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Wyniki wyszukiwania dla: REVERSE PHASE COLUMN
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Development of Safirinium dyes for new applications: fluorescent staining of bacteria, human kidney cells, and the horny layer of the epidermis
PublikacjaLow-molecular synthetic fluorophores are convenient tools in bioimaging applications. Several derivatives of Safirinium dyes as well as their reactive N-hydroxysuccinimide (NHS) esters bearing diverse substituents were synthesized and evaluated experimentally in terms of their lipophilicity by means of reverse-phase and immobilized artificial membrane high-performance liquid chromatography. Subsequently, the selected compounds...
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Behaviour of deformed steel columns exposed to impact load during earthquakes: numerical analysis
PublikacjaIt has been observed during earthquakes that the so called soft-storey failure of an upper floor of a building leads to considerable vertical impact load acting on structural members of the lower storeys. The aim of this paper is to investigate numerically the behaviour of horizontally deformed columns (deformation as the result of earthquake loading) that are additionally subjected to vertical impact load. In the first stage of...
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Effect of the Cooling Time in Annealing at 350°C on the Phase Transformation Temperatures of a Ni<sub>5</sub><sub>5</sub>Ti<sub>4</sub><sub>5</sub> wt. Alloy
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Magnetic Phase Transition and Exchange Bias in $$\hbox {Ni}_{45}\hbox {Co}_{5}\hbox {Mn}_{35.5}\hbox {In}_{14.5}$$ Ni 45 Co 5 Mn 35.5 In 14.5 Heusler Alloy
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Efficacy, pharmacokinetics, and safety of the biosimilar CT-P10 compared with rituximab in patients with previously untreated advanced-stage follicular lymphoma: a randomised, double-blind, parallel-group, non-inferiority phase 3 trial
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High-performance liquid chromatography of di- and trisubstituted aromatic positional isomers on 1,3-alternate 25,27-dipropoxy-26,28-bis-[3-propyloxy]-calix[4]arene-bonded silica gel stationary phase.
PublikacjaOtrzymano nową fazę stacjonarną na bazie dipropyloksy pochodnej kaliks[4]arenu w konformacji 1,3-naprzemianległej chemicznie związaną z żelem krzemionkowym. Przeprowadzono badanie selektywności i sprawności tej fazy w rozdzielaniu izomerów konstytucyjnych benzenu. Zaprezentowano wyniki badania wpływu warunków chromatograficznych (pH fazy ruchomej, temperatura, stężenie modyfikatora organicznego) na zdolność rodzielczą tej nowej...
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Box-Behnken design optimization of pipette tip solid phase extraction for methyl orange and acid red determination by spectrophotometry in seawater samples using graphite based magnetic NiFe2O4 decorated exfoliated as sorbent
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FLAME ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF TRACE AMOUNTS OF SILVER IN RADIOLOGICAL WASTE SAMPLES AFTER SOLID PHASE EXTRACTION USING MULTI-WALLED CARBON NANO-TUBES MODIFIED BY SODIUM DODECYL SULFATE
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Sustainable recovery of plant essential Nitrogen and Phosphorus from human urine using industrial coal fly ash
PublikacjaCoal-based thermal power plants play a pivotal role in meeting global energy demand. The amount of fly ash generated from these plants increases every year, and its successful use has posed a significant environmental risk in the last decade. In this study, coal fly ash was packed in a fixed-bed adsorption column to remove Urea–N from synthetic human urine. To assess the efficacy of fly ash in the removal of Nitrogen, various process...
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A selection of the optimal eluent components for separation of carnivorous plants metabolites by planar chromatography chromatography
PublikacjaAbstract: The development of the new procedures of the separation components with the complicated chemical structure from natural complex matrix by column chromatography is very difficult and in many cases expensive. Therefore to pre-select the conditions of the separation process the use of thin layer chromatography (TLC) is proffered. The possibility of proceeding the chromatographic process for several mixtures on single plate,...
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Dynamics of fault arc traveling along busbars in high voltage switchboards = Dynamika łuku zwarciowego przemieszczającego się wzdłuż szyn rozdziel-nic wysokiego napięcia
PublikacjaThe paper presents the results of magnetic induction and electrodynamic force calculations acting on arc column during short-circuit in medium voltage air-insulated bus-bars. The gap between the bars was 120 mm and the prospective short-circuit currents ranged from 4 kA to 8 kA. The paper also shows the measurement results of average velocity fault arc depending on currents arc diameter and arc current was established and described....
