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Search results for: GAS CHROMATOGRAPHS,
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Determination of thiocyanate (biomarkers of ETS) and other inorganic ions in human nasal discharge samples using ion chromatography
PublicationEnvironmental tobacco smoke (ETS) is a mixture of air and tobacco smoke containing more than 4000 chemical substances. In view of the health risks of many of these substances, studies are needed to determine biomarkers of exposure to ETS constituents in people who actively or passively are exposed to the toxic compounds. The methodologies for determining most biomarkers from saliva, urine and blood samples are known, but methods...
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A solid phase extraction–ion chromatography with conductivity detection procedure for determining cationic surfactants in surface water samples
PublicationA new analytical procedure for the simultaneous determination of individual cationic surfactants (alkyl benzyl dimethyl ammonium chlorides) in surface water samples has been developed. We describe this methodology for the first time: it involves the application of solid phase extraction (SPE – for sample preparation) coupled with ion chromatography–conductivity detection (IC-CD – for the final determination). Mean recoveries of...
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Analysis of multi-class pharmaceuticals in fish tissues by ultra-high-performance liquid chromatography tandem mass spectrometry
PublicationA new sensitive method based on pressurized liquid extraction (PLE) and purification by gel permeation chromatography (GPC) prior to ultra-high-performance liquid chromatography coupled to tandem mass spectrometry (UHPLC–MS/MS) was developed for the determination in fish homogenate, liver and muscle of twenty pharmaceuticals compounds and metabolites from seven commonly used therapeutic families. An extensive matrix effect evaluation...
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Development of a liquid chromatography–tandem mass spectrometryprocedure for determination of endocrine disrupting compounds infish from Mediterranean rivers
PublicationA new, sensitive and rapid method based on QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe)approach followed by ultra high performance liquid chromatography coupled with tandem mass spec-trometry (UHPLC–MS/MS) was developed for the determination of nineteen endocrine disruptors (EDCs)and related compounds belonging to different classes in various fish species. Matrix effect on the analyti-cal performance was evaluated,...
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Determination of tocopherols and tocotrienols in human breast adipose tissue with the use of high performance liquid chromatography-fluorescence detection
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Process control of leakages in refinery reforming plant by means of Normal Phase High Performance Liquid Chromatography (HPLC)
PublicationPraca dotyczy zbadania możliwości, opracowania nowej procedury badawczej oraz dokonania oznaczeń ¬m-krezolu w strumieniu produktu z procesu reformingu katalitycznego techniką wysokosprawnej chromatografii cieczowej w układzie faz normalnych, z detektorem spektrofotometrycznym typu DAD (NP-HPLC-UV-VIS/DAD). Opracowana procedura stanowi alternatywę dla innych procedur wykorzystujących klasyczne techniki analityczne, albo wykorzystanie...
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Determination of nine high-intensity sweeteners in various foods by high-performance liquid chromatography with mass spectrometric detection
PublicationAn analytical procedure involving solid-phase extraction (SPE) and high-performance liquid chromatography-mass spectrometry has been developed for the determination of nine high-intensity sweeteners authorised in the EU; acesulfame-K (ACS-K), aspartame (ASP), alitame (ALI), cyclamate (CYC), dulcin (DUL), neohesperidin dihydrochalcone (NHDC), neotame (NEO), saccharin (SAC) and sucralose (SCL) in a variety of food samples (i.e. beverages,...
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Application of ion chromatography with pulsed amperometric detection for the determination of trace cyanide in biological samples, including breast milk
PublicationCyanide (CN) is the biomarker of exposure to the components of tobacco smoke, although its presence in biological samples is also due to the consumption of products containing cyanogenic glycosides. In this work, we determine the concentration of the free cyanide in urine, saliva and breast milk matrices, using ion chromatography with pulsed amperometric detection (IC-PAD). IC-PAD is an emerging method, with only few documented...
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pH-Induced modification to stratum corneum lipids investigated using thermal, spectroscopic, and chromatographic techniques
PublicationZbadano jakim zmianom jakościowym i ilościowym ulegają indywidualne klasy lipidów w Stratum Corneum (tkanka rogowa skóry) pod wpływem środowiska o zmiennym pH.
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Ionic chromatographic studies on intercorrelation between cooccuring ions in precipitation waters in the area of Tricity (Poland).
