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Search results for: DISPERSIVE LIQUID-LIQUID MICROEXTRACTION / GAS CHROMATOGRAPHY / POSTOXIDATIVE EFFLUENTS / VOLATILE ORGANOSULFUR COMPOUNDS / WASTEWATER TREATMENT
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Physicochemical and Volatile Compounds Analysis of Fruit Wines Fermented with Saccharomyces cerevisiae: FTIR and Microscopy Study with Focus on Anti-Inflammatory Potential
PublicationThe growing trend in fruit wine production reflects consumers’ interest in novel, diverse drinking experiences and the increasing demand for healthier beverage options. Fruit wines made from kiwi, pomegranates, and persimmons fermented using S. bayanus Lalvin strain EC1118 demonstrate the versatility of winemaking techniques. Kiwifruit, persimmon, and pomegranate wines were analyzed using HPLC and GC-TOFMS analyses to determine...
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Liquid Crystals in Analytical Chemistry: A Review
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Modelling of vibrations of a liquid filled tank
PublicationPrzeprowadzono analizę teoretyczną i numeryczną zbiorników długich i krótkich wypełnionych całkowicie lub częściowo cieczą. Wyznaczenie obciążeń hydrodynamicznych dotyczy bezpośrednio wytrzymałości konstrukcji samego zbiornika, a przez to pozwala określić wytrzymałość konstrukcyjną całego kadłuba. Szczególne wymagania stawiane są zbiornikom do przewozu cieczy radioaktywnych, gdyż należy zapewnić bardzo wysoki stopień bezpieczeństwa...
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Liquid crystal thermography experimental application
PublicationPraca przedstawia wykorzystanie termografii ciekłokrystalicznej do badania zjawisk wymiany ciepła z zastosowaniem metod stanu ustalonego i przejściowej.
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Multicomponent ionic liquid CMC prediction
PublicationWe created a model to predict CMC of ILs based on 704 experimental values published in 43 publications since 2000. Our model was able to predict CMC of variety of ILs in binary or ternary system in a presence of salt or alcohol. The molecular volume of IL (Vm), solvent-accessible surface (Sˆ), solvation enthalpy (DsolvGN), concentration of salt (Cs) or alcohol (Ca) and their molecular volumes (Vms and Vma, respectively) were chosen...
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Hydrodynamics of tank partially filled with liquid.
PublicationW artykule podano podstawowe równania dynamiki zbiornika wypełnionego częściowo cieczą. Na modelu tego zbiornika przeprowadzono badania eksperymentalne i wyniki tych badań przedstawiono jako efekt końcowy.
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Chemometric optimization of derivatization reactions prior to gas chromatography–mass spectrometry analysis
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Supervisory Control System for Adaptive Phase and Work Cycle Management of Sequencing Wastewater Treatment Plant
PublicationThe paper presents the design of the integrated control system applied to Sequencing Batch Reactor (SBR) in a biological Wastewater Treatment Plant (WWTP) in Swarzewo, which operates under activated sludge technology. Based on the real data records, ASM2d biological processes model and aeration system model, hierarchical control system for dissolved oxygen tracking and cycle management is designed. Internal Model Controller (IMC)...
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Ion Chromatography in Environmental Analysis of Selected Organic Acids
PublicationLow molecular mass carboxylic acids (LCAs) occur in many environmental compartments dueto natural processes and human activity. When volatile and nonvolatile acids are to be monitored then liquidchromatography, including ion chromatography seems a method of choice. At high pH the acids are inionized form and can be separated as carboxylats by means of anion exchange chromatography. LCAs canalso be separated at low pH by ion exclusion...
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The new silica-based coated SPME fiber as universal support for the confinement of ionic liquid as an extraction medium
PublicationThe new silica-based SPME fiber coating is reported for the first time as universal support purposed to confinement of ionic liquid as an extraction medium. Fiber coating was prepared by the sol-gel process, using potassium silicate (K2SiO3) as a precursor and dimethylformamide (DMF) as a pore-forming medium. The concept of synthesis assumes obtaining a solid porous material on the surface of the glass rod and, being characterized...
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Polymeric porous membranes as solid support and protective material in microextraction processes: A review
PublicationPolymeric porous membranes have proven to be a versatile and efficient material for microextraction processes. In analytical practice, they are used both as a solid support and as a protective medium for improved sample preparation in various analytical applications. Polymeric porous membranes offer unique advantages in microextraction due to their large surface area and controllable pore size, eliminating interfering effects from...
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Organic Acids and Polyphenols Determination in Polish Wines by Ultrasound-Assisted Solvent Extraction of Porous Membrane-Packed Liquid Samples
PublicationIn the near future, Poland is going to have more and more favorable conditions for viticulture. Organic acids and polyphenols are among the most commonly analyzed compounds due to their beneficial properties for human health and their importance in the winemaking process. In this work, a new technique involving ultrasound-assisted solvent extraction of porous membrane-packed liquid samples (UASE-PMLS) was for the first time described...
