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Search results for: ALUMINUM HYPOPHOSPHITE
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Influence of dispersed phase content on the mechanical properties of electroless nanocomposite Ni-P/Si3N4 and hybrid Ni-P/Si3N4/graphite layers deposited on the AW-7075 alloy.
PublicationThe article presents the results of mechanical testing of Ni-P/Si3N4 nanocomposite and hybrid Ni-P/Si3N4/graphite coatings deposited on AW-7075 aluminum alloy using the chemical reduction method. In terms of mechanical testing, microhardness was measured, and surface roughness and adhesion of the coatings to the aluminum substrate were determined using the “scratch test” method. The surface morphology of the deposited layers was...
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Ekspertyza dotycząca przyczyn powstawania korozji ram aluminiowych okien uchylnych
PublicationDokonano analizy spektroskopowej i mikroskopowej produktów korozji na dostarczonym stopie aluminium, oceniono podatność materiału na korozję w aplikowanym środku myjącym oraz oznaczono wytrzymałość powłoki organicznej na stopie aluminium
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Randomly Functionalized Polyethylenes: In Quest of Avoiding Catalyst Deactivation
PublicationWell-defined randomly functionalized polyolefins produced by catalysis form an interesting class of polymers with great potential for various applications. One of the major challenges for the production of these materials forms the incompatibility of the commonly used electrophilic group 4 metal based catalysts and the desired nucleophilic, especially protic functionalities like hydroxyl and carboxylic acid groups. Although pacification...
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Role of reciprocating sliding testing in tribological materials engineering
PublicationPrzedstawiono wyniki badań oporu ruchu i zużycia skojarzeń o styku rozłożonym przy posuwisto-zwrotnym ślizganiu. Badano skojarzenia: żeliwo-stop aluminium przetapiany laserowo w warunkach kriogenicznych oraz żeliwo-kompozyt aluminium-żelazo otrzymany ''in situ''.
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A multi-analytical approach to the characterization of natural organic dyestuffs and inorganic substrates present in the 19th-century artistic oil paints manufactured by a French art materials supplier Richard Aines
PublicationThis paper presents a comprehensive analysis of artistic paints produced in the 19th century by a French art materials supplier Richard Ain`es. Improved mild extraction with hydrofluoric acid enabled the observation of intact organic dyes. Reversed-phase liquid chromatography with diode-array and mass spectrometry detection was utilised for the identification of 35 dyes present in yellow and red paint samples, and in selected plant...
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Emisja akustyczna podczas korozji stopów na bazie metali lekkich
PublicationPrzedstawiono wyniki badań elektrochemicznych metodą polaryzacji cyklicznej oraz emisji akustycznej technicznie czystego aluminium(stop1050) oraz magnezu. W przypadku aluminium aktywność akustyczna jest związana z inicjacją i wzrostem wżerów. Aktywność akustyczna magnezu występuje w obszarze inicjacji i wzrostu wżerów oraz w czasie repasywacji wżerów.
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Chemical investigation of the Al2O3 ultra-thin films
Open Research DataUltra-thin layers of oluminum oxide (Al2O3) were deposited by ALD method. Atomic layer deposition provides precise thickness control down to a single atomic layer. The precursors used were trimethylaluminum (Sigma-Aldrich) and purified water. The deposition of the atomic layer was carried out at 200 °C. Samples with a thickness of 2 and 8 nm of alumina...
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Structure redetermination, transport and thermal properties of the YNi3Al9 compound
PublicationSingle crystals of completely ordered variant of the YNi3Al9 compound were grown by self-flux method with excess of aluminum. The crystal structure of the title compound was redetermined from single crystal X-ray diffraction data. The structure adopts ErNi3Al9 type, space group R32, parameters of the unit cell a = 7.2838(2) Å, c = 27.4004(8) Å. The growth of relatively large single crystals of the YNi3Al9 compound, having completely...
