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Search results for: CALIX[4]ARENES
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4-Point beam tensile test on a soft adhesive
PublicationAn adhesive butt joint with a soft bondline has been studied. A series of experiments was conducted on test pieces constituted of aluminium adherends bonded with a low modulus epoxy adhesive, ScotchWeld™ 2216. The joint was subjected to four point bending, in tension/compression loading, under constant deflection rate, with the bondline being parallel to the applied load. The objective was to examine and evaluate crack nucleation...
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O-substituted tetrahydroxamate derivatives of p-tert-butylcalix[4]arene as receptors for transition and heavy metal cations
PublicationTetrasubstituted O-hydroxamate derivatives of p-tert-butylcalix[4]arene were applied as active materials in ion-selective membrane electrodes and were tested towards Pb-selectivity. The electrodes gave near-Nernstian characteristics for Pb2+ cations. The selectivity coefficients were determined. The influence of plasticizer on the electrode behaviour was studied. The dependence of the chemical structure on selectivity coefficients...
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A novel nucleotide found in human erythrocytes, 4-pyridone-3-carboxamide-1-beta-D-ribonucleoside triphosphate
PublicationZidentyfikowano nowy, nieznany nukleotyd, występujący w erytrocytach osób chorych na przewlekłą niewydolność nerek, w stężeniu porównywalnym do zawartości ATP. Nukleotyd ten wyizolowano chromatograficznie, a jego strukturę określono jako trójfosforan 4-piridono-3-karboksyamido-1-b-D-rybonukleozydu, na podstawie danych spektralnych UV, MS, IR i NMR.
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Graphene hydrogels with embedded metal nanopatricles as efficient catalysts in 4-nitrophenol reduction and methylene blue decolorization
PublicationSynthesis and characterization of the graphene hydrogels with three different metallic nanoparticles, that is Au, Ag and Cu, respectively is presented. Synthesized in a one-pot approach graphene hydrogels with embedded metallic nanoparticles were tested as heterogeneous catalysts in a model reaction of 4-nitrophenol reduction. The highest activity was obtained for graphene hydrogel with Cu NPs and additional reaction of methylene...
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Krzysztof Wilde prof. dr hab. inż.
PeopleKrzysztof Wilde (born January 11th, 1966 in Gdańsk) – expert in bridge structures, structural mechanics and diagnostics of civil structures. He conducted research on vibration reduction systems for bridges exposed to dynamic loads from winds and earthquakes. At present he is interested in the field of nondestructive testing of materials and structural health monitoring systems. Hi is author or coauthor of over 200 publications...
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Toxicity of the New Psychoactive Substance (NPS) Clephedrone (4-Chloromethcathinone, 4-CMC): Prediction of Toxicity Using In Silico Methods for Clinical and Forensic Purposes
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Structure and evolution of the 4-helix bundle domain of Zuotin, a J-domain protein co-chaperone of Hsp70
PublicationThe J-domain protein Zuotin is a multi-domain eukaryotic Hsp70 co-chaperone. Though it is primarily ribosome-associated, positioned at the exit of the 60S subunit tunnel where it promotes folding of nascent polypeptide chains, Zuotin also has off-ribosome functions. Domains of Zuotin needed for 60S association and interaction with Hsp70 are conserved in eukaryotes. However, whether the 4-helix bundle (4HB) domain is conserved remains...
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Nanocrystalline Polymer Impregnated [Fe(pz)Pt(CN)4] Thin Films Prepared by Matrix-Assisted Pulsed Laser Evaporation
PublicationIn this work, the fabrication of [Fe(pz)Pt(CN)4] (pz = pyrazine) thin films by means of matrix-assisted pulsed laser evaporation (MAPLE) was investigated. As starting material, a cryogenically cooled suspension of anocrystalline [Fe(pz)Pt- (CN)4] (0.35wt.-%) in a mixture of 1,1-dichloroethane and polyethylene glycol (PEG) was used. Films of a thickness up to 150–200 nm were deposited on Si substrates by laser ablation at λ = 1064...
