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Search results for: SPECT
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Objective, observer-independent evaluation of myocardial perfusion and function: the role of SPECT
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SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY
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SPECTROSCOPY AND SPECTRAL ANALYSIS
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Combined Spectroscopic Methods of Determination of Density of Electronic States: Comparative Analysis of Diffuse Reflectance Spectroelectrochemistry and Reversed Double-Beam Photoacoustic Spectroscopy
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Spectroscopic and Spectroelectrochemical Studies on Redox Properties of Zinc Sulfide and Their Consequences on Photocatalytic Activity
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The instantaneous frequency rate spectogram
PublicationAn accelerogram of the instantaneous phase of signal components referred to as an instantaneous frequency rate spectrogram (IFRS) is presented as a joint time-frequency distribution. The distribution is directly obtained by processing the short-time Fourier transform (STFT) locally. A novel approach to amplitude demodulation based upon the reassignment method is introduced as a useful by-product. Additionally, an estimator of energy...
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Spectroelectroanalytical properties of antitumor agent C1311
PublicationZastosowano kilka metod woltamperometrycznych dla charakterystyki właściwości elektrochemicznych przeciwnowotworowej pochodnej imidazoakrydonu o symbolu C-1311. Wyniki wskazały, że możliwym będzie zastosowanie metod elektrochemicznych do badania oddziaływań badanego związku z DNA. Badania spektroelektrochemiczne ujawniły, że oscylacyjne zmiany absorbcji związku obserwowane po cyklicznej polaryzacji elektrody. Oscylacje te znikały...
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Five years of innovations in development of glow discharges generated in contact with liquids for spectrochemical elemental analysis by optical emission spectrometry
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Exosomes – Spectacular role in reproduction
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Spectrofotometric titration of dsDNA by nitroacridines - chemometrics approach
PublicationW pracy zastosowano podejście chemometryczne do analizy zestawów widm absorpcyjnych w obszarze widzialnym, uzyskanych podczas miareczkowania spektrofotometrycznego nitroakrydyn o potencjalnej aktywności przeciwnowotworowej przy pomocy DNA.Zastosowanie analizy głównych składowych (PCA) wykazało, że podczas miareczkowania 1-nitroakrydyn powstają dwa typy kompleksów, podczas gdy w przypadku 3-nitroakrydyn tylko jeden. Iteracyjna procedura...
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Spectroscopy Methods in Nanotechnology 2023
e-Learning CoursesCourse for 2nd degree Students of Nanotechnology, specialization Nanostructures and computer simulations in materials science, sem. 2. The aim of the course is to discuss the basic theoretical and practical issues of spectroscopy and presentation of the various types of spectroscopic methods and ways to interpret spectra, with particular attention paid to the possibility of their use in the study of nanostructured systems.
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Spectroscopy Methods in Nanotechnology 2022
e-Learning CoursesCourse for 2nd degree Students of Nanotechnology, specialization Nanostructures and computer simulations in materials science, sem. 2. The aim of the course is to discuss the basic theoretical and practical issues of spectroscopy and presentation of the various types of spectroscopic methods and ways to interpret spectra, with particular attention paid to the possibility of their use in the study of nanostructured systems.
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Spectroscopy Methods in Nanotechnology 2024
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Electron Paramagnetic Resonance Spectroscopy and Forward Recoil Spectrometry
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CNS SPECTRUMS
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International Spectator
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New concept of a measurement probe for high impedance spectrocopy
PublicationArtykuł przedstawia nową koncepcję sondy pomiarowej służącej jako obwód wejściowy analizatora do spektroskopii wysokoimpedancyjnej. Dzięki wykorzystaniu przetwornika prąd na napięcie uzyskano najmniejszy możliwy wpływ pojemności kabli dołączających mierzony obiekt na wynik pomiaru. Przeprowadzono analizę sondy biorąc pod uwagę najważniejsze parametry wpływające na dokładność pomiaru: pojemności pasożytnicze oraz rzeczywiste parametry...
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Reduction of spectral interferences in atmospheric pressure glow discharge optical emission spectrometry
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Spectroscopy Methods in Nanotechnology - laboratory 2022
e-Learning CoursesCourse for 2nd degree Students of Nanotechnology, specialization Nanostructures and computer simulations in materials science, sem. 2.
