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Effects of V2O5 Additive on Structure and Dielectric Properties of BiNbO4 Ceramics
PublikacjaGoal of the present research was to investigate the influence of V2O5 additive on the structure and dielectric properties of BiNbO4 ceramics. To fabricate BiNbO4 ceramics with V2O5 added the solid state reaction route and pressureless sintering was utilized. Thus obtained ceramics was characterized in terms of its microstructure (SEM), chemical composition (EDS), phase composition and crystalline structure (X-ray phase and structural...
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Study of the influence of thermal factors on the welding process of polyethylene gas pipelines,
PublikacjaA one-dimensional calculation scheme is proposed with the help of which it is possible to determine and set the technological parameters with the accuracy to be realized in production conditions: the temperature of the heating element and the heating time, which allows maximum mechanization of the technological operations of polyethylene gas pipelines welding. The numerical value of the coefficient of temperature for polyethylene...
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THERMODYNAMIC ANALYSIS OF A GENERATION IV SCWR NUCLEAR POWER PLANT CYCLE
PublikacjaThis article presents a flow and thermodynamic analysis of a Generation IV nuclear cycle. An SCWR (Supercritical water reactor) is a high temperature and high pressure reactor that uses water at a temperature above its thermodynamic critical point as the working fluid. The cycle used for the calculations consists of one interstage superheater and 7 regenerative heat exchangers. Division pressure was optimized in view of the cycle efficiency,...
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High-accuracy polarimetric studies on lead germanate single crystals
PublikacjaA high-accuracy polarimetric technique has been used for the characterization of a lead germanate ferroelectric single crystal. The measurement results of the linear and circular birefringence in the [010] direction at a wavelength of 633 nm under the influence of an electric field are presented. Gyration–electric field hysteresis loops at alternative crystal positions in the polarization system have been used to determine the...
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Effects of deviations from thermo-rheologically simple behavior of asphalt mixes in creep on developing of master curves of their stiffness modulus
PublikacjaThe paper presents the deviations from the thermo-rheologically simple behavior of asphalt mixes and their effects on the developing of master curves of stiffness modulus. Eleven different mixes were tested in three point bending test under constant load at temperatures –20°C, –10 °C and 0 °C, and in some cases at +10 °C. The test method was developed at the Gdansk University of Technology, Poland. The applied stress level was...
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Spectroscopic study of atmospheric pressure 915 MHz microwave plasma at high argon flow rate
PublikacjaIn this paper results of optical emission spectroscopic (OES) study of atmospheric pressure microwave 915 MHz argon plasma are presented. The plasma was generated in microwave plasma source (MPS) cavity- resonant type. The aim of research was determination of electron excitation temperature Texc gas temperature Tg and electron number density ne. All experimental tests were performed with a gas flow rate of 100 and 200 l/min and...
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EFFECT OF SURFACE STATE AND STRESS ON AN OXIDATION OF THE ZIRCALOY-2 ALLOY
PublikacjaZr alloys are widely used as materials for nuclear fuel pellets in the nuclear industry. In the case of the LOCA or RIA happen, a temperature may locally reach high values. Even if the high temperature maintains shortly, the zirconium oxides may become permeable, absorb hydrogen appearing in cooling water from decomposition reaction and crack because of formation and brittle failure of hydrides. Such model cannot so far take into...
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Eksperymentalna weryfikacja procedury szacowania wytrzymałości młodego betonu wg normy ASTM C1074
PublikacjaW referacie przedstawiono metodę służącą oszacowaniu wytrzymałości betonu w trakcie procesu dojrzewania (ang. Maturity Method) bazującą na procedurze określonej zgodnie z amerykańską normą, która uwzględnia wpływ połączonych efektów temperatury i czasu na rozwój wytrzymałości betonu. Standardy ASTM C1074 zostały opracowane przez NBS (ang. National Bureau of Standards) z uwagi na powtarzające się wypadki na palcu budowy wynikające...
