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Wyniki wyszukiwania dla: size exclusion chromatography
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Laser-Assisted Synthesis and Oxygen Generation of Nickel Nanoparticles
PublikacjaNowadays, more than ever, environmental awareness is being taken into account when it comes to the design of novel materials. Herein, the pathway to the creation of a colloid of spherical, almost purely metallic nickel nanoparticles (NPs) through pulsed laser ablation in ethanol is presented. A complex description of the colloid is provided through UV-vis spectroscopy and dynamic light scattering analysis, ensuring insight into...
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Guided waves for monitoring of plate structures with linear cracks of variable length
PublikacjaDamage occurring at the work of plate structures may grow to a considerable size. The joint action – the detection of a defect at the earliest possible stage, the monitoring of its growth and the determination of its critical size in the context of structural reliability allows optimizing the cost of the maintenance and repair of structural elements. Thus the development of monitoring systems for permanent observation of fault...
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The Role of a Software Product Manager in Various Business Environments
PublikacjaThe aim of the paper is to identify the role of the software product manager depending on the size of the company and the characteristics of the product they are working on. This has been achieved in cooperation with 15 experts from the IT industry. The companies were divided into 4 levels of size: micro-enterprises, small businesses, medium businesses and large enterprises. The characteristics of the products were divided into...
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Seminarium dyplomowe 2023_sem 8
Kursy OnlineSeminarium dyplomowe dotyczy zagadnień niezbędnych do opracowania projektu dyplomowego. Tematyka zajęć: Zasady sporządzania opisu technicznego (zakres w projekcie budowlanym a książeczka dyplomowa); Zagospodarowanie terenu (wytyczne wg normy, zakres, grubości linii itp. + przykładowe rysunki); Rzuty – zasady zapisu projektu budowlanego (wymiarowanie, grubości linii, stolarka, szrafy – wg normy, opisy itp. + przykładowe rysunki); Przekroje...
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Validated GC–MS method for determination of bisphenol a and its five analogues in dietary and nutritional supplements
PublikacjaBisphenol A (BPA) and its analogues showing structural and functional similarity to BPA are commonly applied in various industrial applications and thus are becoming ubiquitous in the environment. At the same time there is increasing scientific evidence that exposure to these chemicals may lead to adverse health effects in human and wildlife. In recent years dietary and nutritional supplements dedicated for athletes have become...
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Obtaining of coumarone-indene resins based on light fraction of coal tar 2. Coumarone-indene resins with epoxy groups
PublikacjaCoumarone-indene resins (CIR) with carboxy groups were synthesized via cooligomerization of unsaturated compounds presented in light fraction of coal tar and its fraction boiling out within 423–463 K with the addition of such industrial monomers as styrene, maleic anhydride, glycidyl methacrylate and methacrylic acid. 2,2`-Azobis(2-methylpropionitrile) in the form of 0.2 M solution in toluene was used as an initiator. The effect...
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The use of HPLC-Q-TOF-MS for comprehensive screening of drugs and psychoactive substances in hair samples and several “legal highs” products
PublikacjaNon-targeted screening of drugs present in herbal products, known as “legal high” drugs and in hair as a biological matrix commonly used in toxicological investigations was accomplished with the use of high pressure liquid chromatography coupled with quadrupole time-of-flight mass spectrometry (HPLC-Q-TOF-MS). In total, 25 and 14 therapeutical drugs and psychoactive substances/metabolites were detected in investigated hair samples...
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Molecular basis of the osmolyte effect on protein stability: a lesson from the mechanical unfolding of lysozyme
PublikacjaOsmolytes are a class of small organic molecules that shift the protein folding equilibrium. For this reason, they are accumulated by organisms under environmental stress, and find applications in biotechnology where proteins need to be stabilized or dissolved. However, despite years of research, debate continues over the exact mechanisms underpinning the stabilizing and denaturing effect of osmolytes. Here, we simulated the mechanical...
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Characteristics of volatile organic compounds emission profiles from hot road bitumens
PublikacjaA procedure for the investigation and comparison of volatile organic compounds (VOCs) emission profiles to the atmosphere from road bitumens with various degrees of oxidation is proposed. The procedure makes use of headspace analysis and gas chromatography with universal as well as selective detection, including gas chromatography–mass spectrometry (GC–MS). The studies revealed that so-called vacuum residue, which is the main component...
