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Wyniki wyszukiwania dla: PROPERTIES OF PHYSICO-CHEMICAL
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Chemical recycling of plastic waste as a mean to implement the circular economy model in the European Union
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Decision Support System to Improve the Effectiveness of Chemical Control Against Cutworms in Sugar Beet
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Effect of glycols used as glycolysis agents on chemical structure and thermal stability of produced glycolysates
PublikacjaZaprezentowano warunki glikolizy poliuretanowych odpadów piankowych, przy użyciu różnych glikoli oraz wyniki badań budowy chemicznej glikolizatów oraz ich właściwości termicznych.
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Offal Chemical Composition from Veal, Beef, and Lamb Maintained in Organic Production Systems
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Estimation of the environmental risk posed by landfills using chemical, microbiological and ecotoxicological testing of leachates
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Effect of chemical composition on corrosion and wear behaviour of the composite Ni-Fe-Al2O3 coatings.
PublikacjaPrzedstawiono wyniki badań powłoki kompozytowej otrzymanej przez osadzanie katodowe galwaniczne w roztworze zawierającym sole niklu, żelaza oraz cząstki ceramiki Al2O3 o różnej wielkości i stężeniu. Wykazano, że charakterystyka ceramiki posiada wpływ na szybkość korozji i zużycia ściernego. W szczególności, zawartość ceramiki wpływa dodatnio na odporność na zużycie ścierne, ale nieco obniża odporność na zużycie korozyjne.
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On the Formation of Single-Walled Carbon Nanotubes in Pulsed-Laser-Assisted Chemical Vapor Deposition
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Quality Assurance and Quality Control in the Analytical Chemical Laboratory. A practical approach : Second edition
PublikacjaThe second edition defines the tools used in QA/QC, especially the application of statistical tools during analytical data treatment. Clearly written and logically organized, it takes a generic approach applicable to any field of analysis. The authors begin with the theory behind quality control systems, then detail validation parameter measurements, the use of statistical tests, counting the margin of error, uncertainty estimation,...
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Storm petrels as indicators of pelagic seabird exposure to chemical elements in the Antarctic marine ecosystem
PublikacjaData on trace element bioavailability in the south-polar marine ecosystem is still scarce, compared to that relating to temperate zones. Seabirds can be used as indicators of ecosystem health and sentinels of environmental pollution, constituting a link between marine and terrestrial environments. Here, we analysed the concentration of 17 elements (with special emphasis on mercury, Hg) in feathers of adults and chicks of two pelagic...
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Effect of chemical structure on complexation efficiency of aromatic drugs with cyclodextrins: The example of dibenzazepine derivatives
PublikacjaIt is widely believed that the hydrophobic effect governs the binding of guest molecules to cyclodextrins (CDs). However, it is also known that high hydrophobicity of guest molecules does not always translate to the formation of stable inclusion complexes with CDs. Indeed, a plethora of other factors can play a role in the efficiency of guest–CD interactions, rendering structure-based prediction of the complexation efficiency with...
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Quality of groundwater contaminated by leachates from seven Polish landfills - chemical and ecotoxicological classifications
PublikacjaArtykuł prezentuje rezultaty badań toksyczności ostrej i chronicznej próbek wód podziemnych pobranych spod składowisk odpadów komunalnych. Uzyskane wyniki porównano z wynikami badań parametrów fizykochemicznych. Jednocześnie dokonano klasyfikacji jakości badanych próbek w oparciu o zalecenia Komisji Helsińskiej, system oparty na wyznaczaniu parametru pT i kryteria ustanowione przez Persoone'a i współpracowników.
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The influence of polypropylene-block/graft-polycaprolactone copolymers on melt rheology, morphology, and dielectric properties of polypropylene/polycarbonate blends
PublikacjaThe paper discusses the relationship between rheology and morphology of immiscible polypropylene (matrix))/polycarbonate (dispersed phase) blends compatibilized with novel polypropylene-polycaprolactone block and graft copolymers. Transmission electron microscopy (TEM) experiments revealed uniform droplet morphologies and a reduction of the average size of the dispersed phase upon addition of the compatibilizer. The results suggested...
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Influence of friction stir welding technological parameters on the properties of the joints of selected aluminum alloys
PublikacjaThe purpose of this dissertation was to determine the effect of friction stir welding technological parameters on the properties of selected aluminum alloy joints, with consideration of the residual stresses and dislocation density in the joints. The goal of the present work was also to produce defect-free joints with high mechanical and electrochemical properties. In the dissertation, similar welds of AA6082 alloy and dissimilar...
