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Search results for: NMR-RELAXATION
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Secure access control and information protection mechanisms in radio system for monitoring and acquisition of data from traffic enforcement cameras
PublicationThe study presents the architecture of the Radio System for Monitoring and Acquisition of Data from Traffic Enforcement Cameras (in short: RSMAD), particularly concerning access control and protection of confidential data. RSMAD security structure will be discussed in relation to network security issues. Additionally, the paper presents the results of the work associated with the modelling of potential threats to system security.
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<i>N,N</i>'-diphenylthiourea acetone monosolvate
PublicationIn the title compound, C13H12N2S·C3H6O, the phenyl rings of the thiourea molecule are in syn and anti positions in relation to the C=S bond. Two molecules are connected by N-HS=C hydrogen bonds into a centrosymmetric dimer. An additional N-HO=C hydrogen bond to the acetone solvent molecule and some weak C-H interactions reinforce the crystal structure.
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Image as a key factor of brand value at social media
PublicationThe paper aims to investigate the relationship between social media presence and activities and brand value for the most valuable Global Brands 2012 (Interbrandt 2013). Social media communication is an innovative way of communication. Brand value is a key performance indicator of brand strategy for managers. Brand and category image realized to be the key factor of investigated relation.
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Concept of Compatibility Region for the Evaluation of IR UWB Electromagnetic Compatibility
PublicationThis paper presents a new proposal for the unified evaluation of ultra wideband and narrowband radio communication systems electromagnetic compatibility, called “compatibility region”. The idea of compatibility region is based on the relation between the ratio of narrowband to ultra wideband signal power in a receiver and some transmission quality indicators (bit error rate, effective data rate).
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A distillery by-product as an external carbon source for enhancing denitrification in mainstream and sidestream treatment processes
PublicationThe use of fusel oil as an 'alternative' carbon source for denitrification in the mainstream and sidestream treatment processes was studied. Research comprised two kinds of batch experiments as well as acclimation of process biomass to external carbon sources. In the conventional nitrate utilization rate (NUR) measurements (one-phase experiments with non-acclimated biomass), the NUR with fusel oil was 1.4-1.7 g N/(kg VSS•h which...
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DNA methylation as a mediator of HLA-DRB1*15:01 and a protective variant in multiple sclerosis
PublicationThe human leukocyte antigen (HLA) haplotype DRB1*15:01 is the major risk factor for multiple sclerosis (MS). Here, we find that DRB1*15:01 is hypomethylated and predominantly expressed in monocytes among carriers of DRB1*15:01. A differentially methylated region (DMR) encompassing HLA-DRB1 exon 2 is particularly affected and displays methylation-sensitive regulatory properties in vitro. Causal inference and Mendelian randomization...
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The Taste of Waste: The Edge of Eggshell Over Calcium Carbonate in Acrylonitrile Butadiene Rubber
PublicationRubber technology experiences a new age by the use of biowaste or natural fillers. In this regard, taking properties of reinforcing agents from biowaste fillers remains as the challenging matter. Chicken eggshell (ES) biowaste has recently been introduced to substitute calcium carbonate (CaCO3) duo to its superior properties and low price. In this work, composites based on acrylonitrile butadiene rubber (NBR) reinforced with ES...
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Using Evidence-based Arguments to Support Dependability Assurance-Experiences and Challenges
PublicationThe article introduces to the problem of evidence-based arguments and their applications. Then, based on the experiences collected during commercial deployment of a concrete solution to this problem (system NOR-STA) we overview selected challenges and the ways of addressing them
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Janusz Kozak prof. dr hab. inż.
PeopleJanusz KOZAK Born 04.07.1953 Puck, Poland Intermediate school” Technikum Budowy Okrętów „Conradinum” Gdansk, 1973. Graduated on Faculty of Shipbuilding of Gdańsk University of Technology, Poland, 1978. Employed: From 1978 - Gdynia Shipyard 1978 as designer, from 1980 as a specialist in Chair of Technology in Faculty of Shipbuilding of Gdańsk University of Technology, 1993 as assistant, PhD (1993), “Method for assessment...
