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Search results for: 5-phase motor
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Computational analysis of substituent effects on proton affinity and gas-phase basicity of TEMPO derivatives and their hydrogen bonding interactions with water molecules
PublicationThe study investigates the molecular structure of 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) and its derivatives in the gas phase using B3LYP and M06-2X functional methods. Intermolecular interactions are analyzed using natural bond orbital (NBO) and atoms in molecules (AIM) techniques. NO2-substituted TEMPO displays high reactivity, less stability, and softer properties. The study reveals that the stability of TEMPO derivatives...
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A method for a comprehensive lipidomic analysis of flaxseed (Linum usitatissimum) with the use of LC–Q-TOF-MS and dispersive micro-solid-phase (μDSPE) extraction
PublicationFlaxseed (FS) is one of the richest sources of α-linolenic acid oil and lignans, and it is suggested that the consumption of flaxseed may contribute to the prevention of certain chronic diseases such as many types of cancer, diabetes, cardiovascular diseases and cerebrovascular stroke. Here, we demonstrate a new method for comprehensive FS lipidome profiling with the use of LC–Q-TOF-MS and dispersive micro-solid-phase extraction....
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Oxidative Dimerisierung von Phosphanen und Hinweise auf das intermediare Auftreten des Phosphinophosphinidens tBu2P-P in Reaktionen von [(eta^5^-C5H5)2TiCl2] und [(eta^5^-C5H5)(eta^5^-C5Me5)TiCl2] mit tBu2P-P(SiMe3)Li und tBu2P-P(Li)-P-tBu2. Bildung von Titan(III)- Fulvalen-Komplexen.
PublicationReakcja dichlorku tytanocenu z tBu2P-P(Li)-P-tBu2 albo tBu2P-P(SiMe3)Li prowadzi do kompleksów Ti(III). Jednocześnie grupy fosfanowe dimeryzują dając (tBu2P)2P-P(P-tBu2)2 lub (tBu2P-PSiMe3)2. Znaleźliśmy produkty, które sugerują przejściowe występowanie tBu2P-P.
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Corrosion degradation monitoring of ship stiffened plates using guided wave phase velocity and constrained convex optimization method
PublicationThe study presents an experimental investigation on the corrosion degradation level assessment using nondestructive wave-based methods. The degradation level of ship structural elements has been assessed in two different ways. The first one is based on the spectral decomposition and zero-crossing incorporated reconstruction of the dispersion curve approach of the antisymmetric Lamb wave mode and the best matching of the theoretical...
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Studies on applicability of new solid-phase microextraction fibers for the selective extraction and determination of short - chain monocarboksylic acids
PublicationShort-chain monocarobxylic acids, sometimes referred to as volatile fatty acids (VFA), are a group of low molecular weight alkyl monocarboxylic acids that are widely distributed within the environment. These molecules contain any from 2 to 8 carbon atoms and originate from the anaerobic biodegradation of organic matter such as carbohydrates, proteins, and fats. These compounds are commonly found in the effluents from animal farming,...
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Application of normal-phase high-performance liquid chromatography followed by gas chromatography for analytics of diesel fuel additives
PublicationThe paper presents the results of investigations on new procedures of determination of selected cleaning additives in diesel fuel. Two procedures: one-step analysis using gas chromatography with flame ionization detection (GC-FID) or mass spectrometry (GC-MS) and a two-step procedure in which normal-phase high-performance liquid chromatography (NP-HPLC) was used for preliminary separation of the additives, were compared. The additive...
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Emissions and toxic units of solvent, monomer and additive residues released to gaseous phase from latex balloons
PublicationThis study describes the VOCs emissions from commercially available latex balloons. Nine compounds are determined to be emitted from 13 types of balloons of different colors and imprints in 30 and 60°C. The average values of total volatile organic compounds (TVOCs) emitted from studied samples ranged from 0.054 up to 7.18 μg∙g-1 and from 0.27 up to 36.13 μg∙g-1 for 30oC and 60oC, respectively. The dataset is treated with principal...
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Numerical and experimental investigation of guided ultrasonic wave propagation in non-uniform plates with structural phase variations
PublicationThe article presents the results of numerical and experimental investigations of guided wave propagation in aluminum plates with variable thickness. The shapes of plate surfaces have been specially designed and manufactured using a CNC milling machine. The shapes of the plates were defined by sinusoidal functions varying in phase shift, which forced the changes in thickness variability alongside the propagation path. The main aim...
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Miniaturized Solid Phase Extraction techniques for different kind of pollutants analysis: State of the art and future perspectives – PART 1
PublicationSolid Phase Extraction (SPE) has been practiced in a modern form for more than half a century. It was constantly developing, driven by the analysts needs. These needs are coming from the importance to select an appropriate analytical method, which should have satisfactory accuracy, precision and sensitivity. In the case of sorbent-based microextraction techniques, the choice of miniaturized variants that meet these requirements...