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Effect of illumination on noise of silicon solar cells
PublikacjaTransport and noise properties of silicon solar cells in darkness and under illumination have been studied. The measurements were carried out for both reverse and forward bias of the device. The changes in the sample behaviour are due to the variation of PN junction dynamic resistance and, also, the occurence of both 1/f and generation-recombination noise components
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“Dilute & Shoot” approach for rapid determination of trace amounts of nicotine in zero-level e-liquids by reversed phase liquid chromatography and hydrophilic interactions liquid chromatography coupled with tandem mass spectrometry-electrospray ionization
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Application of Box–Behnken design in the optimization of a simple graphene oxide/zinc oxide nanocomposite-based pipette tip micro-solid phase extraction for the determination of Rhodamine B and Malachite green in seawater samples by spectrophotometry
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Experimental study on the behaviour of steel columns under seismic-induced axial impact load
PublikacjaIt has been observed during major earthquakes that the so called soft-storey failure of an upper floor of a structure results in large impact load acting on structural members of the lower storeys. It may further lead to progressive collapse of the whole structure substantially intensifying human and material losses. Therefore, the aim of this paper is to investigate experimentally the behaviour of columns under bending (observed...
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Sposoby przykładania obciążenia zmiennego na konstrukcję płytowo-słupową
PublikacjaW pracy przedstawiono analizę porównawczą wybranych metod zadawania obciążenia zmiennego na konstrukcje płytowo-słupową. Przeanalizowano pięć sposobów rozkładu obciążenia na płytę stropową. Wyniki momentów zginających i przemieszczeń w wybranych punktach dla analizowanych przypadków porównywano z wartościami ekstremalnymi obliczonymi na podstawie powierzchni wpływu (Wariant 1). Wykonane obliczenia pozwoliły na wskazanie zalecanej...
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Torsional buckling and post-buckling of columns made of aluminium alloy
PublikacjaThe paper concerns torsional buckling and the initial post-buckling of axially compressed thin-walled aluminium alloy columns with bisymmetrical cross-section. It is assumed that the column material behaviour is described by the Ramberg–Osgood constitutive equation in non-linear elastic range. The stationary total energy principle is used to derive the governing non-linear differential equation. An approximate solution of the equation...
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Studies on solid phase microextraction-gas chromatographic determination of volatile chloroorganic pollutants in soil. badanie lotnych związków chloroorganicznych w glebie przy użyciu techniki mikroekstrakcji do fazy stacjonarnej i chromatografii gazowej.
PublikacjaLotne związki chloroorganiczne (VOXs) mogą być obecne w powietrzu, wodzie i glebie. Związki te mają właściwości kancerogenne, dlatego też ich ilość w środowisku powinna być monitorowana. W pracy przedstawiono badania nad możliwością zastosowania techniki izolacji i wzbogacania jaką jest mikroekstrakcja do fazy stacjonarnej, jej przydatność w analizie lotnych węglowodorów chloroorganicznych w różnych typach gleb z wykorzystaniem...
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Semantic Driven Table Understanding in Born-Digital Documents
PublikacjaThis paper presents a new approach to table understanding, suitable for born-digital PDF documents. Advance beyond the current state of the art in table understanding is provided by the proposed reverse MVC method, which takes advantage of only partial logic structure loss (degradation) in born-digital PDF documents, as opposed to unrecoverable loss (deterioration) taking place in scan based PDF documents.
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Sensitivity analysis of flexural and torsional buckling loads of laminated columns
PublikacjaThe paper concerns first order sensitivity analysis of flexural and torsional bucklin g loads of axiallycompressed thin-walled columns with bisymmetric or axisymmetric cross-section made of unidirectional fibre-reinforcedlaminate. The first variation of critical loads versus some variations of the column material properties and cross-sectionaldimensions is derived. Numerical examples dealing with simply supported I-columns are...
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Behaviour of deformed steel columns exposed to impact load during earthquakes - experimental study
PublikacjaIt has been observed during major earthquakes that the so called soft-storey failure of an upper floor of a structure results in large impact load acting on structural members of the lower storeys. It may further lead to progressive collapse of the whole structure substantially intensifying human and material losses. The aim of this paper is to investigate experimentally the behaviour of horizontally deformed columns (deformation...
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Birch sap concentrate as a potential modern food product
PublikacjaThis paper presents birch sap concentrate obtained by the reverse osmosis method. It is characterized by sweet taste, high content of minerals and no risk to consumers in terms of content of heavy metals standardized in the European Union food legislation. This beverage has all the features of a modern food product, i.e. it has an attractive taste, is obtained using new technology, meets the clean label requirements and can be...