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Mariusz Jaczewski dr inż.
People -
Wojciech Litwin dr hab. inż.
People1992÷1996 - study on Mechanical Department at Gdansk University of Technology1996 – employed in the Faculty of Ocean Engineering and Ship Technology at the Gdansk University of Technology2004 – PhD2014 – habilitation2016 - vice dean for science at Faculty of Ocean Engineering2020 - dean of the Faculty of Ocean Engineering2021 - head of Institute of Naval Architecture He participated in a number of designing and research programs...
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Analyzing the Effectiveness of the Brain–Computer Interface for Task Discerning Based on Machine Learning
PublicationThe aim of the study is to compare electroencephalographic (EEG) signal feature extraction methods in the context of the effectiveness of the classification of brain activities. For classification, electroencephalographic signals were obtained using an EEG device from 17 subjects in three mental states (relaxation, excitation, and solving logical task). Blind source separation employing independent component analysis (ICA) was...
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Effects of V2O5 Additive on Structure and Dielectric Properties of BiNbO4 Ceramics
PublicationGoal of the present research was to investigate the influence of V2O5 additive on the structure and dielectric properties of BiNbO4 ceramics. To fabricate BiNbO4 ceramics with V2O5 added the solid state reaction route and pressureless sintering was utilized. Thus obtained ceramics was characterized in terms of its microstructure (SEM), chemical composition (EDS), phase composition and crystalline structure (X-ray phase and structural...
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Influence of Sn and Pb Ions Substitutions on Dielectric Properties of Barium Titanate
PublicationThe results of the microstructural and dielectric measurements of (Ba1-xPbx)(Ti1-xSnx)O3 (BPTSx) (x = 0, 0.05, 0.10, 0.30) polycrystalline samples are presented. The samples were obtained by means of a high temperature synthesis and their expected stoichiometry was confirmed by energy dispersive spectroscopy (EDS) measurements. The dielectric properties of BPTSx were studied with the use of broadband dielectric spectroscopy. The...
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Problems of analytical determination of journal bearing bush fatigue strength estimates
PublicationProblems connected with determination of stress distribution in sliding layer of thinwalled bearing bushes, investigated in bearing fatigue test rigs, have been presented. Using an example of plain bearings tested in the fatigue machine SMOK (built at the Gdask University of Technology) problems with obtaining a convergence of iterative procedure for determining the fatigue strength estimators of bearing alloy surface layer are...
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The Influence of Thin Gold Electrodes on the High-Temperature Impedance of Oxide Glasses
PublicationThe influence of thin gold electrodes on the electrical measurements of glasses at high temperatures was studied using impedance spectroscopy. The impedance was measured several times over a wide frequency range from 10 mHz to 1 MHz and the temperature ranged from 213 to 673 K under air and nitrogen atmospheres. The results showed a drop in the conductivity of more than an order of magnitude at a temperature around 603 K during...
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Analysis of the Capability of Deep Learning Algorithms for EEG-based Brain-Computer Interface Implementation
PublicationMachine learning models have received significant attention for their exceptional performance in classifying electroencephalography (EEG) data. They have proven to be highly effective in extracting intricate patterns and features from the raw signal data, thereby contributing to their success in EEG classification tasks. In this study, we explore the possibilities of utilizing contemporary machine learning algorithms in decoding...
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Share of gross value added by factors of production prices generated by the enterprise sector in Poland and in the EU countries in the GDP of individual countries
Open Research DataCompanies operating in the EU countries are characterized by a greater contribution to the creation of GDP than Polish enterprises. Discrepancies in shaping the described value also result from a different industry structure of companies. In other EU countries, more companies are involved in services, and in Poland, enterprises conducting commercial...
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Green strength (buildability performance) of concretes containing magnetite aggregate (M0-M100) mixes
Open Research DataRaw data for determination of buildability (green strength) properties of concrete mixes determined by squeezing test using QuantumX MX840B with CATMAN-EASY software, determined after 15, 30, 45 and 60 minutes. Values present force and two displacement measurements by LVDT.Additionally, an Origin (*.opju) file with processed data presenting stress-strain...