PublicationObszar Trójmiasta jest terenem bardzo zurbanizowanym. Duża koncentracja przemysłu na małej powierzchni stanowi poważne zagrożenie dla powietrza atmosferycznego. Analiza emisji zanieczyszczeń wskazuje na zróżnicowanie ich źródeł. Najważniejsze są substancje które tworzą się podczas energetycznego spalania paliw. 80% emisji ditlenku siarki, ditlenku azotu, pyłu, tlenku węgla i sadzy węglowej pochodzi z Gdańska i Gdyni, głównych centrów...
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Application of the chromatographic retention index system for theestimation of the calibration constants of permeation passivesamplers with polydimethylsiloxane membranes
PublicationW pracy przedstawiono wyniki badań z zastosowaniem pasywnych dozymetrów typu permeacyjnego, wyposażonych w membrany wykonane z PDMS. Badania dotyczyły oszacowania wartości stałych kalibracyjnych dozymetrów przy wykorzystaniu systemu indeksów retencji, wyznaczanych chromatograficznie, w warunkach liniowego narostu temperatury pracy kolumny (LTPRI). Znaleziono korelację pomiędzy wartościami stałych kalibracyjnych próbników typu pasywnego,...
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Fragmental Method KowWIN as the Powerful Tool for Prediction of Chromatographic Behavior of Novel Bioactive Urea Derivatives
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Chromatographic separation, determination and identification of ecdysteroids: Focus on Maral root (Rhaponticum carthamoides, Leuzea carthamoides )
PublicationThe review presents general principles for choosing optimal conditions for ecdysteroid separation, identification, and isolation using HPLC/TLC techniques in RP, NP- HILIC or NP modes. Analytics of ecdyteroids pose a still insufficiently resolved problem. Plant-derived ecdysteroids are a point of interest of pharmaceutical industry and sport medicine due to their postulated adaptogenic and anabolic properties. In insects, ecdysteroids...
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The state-of-the-art determination of urinary nucleosides using chromatographic techniques “hyphenated” with advanced bioinformatic methods
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Metabolomic Heterogeneity of Urogenital Tract Cancers Analyzed by Complementary Chromatographic Techniques Coupled with Mass Spectrometry
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Chromatographic lipophilicity determination using large volume injections of the solvents non-miscible with the mobile phase
PublicationA new perspective in the lipophilicity evaluation through RP-HPLC is permitted by analysis of the retentionfactor (k) obtained by injecting large volumes of test samples prepared in solvents immiscible withmobile phase. The experiment is carried out on representative groups of compounds with increasedtoxicity (mycotoxins and alkaloids) and amines with important biological activity (naturally occurringmonoamine compounds and related...
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Jan Hupka prof. dr hab. inż.
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Revista de História das Ideias
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Das Mittelalter. Perspektiven mediävistischer Forschung
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Journal of Gay & Lesbian Mental Health
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Journal of Gay & Lesbian Social Services
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GLQ-A JOURNAL OF LESBIAN AND GAY STUDIES
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Revista Medica Clinica Las Condes
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Recent Applications of 1D GC-MS and 2D GC-MS in Foodomics Studies
PublicationGas chromatography coupled with mass spectrometry and food chemistry have been tightly linked since the 1960s. This setup is also an integral part of the omics studies when it comes to low mass metabolites. Therefore, the marriage of GC-MS and foodomics is obvious. Two-dimensional gas chromatography coupled with mass spectrometry fits perfectly within the latest trends in foodomics, since it is tailored for holistic food analysis....
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Characterization of home-made and regional fruit wines by evaluation of correlation between selected chemical parameters
PublicationSince the last decade of the 20th century, there has been rising interest in the production of fruit wines, as evidenced by the high number of published papers and books covering this matter. When aiming to produce quality fruit wines, it is essential to evaluate the analytical parameters of the beverage. In this context, there are a large number of analyses for the evaluation of wines and fruit wines. This article characterizes...
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FTIR spectra of gas mixtures from the process of biogas dry reforming using Al2O3/5%Cu catalyst
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using AlOOH/1%Cu nanocatalyst. The specatra were collected every 1 minute from 800C to 500C. Reagent flow was set to 20ml/min.
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FTIR spectra of gas mixtures from the process of biogas dry reforming using CeO2/5%Cu catalyst
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using CeO2/5%Cu nanocatalyst. The specatra were collected every 1 minute from 800C to 500C. Reagent flow was set to 20ml/min.
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FTIR spectra of gas mixtures from the process of biogas dry reforming using Al2O3/5%Cu catalyst
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using Al2O3 (TMDAR)/5%Cu nanocatalyst. The specatra were collected every 1 minute from 800C to 500C. Reagent flow was set to 20ml/min.