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Targi Budownictwa i Architektury BUDMA, 4-7 lutego, Poznań
EventsNa targach powstanie strefa Start-up, gdzie zostaną zaprezentowane „technologie jutra”, czyli zaawansowane rozwiązania dla budownictwa i architektury. W tej strefie będą obecni przedstawiciele CTWiT PG.
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Algebraic periods and minimal number of periodic points for smooth self-maps of 1-connected 4-manifolds with definite intersection forms
PublicationLet M be a closed 1-connected smooth 4-manifolds, and let r be a non-negative integer. We study the problem of finding minimal number of r-periodic points in the smooth homotopy class of a given map f: M-->M. This task is related to determining a topological invariant D^4_r[f], defined in Graff and Jezierski (Forum Math 21(3):491–509, 2009), expressed in terms of Lefschetz numbers of iterations and local fixed point indices of...
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Weak localization competes with the quantum oscillations in a natural electronic superlattice: The case of Na1.5(PO2)4(WO3)20
PublicationWe report an investigation of the combined structural and electronic properties of the bronze Na1.5(PO2)4(WO3)20. Its low-dimensional structure and possible large reconstruction of the Fermi surface due to charge density wave instability make this bulk material a natural superlattice with a reduced number of carriers and Fermi energy. Signatures of multilayered two-dimensional (2D) electron weak localization are consequently reported,...
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Seminarium dyplomowe, sem.4
e-Learning CoursesSeminarium dyplomowe, sem.4, dr Karolina Tura-Gawron.
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Lead(II) coordination polymers with imidazole-4- and pyrazole-3-carboxylate isomeric linkers: Structural diversity and luminescence properties
PublicationUsing 1H-imidazole-4-carboxylic acid (4imCOOH) and 1H-pyrazole-3-carboxylic acid (3pyrCOOH) coordination polymers [Pb(4imCOO)2(H2O)]n (1) and [Pb2(3pyrCOO)4]n (2) were constructed. Obtained polymers were characterized via FT-IR, X-ray, PL and TG methods. The coordination polyhedron around Pb(II) in 1 is described as distorted pentagonal pyramid with hemidirected coordination sphere (based on DFT calculations). Compound 2 consists...
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NOMINATION DOSSIER, The Modernist Centre of Gdynia, parts 4 - 7
PublicationThe city of Gdynia is commonly known in Poland as a symbol of the country’s independence and evidence of the foresight of planners and politicians. It is the outcome of the efforts and aspirations of generations of people from all kinds of backgrounds who made Gdynia their home. Document prepared by researchers from Gdansk University of Technology and other experts is the important part of the Nomination Dossier prepared for international...
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Atropoisomerism in Mono- and Diaryl-Substituted 4-Amino-2,6-lutidines
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Selected Rheological Properties of RS3/4 Type Resistant Starch
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Chlorido(4-morpholinecarbodithioato-k2S,S')(triphenylphosphine)nickel(II)
PublicationPrzeprowadzono syntezę oraz wyznaczono strukturę związku [Ni(C5H8NOS2)Cl(C18H15P)]. Tytułowy kompleks chloro(morfolinoditiokarbaminiano-S,S')(trifenylofosfina)-nikiel(II) posiada nieznacznie zniekształcony płaski kwadratowy rdzeń NiClS2P.
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Rozdział 4. Mutagenne, rakotwórcze i przeciwrakotwórcze składniki żywności
PublicationMutagenami są nazywane czynniki i substancje mogące powodować zmiany w zapisie genetycznym, kancerogenami lub czynnikami rakotwórczymi natomiast te, które przyczyniają się do powstawania nowotworów, z wyłączeniem podatności uwarunkowanej genetycznie. Przetwórstwo, a w szczególności obróbka termiczna żywności, jest główną przyczyną tworzenia się mutagenów i kancerogenów; niemniej jednak zwiększają one trwałość żywności. Badania...