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Chemical analysis of low carbon content coals and their applications as dye adsorbent
PublicationCoal is primarily a fuel material but lately it has been utilized as an adsorbent for removing toxic metal ions. However, its usage for removing organic pollutants is not well studied. We report here a systematic study on the use of coal samples of varying carbon contents as adsorbents for removing Basic Blue 41 as a model cationic dye. The coal samples were collected from coal mines and were thoroughly characterized. The concentrations...
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Algorithm for Automatic Wear Estimation of Railway Contact Strips Based on 3D Scanning Results
PublicationElectric rail vehicles use current collection system which consists of overhead contact line and a current collector (pantograph) mounted on the roof of a vehicle. A pantograph is equipped with contact strips, which slide along the contact wire, ensuring steady electric contact. Contact strips are made of carbon layer, fixed to an aluminum carrier. The carbon layer wears down due to friction. Using overly worn contact strips increases...
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An investigation of microstructural basis for corrosion behavior of Al-CNT composites fabricated by SPS
PublicationIn this research effect of the addition of multi-wall carbon nanotubes (MWCNTs) as additive powder on microstructure and corrosion behavior of fabricated Al-CNT composites was studied. The aluminum powder and CNTs were mixed with high energy planetary ball-mill. It is observed that by increasing milling time, the uniformity of CNTs on aluminum matrix and consequently corrosion resistance of Al-CNT composite is increased. On the...
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FTIR spectra of gas mixtures from the process of biogas dry reforming using alumina catalyst - blank
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of blank sample Al2O3 for dry reforming of biogas (60/40 CH4-CO2). The specatra were collected every 1 minute.
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Strontium-based nanosized phosphates as anticorrosive fi llers of epoxy and polyurethane coating compositions
PublicationAnticorrosive epoxy and polyurethane coatings were compounded using zinc-free nanosized phosphates of strontium (SP) or strontium and aluminum (SAP). For comparison, a nanosized calcium aluminum ammonium phosphate (CAP) and a microsized zinc phosphate (ZP) were tested. Results of salts spray and cyclic corrosion tests revealed better anticorrosive properties of the SAP-based coatings...
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Mechanism of hopping conduction in Be–Fe–Al–Te–O semiconducting glasses and glass–ceramics
PublicationElectrical properties of beryllium-alumino-tellurite glasses and glass–ceramics doped with iron ions were studied using impedance spectroscopy. The conductivity was measured over a wide frequency range from 10 mHz to 1 MHz and the temperature range from 213 to 473 K. The D.C. conductivity values showed a correlation with the Fe-ion concentration and ratio of iron ions on different valence states in the samples. On the basis of...
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The microstructure of AA5754 alloy under corrosion in alkaline media (pH=11) with 4.5 mM of various carboxylic acids
Open Research DataThis dataset contains scanning electron microscopy (SEM) micrographs taken for polished aluminum AA5754 alloy samples, exposed for 100 min in bicarbonate buffer (pH=11) with the addition of 4.5 mM of carboxylic acids, namely: citric acid, malic acid, maleic acid, succinic acid, tartaric acid, tricarballylic acid and serine. The goal of this study was...
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The microstructure of AA5754 alloy under corrosion in alkaline media (pH=11) with 20 mM of various carboxylic acids
Open Research DataThis dataset contains scanning electron microscopy (SEM) micrographs taken for polished aluminum AA5754 alloy samples, exposed for 100 min in bicarbonate buffer (pH=11) with the addition of 20 mM of carboxylic acids, namely: citric acid, malic acid, maleic acid, succinic acid, tartaric acid, tricarballylic acid and serine. The goal of this study was...
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TGA data of MXenes catalysts
Open Research DataData contain results from TGA measurement of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios. ...
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Adsorption and desorption of N2 measurement of MXenes catalysts
Open Research DataData contain results from adsorption and desorption of N2 measurement of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y...
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Mechanizm nanokrystalizacji warstwy wierzchniej stopu Al-Si nadtapianego laserem w niskiej temperaturze.