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Spectroscopy Methods in Nanotechnology - laboratory 2023
e-Learning CoursesCourse for 2nd degree Students of Nanotechnology, specialization Nanostructures and computer simulations in materials science, sem. 2.
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Spectroscopy Methods in Nanotechnology - laboratory 2024
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Validation of dynamic electrochemical impedance spectrograms using autocorrelation function
PublicationValidation of impedance data is essential for checking the reliability of experimental data. Kramers – Kronig transformation is used to verify data obtained from classical Electrochemical Impedance Spectroscopy (EIS) measurements. Data obtained from Dynamic Electrochemical Impedance Spectroscopy (DEIS) could be validated in the same way, but in this case, there is no information about internal consistency between every single spectrum...
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Resistance Noise Higher-Order Spectrums in Nanoparticle Gas Sensors.
PublicationPrzedstawiono badania fluktuacji rezystancji sensora gazu wykonanego z nanocząstek WO3. Stwierdzono występowanie składowych o rozkładzie prawdopodobieństwa różnym od rozkładu Gaussa. W celu zwiększenia czułości i selektywności wykrywanych gazów zastosowan do analizy obserwowanych fluktuacji spektra wyższych rzędów.
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Spectrum
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OR SPECTRUM
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PHOTONICS SPECTRA
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Microfluidic devices for photo-and spectroelectrochemical applications
PublicationThe review presents recent developments in electrochemical devices for photo- and spectroelectrochemical investigations, with the emphasis on miniaturization (i.e., nanointerdigitated complementary metal-oxide-semiconductor devices, micro- and nano-porous silicon membranes or microoptoelectromechanical systems), silica glass/microreactors (i.e., plasmonic, Raman spectroscopy or optical microcavities) or polymer-based devices (i.e.,...
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The control software of the portable raman spectrometer
PublicationThe paper contains a description of the control software of a portable Raman spectrometer which was built in the Department of Optoelectronics and Electronic Systems Faculty of Electronics, Telecommunications and Informatics Gdansk University of Technology. The software has modular structure, which includes the laser control module and the spectrum acquisition module (laser power selection, working mode and data acquisition time)...
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Mobile chromatographs and spectrometers for the analysis of chemical warfare agents
PublicationThis article describes the technological state of readiness regarding mobile chromatographs and spectrometers and their appiicability for the analysis of chemical warfare agents (CWAs), degradation products, simulants, and precursors.
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JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY
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Vibrational spectroscopic studies of N,N'-dimethylpropyleneurea-water system: Affected solvent spectra and factor analysis
PublicationZmierzono widma FT-IR układu N,N'-dimetylopropylenomocznik (DMPU) - woda w całym zakresie składów w zakresie 4000-500 cm-1 przy użyciu techniki całkowitego wewnętrznego odbicia (ATR). Hydratacja DMPU została dodatkowo zbadana przy pomocy transmisyjnej spektroskopii FT-IR izotopowo rozcieńczonej HDO w H2O. Widma zanalizowano przy użyciu ilościowej wersji metody widm różnicowych, prowadzącej do wyizolowania widma rozpuszczalnika...
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Usage of concentrated spectrogram for analysis of acoustical signals
PublicationA novel precise method of signal analysis in the time-frequency domain is presented. A signal energy distribution is estimated by discard and displacement of energy parts of the classical spectrogram. A channelized instantaneous frequency and a local group delay are used in order to energy replacement. Additionally, newly introduced representations such as: a channelized instantaneous bandwidth and a local group duration are used...
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Multi-Technique Investigation of Grave Robes from 17th and 18th Century Crypts Using Combined Spectroscopic, Spectrometric Techniques, and New-Generation Sequencing
PublicationThe textile fragments of the funeral clothes found in the 17th and 18th century crypts were subjected to spectroscopic, spectrometric, and microbial investigation. The next-generation sequencing enabled DNA identification of microorganisms at the genus and in five cases to the species level. The soft hydrofluoric acid extraction method was optimized to isolate different classes of dyes from samples that had direct contact with...
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INTERNATIONAL JOURNAL OF MASS SPECTROMETRY
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Validity of impedance spectra obtained by dynamic electrochemical impedance spectroscopy verified by Kramers-Kronig transformation.