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Model of the combustion process in the marine 4-stroke diesel engine
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Influence of processing conditions on crystal structure of BiNbO 4 ceramics
PublicationBismuth niobate (BiNbO4) has attracted attention as a low-fired ceramics with promising microwave application potential. It belongs to the bismutocolumbite oxides with similarly to scheelite-like stibiotantalite structure (SbTaO4) A3+B5+O4. Aim of the present research was to fabricate BiNbO4 ceramics by solid state reaction route from the mixture of simple oxides viz. Bi2O3, and Nb2O5, and study its phase composition as well as...
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Międzynarodowa Konferencja ''Dziedzictwo Techniki - spojrzenie z Gdańska 4''
PublicationOmówiono tło i przebieg przedmiotowej konferencji, która odbyła się w ramach uroczystości Jubileuszu 100-lecia politechniki w Gdańsku i 60-lecia Politechniki Gdańskiej.
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The template synthesis and complexation properties of the methoxypyrogal-lo[4]arene
PublicationZaprezentowano metodę syntezy templatowej MPA. Obserwowano kompleksowanie silnych akceptorów elektronów przez MPA. Analiza widm ESI-MS wykazała właściwości kompleksujące w stosunku do kationów metali alkalicznych. Właściwości jonoforowe związku badano w membranowych elektrodach jonoselektywnych.
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Dissociative Electron Attachment to 5-Iodo-4-thio-2′-deoxyuridine: A Potential Radiosensitizer of Hypoxic Cells
PublicationIn the search for effective radiosensitizers for tumor cells, halogenated uracils have attracted more attention due to their large cross section for dissociation upon the attachment of low-energy electrons. In this study, we investigated dissociative electron attachment (DEA) to 5-iodo-4-thio-2'-deoxyuridine, a potential radiosensitizer using a crossed electron-molecule beam experiment coupled with quadrupole mass spectrometry....
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Influence of Wood Moisture on Strength and Elastic Modulus for Pine and Fir Wood Subjected to 4-point Bending Tests
PublicationThe main purpose of this research paper was to determine the influence of the wood moisture on the strength and elastic modulus of pine and fir wood specimens subjected to the 4-point bending tests. Six bending tests for each wood species and for two different moisture level have been performed. Then, the advanced statistical analysis of the results has been carried out. On the basis of the obtained results, it has been noted that...
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Kwas stearidonowy C18:4 (n-3) - źródła roślinne i potencjalne znaczenie w żywieniu człowieka
PublicationPrzedmiotem publikacji jest omówienie znaczenia wielonienasyconych kwasów tłuszczowych (WNKT) w żywieniu człowieka, roli kwasu stearidonowego C18:4 n-3 (SDA) w łańcuchu metabolicznym i przedstawienie źródeł olejów roślinnych zawierających SDA. Na celowość stosowania roślinnych źródeł SDA w żywieniu człowieka wskazuje ogólny deficyt długołańcuchowych WNKT n-3 w typowej diecie europejskiej, związany głównie z małą popularnością produktów...
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THE GENE CLONING, OVEREXPRESSION, PURIFICATION AND BIOCHEMICAL CHARACTERISATION OF A NEW COLD-ADAPTED β–GALACTOSIDASE FROM ARTHROBACTER SP. VII-4
PublicationINTRODUCTION. β-Galactosidase [EC 3.2.1.23] is an enzyme that catalyzes the hydrolysis of O-glycosidic linkages in galactosides. It is commercially used in dairy industry for the production of milk with reduced lactose content. Potentially, the best method for lactose removal under cooling conditions should be carried out with a cold-adapted enzyme. AIM. The aim of this study was to determine the taxonomic affiliation of the isolate...