PublicationPrzedstawiono mechanizm nanokrystalizacji stopu aluminium nadtapianego laserowo po schłodzeniu do niskiej temperatury w powiązaniu z obserwacjami struktury warstwy wierzchniej.
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The effectiveness of polymer adhesive in reduction of vibrations of structural members
PublicationIn this paper, the idea of using polymer adhesive as a damping layer is proposed. An experimental study of two aluminium cantilevered beams has been conducted. One of them presents a plain cantilevered beam, while the second one considers two aluminium beams bonded with a polymer adhesive of different thickness (0,5; 1,2; 1,75; 3,1 and 5 mm). The polymer adhesive considered in the study is a specially designed flexible...
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XRD patterns of MXenes catalysts
Open Research DataData contain results from XRD measurements of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios....
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Raman spectra of MXenes catalysts
Open Research DataData contain results from Raman spectroscopy of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios. ...
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SEM images of MXene catalysts
Open Research DataData contain results SEM measurements of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios. MAX...
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Manufacturing of resistant joints by rolling for light tubular structures
PublicationKoncepcja łączenia aluminiowych elementów rurowych z zastosowaniem nagniatania plastycznego jest alternatywą do istniejących metod łączenia przez spawanie i skręcanie. W artykule prezentowane są oryginalne wyniki badań wpływu parametrów nagniatania wewnętrznego i zewnętrznego oraz różnych postaci powierzchni łączonych na wytrzymałość złącza (aluminium-aluminium) pod wpływem rozciągających sił osiowych.Badania przeprowadzono na...
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Damage localisation in a stiffened plate structure using a propagating wave
PublicationThe paper presents an application of changes in propagating waves for damage detection in a stiffened aluminium plate. The experimental investigation was conducted on an aluminium plate with riveted two L-shape stiffeners. The wave has been excited with a piezoelectric transducer and measured with the Laser Scanning Doppler Vibrometer. Recorded signals were analysed using the special signal processing techniques developed for damage...
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Investigation of behaviour of metal structures with polymer dampers under dynamic loads
PublicationA large number of accidents concerning structures subjected to dynamic loads have been recently observed. One of the examples of such a structure is a temporary steel grandstand erected using scaffolding system. Dynamic load that is generated by crowd movement has a significant influence on the behaviour of the structure and may lead to excessive structural vibrations. The aim of the study is to consider the idea of using polymer...
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Production of new non-matrix reference material of ethene
PublicationThe main objective of the research is to produce new non-matrix reference materials of ethene. The study are based on thermal decomposition of surface compound chemically bonded with the surface of glass fibers coated with thin layer of aluminum. Positivehomogeneity test, stability test and organization of inter-laboratory comparison are leading to find new non-matrix reference materials which are indispensable tools in the analysis...
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Kazimierz Darowicki prof. dr hab. inż.
PeopleStudia wyższe ukończyłem w czerwcu 1981 roku po zdaniu egzaminu dyplomowego i obronie pracy magisterskiej. Opiekunem pracy magisterskiej był dr hab. inż. Tadeusz Szauer. W roku 1991, 27 listopada uzyskałem stopień naukowy broniąc pracę doktorską zatytułowaną „Symulacyjna i korelacyjna analiza widm immitancyjnych inhibitowanej reakcji elektrodowej”. Promotorem pracy był prof. dr hab. inż. Józef Kubicki (Wydział Chemiczny...
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Sol-gel Al2O3 antireflection coatings for silicon solar cells
PublicationPurpose: This paper presents the results of investigations on morphology and opticalproperties of the prepared aluminium oxide thin filmsDesign/methodology/approach: Thin films were prepared with use of sol-gel spincoating method. The changes of surface morphology were observed in topographic picturesperformed with the atomic force microscope AFM. Obtained roughness coefficients valueswere generated...
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Singlet exciton interactions in solid films of Alq3.
