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Search results for: NMR%20SPECTROSCOPY
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Badania skuteczności ochrony katodowej Nabrzeża Zachodniego odcinek nr 2 (północny) oraz Pirsu C w Porcie Gdynia
PublicationZbadano skuteczność ochrony katodowej północnego odcinka nabrzeża zachodniego oraz pomostu C w Porcie Wojennym w Gdyni. Ochrona realizowana jest za pomocą aluminiowych anod galwanicznych spawanych do ścianki szczelnej oraz pali.
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Femtosecond Er-doped fiber laser source tunable from 872 to 1075 nm for two-photon vision studies in humans
PublicationWe report the development of a widely-tunable femtosecond fiber laser system and its application for two-photon vision studies. The source is based on an Er-doped fiber laser with spectral shift up to 2150 nm, followed by a second harmonic generation module to generate a frequency-doubled beam tunable from 872 to 1075 nm. The source delivers sub-230 fs pulses with nearly-constant duration over the entire tuning range, with output...
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ANALIZA WARUNKÓW PRACY ŁOŻYSKA NR 1 TURBINY AR 1,6MW ORAZ MODERNIZACJA UKŁADU SMAROWANIA I POMIARU TEMPERATURY
PublicationCelem pracy było wykonanie analizy warunków pracy łożyska nr 1 turbozespołu AR 1,6MW oraz modernizacja układu pomiaru temperatury. Przeprowadzono analizę budowy węzła łożyskowego, wykonano obliczenia właściwości filmu olejowego oraz opracowano projekt modernizacji łożyska i układu pomiarowego.
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Peryferia elektryki. Biul. Oddz. Białost. SEP**2002 nr 14 s. 29-33, 5 rys.bibliogr. 3 poz.
PublicationPrzedstawiono sposób odwzorowania fragmentu krwioobiegu za pomocą obwoduelektrycznego. Podano zmiany przepływu krwi w przypadku marskości wątroby.
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Experimental and theoretical investigation of the reactivity of [(BDI*)Ti(Cl){η2-P(SiMe3)-PiPr2}] towards selected ketones
PublicationIn this work, we report a new type of reactivity of [(BDI*)Ti(Cl){η2-P(SiMe3)-PiPr2}] (1) towards ketones (BDI* = 2,6-diisopropylphenyl-β-methyldiketiminate ligand). In the reaction of 1 with acetone, cyclopentanone or cyclohexanone, a ketone moiety is inserted into Ti–Pphosphanyl or Ti–Pphosphido bonds to form complexes with a new C–P–P moiety, providing [(BDI*)Ti(Cl){η2-P(SiMe3)-PiPr2-C(Me)2O}] (2a), [(BDI*)Ti(Cl){η2-OC(Me)2P(SiMe3)-PiPr2}]...
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Lanthanide co-doped TiO2: the effect of metal type and amount on surface properties and photocatalytic activity
PublicationPreparation of new rare earth metal-containing TiO2 nanocomposites (Nd3+/Er3+, Nd3+/Eu3+, Eu3+/Ho3+-TiO2) using sol–gel route and their photoactivity under visible and ultraviolet light is reported. The obtained photocatalysts were subsequently characterized by Brunauer–Emmett–Teller (BET) method, UV–Vis diffuse-reflectance spectroscopy (DRS), luminescence spectroscopy, X-ray photoelectron spectroscopy (XPS) and X-ray powder diffraction...
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Study of ultraviolet-visible fluorescence emission following resonant Auger decay of the 2p-1nl core-excited states of argon atoms
PublicationWe have studied the excitation and relaxation of Ar+ ions populated in resonant Auger decay from the Ar 2p−1nl core-excited states by using ultraviolet-visible fluorescence spectroscopy and photon-photon delayed coincidence technique. Fluorescence emission yields were measured in the photon energy range of 240-–255 eV for the 3s23p4(1D)5s(2D) → 3s23p4(1D)4p(2F) (393 nm) and 3s23p4(1D)4d(2F) → 3s23p4(1D)4p(2F) (335 nm) transitions...