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Modeling and MANOVA studies on toxicity and endocrine potential of packaging materials exposed to different extraction schemes
PublikacjaThe stability of the linings of packaging that is in contact with the goods stored has been of major concern during decades of the development of packaging materials. In this work, an attempt was undertaken to assess the applicability of using two bioassays (Microtox® and XenoScreen YES/YAS) in estimating the stability of packaging (cans, caps, multilayer material) and the impact of their degradation on the toxicity of some simulated media....
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The psychrotrophic yeast Sporobolomyces roseus LOCK 1119 as a source of a highly active aspartic protease for the in vitro production of antioxidant peptides
PublikacjaA psychrotrophic yeast strain producing a cold-adapted protease at low temperature was classified as Sporobolomyces roseus. In standard YPG medium, S. roseus LOCK 1119 synthesized an extracellular protease with an activity of approximately 560 U/L. Optimization of medium composition and process temperature considerably enhanced enzyme biosynthesis; an approximate 70% increase in activity (2060 U/L). The native enzyme was purified...
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Effect of isovalent substitution on microstructure and phase transition of LaNb1−xMxO4 (M=Sb, V or Ta; x=0.05–0.3)
PublikacjaLaNb1−xMxO4 oxides with pentavalent elements of different ionic sizes (M=Sb, Ta and V, x=0.05–0.3) were synthesized by the solid state reaction method. Special interest was devoted to the antimony substituted lanthanum niobate which is a new material in this group. Rietveld analysis of the X-ray diffraction patterns was used to determine the influence of the material composition on unit cell parameters. On the basis of dilatometric...
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Comparison of Downdraft and Updraft Gasification of Biomass in a Fixed Bed Reactor
PublikacjaThe aim of this study was to compare and analyze the gasification process of beech wood. The experimental investigation was conducted inside a gasifier, which can be operated in downdraft and updraft gasification system. The most important operating parameter studied in this paper was the influence of the amount of supply air on the temperature distribution, biomass consumption and syngas calorific value. The results show that...
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On the production of electricity in Poland using a geothermal binary power plant - A thermodynamic overview - Part I
PublikacjaPoland has a significant potential of geothermal energy. However, the high-temperature sources that are needed to drive power plants are found in relatively few places. Therefore, the objective of this paper is to consider any location in the northern part of Poland as a possible place to build a binary power plant. A scientific research was confirmed the existence of an elevated temperature gradient in this region. The hot rocks...
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Superconductivity in the intermetallic compound Zr5Al4
PublikacjaPolycrystalline Zr5Al4 was synthesized using the arc-melting method. Powder X-ray diffraction confirms the previously reported crystal structure of the Ti5Ga4-type P63/mcm with lattice parameters: a = 8.4312(6) A , and c = 5.7752(8) A . Electrical resistivity and low-temperature magnetic susceptibility measurements indicate that Zr5Al4 exhibits superconducting behavior below 2 K. The normalized heat capacity jump at Tc= 1.82 K...
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Jeffreys heat conduction in coupled semispaces subjected to interfacial heating
PublikacjaA Jeffreys heat conduction problem for coupled semispaces subjected to the action of an interfacial heat source was defined. An analytical solution of the problem was derived for a polynomial specific power of the heat source using the Laplace transform approach. The asymptotic and parametric analysis was performed for different ratios of thermal conductivities , thermal diffusivities , thermal relaxation times and coefficients...
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The homometallic warwickite V 2 OBO 3
PublikacjaThe synthesis, structure and elementary magnetic characterization of the homometallic warwickite V2OBO3 are reported. The material adopts the orthorhombic warwickite structure type at room temperature, space group Pnma (No. 62) with lattice parameters a = 9.2317(1) Å, b = 3.1172(1) Å, and c = 9.5313(1) Å. Temperature-dependent magnetic susceptibility, electrical resistivity, and specific heat measurements show anomalies near 35 K,...
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On thermal stability of topological qubit in Kitaev's 4D model
PublikacjaWe analyse stability of the four-dimensional Kitaev model-a candidate for scalable quantum memory - in finite temperature within the weak coupling Markovian limit. It is shown that, below a critical temperature, certain topological qubit observables X and Z possess relaxation times exponentially long in the size of the system. Their construction involves polynomial in system size algorithm which uses as an input the results of...