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Raport z badań podczas próbnego obciążenia przęseł nr 4-6 mostu drogowego przez rzekę Wisłę w Tczewie
PublicationW pracy przedstawiono metodykę pomiarów i wyniki badań podczas próbnego obciążenia przęseł nr 4-6 mostu drogowego przez rzekę Wisłę w Tczewie. Sformułowano wnioski dotyczące rzeczywistej pracy konstrukcji i warunków dalszej eksploatacji obiektu
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Fatal intoxication with U-47700 in combination with other NPS (N-ethylhexedrone, adinazolam, 4-CIC, 4-CMC) confirmed by identification and quantification in autopsy specimens and evidences
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Wykonanie badań nieniszczących krzyżownicy oraz śrub sprzęgła Hydrozespołu nr 4 w Elektrowni Wodnej we Włocławku
PublicationCelem badań było określenie stanu technicznego spoin krzyżownicy górnej łożyska prowadzącego generatora hydrozespołu nr 4 w Elektrowni wodnej we Włocławku. Badaniom nieniszczącym VT, UT i MT poddano spoiny czołowe i pachwinowe 12 ramion krzyżownicy, oraz dwa rodzaje śrub sprzęgła. Wykryte niezgodności spawalnicze opisano, podając przyczyny ich powstawania. Opracowano wytyczne technologiczne naprawy, ze szczególnym uwzględnieniem...
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Synthesis, anticandidal activity of N3-(4-methoxyfumaroyl)-(S)-2,3-diaminopropanoic amide derivatives – Novel inhibitors of glucosamine-6-phosphate synthase
PublicationNovel FMDP amiders 4-6 have been synthesized and tested against Candida strains. The anticandidal activity has been confined only to Candida albicans. Anticandidal activity of the tested amides has correlated with their inhibitory activity of glucosamine-6-phosphate synthase in cell free extract from Candida albicans.
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Alternative method for the synthesis of imidazo[5,1-f][1,2,4]triazin-4(3H)-one—a substrate for the preparation of phosphodiesterase (5) inhibitors
PublicationImidazo[5,1-f][1,2,4]triazin-4(3H)-ones, as isosteres of purine, are of interest for pharmaceutical research as potential substrates for the synthesis of cGMP-PDE5 inhibitors. We present a novel, alternative method for the synthesis of imidazotriazinones, that differs from the previously reported ones with respect to the method of construction of the triazinone ring in the molecule. The key step in our approach is condensation...
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Dielectric Properties of BiNbO<sub>4</sub>-Based Ceramic-Polymer Composites with 0-3 Connectivity
PublicationIn the present study two-phase BiNbO4//PVDF composites with 0-3 connectivity were studied by impedance spectroscopy within the frequency range Δν=100Hz-1MHz at room temperature. Polyvinylidene fluoride (PVDF) acted as a matrix whereas bismuth niobate (BiNbO4) powder acted as a dispersed phase. The volume fraction of the ceramic phase was cV=2, 4, 6, 8, 10, 16 and 20vol%. Analysis of the impedance data registered for composites...
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Numerical Analysis of TB32 Crash Tests for 4-cable Guardrail Barrier System Installed on the Horizontal Convex Curves of Road
PublicationHorizontal curves are one of the elements of road infrastructure where statistically a relatively high number of accidents have been reported. In the last ten years in Poland approx. 10% of all road accidents happened on horizontal curves of roads and was responsible for approx. 14% of all fatalities on Polish roads. Thus, this issue is important and requires extensive research and proper road safety treatments. One possible measure...
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Badania odporności warystorów z wykorzystaniem wymagań pomiarowych zawartych w normie PN EN 61000-4-5
PublicationBadania odporności w EN 61000-4-5 są jednymi z podstawowych badań wykonywanych w ramach testów EMC na portach wejścia wyjścia urządzeń elektronicznych. W referacie przedstawiono uproszczoną metodykę doboru warystorów stanowiących zazwyczaj jeden z elementów ochronnych stosowanych na badanych portach. Proponowana metoda doboru powinny być wykonywana przez projektanta/konstruktora na początku procesu projektowego danego urządzenia....
