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Wyniki wyszukiwania dla: cdw
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Biomass estimation using a length-weight relationship in beetle larvae (Coleoptera: Aphodiidae, Histeridae, Hydrophilidae, Staphylinidae) obtained from cow dung
PublikacjaThis research enabled the relationship between length and dry body mass to be determined for 158 beetle larvaetaken from cow dung in north-eastern Poland. The larvae were divided into three morphological types, for which the power and linear function of the body length-weight relationship were determined. The linear regression equation characterizes the relationship between body weight and...
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Quantum and carbon dots conjugated molecularly imprinted polymers as advanced nanomaterials for selective recognition of analytes in environmental, food and biomedical applications
PublikacjaSamples with complex matrix analyzed during explanation of pathogenesis of various diseases and food or environmental monitoring request advanced analytical and instrumental devices. Among the materials used for described purposes, quantum (QDs) or carbon dots (CDs) layered by molecularly imprinted polymer (MIP) shells have gained widespread attention. Unique optical and physicochemical properties of QDs/CDs together with high...
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Simultaneous voltammetric determination of Cd2+, Pb2+, and Cu2+ ions captured by Fe3O4@SiO2 core-shell nanostructures of various outer amino chain length
PublikacjaIn the present study, we examined a novel functionalised magnetic nanoparticles Fe3O4@SiO2-Nn as a nano adsorbent for binding of Cd2+, Pb2+, Cu2+ ions in an aqueous solution. First, we obtained the nanoparticles functionalised with various carbon chains containing different number of amino groups: (3-amino)propyltriethoxysilane (Fe3O4@SiO2-N1), N-(2-aminoethyl)-3-aminopropyltrimethoxysilane (Fe3O4@SiO2-N2) and N1-(3-trimethoxysilylpropyl)diethylenetriamine...
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Retention of selected heavy metals: Cd, Cu, Pb in a hybrid wetland system
PublikacjaWykonano bilans wybranych metali ciężkich Cd2+, Pb2+, Cu2+ dla pilotowej oczyszczalni hydrofitowej w Przywidzu k. Gdańska. Wykazano m.i. że sorpcja była głównym mechanizmem odpowiedzialnym za usuwanie tych pierwiastków ze ścieków.
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Analysis of distance measurement errors in CW FM sonar with MLS code modulation
PublikacjaAlthough used in the classic silent sonar, the CW FM sounding signal has a major flaw which is its inaccuracy in determining the distance to a target. The authors of the article have developed a concept of silent sonar using frequency modulation signals switched by pseudorandom codes, already discussed in their previous work. This article presents a detailed analysis of errors in CW FM sonar with pseudo-random sequence code modulation...
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Measurement of distance, velocity and angle of arrival using FMCW-CW combined waveform
PublikacjaA procedure of tacking small flying object based on a general principle of FMCW and Doppler radar is presented. In order to increase measurement range, this technique uses active signal source on the moving object. For simultaneous measurements of distance, radial velocity and direction (AoA) as well as simplified synchronization a combined FMCW-CW waveform is proposed. The presented measurement system was realized and verified...
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Induction of Secreted Human Immunodeficiency Virus Type 1 (HIV-1) Resistance Factors in CD4-Positive T Lymphocytes by Attenuated HIV-1 Infection
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Thermal treatment of montmorillonite modified with Cd[SC(NH2)2]42+ from two polymorphic salts
PublikacjaMontmorillonite(MMT)/CdS nanocomposites can be obtained using simple ionic exchange between Na(I)-MMT and Cd[SC(NH2)2]42+∙2NO3. The resulting products may be annealed to give (MMT)/CdS nanocomposites as it was proved by XRD analysis.
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Hardening of (Pb,Cd)Te Crystal Lattice with an Increasing CdTe Content in the Solid Solution
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Metal tolerance and Cd phytoremoval ability in Pisum sativum grown in spiked nutrient solution
PublikacjaIn the presented study, the effects of cadmium (Cd) stress and silicon (Si) supplementation on the pea plant (Pisum sativum L.) were investigated. The tendency to accumulate cadmium in the relevant morphological parts of the plant (roots and shoots respectively)—bioaccumulation, the transfer of this element in the plant (translocation) and the physiological parameters of the plant through...
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Land development and forms of heavy metals occurrence (zn, cd, pb) in polish rivers
PublikacjaEkosystemy rzeczne podlegają intensywnej antropopresji. Metale ciężkie występujące w glebie i osadach dennych w różnych formach specjacyjnych mają istotny wpływ na wtórne zanieczyszczenie wody ze względu na takie procesy jak migracja, akumulacja i biowzbogacanie.Przedmiotem badań były próbki gleby, osadów dennych oraz wody pobrane z różnych rzek z południowej części województwa świętokrzyskiego. W trakcie badań próbek wykorzystano...