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Investigation of plasmon resonance in a silver nanoparticles
Open Research DataSilver nanostructures were prepared on borosilicate glass (Corning 1737F) substrates. Thin Ag films (1–9 nm thickness) were deposited using a table-top dc magnetron sputtering coater (EM SCD 500, Leica) in pure Ar plasma (argon, Air Products 99.999%). The Ag target was of 99.99% purity, the rate of layer deposition was about 0.4 nm·s−1, and the incident...
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Chromium Cluster Luminescence: Advancing Near‐Infrared Light‐Emitting Diode Design for Next‐Generation Broadband Compact Light Sources
Open Research DataIn modern technology devices, an energy-saving miniature near-infrared (NIR) light source plays a critical role in non-destructive, non-invasive sensing applications and further advancement of technology. This dataset reports the broadband NIR luminescence of Cr3+ clusters for designing phosphor-converted NIR light-emitting diodes as an alternative...
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Electrochemical impedance spectroscopy measurements - conductivity vs. temperature and conductivity vs. oxygen partial pressure - BaCe0.6Zr0.2Y0.1Tb0.1O3-δ
Open Research DataThe dataset consists of two main catalogs consisting of measurement data: of the electrical conductivity of the BaCe0.6Zr0.2Y0.1Tb0.1O3-δ (BCZYTb) sample as a function of temperature and of the electrical conductivity as a function of oxygen partial pressure (pO2). Measurements as a function of temperature were carried out in dry and wet air (pH2O ~...
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Nonlinear impedance of 45Bi2VO5.5-55SrB4O7 fully crystallized glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrcial properties of 45Bi2VO5.5-55SrB4O7 fully crystallized glass was measured by impedance spectroscopy method.
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Linear impedance of Bi2VO5.5 ceramic of thickness 2.88 mm measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of Bi2VO5.5 ceramic of thickness 2.88 mm was measured by impedance spectroscopy method.
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Linear impedance of 5(2Bi2O3-V2O5)-95SrB4O7 glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe linear electrcial properties of 5(2Bi2O3-V2O5)-95SrB4O7 glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 35Bi2VO5.5-65SrB4O7 fully crystallized glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrcial properties of 35Bi2VO5.5-65SrB4O7 fully crystallized glass was measured by impedance spectroscopy method.
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Linear impedance of 25Na2O–20CaO–5P2O5–50SiO2 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of 25Na2O–20CaO–5P2O5–50SiO2 glass was measured by impedance spectroscopy method.
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Linear impedance of 58(2Bi2O3-V2O5)-42SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrcial properties of 58(2Bi2O3-V2O5)-42SrB4O7 glass was measured by impedance spectroscopy method.
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Linear impedance of 50(2Bi2O3-V2O5)-50SrB4O7 glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe linear electrcial properties of 50(2Bi2O3-V2O5)-50SrB4O7 glass was measured by impedance spectroscopy method.
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Linear impedance of 5(2Bi2O3-V2O5)-95SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrcial properties of 5(2Bi2O3-V2O5)-95SrB4O7 glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 5(2Bi2O3-V2O5)-95SrB4O7 glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrcial properties of 5(2Bi2O3-V2O5)-95SrB4O7 glass was measured by impedance spectroscopy method.
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Linear impedance of Bi2VO5.5 ceramic of thickness 2.52 mm measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm was measured by impedance spectroscopy method.
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Linear impedance of 50(2Bi2O3-V2O5)-50SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrcial properties of 50(2Bi2O3-V2O5)-50SrB4O7 glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 58(2Bi2O3-V2O5)-42SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe nonlinear electrcial properties of 58(2Bi2O3-V2O5)-42SrB4O7 glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 30Bi2VO5.5-70SrB4O7 fully crystallized glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrcial properties of 30Bi2VO5.5-70SrB4O7 fully crystallized glass was measured by impedance spectroscopy method.