PublicationW pracy tej na podstawie pomiarów zależności wydajności fluorescencji od natężenia światła wzbudzjącego, wyznaczono stałą oddziaływania ekscyton singletowy - ekscyton singletowy w warstwie organicznego kompleksu aluminium Alq3.
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Badanie przyczyn korozji skraplaczy aluminiowych.
PublicationPrzeprowadzono badania aluminiowych skraplaczy pracujących w układach chłodzenia tramwajów. Stwierdzono, że problemy z korozją są wynikiem stosowania środków myjących o właściwościach korozyjnych w stosunku do zastosowanego aluminium.
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Unprecedented Adhesive Performance of Propylene-Based Hydroxyl Functionalized Terpolymers
PublicationThe synthesis of hydroxyl functionalized propylene-based terpolymers and their performance as hot melt adhesives were investigated. The products comprise uniformly distributed butyl and 4-hydroxyl-butyl branches along the polypropylene backbone. Despite the low hydroxyl-functionality level of ≤ 0.5 mol%, hydroxyl functionalized terpolymers show formidable adhesion to aluminum and steel providing an adhesive strength exceeding 16...
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Influence of annealing on joint zone of explosive welded and rolled Al-Cuplate
PublicationRosnące wciąż wymagania co do metalowych materiałów jednorodnych przyczyniło się do zwiększenia zainteresowania materiałami platerowanymi. Blachy platerowane często znajdują zastosowanie w przemyśle chemicznym i petrochemicznym jako materiały antykorozyjne odporne na działanie agresywnego środowiska, w przemyśle okrętowym jako łączniki stopów aluminium ze stalą, w budowie zgrzewarek jako połączenia szczęk z blachą stalową, w przemyśle...
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AN OVERVIEW OF HEAT TRANSFER ENHANCEMENT BASED UPON NANOPARTICLES INFLUENCED BY INDUCED MAGNETIC FIELD WITH SLIP CONDITION VIA FINITE ELEMENT STRATEGY
PublicationThe mathematical model of heat generation and dissipation during thermal energy transmission employing nanoparticles in a Newtonian medium is investigated. Dimensionless boundary layer equations with correlations for titanium dioxide, copper oxide, and aluminium oxide are solved by the finite element method. Parameters are varied to analyze their impact on the flow fields. Various numerical experiments are performed consecutively...
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Effect of temperature change on refractive index of an egg white and yolk: a preliminary study
PublicationIn this article, the refractive index of an egg white and yolk depending on temperature in range 30 - 47 °C over 1550 nm was determined. The measurement head was constructed as fiber optic Fabry-Perot interferometer with interference between polished fiber end-face and aluminum weighing dish. The measurement setup has been made of an optical spectrum analyzer, a superluminescent diode with a central wevelength of 1550 nm, 2:1 fiber...
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Maciej Jerzy Głowacki
PeopleMaciej Jerzy Głowacki is an alumnus of the Gdańsk University of Technology. He graduated with honors from the Faculty of Mechanical Engineering (B.Eng., 2017) and the Faculty of Electronics, Telecommunications and Informatics (M.S., 2018). Since 2014 he has been continuously actively involved in a research carried out at the Department of Metrology and Optoelectronics. His scientific activities include a deposition of antibacterial...
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Methods of material parameters identification for isotropic damage in viscoplastic flow conditions
PublicationW pracy zaprezentowano trzy metody identyfikacji parametrów materiałowych dla izotropowego zniszczenia w warunkach lepkoplastycznego płynięcia. Przedstawiono wyniki identyfikacji dla dwóch stopów aluminium, które następnie zweryfikowano porównując wyniki symulacji numerycznych z wynikami eksperymentalnymi.
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Electroconducting polymers as a corrosion protection materials review
PublicationAutorzy przywołują 89 pozycji literaturowych dotyczących użycia polimerów elektroaktywnych w ochronie metali przed korozją. Wykazano, że najczęściej wykorzystywany w tym celu jest polipirol. Przytoczone prace dotyczą ochrony stali, aluminium, cynku oraz stopów magnezu.
