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Search results for: ULTRA-FAST GC
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Fast numerical analysis of dielectric resonators with perturbed rotational symmetry
PublicationW artykule zaprezentowano metody szybkiej analizy rezonatorow o symetrii zblizonej do osiowej metodą różnic skończonych w dziedzinie częstotliwości. Dzięki użyciu techniki rozwinęć funkcyjnych w jednorodnych obszarach uzyskano redukcję rozmiaru i znaczne przyspieszenie zbieżności problemu własnego, reprezentującegowspomniane układy. Dzięki elastycznemu sposobowi łączenia dziedzin z i bez rozwinięć funkcyjnych możliwe było zaadaptowanie...
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Improved Efficacy Behavioral Modeling of Microwave Circuits through Dimensionality Reduction and Fast Global Sensitivity Analysis
PublicationBehavioral models have garnered significant interest in the realm of high-frequency electronics. Their primary function is to substitute costly computational tools, notably electromagnetic (EM) analysis, for repetitive evaluations of the structure under consideration. These evaluations are often necessary for tasks like parameter tuning, statistical analysis, or multi-criterial design. However, constructing reliable surrogate models...
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INTER-LAYER SHARING OF BACKUP PATH CAPACITIES PROVIDING FAST SERVICE RECOVERY IN IP-MPLS/WDM NETWORKS
PublicationIn this paper, we investigate the issue of providing the transmission continuity in IP-MPLS/WDM networks in the presence of failures of nodes/links. Special focus is put on assuring fast restoration of flows affected after a failure in a scenario assuming sharing the backup path capacities in order to decrease the overall bandwidth consumption. In particular, we propose a new approach to inter-layer sharing of link capacity reserved...
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The chromatographic analysis of extracts from poplar (Populus sp.) - Laying program GC-MS
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Endogenous oxidative DNA base modifications analysed with repair enzymes and GC/MS technique
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Evaluation of the usefulness and optimization of the separation conditions in Empty Column Gas Chromatography (EC-GC)
PublicationDotychczasowe badania wykazały, że możliwe jest rozdzielanie wysokowrzących mieszanin techniką chromatografii gazowej z zastosowaniem pustej rurki kapilarnej z topionej krzemionki, zamiast kolumn zawierających fazę stacjonarną. Operacja rozdzielania chromatograficznego ma miejsce jedynie na zasadzie różnicy temperatur wrzenia rozdzielanych substancji. Wysoki stopień podobieństwa warunków rozdzielania, osiąganych w ten sposób, z...
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Derivatization of acidic herbicides with selected tetraalkyl ammonium and trimethyl sulfonium hydroxides for their GC analysis.
PublicationPrzedstawiono badania na temat oznaczania herbicydów z grupy fenoksykwasów (MCPP, MCPA, 2,4-D, 2,4,5-T) i fenoli (Dinoterb, Dinoseb, Pentachlorofenol) z wykorzystaniem chromatografii gazowej po uprzedniej derywatyzacji. Proces derywatyzacji przeprowadzano w dozowniku chromatografu gazowego za pomocą TMPH, TMSH i TMAH. Zbadano wpływ temperatury dozownika chromatografu, środowisko reakcji (rozpuszczalnik) i nadmiar odczynnika na...
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Evaluation of structural change during fast transformation process of cross-linked NR into liquid NR by light pyrolysis
PublicationThe presence of cross-linked networks in rubber creates a tremendous problem for recycling and reusing of waste rubber. Fast transformation of cross-linked natural rubber (NR) into liquid natural rubber was carried out by light pyrolysis in temperature range from 240 to 300 °C in variable time (in range: 1–30 min). The transformation efficiency was evaluated by measuring the sol fraction and the cross-link density of the gel fraction....
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An MOR Algorithm Based on the Immittance Zero and Pole Eigenvectors for Fast FEM Simulations of Two-Port Microwave Structures
PublicationThe aim of this article is to present a novel model-order reduction (MOR) algorithm for fast finite-element frequency-domain simulations of microwave two-port structures. The projection basis used to construct the reduced-order model (ROM) comprises two sets: singular vectors and regular vectors. The first set is composed of the eigenvectors associated with the poles of the finite-element method (FEM) state-space system, while...
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The Prognostic Value of PI-RADS Score in CyberKnife Ultra-Hypofractionated Radiotherapy for Localized Prostate Cancer
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Position of LiF:Mg,Cu,P TL peak as an alternative method for ultra-high-dose dosimetry
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Ultra-stable sandwich shaped flexible MXene/CNT@Ni films for high performance supercapacitor
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Metabolic responses to a 48-h ultra-marathon run in middle-aged male amateur runners
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Application of dynamic headspace and gas chromatography coupled to mass spectrometry (DHS-GC-MS) for the determination of oxygenated volatile organic compounds in refinery effluents
PublicationThe paper presents a new procedure for the determination of oxygenated volatile organic compounds (O-VOCs) in postoxidative effluents from the production of petroleum asphalt using dynamic headspace coupled to gas chromatography-mass spectrometry in the selected ion monitoring (SIM) mode (DHSGC-MS). Among the GC capillary columns tested, a polar SLB-IL111 column with the ionic liquid stationary phase was found to be superior due...