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Asymptotic properties of quadratic stochastic operators acting on the L1 space
PublikacjaQuadratic stochastic operators can exhibit a wide variety of asymptotic behaviours and these have been introduced and studied recently in the ℓ1 space. It turns out that in principle most of the results can be carried over to the L1 space. However, due to topological properties of this space one has to restrict in some situations to kernel quadratic stochastic operators. In this article we study the uniform and strong asymptotic...
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Influence of silver nanoparticles addition on antibacterial properties of PEO coatings formed on magnesium
PublikacjaMagnesium is a biodegradable material and thus could be a choice for bone fixation devices and implants with a specific purpose. This study aims to enhance the anti-corrosive, biocompatible, and antibacterial properties on magnesium-based materials through ceramic coatings formation. To achieve this the silicate-based electrolyte was used to create of Plasma Electrolytic Oxidation (PEO) coatings. During investigation the bioactive...
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Influence of the internal electrolyte composition on amperometric sulphur dioxide sensor properties
PublikacjaIn this work amperometric sulphur dioxide sensor with a liquid electrolyte, a mercury sulphate reference electrode and solid polymer electrolyte (Nafion) covered with gold as a working electrode will be presented. The main goal of this research is to determine the influence of internal electrolyte composition on the sensor properties. Sensor filled with 1M and 5M sulphuric acid has been investigated.
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High-pressure and thermal properties of γ-Mg2SiO4 from first-principles calculations
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Preparation, properties and potential applications of a photocurable varnish with pleasant limonene smell
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Sinusoidal Alternating-Current Voltammetry and Metrological Properties of a Flat Voltammetric Electrode in the Time Domain
PublikacjaIn this paper there were analyzed metrological properties of a flat electrode used to mark ions with the method of sinusoidal alternating-current voltammetry in the situation where on its surface an electrochemical reversible reaction of oxidizing / reduction takes place. The result of the analysis conducted is that such a voltammetric electrode functions like a converter type I. Metrological properties of such an electrode in...
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Effect of polymer fibres reinforcement on selected properties of asphalt mixtures
PublikacjaThe paper presents selected results of the research program concerning fibre reinforced asphalt concrete. Aramid-polyalphaolefin fibres was used in this study. Selected properties responsible for low temperature cracking and resistance to permanent deformation are presented in this paper. Low temperature cracking susceptibility was evaluated with the results obtained from bending test of rectangular beams with constant rate of...
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The influence of rubber recyclate morphology on the properties of rubber-asphalt composite
PublikacjaIn the paper wastes, mostly in the form of used tires, were analyzed. One of the methods of waste tires application use them as a modifier of asphalt. However, the properties of rubber-asphalt composites depend on the morphology of waste tiregranulate and kind of tire recycled (car/truck). In this chapter, the influence of grinding methods of waste tire on the prop¬erties of rubber-asphalt composites were studied. SEM analysis...
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Mechanical Properties of a Dike Formed from a Soil-ash Composite
PublikacjaThe paper presents the research results on application of composite soils for dike construction. The composite soil is produced by mixing bottom ash (by-product of energetics) with dredged material (sand) taken from the mouth of The Vistula river. The optimum composite for dike core was chosen with respect to mechanical parameters: high internal friction angle, good compaction and reduced hydraulic conductivity. The test dike was...
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Immunosuppressive properties of amino acid and peptide derivatives of mycophenolic acid
PublikacjaMycophenolic acid (MPA) was coupled with amino acids and biologically active peptides including derivatives of tuftsin to modify its immunosuppressive properties. Both amino acid unit in the case of simple MPA amides and modifications within peptide moiety of MPA - tuftsin conjugates influenced the observed activity. Antiproliferative potential of the obtained conjugates was investigated in vitro and MPA amides with threonine methyl...
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SAWING PROCESS AS A NEW ALTERNATIVE WAY OF DETERMINING SOME WOOD PROPERTIES
PublikacjaCutting forces (power) could be considered from a point of view of modern fracture mechanics. The developed cutting model, derived from fracture mechanics, includes work of separation (fracture toughness) in addition to plasticity and friction, and also dullness of the cutting edge described by the cutting edge radius. Moreover, forecasting of the shear plane angle for the cutting models, broaden possibilities of energetic effects...