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The impact of QDgreen, QDgreen−β−CD−FA, β−CD, C−2028, β−CD(C−2028), QDgreen−C−2028, and QDgreen−β−CD(C−2028)−FA nanoconjugates on lysosomal content in the cancer (H460, Du-145, LNCaP) and normal (MRC-5, PNT1A) cells
Open Research DataThe impact of QDgreen, QDgreen−β−CD−FA, β−CD, C−2028, β−CD(C−2028), QDgreen−C−2028, and QDgreen−β−CD(C−2028)−FA nanoconjugates on lysosomal content in the cancer (H460, Du-145, LNCaP) and normal (MRC-5, PNT1A) cells was performed by Confocal Laser Scanning Microscopy (63× magnification; ZEISS LSM T-PMT, Magdeburg, Germany). To explore the influence...
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VUV irradiation studies of plasmid DNA in aqueous solution
PublicationInteractions of VUV light and DNA samples in aqueous solutions are reported. The damage induced by such radiation is quantified by monitoring both loss of supercoiled DNA and formation of single and double strand breaks using agarose gel electrophoresis. Irradiations were performed using synchrotron VUV photons of 130, 150, 170 and 190 nm. VUV irradiation experiments revealed enhanced damage upon irradiation with 170 nm photons...
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Using Evidence-based Arguments to Support Dependability Assurance - Experiences and Challenges
PublicationThe presentation introduces to the problem of evidence-based arguments and their applications. Then, based on the experiences collected during development and commercial deployment of a concrete solution to this problem (system NOR-STA) we overview selected challenges and the ways of addressing them.
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Recent Achievements in Constitutive Equations of Laminates and Functionally Graded Structures Formulated in the Resultant Nonlinear Shell Theory
PublicationThe development of constitutive equations formulated in the resultant nonlinear shell theory is presented. The specific features of the present shell theory are drilling rotation naturally included in the formulation and asymmetric measures of strains and stress resultants. The special attention in the chapter is given to recent achievements: progressive failure analysis of laminated shells and elastoplastic constitutive relation...
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Dimensionally Consistent Nonlinear Muskingum Equation
PublicationAlthough the Muskingum equation was proposed nearly 75 years ago, it is still a subject of active research. Despite of its simple form, the real properties of this equation have not been comprehensively explained. This paper proposes a new interpretation of the linear McCarthy’s relation. This relation can be interpreted only together with the storage equation, whereas the Muskingum equation can be derived directly from the system...
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In search of molecular precursors for cadmium sulfide-new complexes with a sulfur-rich kernel: cadmium(II) tri-tert-butoxysilanethiolates with additional diethyldithiocarbamato ligand
PublicationW ramach rozprawy opracowano metodę syntezy związków koordynacyjnych kadmu zawierających mieszane ligandy S-donorowe, które stanowią reszta tri-tert-butoksysilanotiolanowa oraz ditiokarbaminianowa. Zostały one poddane badaniom za pomocą analizy składu pierwiastkowego, metod spektroskopowych (FTIR, FIR, UV-Vis, NMR, MS) oraz termicznych. W celu osadzenia cienkich warstw wybranych związków posłużono się techniką nakładania obrotowego...
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The CON−H…+NH2 Blue-Shifting H-Bond Stabilizing Effect on Z Secondary Amides and Cyclic System Conformational Rearrangement through an Alkylamine-Chain Migration Pathway
PublicationThe paper is focusing on the amide linkage exceptional properties and usage of chemistry (conformational rearrangement, geometrical stereoisomers, spectroscopic blue shift phenomenon, protonation and deprotonation reactions, synthetic scope, and mechanistic implications). Hydrogen-bond-stabilized acylation reactions of a diamine with thioamides or nitriles reveal how substituents influence both the outcome of stereoselectivity...
