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Search results for: bis-tetrazole
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Azo and azoxythiacrown ethers: synthesis and properties
PublicationA series of 16- and 18-membered azo- and azoxythiacrown ethers have been synthesized by reductive macrocyclization of the respective bis(nitrophenoxy)oxaalkanes. The aromatic residues located in the polyether region of the molecule were introduced to macrocyclic skeletons and their affinities toward different groups of metal cations in ion-selective electrodes were described. X-ray structures for one dinitropodand and one azoxybenzothiacrown...
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Occurrence and Levels of Biogenic Amines in Beers Produced by Different Methods
PublicationThe concentration of biogenic amines (BAs) in beer depends, among other factors, on the activity of microorganisms, in particular lactic acid bacteria. In this work an analytical method based on derivatization with tosyl chloride and high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) was used to determine 17 BAs in samples of commercially available beers, and to monitor the changes in concentration of...
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Phytoremediation—From Environment Cleaning to Energy Generation—Current Status and Future Perspectives
Publication:Phytoremediationis a technology based on the use of green plants to remove, relocate, deactivate, or destroy harmful environmental pollutants such as heavy metals, radionuclides, hydrocarbons, and pharmaceuticals. Under the general term of phytoremediation, several processes with distinctively different mechanisms of action are hidden. In this paper, the most popular modes of phytoremediation are described and discussed. A broad...
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Literature update of analytical methods for biogenic amines determination in food and beverages
PublicationBiogenic amines (BAs) have been reported in a variety of foods, such as fish, meat, cheese, and wines. The formation of BAs in food by the microbial decarboxylation of amino acids can result in human allergic reactions, characterized by difficulty in breathing, rash, vomiting, and hypertension. Control measures to prevent biogenic amine formation in foods and/or reduce their levels should be considered. Therefore, monitoring of...
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A General Synthesis of Diaryl Cyclic Diamidines
PublicationA convenient and general method has been developed for directly converting bis-nitriles, e.g., I, to cyclic diamidines, e.g., II, using reagents derived from diaminoalkanes, e.g., H2NCH2CH2NH2, satd. with hydrogen sulfide. A 1:1 mixt. of a diaminoalkane and Et alc. (or without) was effective in most cases (72-88%). The synthetic utility of this methodol. in the prepn. of tetrakis(cyclic amidino)pyrenes III (R = H, Me) from 1,3,6,8-tetracyanopyrene...
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Local impedance spectroscopy of membranes
PublicationCelem niniejszej publikacji jest zaprezentowanie zastosowania techniki Lokalnej Elektrochemicznej Spektroskopii Impedancyjnej (LEIS) do uzyskania lokalnej charakterystyki membran. Membranę wykonaną z polichlorku winylu (PCV), plastyfikowaną sebacynianem bis(2etyloheksylu) i domieszkowaną boranem tetradodecyloamoniowym zbadano pod kątem równomiernego rozkładu przewodnictwa na powierzchni badanej próbki. Lokalne pomiary impedancyjne,...
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A prototype of electrochemical sensor for measurement of carbonyl compounds in air
PublicationThe paper presents the results of investigation on a prototype sensor for measurement of benzaldehyde and formaldehyde in air. Sensitivity, limit of quantification and coefficient of selectivity of the sensor have been determined as a function of membrane thickness and electrode type using square wave voltammetry (SWV) technique. The working and counter electrodes were made of platinum and gold. Ionic liquids 1-hexyl, 3-methylimidazolium...
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Problematyka doboru zabezpieczeń dławików kompensacyjnych pracujących w sieciach najwyższych napięć
PublicationW artykule przedstawiono trudności, jakie napotyka się podczas projektowania systemu zabezpieczeń dla dławików przyłączanych bezpośrednio do sieci najwyższych napięć (NN). Bazując na przykładzie budowanej aktualnie stacji 400 kV Ełk Bis, pokazano, że możliwości zabezpieczenia dławika, oparte na układach EAZ wykorzystujących pomiary sygnałów elektrycznych z przekładników prądowych i napięciowych, mają swoje ograniczenia i w pewnych...
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Wybrane problemy doboru zabezpieczeń dławików kompensacyjnych pracujących w sieciach najwyższych napięć
PublicationW referacie przedstawiono trudności jakie napotyka się podczas projektowania systemu zabezpieczeń dla dławików przyłączanych bezpośrednio do sieci najwyższych napięć (NN). Referat, bazując na przykładzie budowanej aktualnie stacji 400 kV Ełk Bis, pokazuje, że możliwości zabezpieczenia dławika, oparte na układach EAZ wykorzystujących pomiary sygnałów elektrycznych z przekładników prądowych i napięciowych mają swoje ograniczenia...