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Progressing Pollutant Elution from Snowpack and Evolution of its Physicochemical Properties During Melting Period— a Case Study From the Sudetes, Poland
PublikacjaMain aim of the work assumed recognition of physicochemical changes in snowpack occurring during the melting period. Properties of snow cover had been identified at two sites in Western Sudetes mountains (860 and 1228 m asl) in SW Poland since the end of January, and monitored until the disappearance of snow in late Spring. Snow pit measurements and sample collection at both sites were made followed by chemical analyses with the...
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Nutritional and Pharmaceutical Properties of Bioactive Compounds in Organic and Conventional Growing Kiwifruit
PublikacjaThe bioactivity of two kiwifruit’s cultivars growing under organic and conventional conditions were studied and compared. The bioactive compounds were extracted with water and ethanol using similar conditions which are applied in pharmaceutical applications and for daily fruit consumption such as tea drink. Antioxidant radical scavenging assays [ferric-reducing/antioxidant power (FRAP); cupric reducing antioxidant capacity (CUPRAC);...
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Experimental determination of basic mechanical properties of elastomeric polymer
PublikacjaThere are a lot of different methods of repairing and reinforcing damaged structures, but when it comes to historical buildings and other cultural heritage objects, it is as much about mechanical safety as the aesthetical aspects. Recently, a new and innovative method of repairing damaged structures by filling the cracks with a specially prepared polymer mass has been proposed. This new and innovative technique, known as the Flexible...
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Effect of porosity on physical properties of lightweight cement composite with foamed glass aggregate
PublikacjaThis paper reports on a study of physical properties of lightweight cement composite. We investigate the possibility of replacing traditional aggregate with Granulated Ash Aggregate (GAA) and above all with Granulated Expanded Glass Aggregate (GEGA). For this purpose, 15 specimens of different percentage share of each aggregate in total aggregate volume were tested: 0%, 25%, 50%, 75% or 100% of foam glass aggregate (GEGA) partially...
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Characterization of Optical and Electrical Properties of Transparent Conductive Boron-Doped Diamond thin Films Grown on Fused Silica
PublikacjaA conductive boron-doped diamond (BDD) grown on a fused silica/quartz has been investigated. Diamond thin films were deposited by the microwave plasma enhanced chemical vapor deposition (MW PECVD). The main parameters of the BDD synthesis, i.e. the methane admixture and the substrate temperature were investigated in detail. Preliminary studies of optical properties were performed to qualify an optimal CVD synthesis and film parameters...
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Influence of Water-Induced Degradation of Polytetrafluoroethylene (PTFE)-Coated Woven Fabrics Mechanical Properties
PublikacjaThe impact of water-induced degradation on the mechanical properties of the chosen two PTFE-coated, glass threads woven fabrics is investigated in this paper. The paper begins with a survey of literature concerning the investigation and determination of coated woven fabric properties. The authors carried out the uniaxial tensile tests with an application of flat and curved grips to establish the proper values of the ultimate tensile...
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Structural and Thermo-Mechanical Properties of Poly(ε-caprolactone) Modified by Various Peroxide Initiators
PublikacjaThe modification of poly(ε-caprolactone) (PCL) was successfully conducted during reactive processing in the presence of dicumyl peroxide (DCP) or di-(2-tert-butyl-peroxyisopropyl)-benzene (BIB). The peroxide initiators were applied in the various amounts of 0.5 or 1.0 pbw (part by weight) into the PCL matrix. The effects of the initiator type and its concentration on the structure and mechanical and thermal properties of PCL were...
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The change of mechanical properties of selected wood species after drying process under various conditions
PublikacjaThe result of mechanical properties change of selected wood species after drying process under various parameters are presented. The global elasticity modulus and bending strength for steam dried, air-steam mixture dried and air dried samples as reference were measured. It allowed to reveal the effect of wood stream, air-steam mixture and their temperature on mechanical properties of wood. It has been recognized that steam and...
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Quality of limes juices based on the aroma and antioxidant properties
PublikacjaKaffir (Citrus hystrix) and Key (Citrus aurantifolia) limes juices were investigated and compared. Two dimensional gas chromatography coupled with time-of-flight mass spectrometry (GC×GC-TOF-MS) was applied to assess the botanical origin of Kaffir and Key limes juices, based on volatile substances. The biggest differences in the contents of selected terpenes in Kaffir and Key limes occur in chemical compounds such as Limonene,...