PublicationArtykuł przedstawia weryfikację wiarygodności widm impedancyjnych otrzymanych za pomocą niedawno wprowadzonej techniki eksperymentalnej - Dynamicznej Elektrochemicznej Spektroskopii Impedancyjnej (Dynamic Electrochemical Impedance Spectroscopy, DEIS). Technika ta zakłada, że badany system jest pseudostacjonarny jeśli czas pomiaru jest odpowiednio krótki. Czas potrzebny na otrzymanie pojedynczego spektrum zależy od długości okna...
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Portable Raman spectrometer - design rules and applications
PublicationRaman spectroscopy has become more popular due to its new prospective field applications in forensic sciences, war against terrorism, environment protection and other field chemical analysis. Raman spectrometers can be miniaturised to portable devices and their price is decreasing due to development of optoelectronics components. Unfortunately, this technology has still numerous limitations that influence their design and limit...
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Detection of illicit chemicals by portable Raman spectrometer
PublicationThe Raman spectrometers can be built as the portable devices and can be used in various places to detect illicit chemicals. This method has become popular due to deficiency of other fast methods that could be applied against terrorist attacks or could help police at their work. The conception of a portable Raman spectrometer has been presented. The description enclosures presentation of the prepared device and its possible applications...
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Portable raman spectrometer with two excitation wavelengths
PublicationSelected problems of development of a portable Raman spectrometer having small size, reduced power consumption and robust construction are shown. The device dedicated for semiskilled personnel uses two lasers: 785nm and 355nm. Results of preliminary tests are presented. Also data processing procedures as well as problems referred to Raman signals acquisition through packages and influence of interfering signals are discussed.
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Portable raman spectrometer for maritime security applications
PublicationThe fast identification of explosives, narcotics and other chemicals carried on board of ships or transported in containers to the harbors is an important problem of maritime security. Raman spectroscopy is widely used for fast identification of various chemicals. Continuous progress in the field of photonics has resulted in commercial availability of low-power compact Raman spectrometers which can be integrated into portable systems....
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Donor properties of water in organic solvents derived from infrared spectraof HDO
PublicationPrzedyskutowano niektóre ilościowe aspekty kooperatywności wiązań wodorowych wody. Zaproponowano skalę własności elektronodonorowych wody w środowisku aprotycznych rozpuszczalników organicznych, pochodną w stosunku do skali liczb donorowych Gutmanna.
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Resonance-Raman spectro-electrochemistry of intermediates in molecular artificial photosynthesis of bimetallic complexes
PublicationThe sequential order of photoinduced charge transfer processes and accompanying structure changes were analyzed by UV-vis and resonance-Raman spectroscopy of intermediates of a Ru(II) based photocatalytic hydrogen evolving system obtained by electrochemical reduction.
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Absorption spectroscopy setup for determination of whole human blood and blood–derived materials spectral characteristics
PublicationA dedicated absorption spectroscopy system was set up using tungsten-halogen broadband source, optical fibers, sample holder, and a commercial spectrometer with CCD array. Analysis of noise present in the setup was carried out. Data processing was applied to the absorption spectra to reduce spectral noise, and improve the quality of the spectra and to remove the baseline level. The absorption spectra were measured for whole blood...
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Extraction of mass spectra free of background and neighboring component contributions from gas chromatography/mass spectrometry data
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A novel method of time-frequency analysis: an essential spectrogram
PublicationA novel precise method of time-frequency analysis is presented. In the algorithm, a new energy distribution is estimated by simultaneously discard or displacement of the classical spec- trogram energy. A channelized instantaneous frequency and a local group delay are used in order to replacement in the same manner as formulated by Kodera et al. [1, 2]. Additionally, new representations: a channelized instantaneous bandwidth and...
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Using concentrated spectrogram for analysis of audio acoustic signals
PublicationThe paper presents results of time-frequency analysis of audio acoustic signals using the method of Concentrated Spectrograph also known as ''Cross-spectral method'' or ''Reassignment method''. Presented algorithm involves signal's local group delay and channelized instantaneous frequency to relevantly redistribute all Short-time Fourier transform lines in time-frequency plain. The main intention of the paper is to compare various...