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Modyfikacja połączenia dźwigara ze słupem w konstrukcji stalowej Terminalu T2 Portu Lotniczego w Gdańsku
PublikacjaW2015 r. ukończono rozbudowę Terminalu T2 Portu Lotniczego im. Lecha Wałęsy wGdańsku. Politechnika Gdańska pełniła nadzór naukowy nad rozbudową obiektu. Wykonano wiele analiz, których celem była weryfikacja pracy konstrukcji w fazach montażu oraz w stanie docelowym. Wnioski z przeprowadzonych badań doprowadziły do modyfikacji oparcia dźwigarów dachowych na stalowych słupach nośnych, z uwagi na stwierdzone lokalne przekroczenia...
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On the Mechanism of Electrochemical Oscilations in Three-Phase System Containing Nitrobenzene with Picric Acid as Liquid Membrane.O mechaniźmie oscylacji róznicy potencjału elektorchemicznego w trójfazowych układach zawierających nitrobenzen z kwasem pikrynowym jako membraną ciekłą.
PublikacjaPodano składowe różnicy potencjału elektrochemicznego między fazami wodnymi oscylatora z nitrobenzynową membraną ciekłą. Na tej podstawie oraz zmian stężeń składników układu w trakcie procesu zaproponowano mechanizm powstawania oscylacji w którym najważniejszą rolę odgrywają procesy adsorpcji/desorpcji surfaktantu na granicach faz.
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Application of polyethylene glycol-coated iron oxide nanoparticles for magnetic solid phase extraction of copper from seawater samples and its determination by graphite furnace atomic absorption spectrometry using response surface methodology for optimization of extraction
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Chemical Vapor Transport Route toward Black Phosphorus Nanobelts and Nanoribbons
PublikacjaChemical vapor transport (CVT) method is widely used for bulk black phosphorus (BP) fabrication. In this work, we demonstrate that CVT provides a route for the fabrication of BP nanoribbons and nanobelts. This method consists of a two-step procedure, including initial BP column growth using the CVT technique, followed by ultrasonic treatment and centrifugation. The obtained nanostructures preserve BP column dimensions, forming...
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Chemical Vapor Transport Route toward Black Phosphorus Nanobelts and Nanoribbons
PublikacjaChemical vapor transport (CVT) method is widely used for bulk black phosphorus (BP) fabrication. In this work, we demonstrate that CVT provides a route for the fabrication of BP nanoribbons and nanobelts. This method consists of a two-step procedure, including initial BP column growth using the CVT technique, followed by ultrasonic treatment and centrifugation. The obtained nanostructures preserve BP column dimensions, forming...
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Development and Validation of SPE-HPLC-MS/MS Method for Determining Cyclophosphamide in Surface Waters
PublikacjaA rapid and selective method for trace amounts determination of cyclophosphamide in surface water samples has been developed. A solid phase extraction SPE method for extraction and clean-up procedure has been optimized for determination by reversed-phase high-performance liquid chromatography with tandem mass spectrometry. The analyses proceed in the positive ion mode by means of the electrospray ionization method (ESI). Clean...
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Effect of Base-Connection Strength and Ductility on the Seismic Performance of Steel Moment-Resisting Frames
PublikacjaColumn-base connections in steel moment-resisting frames (SMFs) in seismic regions are commonly designed to develop the capacity of adjoining column with an intent to develop a plastic hinge in the column member, rather than in the connection (i.e., a strong-base design). Recent research has shown base connections to possess high ductility, indicating that this practice may be not only expensive but also unnecessary. This suggests...
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Engineering TADF, Mechanochromism, and Second Harmonic Up- conversion Properties in Regioisomeric Substitution Space
PublikacjaThis research article explores the distinct TADF efficiency of three donor-acceptor based regio-isomers: DPAOCN (ortho- isomer), DPAMCN (meta-isomer), and DPAPCN (para-isomer). DPAPCN exhibits maximum TADF efficiency in both solution and solid-state with an impressive reverse inter-system crossing (RISC) rate of ~ 106 s-1; the underlying cause being the minimum singlet-triplet splitting energy or ∆EST and maximum SOC (spin-orbit...
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Processing of point cloud data retrieved from terrestrial laser scanning for structural modeling by Finite Element Method
PublikacjaFinite Element Method is one most popular contemporary method of strength analysis. The method is an advanced method for solving differential equations, based on discretization, which means that area is divided into finite elements. Each finite element has a solution of the equation approximated by specific functions and performing the actual calculations only for nodes of this division. Finite Element Method is widely used in...