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Injectable poloxamer/graphene oxide hydrogels with well‐controlled mechanical and rheological properties
PublikacjaAlthough significant progress has been made in the design and application of injectable hydrogels for biomedical applications, concurrent control of rheological and mechanical properties of injectable hydrogels has remained as an open challenge to the researchers. In this work, we introduce and put into practice a photo‐curable poloxamer (also known as Pluronic)/graphene oxide (Plu/GO) injectable hydrogel with well‐controlled rheological...
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Microbial and chemical quality assessment of the small rivers entering the South Baltic. Part II: Case study on the watercourses in the Puck Bay catchment area
PublikacjaDue to its location, Puck Bay is an area particularly vulnerable to pollution of anthropogenic origin. The aim of the study was to assess the water quality of small watercourses entering the inner part of Puck Bay. The paper presents the results of chemical and microbiological analyses of 10 rivers and canals at their estuaries located on the western shore of the internal Puck Bay. The following environmental parameters were analyzed:...
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THE PROPERTIES OF NANOSILVER – DOPED NANOHYDROXYAPATITE COATING ON THE Ti13Zr13Nb ALLOY
PublikacjaThe aim of this research was to study the properties of nanohydroxyapatite (nanoHAp) and nanohydroxyapatite, doped with nanosilver (nanoHAp/nanoAg), coatings obtained by an electrophoretic deposition process. The suspensions was prepared by dispersing 0.1 g of HAp nanopowder for nanoHAp coatings and 0.1 g of nanoHAp and 0.025 g nanoAg for nanoHAp/nanoAg coatings. The deposition was carried out for 1 min at 50 V voltage followed...
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Phosphinophosphoranes: Mixed-Valent Phosphorus Compounds with Ambiphilic Properties
PublikacjaHerein, we present a simple synthesis of mixed-valent phosphinophosphoranes bearing three- and five-coordinate phosphorus centers. Compounds with phosphorus–phosphorus bonds were synthesized via a reaction of lithium phosphides RR′PLi with cat2PCl (cat = catecholate), whereas derivatives with methylene-linked phosphorus centers were obtained via a reaction of phosphanylmethanides RR′CH2Li with cat2PCl. The presence of accessible...
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Synergistic effect of MWCNTs and MA-g-PP on the thermal and viscoelastic properties of immiscible PTT/PP blends
PublikacjaThe properties of immiscible blends of PTT and PP were modified by grafting and nanoparticle inclusion. The observed synergistic effect of MWCNTs and MA-g-PP on the thermal and viscoelastic properties of PTT/PP blends was studied in detail and the properties of the composites were compared with those of ungrafted PP.
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Properties of Nasicon-based CO2 sensors with Bi8Nb2O17 reference electrode
PublikacjaPotentiometric CO2 sensors based on Nasicon (Na+ conductor, Na3Zr2Si2PO12) electrolyte, Bi8Nb2O17/Pt reference electrode and different sensing electrodes have been prepared. Besides the sensing electrode material, sensors differ from each other in the reference electrode preparation technique. The main aim of this study is to investigate sensor construction and electrode fabrication process influence on sensor properties. The optimal...
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Influence of cooling rate and additives on low-temperature properties of asphalt mixtures in the TSRST
PublikacjaThe paper presents the results and analysis of low-temperature properties of asphalt mixtures according to Thermal Stress Restrained Specimen Test (TSRST) and Indirect Tensile Test methods. Different groups of bitumen were investigated: neat, SBS-modified and highly SBS-modified. Influence of cooling rates (1 C/h, 3 C/h, 5 C/h and 10 C/h) and additives (aramid fibres and crumb rubber) was identified as well. Moreover, for each...
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Influence of controlled crystallization and SrF2 content on the structure and properties of Eu3+ doped phosphate glasses
PublikacjaNew phosphate glasses and glass-ceramics P2O5–Bi2O3–K2O–Nb2O5-SrF2 doped with Eu were synthesized and studied in this work. The influence of the SrF2 content (0–15 mol%) and the parameters of the heat treatment on their structural and optical properties were investigated. For the above purpose, the structural characterization by FTIR spectroscopy and XRD measurements was carried out, which showed a significant effect of SrF2 on...