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain alkane monocarboxylic acids in aqueous samples
PublicationCelem prowadzonych badań było opracowanie metodyki oznaczania krótkołańcuchowych kwasów alkanomonokarboksylowych (KKA), opartej na ich izolowaniu i wzbogacaniu za pomocą techniki HS-SPME, a następnie oznaczaniu za pomocą chromatografii gazowej sprzężonej ze spektrometrią mas (GC-MS). Do ekstrakcji zastosowano włókno pokryte polarną fazą stacjonarną opartą na glikolu polietylenowym (PEG). Dla celów porównawczych zastosowano również...
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The role of SSVF and SSHF beds in concentrated wastewater treatment, design recommendation
PublicationThe return flows of reject water from sewage sludge dewatering alter the activated sludge process ina conventional WWTP and increase TN concentration in the final effluent from WWTP. The objectiveof the investigation carried out was to consider the application of multistage treatment wetland(MTW) for the treatment of reject water from sewage sludge dewatering in a centrifuge (RWC). Thispaper aims to present the design and performance...
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Structure and the Biochemical Potential of the Bacterial Community in Wastewater Treatment Plant Effluent and in Receiving Waters: Northern Poland Case Study
PublicationWastewater treatment processes are monitored mainly in terms of biogenic substance removal efficiency. Little is known about the treated wastewater microbiome and its influence on the recipient. In this study, a wide range of methods (cultivation, microscopic analysis, New Generation Sequencing and Real Time PCR) were employed to determine the bacterial community composition of the treated wastewater and its receiver. Preliminary...
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Rural domestic wastewater treatment in Norway and Poland: experiences, cooperation and concepts on the improvement of constructed wetland technology
PublicationThis article describes Norwegian and Polish experiences concerning domestic wastewatertreatment obtained during nearly 20 years of operation for constructed wetland (CW) systemsin rural areas and scattered settlements. The Norwegian CW systems revealed a highperformance with respect to the removal of organic matter, biogenic elements and faecalindicator bacteria. The performance of the Polish CW systems was unstable, and varied...
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Atmospheric Pressure Glow Discharges Generated in Contact with Flowing Liquid Cathode: Production of Active Species and Application in Wastewater Purification Processes
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Fundamentals of Steam and Gas Turbines OASIV
e-Learning CoursesApplication of turbines in industry and sea power plants. Basic thermodynamics and fluid flow mechanics in turbomachinery. Steam turbine power cycle and plants. Gas turbine power cycle and plants. Turbine blading systems operation.
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Steroid profiles as potential biomarkers in patients with urogenital tract cancer for diagnostic investigations analyzed by liquid chromatography coupled to mass spectrometry
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Molecularly imprinted stir bar sorptive extraction coupled with high-performance liquid chromatography for trace analysis of naphthalene sulfonates in seawater
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The efficiency comparison of ramentaceone isolation from Drosera aliciae plants using normal and reversed phase preparative liquid chromatography technique
PublicationW pracy zaprezentowano optymalne warunki otrzymywania ramentaceonu z chloroformowego ekstraktu z rośliny D. muscipula. Opracowano i przedstawiono dwie procedury otrzymywania ramantaceonu z wykorzystaniem NP-PLC i RP-PLC. Dla produktu o określonej czystości, porównano maksymalny stopień przeładowania kolumny, efektywność procesu wyrażoną jako ilość substancji otrzymanej w jednostce czasu oraz produktywność kolumny, wyrażoną jako...
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Separation of Monovinyl and Divinyl Protochlorophyllides Using C30 Reverse Phase High Performance Liquid Chromatography Column: Analytical and Preparative Applications
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Quantification of DNA Modifications Using Two-Dimensional Ultraperformance Liquid Chromatography Tandem Mass Spectrometry (2D-UPLC-MS/MS)
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Analysis of serum homocysteine in the laboratory practice - comparison of the direct chemiluminescence immunoassay and high performance liquid chromatography coupled with fluorescent detection
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Determination of robenidine in animal feeds by liquid chromatography coupled with diode-array detection and mass spectrometry after accelerated solvent extraction
PublicationRobenidyna (chlorowodorek 1,3-bis[(4-chlorobenzylideno)amino]guanidyny) jest stosowana w celu zapobiegania i leczenia kokcydiozy - pasożytniczej choroby układu pokarmowego wielu zwierząt hodowlanych (kozy, owce, króliki, drób) wywoływanej przez pierwotniaki należące do rzędu Eimeria tenella, E. Necatrix, E. Acervulina, E. Maxima, E. Brunetti, and E. Mivati. Robenidyna wykazuje stosunkowo wysoką skuteczność terapeutyczną, przy niewielkiej...