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New methodology for determination cationic surfactants in liquid environmental samples
PublikacjaBecause of their specific physical and chemical properties (e.g. amphiphilicity, solubility in polar and nonpolar liquids, ability to form micelles, adsorption at phase boundaries, low toxicity) surfactants (surface-active compounds) are widely applied in industry and in the household. As their applications are on a very large scale, it has become necessary to acquire a more detailed understanding of their environmental fate. Mainly,...
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Chemical and biological characterization of Ocimum basilicum L. phenolic extract and essential oil derived through ultrasound and microwave-assisted extraction techniques
PublikacjaPlant-derived bioactive molecules are increasingly utilized in food processing as natural additives, driven by a growing interest in healthier lifestyles. This trend has spurred industries to reformulate products to meet the demands of health-conscious consumers. This study investigates the phenolic extract and essential oil of O. basilicum L. obtained via ultrasound-assisted extraction and microwave-assisted extraction, respectively. Characterization...
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No Evidence for Sex-specificity in Vitamin C, E and Fatty Acid Content of Human Milk from Healthy Polish Mothers
PublikacjaHuman milk (HM) is a complex fluid that meets the nutritional needs of infants. Its composition idrfs associated with environmental, maternal, and foetal variables. It provides nutrients and bioactive substances, including cytokines, immunoglobulins, and constituents with antioxidative properties. Boys are reportedly more susceptible to oxidative stress. This study aimed to determine the relationship between infant sex and the...
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Polymeric metal‐containing ionic liquid sorbent coating for the determination of amines using headspace solid‐phase microextraction
PublikacjaThis study describes the design, synthesis, and application of polymeric ionic liquid sorbent coatings featuring nickel metal centers for the determination of volatile and semivolatile amines from water samples using headspace solidphase microextraction. The examined polymeric ionic liquid sorbent coatings were composed of two ionic liquid monomers (tetra(3-vinylimidazolium)nickel bis[(trifluoromethyl)sulfonyl]imide [Ni2+(VIM)4]...
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Development and validation of a GC–MS/MS method for the determination of 11 amphetamines and 34 synthetic cathinones in whole blood
PublikacjaPurpose Psychoactive compounds that contain a phenylethylamine structure (such as amphetamine-type stimulants and synthetic cathinones) are one of the major classes of stimulants on the recreational drug market. Approximately 670 new psychoactive substances (NPS) are monitored only in Europe; however, new psychoactive compounds are being developed for illicit trade each year. In this context, the development of new analytical procedures...
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Experimental data of galvanic electric cells measurements
Dane BadawczeInternal temperature of an electric cell can be measured and monitored using microsphere-based fiber-optic sensors with thin ALD ZnO coating. Their compact size will allow to integrate them easily and effectively within the electric cells. Utilization of presented sensors allows to detect, in real time, damages to the structure of the sensor head that...
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UAV Survey Images - 3D Model - Gdansk Church Pw. Św. Wojciecha - MP2
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Kościół Rzymskokatolicki Pw. Św. WojciechaLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: Circle (Point Of Interest) + Free flightTarget Product: 3D ModelDate: 02.04.2022Direct georeferencing: yesMetadata data: yes/GPSGCP: YESGCP Quality: RTKCamera Name:...
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UAV Survey Images - DTM- Gdansk Church Pw. Św. Wojciecha - MP2
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Kościół Rzymskokatolicki Pw. Św. WojciechaLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: Double GridTarget Product: Digital Terrain ModelDate: 02.04.2022Direct georeferencing: yesMetadata data: yes/GPSGCP: YESGCP Quality: RTKCamera Name: Hasselblad L1D-20cModel...
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UAV Survey Images - 3D Model - Allegory of science figure - on the tower of the main building of Gdansk University of Technology - MP1
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Golden figure at the top of the main bulding of Gdansk University Of TechnologyLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: CircleTarget Product: 3D ModelDate: 13.10.2018Direct georeferencing: yesMetadata data: yes/GPSGCP: NoGCP Quality: N/ACamera Name:...
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UAV Survey Images - 3D Model - Allegory of science figure - on the tower of the main building of Gdansk University of Technology - MP2
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Golden figure at the top of the main bulding of Gdansk University Of TechnologyLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: CircleTarget Product: 3D ModelDate: 08.11.2019Direct georeferencing: yesMetadata data: yes/GPSGCP: NoGCP Quality: N/ACamera Name:...