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EFFECTS OF DOPING ON STRUCTURE AND PHASE TRANSITION OF HIGH TEMPERATURE PROTON CONDUCTOR LaNb1-xMxO4-σ (M=As, Sb, V, Ta AND X=0,05 TO 0,3)
PublicationIn this work synthesis of lanthanum orthoniobate has been done. Doping by arsenic, antimony, vanadium or tantalum in 5% to 30% have been introduced. The relationship between doping type and percentage and structural properties of the material have been investigated.
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Modeling two phase flow in large scale fractured porous media with an extended multiple interacting continua method
PublicationWe present a two phase flow conceptual model, the corresponding simulator (2pMINC) and a workflow for large-scale fractured reservoirs, based on a continuum fracture approach which uses the multiple interacting continua (MINC) method complemented with an improved upscaling technique. The complex transient behavior of the flow processes in fractured porous media is captured by subgridding the coarse blocks in nested volume elements...
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Modelling of energy flow in mechatronic systems. A bond graph approach
PublicationW referacie przedstawiono w sposób jednoliy modelowanie systemów mechatroniki metodą grafów wiązań (GW) w aspekcie symulacji przepływu energii. Omówiono ogólne założenia modelowania w ujęciu GW. Modelowanie przepływu energii rozważano na przykładzie napędu pojazdu hybrydowego PH-MAK.
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A negative effect of carbon phase on specific capacity of electrode material consisted of nanosized bismuth vanadate embedded in carbonaceous matrix
PublicationLithium-ion batteries (LIBs) are widely used all over the world. The LIBs belong to a renewable energy source and energy storage devices. The increase in energy demand causes that new materials of higher energy and higher power densities are still under investigation. Herein, we compare electrochemical properties of bismuth vanadate (BiVO4) embedded and not embedded into carbonaceous matrix as an anode material along with structural...
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Induction of G2/M phase arrest and apoptosis of human pancreatic cancer BxPC-3 cells by potenet antitumor 1-nitroacridine derivative C-1748
PublicationPancreatic ductal adenocarcinoma (PDA) is among the most lethal human cancers, in part because it is insensitive to many chemotherapeutic drugs. Gemcitabine still remains the best chemotherapeutic agent available for the treatment of advanced pancreatic cancer. However, gemcitabine treatment results in only a marginal survival advantage. Thus, there is a strong need for the continuous development of novel therapeutic agents...
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Estimation of platinum in environmental water samples with solid phase extraction technique using inductively coupled plasma mass spectrometry
PublicationZoptymalizowano metodykę oznaczania śladowych poziomów stężeń platyny (IV) w oparciu o technikę ekstrakcji do fazy stałej w połączeniu ze spektrometrią mas z plazmą wzbudzoną indukcyjnie. Na etapie wzbogacania platyny wykorzystano żel krzemionkowy modyfikowany grupami aminopropylowymi. Ilościowy odzysk platyny uzyskano poprzez wykorzystanie 1.0 mol L-1 roztworu tiomocznika jako eluenta. Odchylenie standardowe wyników (RSD) było...
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Entrapment of DyP‐type peroxidase from Pseudomonas fluorescens Pf‐5 into Ca‐alginate magnetic beads
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Search for new tools to combat Gram-negative resistant bacteria among amine derivatives of 5-arylidenehydantoin
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A qualitative 5-country comparison of the perceived impacts of COVID-19 on people living with dementia and unpaid carers
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Children’s Astronomy. Development of the Shape of the Earth Concept in Polish Children between 5 and 10 Years of Age
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Type 2 Diabetes Remission 5 Years After Laparoscopic Sleeve Gastrectomy: Multicenter Cohort Study
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Edukacja społeczeństwa opartego na wiedzy. Kurier**2002 nr 5-6 s. 10-11
PublicationArtykuł opublikowano jako materiał do dyskusji przed zaplanowaną na 2003 r.kolejną konferencją naukowa nt. Nauka-Polityka-Biznes. Omawia aktualną sytu-ację społeczną oraz możliwe przemiany społeczeństwa postindustrialnego wspołeczeństwo oparte na wiedzy - uczące się. W artykule przedstawiono ogólnącharakterystykę sytuacji w kraju oraz możliwości i zagrożenia związane z ja-kościowo nowym etapem rozwoju.
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Potyczki algorytmiczne, czyli Alicja i Bogdan w nowych sytuacjach. 5. Alicja kupuje buty.
PublicationNiniejszy miniesej pokazuje, w jaki sposób można efektywnie przeszukiwać uporządkowane tablice 2-wymiarowe oraz, w jaki sposób można radzić sobie (niekiedy) z trudnymi problemami obliczeniowymi.