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A new Thermus sp. class-IIS enzyme subfamily: isolation of a ''twin'' endo nuclease TspDTI with a novel specificity 5´-ATGAA(N11/9)-3´, related to TspGWI, Taqll and Tth111II. 5´-ATGAA(N11/9)-3´, spokrewnionej z TspGWI, TaqII i Tth111II.
PublicationOdkryto i scharakteryzowano nową subrodzinę enzymów klasy IIS z Thermus sp.
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Implementation of Hermite-Ritz method and Navier’s Technique for Vibration of Functionally Graded Porous Nanobeam Embedded in Winkler-Pasternak Elastic Foundation Using bi-Helmholtz type of nonlocal elasticity
PublicationPresent study is devoted to investigating the vibration characteristics of Functionally Graded (FG) porous nanobeam embedded in an elastic substrate of Winkler-Pasternak type. Classical beam theory (CBT) or Euler-Bernoulli beam theory (EBT) has been incorporated to address the displacement of the FG nanobeam. Bi-Helmholtz type of nonlocal elasticity is being used to capture the small scale effect of the FG nanobeam. Further, the...
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Non-linear static stability of bi-layer carbon nanosheets resting on an elastic matrix under various types of in-plane shearing loads in thermo-elasticity using nonlocal continuum
PublicationIn this research, the shear and thermal buckling of bi-layer rectangular orthotropic carbon nanosheets embedded on an elastic matrix using the nonlocal elasticity theory and non-linear strains of Von-Karman was studied. The bi-layer carbon sheets were modeled as a double-layered plate, and van der Waals forces between layers were considered. The governing equations and boundary conditions were obtained using the first order shear...
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Evaluation of the Impact of Storage Conditions on the Biogenic Amines Profile in Opened Wine Bottles
PublicationA survey of biogenic amine (BA) profiles in opened wine bottles has been established to monitor the level of biogenic amines (BAs) in opened bottles against time and other conditions. Bottles of red and white wine were submitted to different temperatures, stopper type (screw cap, cork), and use of vacuum devices. A total of six wines made from a variety of grapes were obtained from vineyards from regions across Poland. Dispersive...
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IEEE/ACM International Conference on Big Data Computing, Applications and Technologies
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The statistic properties of rms voltage and frequency in the ship's electrical power system
Open Research DataThe dataset is a part of the research results on the quality of supply voltage on bus bars of the main switchboard of the ship's electrical power system in different states of ship exploitation. The attached dataset contains the results of a statistical analysis of rms voltage and frequency in the ship's electrical power system. The following statistical...
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Synthesis, structure and properties of novel poly(hydroxyurethane)s obtained by non-isocyanate route
PublicationNon-isocyanate polyurethanes (NIPUs) can be synthesized by polyaddition of five-membered bis(cyclic carbonate)s and primary diamines. NIPUs are an alternative for the commonly used (in the form of foams, elastomers, coatings or fibers) in the industry polyurethanes obtained using toxic and moisture sensitive diisocyanates, polyols and low-molecular weight chain extenders. The main aim of this work was to synthesize non-isocyanate...
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Electrochemical sensor for measurement of volatile organic compounds employing square wave perturbation voltage
PublicationThe paper presents the results of investigation on a prototype sensor for measurement of benzaldehyde in air. Sensitivity and limit of quantification of the sensor were determined for different internal electrolyte using the square wave voltammetry (SWV) as a detection technique. The working and counter electrodes were made of platinum. Ionic liquids 1-hexyl, 3-methylimidazolium chloride,1-hexyl, 3-methylimidazolium bis (trifluoromethanesulfonyl)...
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Novel and Efficient Methods for the Synthesis of Symmetrical Trisulfides
PublicationWe have developed a convenient methods for the synthesis of symmetrical trisulfides under mild conditions in very good yields. The described methods are based on the straightforward preparation of 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinane-2-disulfanyl derivatives from readily available 5,5-dimethyl-2-sulfanyl-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The symmetrical...
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TBAF Promoted Formation of Symmetrical Trisulfides
PublicationWe have developed a new method for the synthesis of functionalized symmetrical trisulfides based on (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives prepared from readily available 5,5-dimethyl-2-sul-fanyl-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The symmetrical trisulfides can be obtained from aliphatic and aromatic thiols andL-cysteine derivatives...