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Oznaczenie ilości wodoru dyfundującego w stopiwie drutów proszkowych Kobelco DW-A70L
PublikacjaNa zlecenie firmy VELTECH Konrad Matolicz wykonano pomiary ilości wodoru dyfundującego w stopiwie dwóch wytopów drutu proszkowego gatunku Kobelco DW-A70L. Ze względu na klasę badanego drutu (H5) pomiary zrealizowano metodą rtęciową, która jest zalecana przez właściwą normę regulującą badania nawodorowania stopiwa spoiw do spawania. Wyniki pomiarów ilości wodoru dyfundującego w stopiwie drutów proszkowych gatunku Kobelco DW-A70L...
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Wwpływ temperatury suszenia osadów ściekowych na specjację metali ciężkich (Zn, Cu, Cd, Pb) = Influence of thermal drying temperature on heavy metal (Zn, Cu, Cd, Pb) speciation in sewage sludge
PublikacjaPrzedstawiono wpływ temperatury suszenia osadów ściekowych na zmiany specjacji metali ciężkich oraz określono stopień mobilności metali ciężkich w aspekcie ich późniejszego zagospodarowania. Ekstrakcja sekwencyjna metali ciężkich została wykonana wg schematu Tessier'a.
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Species-specific Cd-detoxification mechanisms in lumbricid earthworms Eisenia andrei, Eisenia fetida and their hybrids
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Cadmium complex possessing simultaneously silanethiolato- and dithiocarbamato-ligands. A novel single-source precursor of cadmium sulfide
PublikacjaThermal decomposition of suitable coordination compounds may be used as efficient route for fabrication of semiconducting layers. A new potential CdS precursor—a cadmium complex with all-sulfur Cd-coordination sphere [Cd{l-SSi(OBut)3}(S2CNC4H8)]2 (1) —has been prepared and its properties are investigated. The complex was obtained in the reaction between dimeric bis(tri-tert-butoxysilanethiolato) cadmium(II) [Cd{SSi(OBut)3}2]2 and...
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Effect of chemical structure on complexation efficiency of aromatic drugs with cyclodextrins: The example of dibenzazepine derivatives
PublikacjaIt is widely believed that the hydrophobic effect governs the binding of guest molecules to cyclodextrins (CDs). However, it is also known that high hydrophobicity of guest molecules does not always translate to the formation of stable inclusion complexes with CDs. Indeed, a plethora of other factors can play a role in the efficiency of guest–CD interactions, rendering structure-based prediction of the complexation efficiency with...
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Inelastic X-Ray Scattering Studies of Phonon Dispersion in PbTe and (Pb,Cd)Te Solid Solution
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Zaufanie w zespole badawczym – studium przypadku (projekt CD NIWA realizowany na Politechnice Gdańskiej)
PublikacjaArtykuł dotyczy tematyki klimatu pracy zespołowej, ze szczególnym uwzględnieniem zaufania w zespole jako czynnika warunkującego zaangażowanie, efektywność i innowacyjność zespołu. Przeanalizowano znaczenie oraz wymiary zaufania w zespole badawczym na podstawie koncepcji International Team Trust Indicator, czyli dziesięciowymiarowego modelu zaufania. Celem artykułu jest analiza klimatu współpracy i poziomu zaufania w interdyscyplinarnym...
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Investigating the potential influence of biochar and traditional organic amendments on the bioavailability and transfer of Cd in the soil–plant system
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New nanoadsorbent based on magnetic iron oxide containing 1,4,7,10-tetraazacyclododecane in outer chain (Fe3O4@SiO2-cyclen) for adsorption and removal of selected heavy metal ions Cd2+, Pb2+, Cu2+
PublikacjaMagnetic Fe3O4@SiO2-cyclen nanoparticles were prepared and used as adsorbent for Cd2+, Pb2+ and Cu2+ from aqueous solution removal process controlled with differential pulse anodic stripping voltammetry (DPASV) and hanging mercury drop electrode (HDME). Nanomaterial was synthesised in three-step process co-precipitation of Fe3O4 core, coating with silane and N-(3-(triethoxysilyl)propyl)-1,4,7,10-tetraazacyclododecane-1-carboxamide...