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Syntheses, Structures and Reactivity of Terminal Phosphido Complexes of Iron(II) Supported by a β-Diketiminato Ligand
PublicationWe report the synthesis of the first series of terminal phosphido iron complexes supported by a β‐diketiminato ligand (Dippnacnac) and their catalytic activity in dehydrocoupling of secondary phosphines. Anionic and neutral mono‐ or diphosphido complexes were obtained from the reaction of [(Dippnacnac)FeCl2Li(dme)2] with the R2PLi (R = iPr, tBu, Cy, Ph) phosphides by tuning the stoichiometric ratio, polarity of the solvent, and...
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Inactivation of glucosamine-6-phosphate synthase by N3-oxoacyl derivatives of L-2,3-diaminopropanoic acid
PublicationN3-oksoacylowe pochodne kwasu l-2,3-diaminopropanowego zawierające ugrupowanie epoksydowe lub układ sprzężonych wiązań podwójnych inaktywują syntaze glukozamino-6-fosforanu (GlcN-6-P) z S. cerevisiae. Wyniki badań kinetycznych inaktywacji enzymu wskazują na dwuetapowy przebieg tej reakcji, przy czym tworzenie kompleksu enzym:ligand poprzedza nieodwracalną modyfikację enzymu. Badane związki różniły się powinowactwem do centrum aktywnego...
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First Copper(I) and Silver(I) Complexes Containing Phosphanylphosphido Ligands
PublicationThree new complexes with phosphanylphosphido ligands, [Cu4{μ2-P(SiMe3)-PtBu}4](1), [Ag4{μ2-P(SiMe3)-PtBu2}4](2) and [Cu{η1-P(SiMe3)-PiPr2}2]–[Li(Diglyme)2] (3) were synthesized and structurally characterized by X-ray diffraction, NMR spectroscopy, and elemental analysis. Complexes 1 and 2 were obtained in the reactionsof lithium derivative of diphosphane tBu2P-P(SiMe3)Li·2.7THF withCuCl and [iBu3PAgCl]4, respectively....
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Preparation and Characterization of Nanomaterial Consisting of Silica Aerogel & Carbon Tested as an Electrode in Non-Aqueous Media Containing Lithium Salt.
PublicationSilica aerogel (SiO2ag) was combined with carbonaceous material in the pyrolysis process of hydrocarbons. The obtained nanocomposite SiO2ag/C was amorphous, partially preserving the porous structure of SiO2ag. The specific surface area changes from 445.6 m2/g for pure SiO2ag to 205.52 m2/g SiO2ag/C. The 29Si MAS-NMR shows a three-dimensional matrix with silicon atoms connected to other silicon atoms by four...
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Solid-State Modification of Poly(butylene terephthalate) with a Bio-Based Fatty Acid Dimer Diol Furnishing Copolyesters with Unique Morphologies
PublicationCopolyesters based on poly(butylene terephthalate) (PBT) and a bio-based fatty acid dimer diol (FADD) were prepared by solid-state modification (SSM). The chemical incorporation of the FADD into the backbone of the PBT was proven using various techniques. It was clear that the incorporation rate was diffusion-limited rather than reaction-limited. From quantitative 13C NMR a nonrandom chemical microstructure was obtained at all...
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Profiling of polar ionogenic metabolites in Polish wines by capillary electrophoresis-mass spectrometry
PublicationThe composition of wine is determined by a complex interaction between environmental factors, genetic factors (i.e., grape varieties), and winemaking practices (including technology and storage). Metabolomics using NMR spec-troscopy, GC-MS, and/or LC-MS has shown to be a useful approach for assessing the origin, authenticity, and quality of various wines. Nonetheless, the use of additional analytical techniques with complementary...
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Preparation of Allyl Alcohol Oligomers Using Dipicolinate Oxovanadium(IV) Coordination Compound
PublicationCurrently, new precatalysts for olefin oligomerization are being sought in the group of vanadium(IV) complexes. Thus, the aim of our research was to examine the catalytic activity of the oxovanadium(IV) dipicolinate complex [VO(dipic)(H2O)2] 2 H2O (dipic = pyridine-2,6-dicarboxylate anion) in 2-propen-1-ol oligomerization as well as to characterize oligomerization products using matrix-assisted laser desorption/ionization–time-of-flight...