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Emilia Dębińska-Bis
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Ionogel sorbent coatings for determining organophosphorus and pyrethroid insecticides in water and fresh juice samples by headspace-solid phase microextraction
PublicationThe sol–gel method yielded three different ionogel sorbent coatings that were obtained based on a silica material containing ionic liquids (ILs) immobilized in its pores. Two ILs, triethylsulfonium bis(trifluoromethylsulfonyl) imide [Set3][TFSI] and 1-butyl-1-methylpiperidinium bis(trifluoromethylsulfonyl)imide [C4C1Pip][TFSI], as well as their equimolar mixture [Set3/C4C1Pip], were used to obtain ionogel fibers. The developed...
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Tuning the extraction properties of ionogel-coated Solid-phase microextraction fibers based on the solvation properties of the ionic liquids
PublicationA silica-based network was used to immobilize ionic liquid-based ionogels and applied as a fiber coating forsolid-phase microextraction (SPME). The ionogels were prepared by a sol–gel process, using two ionic liquids,triethylsulfonium bis(trifluoromethylsulfonyl)imide ([Set3][TFSI]) and 1-butyl-1-methylpiperidinium bis(tri-fluoromethylsulfonyl)imide ([C4C1Pip][TFSI]), as well as their equimolar mixture. Methyltrimethoxysilane wasused...
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Sustainability objectives and collaboration lifecycle in cluster organizations
PublicationIn our paper, we combine two issues, collaboration in cluster organizations and sustainability, aiming to answer the question: Does complex governance structure of cluster organizations support members in formulating and reaching sustainability objectives? Based on four case studies of cluster organizations and a still novel abductive approach, we present the ways in which sustainability was executed in their functioning. Our study...
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Sustainability of Cluster Organizations as Open Innovation Intermediaries
PublicationThe purpose of the paper is to identify the most important open innovation practices used by cluster organizations (COs). To reflect these practices, the paper uses the concept of the trajectory of relationship development in COs, applied in the Interizon cluster organization. Additionally, this paper introduces the potential sustainability-related implications of open innovation adoption in cluster organizations. An in-depth direct...
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Structure and properties comparison of poly(ether-urethane)s based on nonpetrochemical and petrochemical polyols obtained by solvent free two-step method
PublicationThe application of thermoplastic polyurethanes (TPU) is becoming more and more extensive, and the decreasing of used petrochemical monomers and reduction of energy for the polymerization and processing processes is getting increasingly important. In this paper, we confirmed the positive influence of high bio-based monomers contents (by replacing petrochemical polyol and glycol by bio-based counterparts) on processing and properties...
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Synergy between AgInS2 quantum dots and ZnO nanopyramids for photocatalytic hydrogen evolution and phenol degradation
PublicationDespite the unique properties of single semiconductor nanomaterials and quantum dots, poor photocatalytic activity has characterized them and the fabrication of nanocomposites has become necessary to enhance their photocatalytic performance. Thus, AgInS2 quantum dots (AIS QDs, 4.0±1.6 nm), have been successfully prepared and loaded onto ZnO nanopyramids (ZnO NPy). The effect of the nominal amount of AIS QDs decorating ZnO NPy on...
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Fault detection in electronic circuits using test buses
PublicationA survey of test buses designed for diagnostics of digital and analog electronic circuits is presented: the IEEE 1149.1 bus for digital circuits, the IEEE 1149.4 bus for mixed-signal and the IEEE 1149.6 bus for AC coupled complex digital circuits. Each bus is presented with its structure, solution of key elements, particularly boundary registers and a set of test instructions. Diagnosis with the use of the described buses is...
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Szymon Mania dr inż.
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A versatile and convenient preparation of unsymmetrical diaryl disulfides
PublicationWe have developed a convenient method for the synthesis of unsymmetrical diaryl disulfides under mild conditions in excellent yields. The described method is based on the straightforward preparation of 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinane-2-sulfenyl bromide from readily available 5,5-dimethyl-2-thiolo-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The unsymmetrical...
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Electrochemical sensor for measurement of volatile organic compounds = Elektrochemiczny czujnik do oznaczania lotnych związków organicznych
PublicationPrzedstawiono rezultaty badań prototypowego czujnika do oznaczania benzaldehydu i formaldehydu w powietrzu. Określono czułość wskazań czujnika i jego granice oznaczalności wykorzystując jako technikę detekcyjną woltamperometrię fali prostokątnej (SWV). Elektrodę roboczą i przeciwelektrodę stanowiły elektrody z Pt. Elektrolitem wewnętrznym były ciecze jonowe: chlorek 1-heksylo,3- metyloimidazolinowy i bis(trifluorometylosulfonylo)imidek...