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Stimulated by cyclodextrins high yield synthesis of azocrown analogues comprising pyrrole or imidazole residues
PublikacjaThe influence of cyclodextrins (CDs) on the formation of azocrown ethers comprising pyrrole, imidazole and substituted imidazole has been studied. Pyrrole, imidazole, 2-methyl-, 4-methyl- and 4-phenylimidazole were coupled with bisdiazonium salts derived from bis-1,5-(2-aminophenoxy)-3-oxapentane or bis-1,8-(2-aminophenoxy)-3,6-dioxaoctane to form macrocyclic compounds with two azo units. The syntheses were performed under standard...
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Superior synergy of g-C3N4/Cd compounds and Al-MOF-derived nanoporous carbon for photocatalytic hydrogen evolution
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Zn(II) and Cd(II) coordination polymers with tri-tert-butoxysilanethiol and bipyridines. Synthesis, crystal structure and spectroscopy
PublikacjaTrzy nowe silanotiolany cynku(II) I kadmu(II) [Zn{SSi(OtBu)3}2(μ-bpea) •CH3CN]n 1, [Cd{SSi(OtBu)3}2(μ -bpea) •2CHCl3]n 2 oraz [Cd{SSi(OtBu)3}2(μ -bpey)•C7H8]n 3 otrzymane z użyciem pochodnych bipirydylu [bpea = 1,2-bis(4-pyridyl)etan and bpey = 1,2-bis(4-pyridyl)etylen] zostały zsyntetyzowane i strutkualnie scharakteryzowane przy użyciu rentgenografii strukturalnej XRD. Ich budowa krystaliczna została dodatkowo potwierdzona przy...
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One dimensional coordination polymers generated from Cd(II) tri-tert-butoxysilanethiolates and flexible aliphatic diamines.
PublikacjaPraca ta dotyczy chemii koordynacyjnej tri-tert-butoksysilanotiolanu kadmu(II) z diaminami alifatycznymi. Reakcja dwucentowego [Cd{SSi(OtBu)3}2]2 z poszczególnymi diaminami pozwala otrzymać pięć nowych obojętnych jednowymiarowych polimerów koordynacyjnych o różnej topologii łańcuchów [Cd{SSi(OtBu)3}2(μ-C4H12N2)(CH3OH)]n (1), [Cd{SSi(OtBu)3}2(μ-C5H14N2)(CH3OH)]n (2) [Cd{SSi(OtBu)3}2(μ-C6H16N2)(CH3OH)]n (3), [Cd{SSi(OtBu)3}2(μ-C7H18N2)]n...
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Comparison of the coordination geometries of Zn(II) and Cd(II) ions in complexes with water, methanol and bulky aryloxysilanethiolate ligands
PublikacjaZinc and cadmium complexes containing silanethiolate anions and methanol or water were synthesized and characterized by X-ray diffraction, FT-IR and NMR spectroscopy, and DFT calculations. Contrary to zinc, the cadmium ion utilizes very weak donors to complete its coordination sphere; it forms contacts to phenyl rings of the silanethiolate ligand. Two zinc analogs of the general formula [Zn{SSi(OAr)3}2(L)2] where L = CH3OH (2)...
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The influence of Nigella sativa essential oil on proliferation, activation, and apoptosis of human T lymphocytes in vitro
PublikacjaIn previous work, we tested the immunomodulatory effect of Nigella sativa (NS) fatty oil. Our results demonstrated that unrefined, obtained by cold pressing black cumin seed oil inhibited lymphocytes’ proliferation and induced their apoptosis in a dose-dependent manner. In this study, we examined the immunomodulatory properties of essential oil (EO) obtained from the NS seeds by hydrodistillation and its two main constituents:...
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Evolution of charge density wave order in continuous solid solutions Lu(Ni1-xCox)C2
PublikacjaPseudo-ternary solid solutions, Lu(Ni1-xCox)C2 (0 ≤ x ≤ 1), were studied by means of powder X-ray diffraction, differential thermal analysis as well as electrical resistivity and heat capacity measurements. The crystal structure of the Lu(Ni1-xCox)C2 series, as investigated by means of X-ray powder diffraction, is of structure type CeNiC2, space group Amm2, Pearson symbol oS8. The structural analysis reveals a non-monotonous evolution,...
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Freshwater Ulva (Chlorophyta) as a bioaccumulator of selected heavy metals (Cd, Ni and Pb) and alkaline earth metals (Ca and Mg)
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Binuclear Co(II), Zn(II) and Cd(II) tri-tert-butoxysilanethiolates. Synthesis, crystal structure and spectroscopic studies.