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Linear impedance as a function of A.C. voltage for 50(2Bi2O3-V2O5)-50SrB4O7 glass measured with impedance spectroscopy method
Open Research DataThe linear electrcial properties as a function of A.C. voltage for 50(2Bi2O3-V2O5)-50SrB4O7 glass was measured by impedance spectroscopy method.
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Size Exclusion Coupled to Reversed Phase Liquid Chromatography for the Characterization of Cranberry Products
PublicationA combination of solvent extraction, size exclusion purification, and reversed-phase liquid chromatography with UV absorption and fluorescence detection was here used for the determination of flavan-3-ols and related oligomeric compounds in cranberry products. The method relied on robust, simple, and inexpensive instrumental equipment present in most of routine analytical laboratories. Sample extracts in methanol/water/hydrochloric...
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An Investigation of Polyamides Based on Isoidide-2,5-dimethyleneamine as a Green Rigid Building Block with Enhanced Reactivity
PublicationNovel, semicrystalline polyamides and copolyamides were synthesized from a new carbohydrate-based diamine, namely isoidide-2,5-dimethyleneamine (IIDMA). In combination with 1,6-hexamethylene diamine (1,6-HDA) as well as the biobased sebacic acid (SA) or brassylic acid (BrA), the desired copolyamides were obtained via melt polymerization of the nylon salts followed by a solid-state polycondensation (SSPC) process. Depending on the...
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π-Stacking attraction vs. electrostatic repulsion: competing supramolecular interactions in a tpphz-bridged Ru(ii)/Au(iii) complex
PublicationThe synthesis and characterization of a mixed metal ruthenium(II)/gold(III) complex bridged by tetrapyridophenazine (tpphz) are described. It is isostructural and isoelectronic to the well-known photocatalysts with palladium(II) or platinum(II). Concentration dependent 1H-NMR spectroscopy and XRD studies show that the electrostatic repulsion between the gold(III) moieties exceeds the attractive π-stacking interaction. Theoretical...
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Mechanism of Osmolyte Stabilization–Destabilization of Proteins: Experimental Evidence
PublicationIn this work, we investigated the influence of stabilizing (N,N,N-trimethylglycine) and destabilizing (urea) osmolytes on the hydration spheres of biomacromolecules in folded forms (trpzip-1 peptide and hen egg white lysozyme─hewl) and unfolded protein models (glycine─GLY and N-methylglycine─NMG) by means of infrared spectroscopy. GLY and NMG were clearly limited as minimal models for unfolded proteins and should be treated with...
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Interactions between hydration spheres of two different solutes in solution: The least squares fitting with constraints as a tool to determine water properties in ternary systems
PublicationBiological systems are complex and the problem of their description lies in mutual interactions between their components. This paper is focused on model experiment-based studies which can reduce these difficulties. The ternary aqueous N-methylacetamide (NMA)–Na2HPO4 system has been studied by means of the FTIR spectroscopy. A novel difference spectra method aimed to extract the spectral contribution of water affected simultaneously...
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NOR-Light Strengthening of bilateral Polish-Norwegian cooperation in the field of optoelectronic sensing systems
ProjectsProject realized in Department of Metrology and Optoelectronics from 2017-08-08
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NOR-STA n/d
ProjectsProject realized in Faculty of Electronics, Telecommunications and Informatics according to UDA-POIG.01.03.01-22-142/09 agreement from 2009-09-15
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Molecular basis for the DNA damage induction and anticancer activity of asymmetrically substituted anthrapyridazone PDZ-7
Publicationnthrapyridazones, imino analogues of anthraquinone, constitute a family of compounds with remarkable anti-cancer activity. To date, over 20 derivatives were studied, of which most displayed nanomolar cytotoxicity towards broad spectrum of cancer cells, including breast, prostate and leukemic ones. BS-154, the most potent derivative, had IC50 values close to 1 nM, however, it was toxic in animal studies. Here, we characterize another...
