Oxide Semiconductor Field-Effect Transistor (MOSFET) for simulation of power electronics systems requiring accuracy both in steady-state and in switching conditions. Methods of parameters extraction including nonlinearity of parasitic capacitances and steady-state characteristics are based on manufacturer data sheet and externally measurable characteristics....
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Deep eutectic solvent-based shaking-assisted extraction for determination of bioactive compounds from Norway spruce roots
PublicationPolyphenolic compounds play an essential role in plant growth, reproduction, and defense mechanisms against pathogens and environmental stresses. Extracting these compounds is the initial step in assessing phytochemical changes, where the choice of extraction method significantly influences the extracted analytes. However, due to environmental factors, analyzing numerous samples is necessary for statistically significant results,...
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A new approach for the extraction of tetracyclines from soil matrices: application of the microwave-extraction technique
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