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The effect of agro-waste co-digestion and sludge disposal on carbon footprint in municipal wastewater treatment plants
PublicationThe study presents analysis of the carbon footprint (CF) in 6 wastewater treatment plants in northern Poland with a special focus on the effect of co digestion of sewage sludge and food waste. Although co-digestion increases the on-site energy production, but it has a negative effect on the total CF. To overcome the negative effect, several sludge disposal scenarios were analysed and their effect on the CF reduction was determined....
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Innovations in Wastewater Treatment: Harnessing Mathematical Modeling and Computer Simulations with Cutting-Edge Technologies and Advanced Control Systems
PublicationThe wastewater treatment landscape in Central Europe, particularly in Poland, has undergone a profound transformation due to European Union (EU) integration. Fueled by EU funding and rapid technological advancements, wastewater treatment plants (WWTPs) have adopted cutting-edge control methods to adhere to EU Water Framework Directive mandates. WWTPs contend with complexities such as variable flow rates, temperature fluctuations,...
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Chromatographic behaviour of ionic liquid cations in view of quantitative structure-retention relationship
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Solid phase microextraction: state of the art, opportunities and applications
PublicationSolid phase microextraction is one of the most popular green techniques used for sample preparations in analytical chemistry. It is a simple, rapid, sensitive, and solvent-free technique. Since SPME was first introduced in the early 1990s, there has been an intensification of research in order to elaborate new methodical solutions in many research facilities around the world, which could increase the use of this technique. More...
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A solid phase extraction–ion chromatography with conductivity detection procedure for determining cationic surfactants in surface water samples
PublicationA new analytical procedure for the simultaneous determination of individual cationic surfactants (alkyl benzyl dimethyl ammonium chlorides) in surface water samples has been developed. We describe this methodology for the first time: it involves the application of solid phase extraction (SPE – for sample preparation) coupled with ion chromatography–conductivity detection (IC-CD – for the final determination). Mean recoveries of...
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Identification of volatile compounds in raw spirits of different organoleptic quality
PublicationGłównym celem prezentowanych badań było określenie składu lotnej frakcji destylatów rolniczych, a następnie wyodrębnienie profili zapachowych destylatów rolniczych różniących się właściwościami sensorycznymi ocenionymi na podstawie klasycznej analizy sensorycznej. Profile zapachowe tworzono z wykorzystaniem kapilarnej chromatografii gazowej połączonej ze spektrometrią mas (GC-MS). Do ekstrakcji lotnych związków zastosowano technikę...
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Separation of volatile compounds from fermentation broth by membrane distillation
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Volatile organohalogen compounds in human urine: the effect of environmental exposure
PublicationW pracy przedstawiono wyniki oznaczania lotnych związków chlorowcoorganicznych w próbkach moczu pochodzących m.in. od dawcow narazonych na kancerogeny w miejscu pracy i dawcow spozywajacych wode poddana procesowi uzdatniania przez chlorowanie. Do izolacji i wzbogacania analitów z moczu, posiadającego skomplikowaną matrycę, wykorzystano technikę analizy fazy nadpowierzchniowej nad cienką warstwą cieczy z samoczynną generacją ciekłego...
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Advanced oxidation processes (AOPs) based wastewater treatment - unexpected nitration side reactions - a serious environmental issue: A review
PublicationChemical compounds containing nitro group (nitro-products) are a one of toxic by-products, that can be formed during wastewater treatment processes. In case of presence of nitrite or nitrate ions, the formation of nitro-products during advanced oxidation processes (AOPs) is very common. It is caused by the reactive nitrogen species (RNs) such as nitrate radical (NO3•), nitrite radical (NO2•), nitrogen oxide radical (NO•) and peroxynirite...
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Thermal decomposition of surface compounds for the generation of small quantities of acetaldehyde. Calibration of a thermal desorption gas chromatography flame ionization detection.
PublicationW pracy opisano sposób wytwarzania niewielkich ilości acetaldehydu w procesie termicznego rozkładu związku powierzchniowego uzyskanego w wyniku chemicznej modyfikacji żelu krzemionkowego.Proces rozkładu prowadzony jest w temperaturze 130-190 stopni Celsjusza.Przedstawiono również sposób syntezy prowadzący do uzyskania odpowiedniego związku powierzchniowego.
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The role of fluids in high-pressure polymorphism of drugs: different behaviour of β-chlorpropamide in different inert gas and liquid media
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Application of mechanistic and data-driven models for nitrogen removal in wastewater treatment systems
PublicationIn this dissertation, the application of mechanistic and data-driven models in nitrogen removal systems including nitrification and deammonification processes was evaluated. In particular, the influential parameters on the activity of the Nitrospira activity were assessed using response surface methodology (RSM). Various long-term biomass washout experiments were operated in two parallel sequencing batch reactor (SBR) with a different...