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High-Power Jamming Attack Mitigation Techniques in Spectrally-Spatially Flexible Optical Networks
PublicationThis work presents efficient connection provisioning techniques mitigating high-power jamming attacks in spectrally-spatially flexible optical networks (SS-FONs) utilizing multicore fibers. High-power jamming attacks are modeled based on their impact on the lightpaths’ quality of transmission (QoT) through inter-core crosstalk. Based on a desired threshold on a lightpath’s QoT, the modulation format used, the length of the path,...
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“In situ” observations of carbon nanotube generation in CVD cell coupled to spectrometers
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Mobile Gas Chromatographs Coupled with Mass and Ion Mobility Spectrometers and their Applications
PublicationThe articles describes the developments un combining of mass and ion mobility spectrometers (MS, IMS0 with miniature gas chromatographs (GC). The examples of applications of miniaturised GC-MS and GC-IMS devices are presented.
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Combined analysis of whole human blood parameters by Raman spectroscopy and spectral-domain low-coherence interferometry
PublicationIn this article the simultaneous investigation of blood parameters by complementary optical methods, Raman spectroscopy and spectral-domain low-coherence interferometry, is presented. Thus, the mutual relationship between chemical and physical properties may be investigated, because low-coherence interferometry measures optical properties of the investigated object, while Raman spectroscopy gives information about its molecular...
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Fabrication of a Smartphone-Based Spectrophotometer and Its Application in Monitoring Concentrations of Organic Dyes
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Journal of Spectral Theory
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Surface Science Spectra
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Journal of Spectral Imaging
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Africa Spectrum
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Diabetes Spectrum
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IEEE SPECTRUM
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SOCIOLOGICAL SPECTRUM
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Time-frequency analysis of acoustic signals using concentrated spectrogram
PublicationThe paper presents improved method of time-frequency (TF) analysis of discrete-time signals. The method involves signal's local group delay (LGD) and channelized instantaneous frequency (CIF) to purposely redistribute all Short-time Fourier transform (STFT) lines. Additionally, the energy concentration index (ECI) and some histogram-like statistics are used to evaluate readability of estimated TF distributions of the energy. Recorded...
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Playback detection using machine learning with spectrogram features approach
PublicationThis paper presents 2D image processing approach to playback detection in automatic speaker verification (ASV) systems using spectrograms as speech signal representation. Three feature extraction and classification methods: histograms of oriented gradients (HOG) with support vector machines (SVM), HAAR wavelets with AdaBoost classifier and deep convolutional neural networks (CNN) were compared on different data partitions in respect...
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Trends in biomedical analysis of red blood cells – Raman spectroscopy against other spectroscopic, microscopic and classical techniques
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Mass Spectrometry
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Detection system for optical coherence tomography: Czerny-Turner spectrometer
PublicationResearch methods based on spectral analysis have powerful impact on development in many field of science. Signal spectrum can be a source of useful and important data. It enables to obtain information about physical and chemical properties of tested materials. This paper has been devoted to describe optical design for high resolution spectrometer, which is significant element of optical coherence tomography (OCT) systems. Designed...
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SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY
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Spectrophotometric Investigations of membrane oscillator with hexadecyltrimethylammonium bromide
PublicationZbadano widma absorbcyjne w zakresie UV-VIS roztworów wodnych oscylatora z membraną ciekłą zawierającego bromek heksadecylotrimetyloamoniowy. Stwierdzono, że od początku procesu z membrany ciekłej przechodzą do faz wodnych cząsteczki kwasu pikrynowego i nitrobenzenu.
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Using phase of short-term Fourier transform for evaluation of spectrogram performance
PublicationThe concept of spectrogram performance evaluation which exploits information on phase of short-term Fourier transform (STFT) is presented. A spectrograph which is time-frequency analyzing tool, is compared to a filter bank that demultiplexes a signal. Local group delay (LGD) and channelized instantaneous frequency (CIF) is obtained for each filtered component signal. In presented solution the performance is evaluated using so-called...
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Application of chromogenic dye in biogenic amines determination using spectrophotometry
PublicationBiogenic amines content can be the source of information in the field of freshness and suitability of certain foods for consumption. However, most analytical methods for their determination require complicated sample preparation and expert knowledge. Because of that, a novel approach based on chromogenic dye application was proposed. After the SN1 reaction of an amine with S 0378 dye, the absorbance of the solution was measured...