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New procedure of silica gel surface modification-preparation of gaseous standard mixtures of methyl chloride using the technique of thermal decomposition of the surface compound for calibration of a TD-GC-FID system.
PublicationPrzedstawiono nową procedurę modyfikacji powierzchni żelu krzemionkowego w celu wytworzenia związku powierzchniowego będącego źródłem chlorku metylu. Minimalna temperatura rozkładu (150 st. C) zapewnia trwałość chemicznie modyfikowanego złoża w temp. pokojowej. Badania prowadzono w temperaturze optymalnej (280 st.C). Stwierdzono, że powierzchnia żelu jest obsadzona jednorodnie przez związek powierzchniowy i gazowa mieszanina wzorcowa...
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Fast rns scaling of signed numbers based on the chinese remainder theorem
PublicationPrzedstawiono architekturę szybkiego skalera resztowego dla liczb ze znakiem dla modułów 5-bitowych opartego na chińskim twierdzeniu o resztach. W architekturze zastosowano wyznaczanie projekcji ortogonalnych przy użyciu funkcji logicznych 5 zmiennych, sumator kodulo m/k oraz wejściowy konwerter do systemu resztowego. Operacja modulo m/k jest wykonywana przy zastosowaniu drzewa 4-operandowych sumatorów modulo 2m/k i końcowego...
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?? of the Sky? - automated search for fast optical transients over the whole sky
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A fast algorithm for computing the flux around non-overlapping disks on the plane
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Standard and Fast Selective Catalytic Reduction of NO with NH3on Zeolites Fe-BEA
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Future hosts for fast and high light output cerium-doped scintillator
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Characterization of PLZT Thin Films for Fast Electro-Optical Sampling Circuits
PublicationW artykule omówiono technologię wytwarzania cienkich warstw wybranych kompozycji ceramik ołowiowo-lantanowo-cyrkonowo-tytanowych, nazywanych ceramikami PLZT. Przedstawiono wyniki badań jakości warstw za pomocą techniki XRD. wyniki pomiaru grubości warstw, ich względnej przenikalności dielektrycznej i współczynnika załamania. Omówiono kierunki dalszych prac.
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A new approach to a fast and accurate design of microwave circuits with complex topologies
PublicationA robust simulation-driven design methodology of microwave circuits with complex topologies has been presented. The general method elaborated is suitable for a wide class of N-port unconventional microwave circuits constructed as a deviation from classic design solutions. The key idea of the approach proposed lies in an iterative redesign of a conventional circuit by a sequential modification and optimisation of its atomic building...
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Macromodeling of multiport systems using a fast implementation of the vector fitting method
PublicationMakromodelowanie układów wieloportowych przy użyciu vector fittingu jest czasochłonne oraz wymaga dużych zasobów obliczeniowych w przypadku gdy wszystkie elementy macierzy systemowej dzielą wspólne bieguny. Artykuł prezentuje stabilne rozwiązanie, które usuwa problem rzadkości macierzy poprzez zastosowanie bezpośrednie dekompozycje QR. Jako przykład przedstawiony został 60 portowy układ, który ilustruje oszczędność czasu potrzebnego...
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Fast multiplexer cad using surrogate models for channel filters synthesis
Publicationartykuł przedstawia metodę szybkiego projektowania multiplekserów mikrofalowych wykorzystującą dokładne modele zastępcze na etapie projektowania kanałów. przedstawiony został przykład trój-kanałowego multipleksera z filtrami dwurodzajowymi.
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Fast Full-Wave Multilevel Zero-Pole Optimization of Microwave Filters
PublicationA new concept is proposed for the full-wave computer-aided design of microwave filters. The method consists of two stages and operates on the zeros and poles of the transfer function and their derivatives. These quantities are evaluated from the response computed by a full-wave electromagnetic solver with two levels of accuracy. The two stages make use of different models that are optimized using a low-accuracy electromagnetic...
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Application of smart glasses for fast and automatic color correction in health care
PublicationIn recent years different applications of smart glasses in health care have been proposed. In this paper we present the experiments related to automatic color correction using smart glasses platform developed within the eGlasses project. The color pattern is proposed and tested enabling the automatic detection of the pattern and automatic correction of colors. Additionally, the method for encoding and decoding of patient ID in...