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New imidazoline/alpha2-adrenoceptors affecting compounds - 4(5)-(2-aminoethyl)imidazoline (dihydrohistamine) derivatives. synthesis and receptor affinity studies
Publicationpołączenie struktury agmatyny i imidazoliny pozwoliło na otrzymanie nowej grupy ligandów receptorów imidazolinowych i alfa2-adrenergicznych, pochodnych 4(5)-(2-aminoetylo)imidazoliny. otrzymano oraz zbadano oddziaływanie nowych pochodnycch jak i analogów znanych ligandów - klonidyny, rilmenidyny, idazoksanu i antazoliny w stosunku do receptorów imidazolinowych oraz alfa2-adrenergicznych.
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Technika cyfrowa - laboratorium 2023/4
e-Learning CoursesStrona wspomagajaca kurs Technika cyfrowa - laboratorium 2023/4
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Synthesis, characterization and Luminescent Properties of New Coordination Polymers Based on p-tert Butylcalix[4]arene-tetracarboxylic acid and Lanthanine cations
PublicationA series of new coordination polymers based on p-tert-butylcalix[4]arene-tetracarboxylic acid with Eu3+, Tb3+wrer prepared by hydro and solvothermal methods. the obtained solid compounds were characterized by infrared and luminescence spectroscopy, powder X-ray diffraction, scianning electron microscopy and thermogravimetric anylisis. The infrared curves and the x-ray diffraction patterns indicate that the same crystalline structure...
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The influence of the fuel spray nozzle geometry on the exhaust gas composition from the marine 4-stroke diesel engine
PublicationThe paper presents experimental research on a 4-stroke, 3-cylinder, turbocharged AL25/30 Diesel engine. Research consisted in investigating the effect of the geometry of the fuel injectors on the exhaust gas composition from the engine. During measurements, the engine was operated with a regulator characteristic of a load range from 40 kW to 280 kW, made by electric water resistance. The engine was mechanically coupled to the electric...
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Serum Fatty Acid-Binding Protein 4 is Increased in Patients with Psoriasis
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Effect of the Botanical Origin on Properties of RS3/4 Type Resistant Starch
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Broadband NaK2Li[Li3SiO4]4:Ce Alkali Lithosilicate Blue Phosphors
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Micropatterning of BiVO 4 Thin Films Using Laser-Induced Crystallization
PublicationRelatively high temperatures even up to 500 °C are required to obtain bismuth vanadate (BiVO4) films with the scheelite monoclinic (s-m) structure that shows the highest photocatalytic activity. This requirement limits the possible choice of substrates. Moreover, high quality thin layers of crystalline BiVO4 cannot be prepared with current methods. In this study a light-induced crystallization approach is presented, which is a...
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Synthesis, Molecular Structure, Anticancer Activity, and QSAR Study of N-(aryl/heteroaryl)-4-(1H-pyrrol-1-yl)Benzenesulfonamide Derivatives
PublicationA series of N-(aryl/heteroaryl)-4-(1H-pyrrol-1-yl)benzenesulfonamides were synthesized from 4-amino-N-(aryl/heteroaryl)benzenesulfonamides and 2,5-dimethoxytetrahydrofuran. All the synthesized compounds were evaluated for their anticancer activity on HeLa, HCT-116, and MCF-7 human tumor cell lines. Compound 28, bearing 8-quinolinyl moiety, exhibited the most potent anticancer activity against the HCT-116, MCF-7, and HeLa cell lines,...