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Characterization of Bioactivity of Selective Molecules in Fruit Wines by FTIR and NMR Spectroscopies, Fluorescence and Docking Calculations
PublicationFourier transform infrared (FTIR) and proton nuclear magnetic resonance (1H NMR) spectroscopies were applied to characterize and compare the chemical shifts in the polyphenols’ regions of some fruit wines. The obtained results showed that FTIR spectra (1800–900 cm−1) and 1H NMR (δ 6.5–9.3 ppm) of different fruit wines can be used as main indices of the year of vintage and quality of fruit wines. In addition to the classical determination...
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Application of a smartphone based spectrophotometer for rapid in-field determination of nitrite and chlorine in environmental water samples
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Spectrum Sensing Based on Hybrid Spectrum Handoff in Cognitive Radio Networks
PublicationThe rapid advancement of wireless communication combined with insufficient spectrum exploitation opens the door for the expansion of novel wireless services. Cognitive radio network (CRN) technology makes it possible to periodically access the open spectrum bands, which in turn improves the effectiveness of CRNs. Spectrum sensing (SS), which allows unauthorized users to locate open spectrum bands, plays a fundamental part in CRNs....
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Development of a liquid chromatography–tandem mass spectrometryprocedure for determination of endocrine disrupting compounds infish from Mediterranean rivers
PublicationA new, sensitive and rapid method based on QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe)approach followed by ultra high performance liquid chromatography coupled with tandem mass spec-trometry (UHPLC–MS/MS) was developed for the determination of nineteen endocrine disruptors (EDCs)and related compounds belonging to different classes in various fish species. Matrix effect on the analyti-cal performance was evaluated,...
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Spectroscopic evaluation of a low power atmospheric pressure mixed argon–helium microwave induced plasma combined with the chemical generation of volatile species for the optical emission spectrometric determination of arsenic, antimony and mercury
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Spectacular Oxygen Evolution Reaction Enhancement Through Laser Processing of the Nickel-Decorated Titania Nanotubes
PublicationThe selective, laser-induced modification of the nickel-decorated titania nanotubes provides remarkable enhancement toward oxygen evolution reaction. Particularly, the irradiation of the laterally spaced crystalline TiO2 nanotubes, results in the formation of the tight closure over irradiated end, preserving their hollow interior. The shape of the absorbance spectra is modulated along with applied energy, and the new absorption...
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Spectacular Oxygen Evolution Reaction Enhancement through Laser Processing of the Nickel‐Decorated Titania Nanotubes
PublicationThe selective, laser‐induced modification of the nickel‐decorated titania nanotubes provides remarkable enhancement toward oxygen evolution reaction. Particularly, the irradiation of the laterally spaced crystalline TiO2 nanotubes, results in the formation of the tight closure over irradiated end, preserving their hollow interior. The shape of the absorbance spectra is modulated along with applied energy, and the new absorption...
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Spectroelectrochemical characteristics of poly(3,4-ethylenedioxythiophene) / iron hexacyanoferrate film-modified electrodes
PublicationPraca dotyczy pomiarów spektroelektrochemicznych materiałów hybrydowych złożonych z polimeru elektroaktywnego poli(3,4-etylenodioksytiofenu) i Błękitu Pruskiego. Dla porównania badano również filmy polimerowe z wybranymi przeciwjonami: heksacyjanożelazowym (Fe(CN)63-/4-), chlorkowym (Cl-) i polistyrenosulfonowym (PSS-). Materiały w postaci cienkich filmów otrzymano na elektrodzie szklanej pokrytej tlenkiem indowo-cynowym. Widma...
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Polynomial description of dynamic impedance spectrogram—introduction to a new impedance analysis method
PublicationThis paper presents a polynomial description of spectrograms obtained using Dynamic Electrochemical Impedance Spectroscopy. A method to fit the polynomial degree correctly is discussed. A simple electrical system of a diode connected in parallel with a capacitor was used for testing. Dynamic impedance measurements during potentiodynamic polarization were conducted. This paper presents an alternative analysis method that allows...