PublikacjaA series of Co(II), Zn(II) and Cd(II) complexes have been synthesized in reaction of respective metal tri-tert-butoxysilanethiolates with pyrazine 1 and 2 and 1,2-bis(2-pyridyl)ethylene 3–5. All compounds have been characterized by single-crystal X-ray structure determination, elemental analysis, FT-IR and thermogravimetry. Obtained complexes are bimetallic with the formula of [M{SSi(OtBu)3}2(μ-L)]2 and metal ions bridged by N,N′-spacer....
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Structural, spectral and magnetic properties of Ni(II), Co(II) and Cd(II) compounds with imidazole derivatives and silanethiolate ligands
PublikacjaA series of new metal heteroleptic complexes have been obtained in simple reactions of 1-(3-aminopropyl)-imidazole (api) and 1,4-bis(imidazol-1-yl)-butane (bbi) ligands with metal silanethiolates or acetylacetonates. The obtained complexes are the coordination polymers [Ni{SSi(tBuO)3}2(μ-api)]n1, [Co{SSi(tBuO)3}2(μ-api)]n2, [Cd{SSi(tBuO)3}2(μ-api)·2CH3OH]n3, [Cd{SSi(tBuO)3}2(μ-bbi)·CHCl3]n4 and the dimer [Co{SSi(tBuO)3}2(μ-bbi)·3CH3OH]25....
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Enrichment of Bi-Be-Mo-Cd-Pb-Nb-Ga, REEs and Y in the Permian coals of the Huainan Coalfield, Anhui, China
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Magnetism and charge density waves in RNiC2(R=Ce,Pr,Nd)
PublikacjaWe have compared the magnetic, transport, galvanomagnetic, and specific-heat properties of CeNiC2, PrNiC2, and NdNiC2 to study the interplay between charge density waves (CDW) and magnetism in these compounds. The negative magnetoresistance in NdNiC2 is discussed in terms of the partial destruction of charge density waves and an irreversible phase transition stabilized by the field-induced ferromagnetic transformation is reported....
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Arginine-, d-arginine-vasopressin, and their inverso analogues in micellar and liposomic models of cell membrane: CD, NMR, and molecular dynamics studies
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Facilitated transport of Zn(II), Cd(II) and Pb(II) across polymer inclusion membranes doped with imidazole azocrown ethers
PublikacjaZbadano transport jonów Pb(II), Cd(II) i Zn(II) przez polimerowe membrany inkluzyjne (PIM) przy użyciu imidazolowych azokoron. Badanie prowadzono dla wodnych roztworów azotanów metali o c(Me)=0,001M i pH=5,0. Polimerowe membrany inkluzyjne otrzymywano z trójoctanu celulozy (nośnik), plastyfikatora i jonoforu (jeden z imidazolowych eterów koronowych z ugrupowaniem azowym). Badane azokorony różniły sięmiejscem podstawienia imidazolu...
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Efficiency of ozonation process with calcium peroxide in removing heavy metals (Pb, Cu, Zn, Ni, Cd) from aqueous solutions
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Tetra-n-butylammonium iodido(pyrrolidine-1-carbodithioato-κ2S,S')(tris-tert-butoxysilane-thiolato-κS)cadmate(II)
PublikacjaTytułowy (N,N tetrametylenoditiokarbaminiano)(tri-tert-butoksysilanotiolano)jodokadmian tetra-n-butyloamoniowy krystalizuje w układzie jednoskośnym, w grupie P21/c. W anionie [Cd{SSi(OtBu)3}(S2CNC4H9)I]() wyróżnić można centralny rdzeń o składzie CdS3I. Ułożenie atomów donorowych może być, w pierwszym przybliżeniu, opisane jako zniekształcony (ze względu na obecność S,S'-chelatującego liganda) tetraedr z największym kątem S1-Cd1-S2...
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Sensitive Determination of Cd in Small-Volume Samples by Miniaturized Liquid Drop Anode Atmospheric Pressure Glow Discharge Optical Emission Spectrometry
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Wykorzystanie kapusty białej (brassica oleracea var. capitata) do fitoekstrakcji metali ciężkich (zn, cd, cu, pb) z gleby*
PublikacjaGatunki roślin z rodziny Brassicaceae uważane są za przydatne w fitoremediacjimetali ciężkich z gleby. Przeprowadzone badania mają na celu potwierdzenie zasadności wykorzystaniakapusty białej, odmiany 'Kamienna Głowa' do fitoekstrakcji Zn, Cd, Cu, Pb. Poziomwybranych metali badano w glebie oraz liściach i głąbach kapusty uprawianej na tych glebach,pochodzących z upraw wazonowych (Kraków) oraz polowych (Czapielsk). Zawartość metaliciężkich...