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Characteristic of Morpholinium Ionic Liquids as Gas Chromatography Stationary Phases with McReynolds Constants and Activity Coefficients at Infinite Dilution
PublicationIn this work, four ionic liquids based on N-alkyl-N-methylmorpholinium cation ([Mor1,R] where R= 2, 4, 8, 10) and bis(trifluoromethanesulfonyl)imide anion [TFSI] were synthesized. Using gas-liquid chromatography a number of parameters describing the sorption properties of the investigated ionic liquids were determined. The values of Kovats indices, McReynolds constants, and activity coefficients at infinite dilution were the basis...
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Zanieczyszczenie obecne w próbkach śniegu pobranego z warstw jako źródło informacji o stanie środowiska w dużej aglomeracji miejskiej = Pollutants present in snow samples collected from various layers of snow cover as a source of information about the state of environment in a big urban agglomeration
PublicationPróbki śniegu pobierano przez okres około miesiąca z 12 miejsc zlokalizowanych na terenie Trójmiasta. Sześć z nich znajdowało się w pobliżu dróg komunikacyjnych o różnym natężeniu ruchu. Każde z nich miało swój punkt odniesienia oddalony od niego o około 200 m. W próbkach śniegu oznaczano pH, przewodność, zawartość wybranych anionów i kationów. Wartości pH wyznaczono przy użyciu elektrody szklanej połączonej z pH/tlenomierzem mikrokomputerowym,...
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Discrepancies in determination of biogenic amines in beer samples by reversed phase and hydrophilic interaction liquid chromatography coupled with tandem mass spectrometry
PublicationBiogenic amines (BAs) are nitrogenous organic bases occurring mainly in fermented food and beverages as a result of free amino acids bacterial decarboxylation. The reversed phase liquid chromatography (RPLC) and hydrophilic interaction liquid chromatography (HILIC) based methods were compared in terms of usefulness for determination of BAs in beer samples. Analysis of BAs with the use of RPLC method were carried out after their...
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Exposure to Bisphenol A Analogs and the Thyroid Function and Volume in Women of Reproductive Age—Cross-Sectional Study
PublicationBisphenols (BPs) are commonly known plastifiers that are widely used in industry. The knowledge about the impact of BPs on thyroid function is scarce. Proper thyroid functioning is especially important for women of reproductive age, as hypothyroidism affects fertility, pregnancy outcomes and the offspring. There are no studies analyzing the influence of BPs on thyroid function and volume in non-pregnant young women. The aim of...
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Zadłużenie jednostek samorządu terytorialnego i jego determinanty
PublicationW artykule zbadano przesłanki i skutki zadłużania się jednostek samorządu terytorialnego w Polsce, a także zidentyfikowano determinanty ich zadłużenia w podziale na prawno-finansowe, polityczne, ekonomiczno-społeczne i organizacyjno-zarządcze. Przedstawiono również poziom zadłużenia tych jednostek w latach 2003-2020. Najbardziej zadłużone są miasta na prawach powiatu i gminy, co jest przede wszystkim związane z realizowanymi przez...
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System wynagradzania nauczycieli w Polsce – skutki dla lokalnych budżetów
PublicationArtykuł podejmuje problematykę systemu wynagradzania nauczycieli w Polsce. W pierwszej części przedstawiono oświatę jako zadanie publiczne polskich gmin, powiatów i województw oraz miast na prawach powiatu, które wypełniają zadania zarówno gmin, jak i powiatów. W kolejnej części omówiono kryteria (zwłaszcza dotyczące nauczycieli) podziału części oświatowej subwencji ogólnej z budżetu państwa pomiędzy jednostki samorządu terytorialnego....
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Isolation and 3-dimensional Culture of Primary Murine Intestinal Epithelial Cells
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Induction of Epithelial-mesenchymal Transition in MDCK II Cells
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Global variation in anastomosis and end colostomy formation following left‐sided colorectal resection
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Global wealth disparities drive adherence to COVID-safe pathways in head and neck cancer surgery
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Przedsiębiorczość społeczna w społeczeństwie obywatelskim w Polsce
PublicationW artykule przedstawiono koncepcję i zakres zjawiska przedsiębiorczości społecznej w Polsce, w kontekście funkcjonowania społeczeństwa obywatelskiego. W tym celu autorka analizuje dominujące szkoły badań nad zjawiskiem przedsiębiorczości społecznej, identyfikuje i charakteryzuje podstawowe modele przedsiębiorstw społecznych w Polsce oraz wskazuje na wyzwania związane z badaniem tego typu organizacji. Autorka przedstawia i poddaje...