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Mikrofiltrowany koncentrat soku brzozowego jako innowacyjny, trwały środek spożywczy o wysokiej wartości odżywczej
PublikacjaIntroduction. The forest environment becomes an increasingly popular place of obtaining raw materials, and one of the most promising product is birch sap. The market for bottled birch sap in Poland is monotonous, relying exclusively on pasteurized, acidified and sweetened drinks. A chance to change this situation is to develop a birch sap concentrate obtained by reverse osmosis. It has a sweet taste desired by consumers and particularly...
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On the Characteristic Graph of a Discrete Symmetric Channel
PublikacjaWe present some characterizations of characteristic graphs of row and/or column symmetric channels. We also give a polynomial-time algorithm that decides whether there exists a discrete symmetric channel whose characteristic graph is equal to a given input graph. In addition, we show several applications of our results.
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Experimental and numerical study on deformed steel columns subjected to impact load during earthquakes
PublikacjaThe soft-storey failure is one of the most typical types of damage observed in buildings during earthquakes. The failure of an upper soft storey of a structure results in large impact load acting on the lower floors and if the resistance of the structural members of the lower storeys is not sufficient it may further lead to progressive collapse of the whole building. The aim of the present paper is to investigate the dynamic behaviour...
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Linkages between services and manufacturing as a new channel for GVC development: Evidence from CEE countries
PublikacjaThe goal of the paper is to verify a causal relationship between forward linkages from domestic services to manufacturing and the participation/position of a country in global value chains (GVCs) in selected Central and Eastern European economies. We observed a strong polarisation pattern: the Baltic countries along with the Czech Republic strengthen their positions and participation in GVCs by having a strong relationship between...
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Application of linear buckling sensitivity analysis to economic design of cylindrical steel silos composed of corrugated sheets and columns
PublikacjaThe paper deals with global stability of steel cylindrical silos composed of corrugated walls and vertical columns with loads imposed by a bulk solid following Eurocode 1. The optimum silo design with respect to the steel weight was based on a sensitivity analysis method. The changes of silo column profiles at each design step were performed by means of influence lines for the buckling load factor due to the unit column bending...
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Determination of nine high-intensity sweeteners in various foods by high-performance liquid chromatography with mass spectrometric detection
PublikacjaAn analytical procedure involving solid-phase extraction (SPE) and high-performance liquid chromatography-mass spectrometry has been developed for the determination of nine high-intensity sweeteners authorised in the EU; acesulfame-K (ACS-K), aspartame (ASP), alitame (ALI), cyclamate (CYC), dulcin (DUL), neohesperidin dihydrochalcone (NHDC), neotame (NEO), saccharin (SAC) and sucralose (SCL) in a variety of food samples (i.e. beverages,...
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Effect of initial imperfection on buckling of thin-walled I columns
PublikacjaEffects of initial geometrical imperfections on critical buckling loads of thin-walled I columns are investigated. Torsional and flexural buckling are taken into account. The column behaviour is described in accord to the theory of thin-walled beams with nondeformable cross-section. Some numerical examples and conclusions related to effects of imperfections on properties of the critical loads are presented.
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Influence of the Shear Cap Size and Stiffness on the Distribution of Shear Forces in Flat Slabs
PublikacjaThe scope of this paper is to investigate analytically and numerically the influence of shear cap size and stiffness on the distribution of shear forces in flat slabs in a slab–column-connections-reinforced concrete structure. The effect of support (shear cap) stiffness on the calculation of the length of the shear control perimeter according to the available methods is presented. Based on the analysis, the authors indicate in...
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Determination of carbonyl compounds in distilled alcoholic beverages using gas chromatography and head-space solid phase microextraction. Oznaczanie związków karbonylowych w napojach alkoholowych z użyciem chromatografii gazowej i mikroekstrakcji do fazy stacjonarnej z fazy nadpowierzchniowej
PublikacjaW pracy przedstawiono badania nad opracowaniem procedury oznaczania związków karbonylowych z użyciem mikroekstrakcji do fazy stacjonarnej w wersji analizy fazy nadpowierzchniowej (HS-SPME), chromatografii gazowej z detekcją wychwytu elektronów(GC-ECD) oraz derywatyzacji pentafluorobenzylohydroksyloaminą (PFBHA). Opisano wpływ parametrów: temperatury, mieszania, czasu ekspozycji włókna, dodatku soli, stężenia alkoholu. Opracowaną...
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Inżynieria odwrotna bazy paliw płynnych w Gdańsku
PublikacjaArtykuł prezentuje prace z zakresu pozyskania danych o zbiornikach bazy paliw płynnych w Gdańsku. Przedstawione rozwiązanie nie ogranicza się tylko do stworzenia (rejestracji) chmury punktów, ale jest próbą wskazania użycia naziemnego skaningu laserowego do stworzenia bazy informacji o bazie paliw – w tym głównie geometrii zbiorników. Autorzy prezentują proces inwentaryzacji, rejestrację chmury punktów oraz wskazują zasady tworzenia...