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The innovative experimental rig for wood steam drying at atmospheric pressure
PublikacjaThe high cost of fossil fuel and soaring consumer interest have encouraged people in the wood industry to look for faster and more energy-efficient methods to dry lumber. The air-steam mixture as medium of drying process was used in a laboratory kiln especially arranged for that reason. Experimental rig is based on automatic control system. At the time of drying measurements of the internal temperature, wood temperature, moisture...
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Electrical conductivity and relaxation processes in V2O5 nanorods prepared by sol–gel method
PublikacjaProperties of high purity V2O5 nanorods prepared by a sol – gel method are presented. The studied materials were characterized by: X-ray diffractometry (XRD), scanning electron microscopy (SEM), and X-ray photoelectron spectroscopy (XPS). The electrical impedance was measured as a function of temperature and frequency. The obtained results show that the electrical conductivity increases with increasing temperature. The d.c. conductivity...
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Interactions between components of SrTi0.98 Nb0.02O3-δ-YSZ and SrTi0.98 Nb0.02O3-δ -CeO2 composites
PublikacjaComposites consisting of SrTiO3-based perovskite and either yttria-stabilized zirconia or ceria were investigated. The mechanical compatibility and possible inter-diffusion between phases were characterized by scanning electron microscopy, X-ray diffraction, and energy-dispersive X-ray spectroscopy. A gradual disappearance of Ce-containing phases with an increase in the temperature of reduction in hydrogen was noticed. Moreover,...
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Intergranular Corrosion Detection Using Electromagnetic Transducers for Ultrasonic Testing
PublikacjaThe aim of this paper is to create a research methodology that allows a quick analysis of the structural state of high alloy austenitic steels using non-destructive ultrasonic tests, in contrast to destructive standard methods. Electromagnetic acoustic transducers (EMAT) are used to generate and receive the ultrasonic wave and detect the microstructural changes caused by sample sensitization in elevated temperature, even after...
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Vibrational Properties of LaNb0.8M0.2O4-δ (M=As, Sb, V, and Ta)
PublikacjaLaNb0.8M0.2O4-δ (where M=As, Sb, V, and Ta) oxides with pentavalent elements of different ionic sizes were synthesized by a solid-state reaction method. The vibrational properties of these oxides have been investigated. These studies revealed that the substituent element influences both Debye temperature value as well as the Raman active vibrational modes. Additionally, the low-temperature vibrational properties of LaNb0.8Sb0.2O4-δ...
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Heat Dissipation from the Power Cable in the Casing Pipe
PublikacjaThe current carrying capacity of a power cable determines its ability to carry a specific current and is related to the efficiency of dissipation of heat generated in the cable laid in a specific environment. The studies were conducted in order to determine how the characteristics of the medium around the cable affected its temperature, and thus the ability of the cable to transmit electricity. The experimentation in the lab and...
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Polymer based thick films - material quality and interface resistance evaluation
PublikacjaThe properties of polymer based thick film layers mede using different resistive pastes and dipping silvers have been studied. The composite of carbon and graphite (C/Gr) conducting particles suspended in different polymer vehicles were used for preparation resistive layers. Interface resistance Rc created between dipping silver (DiAg) contact layer and resistive layer was determined from the surface potential distribution measurements...
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ATTEMPTS OF THERMAL IMAGING CAMERA USAGE IN ESTIMATIONS OF THE CONVECTIVE HEAT LOSS FROM A VERTICAL PLATE
PublikacjaIn this paper a new method for determining heat transfer coefficients using a gradient method has been developed. To verify accuracy of the proposed method vertical isothermal heating plate with natural convection mechanism has been examined. This configuration was deliberately chosen, because of the fact that such case is historically the earliest and most thoroughly studied and its rich scientific documentation - the most reliable....
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Chemically reduced graphene oxide based aerogels - Insight on the surface and textural functionalities dependent on handling the synthesis factors
PublikacjaEfficient adjusting of reduced graphene oxide aerogels properties requires information about experimental factor-aerogel property relationship. In this work, the reduced graphene oxide aerogels surface and textural functionalities in relation to precursor concentration, gelation time and hydrogel freezing temperature were studied in detail, with the use of dynamic adsorption method of gaseous organic probes and experimental design....