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Rain Gardens GC_MS analysis dataset
Open Research DataThis dataset contains the results of samples analysis (no-target analysis: scan mode) using gas chromatography coupled with mass spectrometry GC–MS (GC-2030 NEXIS MS, Shimadzu, Japan or Thermo Scientific, Waltham, USA).
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Kinetics of hexane and cyclohexane biodegradation using Candida subhashii in mineral salt medium in the presence of DES solution
Open Research DataDataset presents results of investigations on kinetics of biodegradation of hexane and cyclohexane in Candida subhashii.
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Quantitative structure—retention relationship modeling of the retention behavior of selected antipsychotic drugs in normal-phase thin-layer chromatography
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Determination of nonsteroidal antiinflammatory drugs in water samples using liquid chromatography coupled with diode-array detector and mass spectrometry
PublicationOpracowano i zwalidowano metodykę do oznaczania śladowych ilości sześciu różnych związków z grupy niesteroidowych leków przeciwzapalnych w próbkach wodnych. Anality zostały wybrane spośród najczęsciej sprzedawanych leków w Polsce. Sprawdzono kilka różnych kolumienek ekstrakcyjnych i wybrano RP-18 jako najlepsze wypełnienie do wzbogacania oznaczanych związków. Opracowaną metodykę z powodzeniem zastosowano do analizy próbek rzeczywistych.
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An evaluation of sucrose as a possible contaminant in e-liquids for electronic cigarettes by hydrophilic interaction liquid chromatography–tandem mass spectrometry
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Determination of flavanols by liquid chromatography with fluorescence detection. Application to the characterization of cranberry-based pharmaceuticals through profiling and fingerprinting approaches
PublicationIn this work, a new method based on reversed-phase high-performance liquid chromatography (HPLC) with fluorescence detection (FLD) was established for the determination of catechins and related oligomeric proanthocyanidins (PACs) in cranberry-based pharmaceuticals. Compounds were recovered by liquid extraction using methanol/water/hydrochloric acid (60:39:1, v:v:v) as the extraction solvent. The chromatographic separation was carried...
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Development of an Analytical Protocol for Determination of Cyanide in Human Biological Samples Based on Application of Ion Chromatography with Pulsed Amperometric Detection
PublicationA simple and accurate ion chromatography (IC) method with pulsed amperometric detection (PAD) was proposed for the determination of cyanide ion in urine, sweat, and saliva samples. The sample pretreatment relies on alkaline digestion and application of Dionex OnGuard II H cartridge. Under the optimized conditions, the method showed good linearity in the range of 1–100 μg/L for urine, 5–100 μg/L for saliva, and 3–100 μg/L for sweat...
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A Fast and Validated Method for the Determination of Malondialdehyde in Fish Liver Using High-Performance Liquid Chromatography with a Photodiode Array Detector
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Determination of Pesticide Residues in Honeybees using Modified QUEChERS Sample Work-Up and Liquid Chromatography-Tandem Mass Spectrometry
PublicationIncreasing emissions of chemical compounds to the environment, especially of pesticides, is one of factors that may explain present honeybee colony losses. In this work, an analytical method employing liquid chromatography-tandem mass spectrometry (LC-MS/MS) was optimized for the simultaneous screening of 19 pesticides which have not been yet determined in honeybee samples from northern Poland (Pomerania). The sample preparation,...
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An evaluation of sucrose as a possible contaminant in e-liquids for electronic cigarettes by hydrophilic interaction liquid chromatography–tandem mass spectrometry
PublicationThe influence of sucrose combustion products on smoking and nicotine addiction is still controversial because the presence of the sucrose may be treated as a source of aldehydes and organic acids. In e-liquids used as refills for electronic cigarettes, which are made primarily of poly(propylene glycol), glycerine and ethanol, sucrose may be present at trace levels, and its impact on mainstream smoke formation, and hence on human...
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Determination of Nine Intense Sweeteners in Foodstuffs by High-Performance Liquid Chromatography and Evaporative Light-Scattering Detection: Interlaboratory Study
PublicationW pracy przedstawiono wyniki badań międzylaboratoryjnych, opracowanej wcześniej metody jednoczesnego oznaczania dziewięciu słodzików o wysokiej mocy w produktach żywnościowych. W badaniach wzięło udział siedem laboratoriów (Belgia, Niemcy, Portugalia). W rezultacie dowiedziono, iż opracowana metoda umożliwia uzyskanie dokładnych, powtarzalnych i odtwarzalnych wyników analiz dla wszystkich badanych słodzików i typów żywności.