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Comparison of hydrogen bonds and diverse weak interactions of the nitro group in 2-methyl-4-nitroanilinium nitrate, bisulfate and two hexafluoridosilicates: elementary graph-set approach
PublicationCrystal structures of (H2m4na)NO3 (1), (H2m4na)HSO4 (2), (H2m4na)2SiF6 (3) and (H2m4na)2SiF6*2H2O (4), where 2m4na = 2-methyl-4-nitroaniline, are presented. Two layers of interactions occur in the structures, N—H...O/F hydrogen bonds and interactions with the nitro group. Although diverse, hydrogen-bonding patterns are compared with each other by means of interrelations among elementary graph-set descriptors and descriptors of hydrogen-bonding...
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Identification of novel psychoactive substances 25B-NBOMe and 4-CMC in biological material using HPLC-Q-TOF-MS and their quantification in blood using UPLC–MS/MS in case of severe intoxications
PublicationThis paper describes cases of poisoning caused by new psychoactive substances such as: 25BNBOMe (2-(4-bromo-2,5-dimethoxyphenyl)-N-[(2-methoxyphenyl)methyl]ethanamine) and 4-CMC (1-(4-chlorophenyl)-2-(methylamino)-1-propanone). The analytical procedure includes rapid and selective method for the extraction and determination of 4-CMC and 25B-NBOMe in blood samples using UPLC–MS/MS technique. To the best of our knowledge,this is...
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Sylwester Kaczmarek dr hab. inż.
PeopleSylwester Kaczmarek received his M.Sc in electronics engineering, Ph.D. and D.Sc. in switching and teletraffic science from the Gdansk University of Technology, Gdansk, Poland, in 1972, 1981 and 1994, respectively. His research interests include: IP QoS and GMPLS and SDN networks, switching, QoS routing, teletraffic, multimedia services and quality of services. Currently, his research is focused on developing and applicability...
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4-[(tert-Butyldimethylsilyl)oxy]-6-methoxy-7-methyl-5-(oxiran-2-ylmethyl)-2-benzofuran-3(1H)-one
PublicationThe title compound, C19H28O5Si, was obtained in the reaction of 1,3-dihydro-4-[(tert-butyldimethylsilyl)oxy]-6-methoxy-7-methyl-3-oxo-5-(prop-2-enyl)isobenzofuran with meta-chloroperbenzoic acid. This reaction is one of the stages of the total synthesis of mycophenolic acid, which we attempted to modify. The title compound forms crystals with only weak intermolecular interactions. The strongest stacking interaction is found between...
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Analiza przyczyn powstawania uszkodzeń na gzymsach obiektu GM 1-2 wykonanego w ramach zadania „Budowa drogi publicznej drogowej trasy średnicowej Katowice - Gliwice, część „zachód" od ul. Baildona w Gliwicach do terenu miasta Zabrze od km 4+037,37 do km 5+320,00 (odcinek nr G2/4)", roboty gwarancyjne
PublicationCelem opracowania jest określenie przyczyn powstania uszkodzeń (zarysowania i zacieki) na gzymsach obiektu GM1-2 wykonanego w ramach zadania „Budowa drogi publicznej drogowej trasy średnicowej Katowice - Gliwice, część „zachód" od ul. Baildona w Gliwicach do terenu miasta Zabrze od km 4+037,37 do km 5+320,00 (odcinek nr G2/4)".
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The CFD analysis of influence the start of fuel injection (SOI) on combustion parameters and exhaust gas composition of the marine 4-stroke engine
PublicationThe paper presents a theoretical analysis of the impact of injection timing on the parameters of the combustion process and the composition of exhaust gas from a 4-stroke engine designed to shipbuilding. The analysis was carried out based on a three-dimensional multi-zone model of the combustion process. This model has been prepared on the basis of properties of the research facility. The input data to the model were obtained through...
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Koncert: Muzyka chóralna z 4(41) stron świata
EventsKoncert w ramach Politechniki Otwartej: „Muzyka chóralna z 4(41) stron świata” w wykonaniu Chóru Kameralnego 441 Hz. Wstęp wolny.