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Corncob-supported calcium oxide nanoparticles from hen eggshells for cadmium (Cd-II) removal from aqueous solutions; Synthesis and characterization
PublikacjaThis study investigated the efficient removal of cadmium ions from aqueous solutions using calcium oxide nanoparticles (CaO NPs) synthesized from waste hen eggshells using a Sol-gel method and supported on corncob bio-adsorbent. The synthesized CaO NPs were characterized using FT-IR, XRD, specific surface area, and TGA. Batch adsorption experiments were conducted to examine the influence of process parameters such as adsorbent...
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Reply to “Enrichment of Bi-Be-Mo-Cd-Pb-Nb-Ga, REEs and Y in the Permian coals of the Huainan Coalfield, Anhui, China: Discussion”
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A comparative study of sequential extraction methods for identification of trace elements fractions (Cr, Ni, Pb, Cd) in urban soils from several parks
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Bioaccumulation of alkaline soil metals (Ca, Mg) and heavy metals (Cd, Ni, Pb) patterns expressed by freshwater species of Ulva (Wielkopolska, Poland)
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The Arctic mutation alters helix length and type in the 11–28 β-amyloid peptide monomer—CD, NMR and MD studies in an SDS micelle
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Facilitated transport of Zn(II), Cd(II) and Pb(II) ions trough polymer inclusion membranes with calix[4]-crown-6 derivaties
PublikacjaBadano transport mieszaniny równomolowych ilości jonów Zn(II), Cd(II) i Pb(II)z wodnej fazy azotanowej (cMe=0,001M) przez polimerowe membrany inkluzyjne(PIM) zawierające pochodne kaliks[4]korony-6 jako nośniki jonów. Badany był wpływ różnych podstawników na wydajność procesu. Selektywność transportu przez membrany zawierające jonofory 4 i 5 malała w kolejności Pb(II), Zn(II), Cd(II), natomiast z jonoforem 3 Pb(II), Zn(II)Cd(II)....
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Studies on removal of Zn(II), Cd(II) and Pb(II) ions in polymer inclusion membrane transport with calix[4]-crown-6 derivatives
PublikacjaZbadano selektywność procesu wydzielania jonów cynku(II), kadmu(II) i ołowiu(II) z wodnych roztworów azotanowych zawierających równomolową mieszaninę tych trzech metali (cMe= 0,01 M) w procesie transportu przez polimerowe membrany inkluzyjne (PIM) przy użyciu w roli przenośników jonów pochodnych kaliks[4]-korony-6. Membrany typu PIM syntezowano z trójoctanu celulozy (nośnik), eteru o?nitrofenylopentylowego (pastyfikator) i pochodnych...
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Exploring novel Cd(ii) complexes with 5-methyl-4-imidazolecarboxaldehyde: synthesis, structure, computational insights, and affinity to DNA through switchSense methodology
PublikacjaA series of four Cd(II) complexes with 5-methyl-4-imidazolecarboxaldehyde (L) with different inorganic anions within or outside the coordination sphere of general formula: [CdCl2 L2 ] (1), [CdBr2 L 2] (2), [CdI2L 2] (3), and [CdL4 ](PF6 )2 ·3H2 O (4) was synthesized through one-step and two-step reactions, respectively. All complexes were obtained as colorless crystals without the need for recrystallization and exhibited solubi- lity...
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Influence of Cd(II), Cr(VI) and Fe(III) on early steps of deetiolation process in wheat: fluorescence spectral changes of protochlorophyllide and newly formed chlorophyllide
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Coordination complexes of Mn(II), Co(II), Ni(II), Zn(II) and Cd(II) with histaminol – Crystal structures and formation constants in aqueous solution
PublikacjaStability constants were determined for a series of coordination complexes of Mn(II), Co(II), Ni(II), Zn(II) and Cd(II) with histaminol in aqueous solution. The tendency of histaminol to form chelate complexes has been confirmed by the isolation of several complex species in the monocrystalline form and determination of their molecular structures.
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Bamboo-biochar and hydrothermally treated-coal mediated geochemical speciation, transformation and uptake of Cd, Cr, and Pb in a polymetal(iod)s-contaminated mine soil
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Flowing Liquid Anode Atmospheric Pressure Glow Discharge as an Excitation Source for Optical Emission Spectrometry with the Improved Detectability of Ag, Cd, Hg, Pb, Tl, and Zn
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