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UAV Survey Images - orthophotomap- Gdansk University of Technology campus photogrametry test field- MP2
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: The photogrametry test field within Gdansk University Of Technology CampusLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: Single GridTarget Product: 3D ModelDate: 17.05.2022Direct georeferencing: yesMetadata data: yes/GPSGCP: YESGCP Quality: RTKCamera Name:...
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Method of lines for physiologically structured models with diffusion
PublikacjaWe deal with a size-structured model with diffusion. Partial differential equations are approximated by a large system of ordinary differential equations. Due to a maximum principle for this approximation method its solutions preserve positivity and boundedness. We formulate theorems on stability of the method of lines and provide suitable numerical experiments.
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Informator dotykowy na ciągach pieszo-rowerowych
WynalazkiPrzedmiotem wynalazku jest informator dotykowy do pozyskiwania informacji przez osoby z problemami ze wzrokiem na ciągach pieszo-rowerowych. Zastosowanie ma doprowadzić do zwiększenia bezpieczeństwa użytkowników poprzez ułatwienie rozpoznania kierunku przebiegu ciągów.
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Assessment of usefulness of different tacks in laparoscopic ventral hernia repair
PublikacjaLaparoscopic ventral hernia repair is becoming a popular technique with good results and fast postoperative recovery. The mesh is placed directly under the peritoneum and anchored with transabdominal sutures and tacks. However, the ideal size of the mesh covering the hernia orifice is know, nor the ideal type or amount of tacks has to be described.
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Rapid multi-objective design optimization of miniaturized impedance transformer by Pareto front exploration
PublikacjaFast multi-objective optimization of compact impedance transformer is discussed. A set of alternative designs representing possible trade-offs between conflicting design criteria, i.e., electrical performance (here, wideband matching) and the structure size, is obtained through Pareto front exploration by means of surrogate-assisted methods.
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Analiza Matematyczna 1 MAT 1001/1
Kursy OnlineAnaliza Matematyczna 1 semestr 1 kod MAT 1001/1
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A Comparability of Renal Length and Volume Measurements in MRI and Ultrasound in Children
PublikacjaIntroduction: Despite the significant increase in use of magnetic resonance imaging (MRI) in children, there is still a lack of normal reference values of renal size in this method and reference values are being interpolated from the ultrasound (US) studies. The study provides comparative analysis of agreement in renal length and volume measurements between MRI and ultrasound. Materials and Methods: Ninety-three children with a...
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Effect of Thermal Treatment of Birch Wood by Saturated Water Vapor on Granulometric Composition of Chips from Sawing and Milling Processes from the Point of View of Its Processing to Composites
PublikacjaThe goal of this work is to investigate the impact of thermal modification of birch wood with saturated steam on the particle size distribution of the sawing and milling process. Birch wood (Betula pendula Roth) is an excellent source to produce plywood boards. Wastes from mechanical processing of birch wood are suitable to produce composite materials. Granulometric analyses of chips from sawing processes on the PRW 15M frame saw,...
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Probabilistic seismic assessment of RC box-girder highway bridges with unequal-height piers subjected to earthquake-induced pounding
PublikacjaThis paper uses the probabilistic seismic assessment to study the effects of pounding and irregularity on the seismic behavior of typical concrete box-girder bridges with four levels of altitudinal irregularity. To extend the results for all bridges in the same class, uncertainty related to the earthquake, structural geometries, and materials are considered. Pounding is likely to take place in two cases: the first one concerns...
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Narzędzie wiertnicze
WynalazkiCelem projektu jest wprowadzenie na rynek nowego urządzenia otworowego umożliwi optymalizację geometrii odwiertu tuż przed operacją cementowania. Doprowadzi to do znacznej poprawy dokładności i jakości cementowania, dzięki czemu zmniejszy się ryzyko skażenia środowiska i minimalizacji kosztów pozyskiwania surowca.Narzędzie to wytwarzane będzie w 5 skalowanych rozmiarach w zależności od średnicy cementowanej rury okładzinowej.