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Mikrobiologiczne obrastanie podłoży mineralnych. BIT**2003 nr 3 s. 32-33, 5 fot.
PublicationArtykuł omawia nasilające się zjawisko obrastania elewacji glonami i poros- tami. W artykule prezentowano przyczyny porastania mikrobiologicznego ele- wacji wskazano warunki jakie sprzyjają obrastaniu elewacji oraz przedstawio-no sposoby ograniczenia tego procesu.
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Approximation of Message Inter-Arrival and Inter-Departure Time Distributions in IMS/NGN Architecture Using Phase-Type Distributions
PublicationCurrently it is assumed that requirements of the information society for delivering multimedia services will be satisfied by the Next Generation Network (NGN) architecture, which includes elements of the IP Multimedia Subsystem (IMS) solution. In order to guarantee Quality of Service (QoS), NGN has to be appropriately designed and dimensioned. Therefore, proper traffic models should be proposed and applied. This requires determination...
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Thermal analysis and experimental verification of permanent magnet synchronous motor by combining lumped-parameter thermal networks with analytical method
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Solid Phase Micro-Extraction, a Versatile and Handy Tool in Environmental Trace Organic Analysis, Gets a New Class of Coatings, Polymeric Ionic Liquids
PublicationSolid phase microextraction (SPME) fundamentals, characteristics and application are described. The special stress is put on characteristics of sorbents used as SPME fiber coatings. Description of commercially available fibers and the present-day trends in development of new sorbents for SPME are given. Discussion is focused on possibility of application of ionic liquids (IL) and polymeric ionic liquids (PIL) as SPME fiber coatings....
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Determination of antifreeze substances in the airport runoff waters by solid-phase microextraction and gas chromatography–mass spectrometry method
PublicationA new method has been developed for the determination of antifreeze agents such as ethylene glycol (EG), propylene glycol (PG), and diethylene glycol (DEG) in the samples of airport runoff water. The method is based on headspace solid–phase microextraction (HS–SPME) of target analytes, which is coupled with gas chromatography–mass spectrometry (GC–MS). Until now, there was a lack of appropriate methodology for collecting reliable...
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Tuning the extraction properties of ionogel-coated Solid-phase microextraction fibers based on the solvation properties of the ionic liquids
PublicationA silica-based network was used to immobilize ionic liquid-based ionogels and applied as a fiber coating forsolid-phase microextraction (SPME). The ionogels were prepared by a sol–gel process, using two ionic liquids,triethylsulfonium bis(trifluoromethylsulfonyl)imide ([Set3][TFSI]) and 1-butyl-1-methylpiperidinium bis(tri-fluoromethylsulfonyl)imide ([C4C1Pip][TFSI]), as well as their equimolar mixture. Methyltrimethoxysilane wasused...
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A Comparative Quantitative Structure-Retention Relationships Study for Lipophilicity Determination of Compounds with a Phenanthrene Skeleton on Cyano-, Reversed Phase-, and Normal Phase-Thin Layer Chromatography Stationary Phases
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3-Acyloketeny generowane z 5-acylo-2,2-dimetylo-1,3-dioksa-4,6-dionów w syntezie mono i bicyklicznych układów β-laktamowych
PublicationZakres rozprawy obejmuje dwa zróżnicowane tematycznie zagadnienia. Zasadniczy fragment opisuje próby stereoselektywnej syntezy układów β-laktamowych na drodze cykloaddycji ketenów generowanych termicznie z pochodnych kwasu Meldruma z iminami. Pozostałą część badań stanowi wątek cyklizacji metatetycznych. Zagadnienie stereoselektywnej syntezy β-laktamów w wyniku cykloaddycji aldimin do generowanych termicznie z rozkładu pochodnych...
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Algorytmy sterowania trakcją pojazdu autonomicznego z elektrycznymniezależnym napędem kół
PublicationW ostatnich latach rośnie zainteresowanie pojazdami autonomicznymi o napędzie elektrycznym lub hybrydowym. Na szczególną uwagę zasługują wielosilnikowe napędy, pozwalające dostosować moment na każdym kole pojazdu do warunków drogowych. Odpowiednie sterowanie momentem poszczególnych kół w każdej fazie ruchu pojazdu, zwłaszcza na krętej drodze oraz w warunkach niskiej, nierównomiernej i zmieniającej się w czasie przyczepności nawierzchni,...
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Application of response surface methodology to optimize solid-phase microextraction procedure for chromatographic determination of aroma-active monoterpenes in berries
PublicationMost of scientific papers concern the qualitative or semi-quantitative analysis of aroma-active terpenes in liquid food matrices. Therefore, the procedure based on solid-phase microextraction and comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry for determination of monoterpenes in fresh berries was developed. The optimal extraction conditions using divinylbenzene-carboxen-polydimethylsiloxane fiber...