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Network Graph Transformation Providing Fast Calculation of Paths for Resilient Routing
PublicationProtection of transmission against failures can be appropriately dealt with by alternative paths. However, common schemes (e.g., Bhandaris scheme) are characterized by a remarkable delay while determining the transmission paths. This in turn may have a serious impact on serving dynamic demands (characterized by relatively short duration time). As a remedy to this problem, we introduce an approach to pre-compute the sets of disjoint...
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Novel fast non-linear electrochemical impedance method for corrosion investigations
PublicationThe paper presents a novel approach to corrosion rate monitoring using non-linear electrochemical impedance spectroscopy. The authors propose a new variant of non-linear impedance measurement using amplitude-modulated multi-frequency ac perturbation signal. It allows shortening of measurement duration so it is possible to monitor corrosion rate of the systems experiencing rapid changes. In this way a limitation resulting from lack...
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Fast Design Optimization of Waveguide Filters Applying Shape Deformation Techniques
PublicationThis paper presents an efficient design of microwave filters by means of geometry optimization using shape deformation techniques. This design procedure allows for modelling complex 3D geometries which can be fabricated by additive manufacturing (AM). Shape deforming operations are based on radial basis function (RBF) interpolation and are integrated into an electromagnetic field simulator based on the 3D finiteelement method (FEM)....
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Fast description of medical images using run length encoded regions.
PublicationZaprezentowano szybką, adaptacyjną metodę progowania oraz opisu obrazów medycznych w oparciu o ich reprezentację za pomocą kodów długości serii (RLC). Przedstawiono możliwości wyznaczania deskryptorów kształtu oraz analizy porównawczej regionów. Omówiono właściwości metody oraz przykładowe rezultaty.
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Fast recursive basis function estimators for identification of time-varying processes
PublicationW pracy wprowadzono nową kategorię filtrów adaptacyjnych opartych na metodzie funkcji bazowych i wykorzystujących koncepcję postfiltracji. Proponowane algorytmy pozwalają połączyć niską złożoność obliczeniową i dobre właściwości śledzące.
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GC-MS-based untargeted metabolomics of plasma and urine to evaluate metabolic changes in prostate cancer
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Validated GC–MS method for determination of bisphenol a and its five analogues in dietary and nutritional supplements
PublicationBisphenol A (BPA) and its analogues showing structural and functional similarity to BPA are commonly applied in various industrial applications and thus are becoming ubiquitous in the environment. At the same time there is increasing scientific evidence that exposure to these chemicals may lead to adverse health effects in human and wildlife. In recent years dietary and nutritional supplements dedicated for athletes have become...
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Determination of environmental pollutants in soil and sediments - some aspects of sample clean-up and GC analysis
PublicationPrzedstawiono wstępne wyniki badań nowej procedury analitycznej przeznaczonej do badań próbek i osadów dennych na zawartość związków organicznych (WWAPCB). Procedura składa się z następujących etapów: - ekstrakcji analitów z wykorzystaniem techniki ASE, - oczyszczania ekstraktów (kolumienki), - chromatograficznego rozdzielania i oznaczania analitów.
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Distillation cleanup preceded gc determination of short-chain monocarboxylic acids in aqueous and solid samples of wastewater origin = Oznaczanie krótkołańcuchowych kwasów monokarboksylowych w próbkach wodnych i stałych pochodzących z oczyszczalni ścieków z wykorzystaniem chromatografii gazowej poprzedzonej destylacją
PublicationShort-chain monocarboxylic acids (SCMAs) (C2-C5) formed in the process of aerobic biodegradation of larger organic molecules should often be monitored to optimize wastewater biological treatment and study the processes of converting organic waste matter into methane, etc. Gas chromatography (GC) seems a method of choice for such a task. Majority of samples require clean up before they can be injected into GC system. In this work...
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The use of fast molecular descriptors and artificial neural networks approach in organochlorine compounds electron ionization mass spectra classification
PublicationDeveloping of theoretical tools can be very helpful for supporting new pollutant detection. Nowadays, a combination of mass spectrometry and chromatographic techniques are the most basic environmental monitoring methods. In this paper, two organochlorine compound mass spectra classification systems were proposed. The classification models were developed within the framework of artificial neural networks (ANNs) and fast 1D and...
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Multi-Site Cation Control of Ultra-Broadband Near-Infrared Phosphors for Application in Light-Emitting Diodes
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Person Tracking in Ultra-Wide Band Hybrid Localization System Using Reduced Number of Reference Nodes
PublicationIn this article a novel method of positional data integration in an indoor hybrid localization system combining inertial navigation with radio distance measurements is presented. A point of interest is the situation when the positional data and the radio distance measurements are obtained from less than thee reference nodes and it is impossible to unambiguously localize the moving person due to undetermined set of positional equations....