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Linear and Nonlinear Optical Properties of Azobenzene Derivatives Modified with an (Amino)naphthalene Moiety
PublikacjaThe design of two-photon absorbing azobenzene (AB) derivatives has received much attention; however, the two-photon absorption (2PA) properties of bis-conjugated azobenzene systems are relatively less explored. Here, we present the synthesis of six azobenzene derivatives and three bisazobenzenes substituted (or not) at para position(s) with one or two amino group(s). Their linear and nonlinear absorption properties are studied...
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QRS Morphology-Based EDR Signal—Factors Determining its Properties
PublikacjaRespiration-induced signals contain a clinically significant information. It could be obtained utilizing both direct and indirect methods. ECG-Derived Respiration (EDR) method is the latter one. However, in this case, two approaches could be distinguished. First one is based on determining changes in the morphology of QRS complexes while the second one is based on the Respiratory Sinus Arrhythmia (RSA) mechanism. The former approach...
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On tracking properties of real-valued generalized adaptive notch filters
PublikacjaGeneralized adaptive notch filters (GANFs) are used for identification/tracking of quasi-periodically varying dynamic systems and can be considered an extension, to the system case, of classical adaptive notch filters. The paper presents results of local performance analysis of a real-valued GANF algorithm, i.e., algorithm designed to track parameters of a real-valued system. This is an extension of the previous work which focused...
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Physicochemical Properties and Application of Silica-Doped Biochar Composites as Efficient Sorbents of Copper from Tap Water
PublikacjaThis article concerns research on new sorption materials based on silica-doped activated carbon. A two-stage synthesis involved pyrolysis of plant material impregnated in a water glass solution , followed by hydrothermal activation of the pyrolysate in KOH solution. The resulting composite can be used as a sorbent in drinking water filters. The proposed method of synthesis enables the design of materials with a surface area...
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Magnetic properties of α-KCoPO4 compound with a chiral polar crystal structure
PublikacjaWe have obtained polycrystalline samples of a metastable α variant of KCoPO4 by low temperature (350–400 °C) solid state metathesis reaction of potassium oxalate and ammonium cobalt orthophosphate. The material crystallizes in a polar chiral structure (sg. P63, no. 173). Measurements of magnetic properties reveal antiferromagnetic interactions and no ordering observed down to T = 1.9 K, well below the Weiss temperature |Θcw| =...
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Interrelationship between total volatile organic compounds emissions, structure and properties of natural rubber/polycaprolactone bio-blends cross-linked with peroxides
PublikacjaNatural rubber/polycaprolactone (NR/PCL) bio-based blends with different organic peroxides were prepared using an internal batch mixer and subsequently cross-linked at 170°C. Two types of commonly used organic peroxides, dicumyl peroxide and di(tert-butylperoxyisopropyl)benzene peroxide, were applied as free-radical initiator. Cross-linking efficiency of NR/PCL blends were investigated using oscillating disc rheometer measurements,...
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Mechanical properties of sisal fiber-reinforced soybean oil-based polyurethane biocomposites
PublikacjaIn this paper the results of the mechanical properties of polyurethane biocomposites reinforced with short sisal fibers are presented. The fillers were added in different amount: 5, 10 and 15% by mass. Tensile test, hardness, abrasion resistance, elasticity were determined according to the standards.
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Tuning of the Electrochemical Properties of Transparent Fluorine-doped Tin Oxide Electrodes by Microwave Pulsed-plasma Polymerized Allylamine
PublikacjaWe report here the dry, one-step, and low-temperature modification of FTO surfaces using pulsed plasma polymerization of allylamine (PPAAm). PPAAm/FTO surfaces were characterized by X-ray photoelectron spectroscopy, spectroscopic ellipsometry, and contact angles to understand the morphological, structural, and optical properties. FTO were coated with a very thin layer of adherent cross-linked, pinhole-, and additive-free allylamine...
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Rigid polyurethane foams with different flame retardants and their physical and mechanical properties
PublikacjaRigid polyurethane foams (PUFs) containing 3, 6 or 9 % of one of of two selected fire retardants (FR): oligomeric ethyl ethylene phosphate (Fyrol PNX) and expandable graphite (EG) were prepared, inspected and compared to foam without that fillers as the control. The thermal stability of PUFs was described by horizontal test according to norm: UL 94 HB. Compressive strength and physical properties (density, fragility and water absorption)...