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The use of spectrometric diagnostics in identification of the technical condition of tribological systems
PublicationThe paper presents, as an effect of the analysis of investigation results, a possibility of using the spectrometric diagnostics in the tribological system technical condition supervision arrangement. A model, based on the emission of solid particles in tribological system operation, allows to identify the system technical condition. After the analysis of tests carried out with the use of that model, it has been found that the content...
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EARTHQUAKE SPECTRA
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Validation of Interpolation Algorithms for Multiscale UV-VIS Imaging Using UAV Spectrometer
PublicationIn this study, we present a comparison of popular methods for the interpolation of irregular spatial data in order to determine the applicability of each algorithm for hyperspectral reflectance estimation. The algorithms were benchmarked against a very high-resolution orthoimage from an RGB camera and medium-resolution satellite imagery from Sentinel-2A. We tested five interpolation algorithms: Triangulated Irregular Network (TIN),...
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A simple graphene-based pipette tip solid-phase extraction of malondialdehyde from human plasma and its determination by spectrofluorometry
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Sea spectra revisited
PublicationPokazano, że widma falowania ITTC, wywodzące się z widma Bretschneidera, zależnego od dwóch parametrów, można zredukować do wspólnego widma bezwymiarowego, co oznacza, że są one geometrycznie powinowate. To samo dotyczy widma JONSWAP, które dodatkowo charakteryzuje trzeci paprametr, związany z kształtem piku. Umożliwia to aproksymację tych widm za pomocą rozkładu log-normalnego, co zapewnia realistyczny parametr szerokości widma,...
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Spectrophotometric Investigations of Nitrobenzene Liquid Membrane Oscilator With Hexadecyltrimethylammonium Bromide.
PublicationPrzedstawiono osylacje różnicy potencjału między fazami wodnymi oscylatora z membraną ciekłą zawierającego kationowy surfaktant. Ustalno zmiany stężeń nitrobenzenu i kwasu pikrynowego w czasie procesu metodą spektrafotometryczną. Stwierdzono, że nitrobenzen przechodzi do faz wodnych od początku procesu, zaś anion pikrynowy przechodzi tylko do fazy akceptorowej. W oparciu otrzymane wyniki stwierdzono, że transport składników membrany...
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Music Theory Spectrum
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HortFlora Research Spectrum
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JNCI Cancer Spectrum
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Spectroelectrochemical analysis of TiO 2 electronic states – Implications for the photocatalytic activity of anatase and rutile
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Optically transparent boron-doped nanocrystalline diamond films for spectroelectrochemical measurements on different substrates
PublicationFabrication process of optically transparent boron nanocrystalline diamond (BNCD) electrode on silicon and quartz substrate was shown. The B-NCD films were deposited on the substrates using Microwave Plasma Assisted Chemical Vapor Deposition (MWPACVD) at glass substrate temperature of 475 ºC. A homogenous, continuous and polycrystalline surface morphology with high sp3 content in B-NCD films and film thickness depending from substrate...
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VIBRATIONAL SPECTROSCOPY
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ATOMIC SPECTROSCOPY
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Spectroscopy Europe
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OPTICS AND SPECTROSCOPY
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SPECTROSCOPY-US
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Quasi Real-Time XRF Spectrometer in Source Apportionment of PM10 in a Typical Suburban Area
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X-RAY SPECTROMETRY
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Clinical Mass Spectrometry
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Mass Spectrometry Letters
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JOURNAL OF MASS SPECTROMETRY
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Chemometric Method of Spectra Analysis Leading to Isolation of Lysozyme and CtDNA Spectra Affected by Osmolytes
PublicationW niniejszej pracy zaprezentowana została chemometryczna metoda analizy danych widmowych, prowadząca do wyizolowania widm FTIR biomakrocząsteczek (lizozymu z białka jaja kurzego i ctDNA) zaburzonych przez wybrane osmolity (TMAO, betainę) w roztworach wodnych. Została ona oparta na metodzie widm różnicowych, wykorzystywanej pierwotnie do określania struktury rozpuszczalnika wokół cząsteczek substancji rozpuszczonej. Cykliczne wykorzystanie...
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The amplitude analysis of impedance spectra
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The simultaneous detection of food dyes from different samples in a 96-well plate by spectrophotometry
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A rapid spectrofluorimetric method for the determination of malondialdehyde in human plasma after its derivatization with thiobarbituric acid and vortex assisted liquid–liquid microextraction
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