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Determination of impurities in pharmaceutical products using LC-MS
PublikacjaPharmaceutical products can be contaminated by residues of solvents, reagents (used for the synthesis) or degradation products. Impurities in drug may pose a risk to human health and life, therefore analysis and identification of impurities in pharmaceutical products is veryimportant and inevitable.High performance liquid chromatography coupled with mass spectrometry (MS) is very useful technique for identification impurities in...
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Exploration of optical fibres as a carrier for new benzene and toluene matrix-free reference materials
PublikacjaTo meet high expectations concerning precision and accuracy of reference materials, preparation of matrixfree reference materials using thermal decomposition-gas chromatography-mass spectrometry (TD-GC-MS) was proposed in this study. In the paper, the results obtained in preparation of the new reference materials for benzene and toluene are presented, based on the thermal decomposition technique of compounds chemically bound to...
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Synergistic Effects of Bitumen Plasticization and Microwave Treatment on Short-Term Devulcanization of Ground Tire Rubber
PublikacjaGround tire rubber (GTR) was mechano-chemically modified with road bitumen 160/220 and subsequently treated using a microwave radiation. The combined impact of bitumen 160/220 content and microwave treatment on short-term devulcanization of GTR was studied by thermal camera, wavelength dispersive X-ray fluorescence spectrometry (WD-XRF), static headspace, and gas chromatography-mass spectrometry (SHS-GC-MS), thermogravimetric analysis...
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The difficulties in polybrominated diphenyl ethers identification by GC-EI-MS technique
PublikacjaAwareness about the harmful effects of brominated flame retardants on living organisms increases mainly due to link their presence in the human environment with health disorders. Therefore is a need to conduct research aimed at content control of these chemicals in the environment. Recent improvements in injection techniques and mass spectrometer ionization methods have led to a variety of options to determine PBDEs in environmental...
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Electroelastic biaxial compression of nanoplates considering piezoelectric effects
PublikacjaIn the present theoretical work, it is assumed that a piezoelectric nanoplate is connected to the voltage meter which voltages have resulted from deformation of the plate due to in-plane compressive forces whether they are critical buckling loads or arbitrary forces. In order to derive governing equations, a simplified four-variable shear deformation plate theory has been employed using Hamilton’s principle and Von-Kármán...
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Coplanar Waveguide-Fed Broadband Microwave Devices with (or without) a Thin Dielectric Substrate for Use in Flexible Electronic Systems
PublikacjaTwo examples of microwave devices, fed by a coplanar waveguide and realized on a thin substrate (or without such a substrate), are employed to investigate the influence of devices’ curvatures and the proximity of different materials on their parameters. To perform the tests, a broadband antenna and a low-pass filter are chosen. A feeding coplanar waveguide is realized on a dielectric material brick attached to an SMA connector...
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Time versus space trade-offs for randezvous in trees
PublikacjaTwo identical (anonymous) mobile agents start from arbitrary nodes of an unknown tree and have to meet at some node. Agents move in synchronous rounds: in each round an agent can either stay at the current node or move to one of its neighbors. We consider deterministic algorithms for this rendezvous task. The main result of this paper is a tight trade-off between the optimal time of completing rendezvous and the size of memory...
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Low-cost multi-objective design of compact microwave structures using domain patching
PublikacjaA good compromise between size and electrical performance is an important design consideration for compact microwave structures. Comprehensive information about size/performance trade-offs can be obtained through multi-objective optimization. Due to considerable electromagnetic (EM) cross-couplings in highly compressed layouts, the design process has to be conducted at the level of high-fidelity EM analysis which is computationally...
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Impact damage in SiO2 nanoparticle enhanced epoxy – Carbon fibre composites
PublikacjaLow velocity impact behaviour of nano-SiO2 enhanced carbon fibre/epoxy composites for naval applications is reported. Epoxy resin matrix was enhanced by 1- 8 wt% SiO2 nanoparticles, based on industrial surface-modified nanosilica. Impact parameters: force, deformation, energy, damage size were recorded. The most pronounced effect was damage size decrease; e.g. ∼28% recorded by infrared thermography and X-ray computed radiography...
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Temperature-dependent structure-property modeling of viscosity for ionic liquids
PublikacjaIn this paper we present the methodology for assessing the ionic liquids' viscosity at six temperature points (25, 35, 45, 50, 60 and 70 [C]), which utilizes only the in silico approach. The main idea of such assessment is based on the "correction equation" describing the correlation between experimentally measured viscosity and theoretically derived density (calculated with use of molecular mechanics), given at 6 different temperature...