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Direct-contact condensation from vapour- gas mixture in a spray ejector condenser for negative CO2 power plant
PublikacjaDirect-contact condensation of vapour containing the inert gas on a spray of subcooled liquid exists in a number of technical applications. For example, it may be found in the nuclear industry (e.g. pressurized jet under normal operating conditions, in safety analyses) or in the chemical industry (e.g. mixing-type heat exchanger, degasser, sea water desalting). The problem is also essential to modelling and analysis of some...
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A NOVEL CONCEPT OF H2/O2 STEAM GENERATOR
PublikacjaThis paper presents an idea of hydrogen utilization to steam generation to drive a turbine and produce electricity or to supply a condenser as an element of heating system. Electrolysis process is considered as a source of hydrogen as well as oxygen. Hydrogen combustion with a stoichiometric ratio of pure oxygen produces steam at very high temperature. Steam temperature can be controlled by mixing the generated steam with liquid...
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A novel concept of H2/O2 steam generator
PublikacjaThis paper presents an idea of hydrogen utilization to steam generation to drive a turbine and produce electricity or to supply a condenser as an element of a heating system. Electrolysis process is considered as a source of hydrogen as well as oxygen. Hydrogen combustion with a stoichiometric ratio of pure oxygen produces steam at very high temperature. Steam temperature can be controlled by mixing the generated steam with liquid...
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Evaluation of thermal cracking probability for asphalt concretes with high percentage of RAP
PublikacjaThe paper presents determination of the probability of thermal cracking of asphalt mixtures with different reclaimed asphalt pavement (RAP) content on the basis of laboratory tests and analytical evaluation using thermal stress development method. Probability was evaluated taking into consideration: the type and gradation of the mixture and the quality and content of RAP. Thermal stresses were determined using two models: elastic and...
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Wpływ wprowadzenia norm europejskich na konstrukcję wsporczych napowietrznych linii elektroenergetycznych
PublikacjaKonstrukcje wsporcze linii elektroenergetycznych były i są projektowane zgodnie ze specjalistycznymi normami, innymi niż stosowane w budownictwie. Dotyczą one zarówno oddziaływań środowiskowych, takich jak temperatura, wiatr, oblodzenie i oddziaływania stałe (naciąg, przewodów, osprzęt), jak i zasad wymiarowania. W artykule przedstawiono wyniki analiz porównawczych dotyczących wpływu zmian wprowadzanych w normach europejskich na...
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Szacowanie estymaty menzurandu temperatury skóry człowieka podczas próby wysiłkowej
PublikacjaW artykule zaprezentowano wyniki pomiarów temperatury skóry człowieka podczas próby wysiłkowej. Ponieważ uzyskane wyniki nie podlegają rozkładowi normalnemu, wyznaczono wartości pięciu różnych estymatorów menzurandu. Otrzymane rezultaty wykazały, że w rozważanym przypadku najlepszy estymator menzurandu otrzymujemy z metody bootstrap, ponieważ charakteryzuje się on najmniejszym odchyleniem standardowym.
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Crossover from charge density wave stabilized antiferromagnetism to superconductivity in Nd1−xLaxNiC2 compounds
PublikacjaThe path from the charge density wave antiferromagnet NdNiC2 to the noncentrosymmetric superconductor LaNiC2 is studied by gradual replacement of Nd by La ions. The evolution of physical properties is explored by structural, magnetic, transport, magnetoresistance, and specific heat measurements. With the substitution of La for Nd, the Peierls temperature is gradually suppressed, which falls within the BCS mean-field relation for...
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Synthesis, microstructure and electrical properties of nanocrystalline calcium doped lanthanum orthoniobate
PublikacjaThe single phase lanthanum orthoniobate with tetragonal structure has been synthesized by the means of mechanosynthesis method. The studies have shown the crystal structure of La0.98Ca0.02NbO4 depends on the synthesis stage. The samples were predominantly in the tetragonal phase with a trace amount of the monoclinic phase. The SEM studies of morphology and microstructure have shown nanocrystallinity of the materials. The Raman...