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Fast tolerance-aware design optimization of miniaturized microstrip couplers using variable-fidelity EM simulations and re-sponse features
PublicationManufacturing tolerances and other types of uncertainties may considerably affect operation and performance of microwave components and systems. Quantification of these effects is therefore an important part of the design process. It is even more important to obtain designs whose sensitivity to parameter deviations is reduced as much as possible. All of these require statistical analysis carried out at the level of electromagnetic...
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Novel fast analytical method for indirect determination of MCPD fatty acid esters in edible oils and fats based on simultaneous extraction and derivatization
PublicationA novel method for indirect determination of MCPD esters levels in lipid samples has been developed. The method is based on combination of extraction and derivatisation in the same sample preparation step. It is achieved by the application of diethyl ether as extraction solvent for isolation of released from esterified forms analytes from water phase and dilution solvent for solid PBA – derivatisation agent. It is a noteworthy...
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Rapid Re-Design and Bandwidth/Size Trade-Offs for Compact Wideband Circular Polarization Antennas Using Inverse Surrogates and Fast EM-Based Parameter Tuning
PublicationDesign of compact wideband circularly polarized (CP) antennas is challenging due to the necessity of simultaneous handling of several characteristics (reflection, axial ratio, gain) while maintaining a small size of the structure. Antenna re-design for various operating bands is clearly more difficult yet practically important because intentional reduction of the bandwidth (e.g., by moving the lower edge of the operating band up...
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Pi of the Sky – all-sky, real-time search for fast optical transients
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Estimation of Solar Energy Influx to the Sea in the Light of Fast Satellite Technique Development
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SU‐GG‐T‐290: A Fast Optical CT Scanner for Gel Dosimetry
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A note on fast approximate backbone coloring of split graphs with star--like backbones
PublicationDla grafu G = (V, E) z wyróżnionym podgrafem H, kolorowanie szkieletowe jest zdefiniowane jako odwzorowanie c spełniające |c(u) - c(v)| > 1 dla każdej krawędzi z E(H) oraz |c(u) - c(v)| > 0 dla każdej krawędzi z E(G). W pracy przedstawiono 1-przybliżony algorytm kolorowania szkieletowego split grafów ze skojarzeniem w szkielecie o złożoności O(|V|) oraz 1-przybliżony algorytm dla split grafów z rozłącznymi gwiazdami w szkielecie.
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Organic-inorganic materials for fast charging-discharging processes in energy storage devices
PublicationPraca dotyczy materiału kompozytowego złożonego z poli(3,4-etylenodioksytiofenu) i heksacyjanokobaltanu żelaza. Materiał został otrzymany elektrochemicznie bezpośrednio na elektrodzie tytanowej metodą jednoetapowa z zawiesiny zawierającej monomer (EDOT) oraz Fe3[Co(CN)6]2 w postaci proszku. Warstwy pEDOT/FehcCo otrzymane potencjostatycznie ładunkiem od 0,6 do 1,5 C/cm2 charakteryzują się różną grubością (od 1,9 do 4 μm) zależną...
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Fast dynamics in the optical storage with Langmuira-Blodgett films of a diazocrown ether molecule
PublicationMolekuły z resztą azobenzenu badano z punktu widzenia licznych aplikacji wykorzystujących cykle fotoizomeryzacji trans-cis-trans, wiodących do uporządkowania cząsteczek, a nawet do transportu masy w mikroskali. Ważnym ograniczeniem dla tych materiałów jest powolna dynamika procesu porządkowania, wymagającego molekularnych przekształceń. W tej pracy informujemy o filmach Langmuira-Blodgett (LB) pochodnej eteru azokoronowego (29-membered...
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Response features for fast EM-driven design of miniaturized impedance matching transformers
PublicationA framework for low-cost EM-driven design optimization of compact impedance matching transformers is presented. Our technique is based on a bottom-up design where design requirements for the transformer circuit are translated into specifications for its building blocks. These elementary cells are optimized using response features. Subsequently, the entire circuit is fine-tuned using local response surface approximation models and...
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Fast Antenna Optimization Using Gradient Monitoring and Variable-Fidelity EM Models
PublicationAccelerated simulation-driven design optimization of antenna structures is proposed. Variable-fidelity electromagnetic (EM) analysis is used as well as the trust-region framework with limited sensitivity updates. The latter are controlled by monitoring the changes of the antenna response gradients. Our methodology is verified using three compact wideband antennas. Comprehensive benchmarking demonstrates its superiority over both...
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Diagonalized Macromodels in Finite Element Method for Fast Electromagnetic Analysis of Waveguide Components
PublicationA new technique of local model-order reduction (MOR) in 3-D finite element method (FEM) for frequency-domain electromagnetic analysis of waveguide components is proposed in this paper. It resolves the problem of increasing solution time of the reduced-order system assembled from macromodels created in the subdomains, into which an analyzed structure is partitioned. This problem becomes particularly relevant for growing size and...