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Teleopieka domowa w systemie opieki nad osobami starszymi – doświadczenia gmin województwa pomorskiego
PublicationCelem opracowania jest przedstawienie istoty teleopieki domowej oraz dotychczasowych doświadczeń w zakresie jej wdrażania w gminach województwa pomorskiego. Autorka artykułu omówiła założenia idei gminnych powszechnych systemów teleopieki domowej oraz zidentyfikowała warunki konieczne do ich efektywnego funkcjonowania.
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The bile salt/phospholipid ratio determines the extent of in vitro intestinal lipolysis of triglycerides: Interfacial and emulsion studies
PublicationThis study focused on the protein-stabilised triglyceride (TG)/water interfaces and oil-in-water emulsions, and explored the influence of varying molar ratios of bile salts (BSs) and phospholipids (PLs) on the intestinal lipolysis of TGs. The presence of these two major groups of biosurfactants delivered with human bile to the physiological environment of intestinal digestion was replicated in our experiments by using mixtures...
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Analysis of investment stages along with a construction project management project for an investment task regarding the reconstruction and expansion of the locomotor system rehabilitation center Krzeszowice SPZOZ in Poland
PublicationAutorzy: Gwóźdź-Lasoń Monika, Tkocz Sebastian.
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Marcin Perzanowski dr inż.
PeopleHello, I work in the Department of Magnatic Materials and Nanostructures in the Institute of Nuclear Physics Polish Academy of Sciences in Kraków, Poland. My current research is focused on: (1) exchange bias in multilayers and nanostructures, (2) supermagnetic effects in low-dimensional materials, (3) perpendicular magnetic anisotropy in thin films and nanostructures. Collaborations, comments, and suggestions are welcomed! If...
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Proximity and Innovation in Clusters: How Close, How Far?
PublicationThe concept of proximity, whilst attractive cognitively, is still a poorly explored area in management sciences. The earliest publications on proximity were published at the end of the twentieth century and the development of this concept was strongly influenced by The French School of Proximity (Kirat & Lung, 1999; Rallet & Torre, 1999; Torre & Gilly, 2000; Carrincazeaux et al., 2001; Torre & Rallet, 2005). However, the most influential...
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Development of cooperation in localized cooperation networks: A comparative study of cluster organizations and technology parks
PublicationThe main aim of the paper is to analyze the level of development of cooperative relationships in localized cooperation networks – among enterprises associated in cluster organizations and park tenants. The author reports the findings from the quantitative study carried out in the selected cluster organizations and technology parks functioning in Poland. The basic method of data collection was a survey questionnaire. The research...
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Development of proximity in cluster organizations
PublicationSustainable development in cluster organizations (COs) is most fully manifested in the synergy effect. In turn, the synergy effect is achieved thanks to the development of proximity among cluster entities. The purpose of the paper is to test two conceptual models reflecting relations between selected dimensions of proximity in cluster organizations. The author reports the findings of a quantitative study conducted in four COs....
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Zarządzanie tożsamością w organizacjach na różnych poziomach zagregowania
PublicationNiniejszy artykuł stanowi naukową refleksję nad pojęciem tożsamości grupowej, odnoszonej do przedsiębiorstw oraz ich agregatów, określanych przez autorkę mianem „organizacji na wyższych poziomach zagregowania”. Głównym celem artykułu jest przegląd literatury z zakresu tożsamości przedsiębiorstwa, a na tej podstawie próba ustalenia czym jest taka tożsamość i co się na nią składa. Na wstępie autorka przedstawia definicje tożsamości...
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Główne bariery w systemie transferu technologii w Polsce
PublicationNiniejszy artykuł poświęcony jest omówieniu najważniejszych barier wy-stępujących w systemie transferu technologii i komercjalizacji wiedzy w Polsce. Na wstępie autorka, opierając się na analizie dostępnych danych źródłowych przytacza te wyniki badań, które obrazują główne obszary problemowe w każ-dym z ogniw tego systemu: przedsiębiorstwach, jednostkach B+R oraz instytu-cjach otoczenia biznesu. W dalszej części artykułu autorka...