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Au nanoparticles identifiction with the use of AFM Volta potential mapping
Dane BadawczeThe specific physical, chemical and electrochemical electrical properties of gold nanoparticles have led to their extensive use as high-performance chemical and biochemical sensors. The described properties relate to surface plasmon resonance, fluorescence quenching or enhancement, high electrical conductivity and light scattering. The described nanoparticles...
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UAV Survey Images - orthophotomap - Gdynia Chwaszczyno - PH4 - AGL 50 m
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Parking place near by Gdynia Chwaszczyno district Location: Gdynia, Pomerania, PolandDrone type: DJI Phantom 4 ProFlight plan: Single GridTarget Product: OrthophotoDate: 11.07.2019Direct georeferencing: yesMetadata data: yes/GPSGCP: Yes - Description and position includedGCP Quality:...
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UAV Survey Images - orthophotomap - Gdynia Container Terminal Day Light- MP1
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Parking place near by Gdynia Container Terminal - day light photosLocation: Gdynia, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Single GridTarget Product: OrthophotoDate: 15.10.2020Direct georeferencing: yesMetadata data: yes/GPSGCP: Yes - Description and position includedGCP...
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UAV Survey Images - orthophotomap - Gdynia Container Terminal Day Light- MP2
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Parking place near by Gdynia Container Terminal - day light photosLocation: Gdynia, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: Single GridTarget Product: OrthophotoDate: 15.10.2020Direct georeferencing: yesMetadata data: yes/GPSGCP: Yes - Description and position includedGCP...
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UAV Survey Images - orthophotomap - Gdynia Chwaszczyno - MP1 - AGL 50 m
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Parking place near by Gdynia Chwaszczyno district Location: Gdynia, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Single GridTarget Product: OrthophotoDate: 11.07.2019Direct georeferencing: yesMetadata data: yes/GPSGCP: Yes - Description and position includedGCP Quality:...
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UAV Survey Images - orthophotomap - Gdynia Container Terminal Night Time- MP2
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Parking place near by Gdynia Container Terminal - night artificial photosLocation: Gdynia, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: Single GridTarget Product: OrthophotoDate: 14.10.2020Direct georeferencing: yesMetadata data: yes/GPSGCP: Yes - Description and position...
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UAV Survey Images - orthophotomap - Klodno Lake - MP1
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Klodno Lake shore lineLocation: Zawory, Kartuskie District, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Single Grid + Obligue imagesTarget Product: OrthophotoDate: 05.08.2018Direct georeferencing: yesMetadata data: yes/GPSGCP: Yes - Description and position includedGCP...
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UAV Survey Images - orthophotomap - Gdynia Chwaszczyno - MP1 - AGL 100 m
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Parking place near by Gdynia Chwaszczyno district Location: Gdynia, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Single GridTarget Product: OrthophotoDate: 11.07.2019Direct georeferencing: yesMetadata data: yes/GPSGCP: Yes - Description and position includedGCP Quality:...
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UAV Survey Images - DEM - Garbage Dump - MP1
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: A garbage dump near by Wladyslawowo cityLocation: Wladyslawowo, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Single GridTarget Product: DEMDate: 14.03.2020Direct georeferencing: yesMetadata data: yes/GPSGCP: Yes - Description and position includedGCP Quality: GNSS RTKCamera...
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UAV Survey Images - orthophotomap - Klodno Lake Zawory Bay - MP1
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Klodno Lake shore lineLocation: Zawory, Kartuskie District, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Single Grid + Obligue imagesTarget Product: OrthophotoDate: 11.08.2019Direct georeferencing: yesMetadata data: yes/GPSGCP: Yes - Description and position includedGCP...
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UAV Survey Images - orthophotomap - Oslonino Shore Line - MP1
Dane BadawczeDataset description: Raw images from photogrammetric survey. Object: Oslonino (sea) shore lineLocation: Oslonino, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Single Grid @ AGL 50m and Single Grid @AGL 100mTarget Product: OrthophotoDate: 02.08.2018Direct georeferencing: yesMetadata data: yes/GPSGCP: noGCP Quality: N/aCamera Name: DJI FC220Model...