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In-Syringe Dispersive Liquid-Liquid Microextraction Coupled with High- Performance Liquid Chromatography for Trace Analysis of Naphthalene Sulfonates in Seawater
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Direct injection liquid chromatography-mass spectrometry (DI-LC-MS) analysis for rapid lipidomic profiling of extracellular vesicles
PublicationExtracellular vesicles (EVs) are small, spherical particles produced by eukaryotic and prokaryotic cells, surrounded by a bilayer membrane and carrying various bioactive molecules, such as proteins, surface receptors, membrane and soluble proteins, lipids, and nucleic acids. EVs are of substantial interest because of their important roles in cell communication, epigenetic regulation and possible application in disease diagnosis...
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Rapid determination of multiple aminoglycoside antibiotics in veterinary formulations by ion-pair chromatography coupled with evaporative light scattering detection
PublicationA fast and simple method for simultaneous determination of eight aminoglycoside antibiotics using ion-pairing liquid chromatography (IPLC) coupled with evaporative light scattering detection (ELSD) has been developed and validated. Separation of amikacin, apramycin, gentamicin (as a sum of gentamicin C1, C2 and C1A), kanamycin A, neomycin B, paromomycin, streptomycin and tobramycin was achieved using C18 column with H2O and MeOH/acetone,...
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Precise Evaluation of Gas–Liquid Two-Phase Flow Pattern in a Narrow Rectangular Channel with Stereology Method
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The application of checklists in the field of complex operation based on the operating experiences of a liquefied petroleum gas handling simulator.
PublicationOmówiono pojęcie list sprawdzających (z ang. checklists). Podano charakterystykę techniczną symulatora operacji ładunkowych gazowca typu LPG znajdującego się w laboratorium Katedry Siłowni Okrętowych Akademii Morskiej w Gdyni wraz z jego możliwościami dydaktycznymi. Przedstawiono zasady tworzenia list sprawdzających czynności obsługowe wraz z przykładem takiej listy.
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Parameter of nonlinearity B/A of three-component systems with separate volumes of liquid, its vapor and a neutral gas
PublicationOtrzymane zostało wyrażenie dla zaburzenia entropii substancji o trzech komponentach jako funkcja zaburzeń jej ciśnienia i gęstości. Na podstawie wzoru prędkość i parametru nieliniowosci fali akustycznej zostały wyliczone jako funkcje i ciśnienia i koncentracji pary i powietrza. Rezultaty są przedstawione w postaci wykresów.
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Ammonia in Fly Ashes from Flue Gas Denitrification Process and its Impact on the Properties of Cement Composites
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Application analysis of a hybrid solid oxide fuel cell-gas turbine system for marine power plants
PublicationThe results of theoretical studies of the possibilities of using hybrid solid oxide fuel cell–gas turbine (SOFC-GT) systems for marine power plants are presented. A 500 kW auxiliary marine power plant scheme using stacks of SOFCs in combination with a regenerative gas turbine operating with over-expansion based on our recent patent application is proposed. The results of mathematical modelling showed the opportunity to obtain a...
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EVALUATION OF LIQUID-GAS FLOW IN PIPELINE USING GAMMA-RAY ABSORPTION TECHNIQUE AND ADVANCED SIGNAL PROCESSING
PublicationLiquid-gas flows in pipelines appear in many industrial processes, e.g. in the nuclear, mining, and oil industry. The gamma-absorption technique is one of the methods that can be successfully applied to study such flows. This paper presents the use of thegamma-absorption method to determine the water-air flow parameters in a horizontal pipeline. Three flow types were studied in this work: plug, transitional plug-bubble,...
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Investigations of the Working Process in a Dual-Fuel Low-Emission Combustion Chamber for an FPSO Gas Turbine Engine
PublicationThis investigation is devoted to an analysis of the working process in a dual-fuel low-emission combustion chamber for a floating vessel’s gas turbine. The low-emission gas turbine combustion chamber with partial pre-mixing of fuel and air inside the outer and inner radial-axial swirlers was chosen as the object of research. When modelling processes in a dual-flow low-emission gas turbine combustion chamber, a generalized method...
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Thermal analysis of macro-encapsulated phase change material coupled with domestic gas heater for building heating
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