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Analiza gospodarki odpadami w Janikowskich Zakładach sodowych przy składowaniu wysokim i eksploatacji stawów nr 20 do 25.
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Value of Perfusion-Weighted MR Imaging in the Assessment of Early Cerebral Alterations in Neurologically Asymptomatic HIV-1-Positive and HCV-Positive Patients
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Analiza nośności stref zakotwień w kablobetonie na przykładzie awarii wiaduktu B-9 nad drogą krajową nr 7
PublicationW pracy została przedstawiona analiza nośności konstrukcji przęsła w czasie sprężania poprzecznego. Bezpośrednim powodem analizy była awaria w strefach zakotwień kabli sprężających poprzecznic. Opisano model wycinkowy MES zastosowany do analizy i zaprezentowano wyniki. Przyjęta metoda okazała się przydatna w diagnozowaniu przyczyn awarii i w określeniu zapasów nośności.
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Polsko-Rossijskoje Sotrudiniczestwo Pomorskogo Wojewodctwa. - Istoriceskaja i Socialno-Obrazowatelnaja Mysl. - T. 7,nr 2,str.115-120
Publication.
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Opracowanie opinii na temat własności materiału podstawowego oraz jakości spoin kotła typu KSBS 380 nr fabryczny 117
PublicationNiniejsza opinia przedstawia odpowiedzi na pytania Sądu wyrażone w w/w postanowieniu, a mianowicie czy zastosowane materiały do produkcji przedmiotowego kotła jak również jakość spoin była przyczyną awarii kotła w dniu 25.12.2014r, w tym również porównanie uzyskanych wyników badań z dokumentacją konstrukcyjna kotła.2. Połączenia spawane w badanej konstrukcji kotła były najsłabszym elementem konstrukcyjnym, w którym na skutek...
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Raport z badań podczas próbnego obciążenia przęseł nr 4-6 mostu drogowego przez rzekę Wisłę w Tczewie
PublicationW pracy przedstawiono metodykę pomiarów i wyniki badań podczas próbnego obciążenia przęseł nr 4-6 mostu drogowego przez rzekę Wisłę w Tczewie. Sformułowano wnioski dotyczące rzeczywistej pracy konstrukcji i warunków dalszej eksploatacji obiektu
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Impedancja nerki. Biul. Oddz. Białost. SEP**2003 nr 16 s. 22-25, 4 rys. bibliogr. 3 poz.
PublicationPrzedstawiono istotę odwzorowania pracy nerki za pomocą obwodu elektrycc- nego. Podano zmiany przepływu krwi w przypadku zmian chorobowych w nerce.
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Olga Ciupak mgr inż.
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The Taste of Waste: The Edge of Eggshell Over Calcium Carbonate in Acrylonitrile Butadiene Rubber
PublicationRubber technology experiences a new age by the use of biowaste or natural fillers. In this regard, taking properties of reinforcing agents from biowaste fillers remains as the challenging matter. Chicken eggshell (ES) biowaste has recently been introduced to substitute calcium carbonate (CaCO3) duo to its superior properties and low price. In this work, composites based on acrylonitrile butadiene rubber (NBR) reinforced with ES...
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Power of the SMR brainwaves in the mental imagery experiment in sport: the "Your Home Venue" scenario.
Open Research DataThe data were collected to perform research on the neural oscillation during mental imagery in sport. The study's main aim was to examine the cortical correlations of imagery depending on instructional modality (guided vs self-produced) using various sport-related scripts. The research was based on the EEG signals recorded during the session with the...