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Improved maximum power point tracking algorithms by using numerical analysis techniques for photovoltaic systems
PublikacjaSolar photovoltaic (PV) panels generate optimal electricity when operating at the maximum power point (MPP). This study introduces a novel MPP tracking algorithm that leverages the numerical prowess of the predictor-corrector method, tailored to accommodate voltage and current fluctuations in PV panels resulting from variable environmental factors like solar irradiation and temperature. This paper delves into the intricate dynamics...
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Phase change thermal energy storage – the experience of the materials preparation for the specific applications.
PublikacjaThermal energy storage and temperature stabilization is very important in many engineering applications. There are three kinds of thermal energy storage: sensible heat, latent heat and reversible chemical reaction heat. Phase change materials (PCM) absorb, store and release large amounts of energy in the form of latent heat, at constant temperature, called the transition temperature. Many innovative applications could be found...
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Solvation of ionic liquids based on N-alkyl-N-methylmorpholinium cations in N,N-dimethylformamide and dimethyl sulfoxide – A volumetric and acoustic study
PublikacjaApparent molar volumes and molar isentropic compressibilities for N-ethyl-N-methylmorpholinium and N-decyl-N-methylmorpholinium tetrafluoroborates in N,N-dimethylformamide (DMF) and dimethyl sulfoxide (DMSO) have been determined from density and speed of sound measurements over the temperature range T = (298.15, 303.15, 308.15, 313.15, 318.15 and 328.15) K at experimental pressure p = 0.1 MPa. This data has been used to calculate...
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Synthesis, thermal, structural and electrical properties of vanadium-doped lithium-manganese-borate glass and nanocomposites
PublikacjaA glassy sample with a nominal formula LiMn1−3x/2VxBO3 (where x = 0.05) was synthesised using the melt-quenching method. Material was characterised by differential thermal analysis (DTA), X-ray diffactometry (XRD) at room temperature and as a function of temperature (HT-XRD), X-ray photoelectron spectroscopy (XPS), impedance spectroscopy (IS) and scanning electron microscopy (SEM). Dependences of glass transition and crystallisation...
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The Laboratory Stand for the Evaluation of Heat Dissipation from the Power Cable in a Casing Pipe
PublikacjaThe current carrying capacity of a power cable determines its efficiency, which depends on its capability to dissipate heat produced inside the cable, as a result of current flow, into the surrounding. The studies were conducted to determine how the characteristics of the medium around the cable affected its temperature and, as a result, its ability to transport electricity. The experimentation in the lab and real measurements...
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The interaction of the pulsed laser irradiation with titania nanotubes - Theoretical studies on the thermal effect
PublikacjaThis paper reports temperature dispersion simulations of titania nanotubes irradiated by the 355 nm, pulsed, nanosecond laser. The modelling with the use of Finite Elements Method concerns titania nanotubes of the length and the wall thickness in the range of 0.5–2 μm and 5–20 nm, respectively. The uniqueness of the morphology was preserved by ensuring the wall thickness variation along the height of the tube, which was determined...
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Przygotowanie przemysłowego obiektu o stalowej konstrukcji nośnej do remontu po pożarze
PublikacjaW artykule przedstawiono warunki i sposób podejścia do naprawy stalowej konstrukcji nośnej kilkukondygnacyjnego obiektu przemysłowego, który uległ uszkodzeniu w wyniku oddziaływania wysokiej temperatury pożaru. Omówiono rodzaje badań i sprawdzeń oraz sposób przeprowadzenia kontroli konstrukcji, które stały się podstawą do wydania oceny technicznej o możliwości odbudowy i remontu obiektu, bez jego nadmiernej rozbiórki. Wskazany...
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Implementation of the Boundary Element Method to Two-Dimensional Heat Transfer with Thermal Bridge Effects
PublikacjaThe work presents an application of the boundary element method applied to a two-dimensional conductive heat transfer. The algorithm of the method is explained and its advantages are outlined. Green's function as a fundamental solution for Poisson's equation in two dimensions was used and the direct approach was applied. The presented results concern building construction elements as typical cases of thermal bridges. Some properties...