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Kompleksy fosfanylofosfidowe z grupami indenylowymi
PublicationPochodne litowe difosfanów są z powodzeniem stosowane jako prekursory ligandów fosfanylofosfinidenowego R2PP oraz fosfanylofosfidowego R2PP(SiMe3) w reakcjach z dichlorometalocenami. Rodzaj powstałych produktów w tego typu reakcjach, w dużej mierze zależy od podstawników w pierścieniu cyklopentadienylowym w cząsteczce metalocenu oraz od właściwości atomu metalu. Zastosowanie dichlorocyrkonocenów z grupami indenylowymi (Ind=C9H7)...
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Projekt formy przestrzennej - Nowy
e-Learning CoursesTematem zajęć projektowych jest przekształcanie. Najpierw kwadratu w płaską graficzną kompozycję. Kolejnym etapem jest kompozycja z zastosowaniem koloru. Efektem finalnym procesu przekształceń jest obiekt przestrzenny, z założenia pozbawiony funkcji utylitarnych. Treści przedmiotu: 1. Grafika. Kompozycja achromatyczna w kontraście bieli i czerni z użyciem form organicznych, geometrycznych lub mieszanych. Realizacja graficzna...
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Comparison of non-linear statical analysis of truss with linear and rotational side supports and 3d roof model
PublicationIn the paper geometrically non-linear analysis of example truss with linear and rotational elastic side supports is compared with geometrically non-linear analysis of part of the roof construction with purlins and truss-bracing. For different stiffness of side-supports a non linear relation between normal force in compressed chord due to out of truss plane displacement has been calculated.
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MULTIEQUATION MODELS AS DIAGNOSTIC TOOLS FOR MEASURING THE OPERATIONAL FLUIDITY OF THE CONTAINER HANDLING TERMINAL
PublicationThe article presents the continuation of the authors’ research on the problem of the operational fluidity of cargo handling sea terminals, based on the example of the DCT. The article presents a solution based on the multiequation models and applied to analyze the operational fluidity of terminals in the transshipment and feeder relation. To provide a solution to the problem of the functioning of sea-land supply chains at the terminal,...
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Enhancing Performance of Switched Parasitic Antenna for Localization in Wireless Sensor Networks
PublicationThis paper presents an Electronically Steerable Parasitic Array Radiator (ESPAR) antenna with enhanced performance of estimating the incoming signal direction. Designed antenna is dedicated for 2.4 GHz ISM applications with emphasis on Wireless Sensor Networks (WSN). The limitations of the existing design approach are illustrated, as well as perspectives and challenges of the proposed solution in relation to the localization in...
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Development of Technical Creativity Featuring Modified TRIZ-AM Inventive Principle to Support Design for Additive Manufacturing
Publicationhe design for additive manufacturing (DFAM) processing was introduced to fully utilise the design freedom provided by additive manufacturing (AM). Consequently, appropriate design methodologies have become essential for this technology. Recently, many studies have identified the importance of DFAM method utilisation to produce AM parts, and TRIZ is a strategy used to formalise design methodologies....
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Global Optimization for Recovery of Clipped Signals Corrupted With Poisson-Gaussian Noise
PublicationWe study a variational formulation for reconstructing nonlinearly distorted signals corrupted with a Poisson-Gaussian noise. In this situation, the data fidelity term consists of a sum of a weighted least squares term and a logarithmic one. Both of them are precomposed by a nonlinearity, modelling a clipping effect, which is assumed to be rational. A regularization term, being a piecewise rational approximation of the ℓ0 function...
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Maillard-reaction (glycation) of biopolymeric packaging films; principles, mechanisms, food applications
PublicationBackground The biodegradable, biocompatible, sustainable, and renewable nature of biomaterials has led to increased interest in developing biopolymeric food packaging films (BFPFs) with green ingredients and strategies. To enhance the performance of these films, biopolymer molecules can be modified or combined with additives like nanomaterials, cross-linkers, bioactive compounds, and other polymers, particularly with Maillard-reaction...