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Transport properties of aqueous ionic liquid microemulsions: influence of the anion type and presence of the cosurfactant
PublicationTransport properties, viz. specific conductivity, dynamic viscosity and apparent diffusion coefficients, were measured as a function of water content in aqueous ionic liquid microemulsions containing 1-butyl-3- methylimidazolium hexafluorophosphate, [BMIM][PF6] and bis(trifluoromethanesulphonyl)imide, [BMIM][Tf2N], stabilized by the nonionic surfactant TX-100, or its mixture with a cosurfactant, i.e. butanol. The investigation covered...
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Identification of pollutants at the adjacent areas to the landfill site using two dimensional gas chromatography with mass spectrometry technique
PublicationMunicipal landfills are considered one of the main sources of air pollutants. In this article is presented the use of a modern analytical technique: a two dimensional gas chromatography to identify the substances in the atmospheric air near a waste processing plant located in Gdansk. In order to determine the types of substances occurring in different atmospheric conditions, the study was conducted from February to April 2016....
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Partitioning of heavy metals in sub-surface flow treatment wetlands receiving high-strength wastewater
PublicationThe retention of heavy metals at two pilot-scale treatment wetlands (TWs), consisting of two vertical flow beds (VSSF) followed by a horizontal flow bed (HSSF) was studied. The TWs received highstrength wastewater: reject waters from sewage sludge centrifugation (RW) and landfill leachate (LL). The concentrations of metals: Fe, Mn, Zn, Al, Pb, Cu, Cd, Co, Ni were measured in treated wastewater, substrate of the beds and in plant...
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The comparison of vodka, whisky and moonshine by using the electronic nose based on the technology of ultra-fast gas chromatography
PublicationVodka andwhisky are produced fromgrain distillates. Formerly these alcohols were very often counterfeited, by the made in home conditions spirit drink called moonshine, which is obtained by distilling a mash from the alcoholic fermentation. This study presents research aimed at checking the usefulness of the electronic nose using ultra-fast gas chromatography for the differentiation of whisky, vodka and moonshine. 12 samples of...
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The comparison of vodka, whisky and moonshine by using the electronic nose based on the technology of ultra-fast gas chromatography
PublicationVodka andwhisky are produced fromgrain distillates. Formerly these alcohols were very often counterfeited, by the made in home conditions spirit drink called moonshine, which is obtained by distilling a mash from the alcoholic fermentation. This study presents research aimed at checking the usefulness of the electronic nose using ultra-fast gas chromatography for the differentiation of whisky, vodka and moonshine. 12 samples of...
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Distinction of citrus fruits based on their volatile composition using the electronic nose
PublicationThe aim of the study was to analyze the volatile fraction of the citrus fruit using an electronic nose device integrated with ultrafast gas chromatography. The subjects were Citrus aurantifolia, Fortunella margarita Swingle and Citrus × floridana. The chromatographic data obtained were analyzed by means of chemometric methods: PCA and SQC. On the basis of the charts obtained, it is possible to distinguish the fruits tested on the...
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Cold atmospheric pressure plasmas as versatile tools for effective degradation of a mixture of hazardous and endocrine disturbing compounds from liquid wastes
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Desalination and Water Treatment
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Long-term operation of Kickuth-type constructed wetland applied to municipal wastewater treatment in temperate climate
PublicationThe purpose of this paper is to discuss the problem of changes of effectiveness of Kickuth-type constructed wetland with subsurface flow applied to domestic wastewater treatment. This study is based on an example of a wetland 3000 m2 in surface, serving 800 inhabitants, located in Poland. The results of chemical analysis showed that after an initial year of ‘start-up time’, the efficiency of pollutant removal gradually increased...
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Textile wastewater treatment by AOPs for brine reuse
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Supervisory Control of Integrated Wastewater Treatment Systems
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Mathematical Modelling in Diagnosis of Wastewater Treatment Plant
PublicationThe paper reports development of mathematical modeling in diagnosis of the WWTP. The algorithm is based on a comparition of data from the mathematical modeling and measurments of real datefrom WWTP, until it will detect any malfunction of the sensors in th case of study.
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Supervisory control of integrated wastewater treatment systems.
PublicationSterowanie zintegrowanym systemem oczyszczania ścieków (sieć kanalizacyjna- oczyszczalnia ścieków), w pełnym zakresie jego obciążeń wymaga zastosowania zaawansowanych algorytmów sterowania optymalizującego. System sterowania jest hierarchicznie zdekomponowany, tworząc wielopoziomową-wielowarstwową. Główną technologią sterowania sterowanie predykcyjne (MPC). Nie jest możliwe wystarczająco efektywne sterowanie takim systemem we wszystkich...