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Laser assisted forming of the surface layer of Al-Si alloy at cryogenic conditions.
PublicationW artykule przedstawiono wpływ powierzchniowego laserowego przetapiania w warunkach kriogenicznych na mikrostrukturę, mikrotwardość i własności korozyjne stopu AlSi13Mg1CuNi. Stwierdzono korzystny wpływ obróbki laserowej na mikrostrukturę, mikrotwardość i odporność na zużycie ścierne badanego stopu aluminium.
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Wear in reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K01
Open Research DataFriction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1 Tribometer.Running time: progressive increments of 10, 15, 30, 60, 180 and 300s. (stored in separate folders).Specimen...
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Wear in reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K04
Open Research DataFriction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1 Tribometer.Running time: progressive increments of 10, 15, 30, 60, 180 and 300s. (stored in separate folders).Specimen...
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Wear in reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K05
Open Research DataFriction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1 Tribometer.Running time: progressive increments of 10, 15, 30, 60, 180 and 300s. (stored in separate folders).Specimen...
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Wear in reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K03
Open Research DataFriction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1 Tribometer.Running time: progressive increments of 10, 15, 30, 60, 180 and 300s. (stored in separate folders).Specimen...
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Experimental Study on the Effectiveness of Polyurethane Flexible Adhesive in Reduction of Structural Vibrations
PublicationThe aim of the present study is to consider the idea of using polyurethane flexible adhesive in to reduce the vibrations in structures exposed to dynamic loads and evaluate their damping properties in relation to large deformations. Firstly, two aluminium cantilever beams, simulating structural elements (without and with polyurethane layer in the form of tape), were analysed, in order to check the damping of the unconstrained polymer...
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Protective properties of Al2O3 + TiO2 coating produced by the electrostatic spray deposition method
PublicationMechanical resistance of Al2O3 + TiO2 nanocomposite ceramic coating deposited by electrostatic spray deposition method onto X10CrAlSi18 steel to thermal and slurry tests was investigated. The coating was produced from colloidal suspension of TiO2 nanoparticles dispersed in 3 wt% solution of Al2(NO3)3, as Al2O3 precursor, in ethanol. TiO2 nanoparticles of two sizes, 15 nm and 32 nm, were used in the experiments. After deposition,...
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Corrosion resistance evaluation of Al-based alloys by means of dynamic electrochemical impedance spectroscopy
PublicationW pracy przedstawiono wyniki badań stopów aluminium wykonane za pomocą dynamicznej elektrochemicznej spektroskopii. Na podstawie uzyskanych widm impedancyjnych zostały pokazane zmiany parametrów elektrycznego schematu zastępczego z potencjałem. Stwierdzono, że dodatek magnezu do badanego stopu obniża właściwości przeciwkorozyjne stopu.
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Możliwości łączenia elementów rurowych z wykorzystaniem technologii nagniatania otworów
PublicationW opracowaniu przedstawiono możliwość użycia głowic nagniatających do otworów w wytwarzaniu złączy rurowych z aluminium AA6060. Zamieszczono wyniki badań laboratoryjnych wpływu konstrukcyjnych i technologicznych parametrów złącza, jak długość i szerokość pierścieni oraz naddatek nagniatania, na wartość osiowej siły rozłączającej.
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VIbration monitoring in reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K05
Open Research DataVIbration monitoring in reciprocating siding friction tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1 Tribometer.Running time: progressive increments of 10, 15, 30, 60, 180...
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Wear in reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - DISTILLED WATER. Specim. set K06
Open Research DataFriction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DISTILLED WATER. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1 Tribometer.Running time: progressive increments of 10, 15, 30, 60, 180 and 300s. (stored in separate...
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Wear in reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - PARAFFIN OIL. Specim. set K08
Open Research DataFriction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: PARAFFIN OIL. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1 Tribometer.Running time: progressive increments of 10, 15, 30, 60, 180 and 300s. (stored in separate...