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NUMERICAL ANALYSIS OF SPECIES DIFFUSION AND METHANOL DECOMPOSITION IN THERMOCATALYTIC REACTOR BASED ON THE INTERMETALLIC PHASE OF Ni3Al FOR LOW REYNOLDS NUMBERS
PublicationNumerical modelling of hydrogen production by means of methanol decomposition in a thermocatalytic reactor using corrugated foil made of the Ni3Al intermetallic phase is shown in the paper. Experimental results of the flow analysis of mixtures containing helium and methanol in a thermocatalytic reactor with microchannels were used for the initial calibration of the CFD calculations (calculations based on the Computational Fluid...
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Mechanism of a Four-Phase Liquid Membrane Oscillator Containing Hexadecyltrimethylammonium Bromide
PublicationBadano zachowanie nitrometanowego oscylatora z membraną ciekłą zawierającego kationowy surfaktant. Początkowo układ składał się z trzech faz: wodnej donorowej zawierającej surfaktant i etanol, membrany ciekłej (kwas pikrynowy w nitrometanie) oraz fazy wodnej akceptorowej zawierającej sacharozę. Podczas procesu oscylacyjnego wytwarzała się nowa fazą X między membraną ciekłą, a fazą akceptorową. Stwierdzono oscylacje różnicy potencjału...
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Single-phase power electronics transformer with active functions for smart grid
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Stability of liquid film formed due to impingement of a two-phase jet
PublicationPrzedstawiono analizę teoretyczną i badania eksperymentalne zjawiska rozrywania się warstwy cieczy powstałej na powierzchni ciała stałego z uderzającej strugi.
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Composite Bioelectrodes Based on Lipidic Cubic Phase with Carbon Nanotube Network
PublicationElektrody z węgla szklistego modyfikowane fazą kubiczną z siecią nanorurek zastosowano do enzymatycznej redukcji tlenu katalizowanej przez lakazę. Zastosowanie nanorurek obniżyło nadpotencjał redukcji tlenu o 0,5 V. W celu zwiększenia gęstości prądu redukcji tlenu zastosowano znany mediator przeniesienia elektronów - ABTS. Mediator adsorbowano na nanorurkach lub wiązano kowalencyjnie z końcami nanorurek. Kowalencyjne związanie...
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Ag/Pt-modified TiO2 nanoparticles for toluene photooxidation in the gas phase
PublicationAg/Pt-modified TiO2nanocomposites were synthesized using the sol–gel method. The effect of metal typeand amount as well as synthesis route on the photocatalytic activity in reaction of toluene removal, usedas a model volatile organic compound, was investigated. Toluene, at the concentration of about 200 ppm,was irradiated over modified TiO2using light-emitting diodes (LEDs, max= 415 nm). The results showedthat toluene could be...
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HYDROGEN PRODUCTION PERFORMANCE IN THERMOCATALYTIC REACTOR BASED ON THE INTERMETALLIC PHASE OF NI3AL
PublicationThe main aim of the following paper is mathematical modelling for momentum, heat and mass transfer, which is accompanied by chemical surface reactions of the flow of the mixture helium and methanol. The thermocatalytic devices used for decomposition of hydrocarbons incorporate vertical microchannels coupling at the ends and heated to 500 oC at the walls. The results of the experiment were compared with CFD calculations to calibrate...
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Simulation and Experiment of a Compact Wideband 90^{circ} Differential Phase Shifter
PublicationArtykuł przedstawia projekt i analizę kompaktowego różnicowego przesuwnika fazy, który jest rozwinięciem konfiguracji zaproponowanej Abbosha poprzez modyfikację obciążenia wrót. Zaproponowana konfiguracja zawiera 3dB sprzęgacz kierunkowy z wrotami transmisyjnymi i sprzężonymi zakończonymi obciążeniami reaktancyjnymi. W artykule przedstawiono model teoretyczny prezentujący zasadę działania układu i jego projekt. Uzyskane wyniki...
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The role of intermolecular interactions in stabilizing the structure of the nematic twist-bend phase
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Thermotropic Biaxial Nematic Phase in Liquid Crystalline Organo-Siloxane Tetrapodes
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Dissociative electron attachment to gas phase thiothymine: experimental and theoretical approaches
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Solid phase extraction of explosives on Ni-doped carbosils prepared by mechanochemistry
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Losses Model of the WPT System with Single-Phase T-Type Inverter
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Strategies for optimizing the phase correction algorithms in Nuclear Magnetic Resonance spectroscopy
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Riboflavin binding protein—Chiral stationary phase: Investigation of retention mechanism
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Pressure-induced phase transition in LiLuF4:Pr3+investigated by an optical technique
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Optical processes in YVO4:Eu3+across zircon-to-scheelite phase transition
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Exergy analysis of operation of two-phase ejector in compression refrigeration systems
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