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UAV spectrometer reflectance and leaf area index for vegetation near Gdynia, Poland
Open Research DataReflectance data from the UAV flights with UV-VIS spectrometer along with leaf area index measurements for vegetaion near Gdynia, Poland.
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Hydrogen migration observed in fragmentation of the pyridine molecules in collisions with the H+, H2+, He+and He++cations
PublicationThe hydrogen atom migration preceding fragmentation of the pyridine molecules by the H+, H2+, He+ and He++ collisions has been investigated in the 5-2000 eV energy range. The pyridine molecule structure is lacking of the NH group, thus formation of the NH radicals is an evidence of the H atom relocation prior to the cation-induced fragmentation. The NH(A3Π) fragmentation yields measured by detecting its A3Π→X3Σ− fluorescence show...
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Akademia ETI dla Technikum nr 3 - Informatyka
e-Learning CoursesZajęcia prowadzone przez nauczycieli akademickich WETI dla Technikum nr 3 w Malborku - Informatyka
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Rola koloidalnych i zawiesinowych związków organicznych w technologii oczyszczania ścieków metodą osadu czunnego z biologicznym usuwaniem związków biogennych
PublicationRolę koloidalnych i zawiesinowych związków organicznych w technologii oczyszczania ścieków metodą osadu czynnego określono na podstawie badań kinetyki wybranych procesów biochemicznych tj. szybkość procesu denitryfikacji (z ang. NUR), poboru tlenu (z ang. OUR), uwalniania fosforanów (z ang. PRR) i poboru fosforanów w warunkach anoksycznych i tlenowych (z ang. PURANOX/PURAERO). Doświadczenia przeprowadzono z użyciem dwóch równoległych...
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Analiza dopuszczalnych parametrów rozruchu silników hydraulicznych w warunkach szoku termicznego.
PublicationPrzedstawiono badania eksperymentalne silników hydraulicznych (satelitowego SOK 100 firmy HYDROSTER i orbitalnego GMR 160 firmy REXROTH) w warunkach szoku termicznego. Pokazano wyniki symulacji komputerowej nagrzewania silnika satelitowego SOK 1600.
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Application of vibrational spectroscopy, thermal analyses and X-Ray diffraction in the rapid evaluation of the stability in solid-state of ranitidine, famotidine and cimetidine
PublicationThis paper reports the study on applicability of Fourier transform infrared (FTIR), near-infrared (NIR) and Raman spectroscopy, differential scanning calorimetry (DSC) and X-ray diffraction (XRD) for the estimation of the chemical stability and photostability of histamine H2-receptor antagonist substances. Ranitidine hydrochloride (RAN), famotidine (FAM) and cimetidine (CIM) were tested and differences in sensitivity were measured...
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Determination of API content in a pilot-scale blending by near-infrared spectroscopy as a first step method to process line implementation
PublicationNear infrared (NIR) spectroscopy was used for estimation of powder blend homogeneity and manufacturing control of a medicinal product powder mixture containing active pharmaceutical ingredient (API). Aiming at initiating a Process Analytical Technology (PAT) activity, the first step was a stationary mode atline evaluation. In this, the content of pharmaceutical active compound in the powder mixtures intended to the direct tabletting...
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Protein thermal stabilization in aqueous solutions of osmolytes
PublicationProteins’ thermal stabilization is a significant problem in various biomedical, biotechnological, and technological applications. We investigated thermal stability of hen egg white lysozyme in aqueous solutions of the following stabilizing osmolytes: Glycine (GLY), N-methylglycine (NMG), N,N-dimethylglycine (DMG), N,N,N-trimethylglycine (TMG), and trimethyl-N-oxide (TMAO). Results of CD-UV spectroscopic investigation were compared...
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Compensation of magnetic disturbances caused by sensors in a differential magnetometric system
PublicationStudy of low magnetic fields necessitates the use of precision magnetometers working in a differential system. Minimization of this error is a substantial issue in the case of magnetometers working in a differential system on a mobile platform. The compensation method of heading error consists in taking measurements of changes in magnetic induction with the use of the tested magnetometer for various locations of the sensor in relation...