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Microstructure and Dielectric Properties of Barium-vanadate Glasses
PublikacjaThe ac and dc conductivity in barium-vanadate glasses was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD) and scanning electron microscopy (SEM) methods. The XRD results show that all samples are amorphous but microscopy investigation reveals that glasses with greater amount of V2O5...
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Cross-linking of epoxy-oligomeric mixtures in the presence of modified phenol-formaldehyde resins
PublikacjaCross-linking of epoxy oligomeric mixtures consisting of industrial epoxy resin ED-20, oligoetheracrylate TGM-3, peroxide derivative of epoxy resin ED-24 and phenol-formaldehyde oligomer with unsaturated methacrylate fragments or peroxide groups was studied in the presence of polyethylenepolyamine at room temperature and heated to 383, 403 or 423 K for 15, 30, 45, 60 and 75 minute. The influence of mixture composition, temperature...
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Application of Headspace Solid-phase Microextraction with Poly(1-vinyl-3- Hexylimidazolium Chloride) Polymeric Ionic Liquid Coating using GC - MS to Determine Volatile Fatty Acids in Dairy Wastewater
PublikacjaVolatile fatty acids were determined in this study using headspace solid-phase microextraction (HS-SPME) with a poly(1-vinyl-3-hexylimidazolium chloride) polymeric ionic liquid coated fiber followed by gas chromatography - mass spectrometry. Experimental parameters such as extraction time and temperature, sample volume as well as desorption time and temperature were optimized. Detection limits of the method were in the range of...
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Superconductivity in the niobium-rich compound Nb5Se4
PublikacjaThe niobium rich selenide compound Nb5Se4 was synthesized at ambient pressure by high-temperature solid–state reaction in a sealed Ta tube. Resistivity and heat capacity measurements reveal that this compound is superconducting, with a Tc = 1.85K. The electronic contribution to the specific heat γ and the Debye temperature are found to be 18.1 mJmol−1K−2 and 298 K respectively. The calculated electron-phonon coupling constant λep...
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Numerical simulation of hardening of concrete plate
PublikacjaThe paper presents a theoretical formulation of concrete curing in order to predict temperature evolution and strength development. The model of heat flow is based on a well-known Fourier equation. The numerical solution is implemented by means of the Finite Difference Method. In order to verify the model, the in situ temperature measurements at the top plate of a road bridge were carried out. A high agreement between numerical...
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Investigations on mixture preparation for two phase adiabatic pressure drop of R134a flowing in 5 mm diameter channel
PublikacjaThe article presents detailed two-phase adiabatic pressure drops data for refrigerant R134a. Study cases have been set for a mass flux varying from 200 to 400 kg/m2 s, at the saturation temperature of 19.4 ◦C. Obtained experimental data was compared with the available correlations from the literature for the frictional pressure drop during adiabatic flow. Influence of mixture preparation on pressure drop was investigated, for...
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Tunable Dielectric Switching of (Quinuclidinium)[MnCl4] Hybrid Compounds
PublikacjaInorganic−organic hybrid QMnCl (Q = quinuclidinium) crystals were synthesized and characterized. The X-ray and variable-temperature IR/Raman analysis demonstrate that the crystals undergo a reversible structural phase transition, which originates from an order−disorder process and is related to the dynamics of the organic Q cation. Dielectric function measurements disclose a switchability between low (“OFF”) and high (“ON”) dielectric...
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Fermi-liquid behavior of binary intermetallic compounds Y3 M (M = Co, Ni, Rh, Pd, Ir, Pt)
PublikacjaA series of polycrystalline samples of Y3 M (M = Co, Ni, Rh, Pd, Ir, Pt), intermetallic binary compounds were synthesized by the arc-melting method. Powder x-ray diffraction (pXRD) confirmed the orthorhombic cementite-type crystal structure and allowed for the estimation of the lattice parameters. Physical properties were investigated by means of electrical resistivity and heat capacity measurements between 1.9 K and 300 K. All...