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The role of glucuronidation in drug resistance
PublikacjaThe final therapeutic effect of a drug candidate, which is directed to a specific molecular target strongly depends on its absorption, distribution, metabolism and excretion (ADME). The disruption of at least one element of ADME may result in serious drug resistance. In this work we described the role of one element of this resistance: phase II metabolism with UDP-glucuronosyltransferases (UGTs). UGT function is the transformation...
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Size-exclusion chromatography for the determination of the boiling point distribution of high-boiling petroleum fractions
PublikacjaThe paper describes a new procedure for the determination of boiling point distribution of high-boiling petroleum fractions using size exclusion chromatography with refractive index detector. Thus far, the determination of boiling range distribution by chromatography has been accomplished using simulated distillation with gas chromatography with the flame ionization detection. This study revealed that in spite of substantial differences...
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Excited-state proton transfer and geminate recombination in the molecular cage of β-cyclodextrin
PublikacjaExcited-state proton transfer and geminate recombination in aqueous heptakis(2,6-di-O-methyl)-β-cyclodextrin have been compared with those in water by monitoring the photoinduced prototropic tautomerization of 6-hydroxyquinoline, which occurs via forming anionic intermediate. Enol deprotonation decelerates by 18 times whereas its reverse process accelerates slightly with encapsulation. The imine protonation of the intermediate...
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Zastosowanie połączenia mikroekstrakcji do fazy stacjonarnej i chromatografii gazowej do oznaczania lotnych kwasów tłuszczowych w próbkach środowiskowych i pokrewnych=Application of combination of solid phase microextraction and gas chromatography for determination of volatile fatty acids in environmental and related samples
PublikacjaOznaczanie lotnych kwasów tłuszczowych (LKT) w próbkach środowiskowych wymaga najczęściej izolacji i wzbogacania analitów na etapie przygotowania próbek oraz zastosowania techniki o dużym potencjale separacyjnym i identyfikacyjnym na etapie oznaczeń końcowych. W pracy dokonano krytycznego przeglądu zastosowań wygodnej i często stosowanej techniki mikroekstrakcji do fazy stacjonarnej (SPME) w połączeniu z wysokosprawną techniką...
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Mobility and biodegradability of an imidazolium based ionic liquid in soil and soil amended with waste sewage sludge
PublikacjaSorption on solids and biodegradation are main phenomena that can mitigate the pollution of soil and water by ionic liquids (ILs). ILs sorbed on soil particles become immobilized (temporarily or permanently) which prevents them from spreading into deeper layers of soil or groundwater but which also makes them less bioavailable. In this study we attempt to examine if amendment of soil with waste sludge has a potential to mitigate...
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COMPUTER-AIDED CONSTRUCTION AT DESIGNING REINFORCED CONCRETE COLUMNS AS PER EC
PublikacjaThe article presents the author’s computer program for designing and dimensioning columns in reinforced concrete structures taking into account phenomena affecting their behaviour and information referring to design as per EC. The computer program was developed with the use of C++ programming language. The program guides the user through particular dimensioning stages: from introducing basic data such as dimensions, concrete...
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Distortional buckling of thin-walled columns of closed quadratic cross-section
PublikacjaThe elastic stability of axially compressed column related to the cross-section distortion is investigated. Two kinds of closed quadratic cross-sections are taken into consideration with internal walls and without it. The governing differential equation is derived with aid of the principle of stationary total potential energy. The critical loads for the simply supported columns are found in an analytical form and compared with...
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Electrochemical and in silico approaches for liver metabolic oxidation of antitumor-active triazoloacridinone C -1305
Publikacja5-Dimethylaminopropylamino-8-hydroxytriazoloacridinone (C-1305) is a promising antitumor compound developed in our laboratory. A better understanding of its metabolic transformations is still needed to explain the multidirectional mechanism of pharmacological action of triazoloacridinone derivatives at all. Thus, the aim of the current work was to predict oxidative pathways of C-1305 that would reflect its phase I metabolism. The...
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Stationary underwater channel experiment: Acoustic measurements and characteristics in the Bornholm area for model validations
PublikacjaThe underwater acoustical channel is time-variant, and even on small time scales there is often existing no ‘acoustical frozen ocean’. Popular is the use of WSSUS-channel transmission modeling (Wide-Sense Stationary Uncorrelated Scattering) for the stochastic description of bandpass signals in GSM mobile phones with moving participants; since this results in a halved number of model parameters. For underwater sound applications...