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Short Term Monitor of Photodegradation Processes in Ranitidine Hydrochloride Observed by FTIR and ATR FTIR
PublicationThe effects of degradation of ranitidine hydrochloride exposed to UVB radiation (l = 310 nm) and oxygen in a weathering chamber were studied by Fourier Transform Infrared spectroscopy (FTIR) and Attenuated Total Reflectance Fourier Transform Infrared spectroscopy (ATR-FTIR). ATR-FTIR profile indicated that the degradation was spatially heterogeneous. Significant amounts of photoproducts were detected only in a directly...
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Influence of the structure of vanadate-phosphate glasses containing alkali ions on their polaronic properties
PublicationBadano wpływ struktury szkieł wanadanowo-fosforanowych zawierających jony metali alkalicznych na ich właściwości polaronowe metodą NMR.
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Effects of consecutive apneas on pial artery pulsation and subarachnoid width in healthy subjects
PublicationHypercapnia is known to dilate the pial artery, disrupt cerebral autoregulation and increase pial artery pulsation. The cerebral blood flow velocity (CBFV) response to hypercapnia is biphasic. Below the threshold for the increase of blood pressure (BP) with carbon dioxide partial pressure (pCO2), the CBFV measurement reflects vascular reactivity to pCO2 alone at a constant BP. Above this threshold, the CBFV measurement provides...
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Development of biocompatible iron oxide-silicon oxide core-shell nanoparticles as subcellular delivery platform for glucosamine-6-phosphate synthase inhibitors
PublicationIn order to develop the preparation of iron oxide-silica coreshell nanoparticles (CSNPs), thesis deeply explores the cetyltrimethylammonium (CTA+) directed silica coating methods of the oleic-acid capped iron oxide nanoparticles (OA-IONPs) initialized under near-neutral pH conditions. It is demonstrated that the initial alkaline hydrolysis of ethyl acetate in the presence of CTA+ and OA-IONPs induces an unusual ligand exchange...
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Homoleptic mono-, di-, and tetra-iron complexes featuring phosphido ligands: a synthetic, structural, and spectroscopic study
PublicationWe report the first series of homoleptic phosphido iron complexes synthesized by treating either the β-diketiminato complex [(Dippnacnac)FeCl2Li(dme)2] (Dippnacnac = HC[(CMe)N(C6H3-2,6-iPr2)]2) or [FeBr2(thf )2] with an excess of phosphides R2PLi (R = tBu, tBuPh, Cy, iPr). Reaction outcomes depend strongly on the bulkiness of the phosphido ligands. The use of tBu2PLi precursor led to an anionic diiron complex 1 encompassing a planar...
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The voltage across and current through the RC model object tested using pulse excitation in impedance spectroscopy measurement method
Open Research DataThe raw data (voltage across and current through RC model object ) obtained using pulse excitation EIS impedance spectroscopy measurement method. The data was acquired using 12-bit ADC (LTC1420) with sampling frequency changed in time segments. The 1V voltage pulse excitation duration was set to 0.1s and the total acqusition time was set to 1000s. For...
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Influence of sintering temperature of porous SrTi0.30Fe0.70O3-d oxygen electrode on electrochemical impedance spectroscopy spectra measured at 800 °C
Open Research DataThis dataset contains results electrochemica impedance spectroscopy (EIS) of symmetrical cells with porous SrTi0.30Fe0.70O3-d oxygen electrodes sintered at different temperatures (800 °C; 900 °C and 1000 °C). Measure temperature was 800 °C (syntetic air, 40 ml min-1). Results converted to electrode surfaces area and dived by two electrodes.
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Electrochemical impedance spectroscopy spectra measured at 700 °C on porous SrTi0.30Fe0.70O3-d oxygen electrodes sintered at different temperatures
Open Research DataThis dataset contains results electrochemica impedance spectroscopy (EIS) of symmetrical cells with porous SrTi0.30Fe0.70O3-d oxygen electrodes sintered at different temperaturs (800 °C, 900 °C and 1000 °C). EIS spectra were measured at 700 °C with synthetic air flow (21% O2, 40 ml min-1). Results converted to electrode surfaces area and dived by two...