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Search results for: FEW-LAYER BLACK PHOSPHORUS1,4-DIAMINE-9,10-ANTHRAQUINONENONCOVALENT FUNCTIONALISATIONELECTROCHEMICAL PROPERTIESELECTROCHEMICAL SENSOR
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Determination of long-chain aldehydes using a novel quartz crystal microbalance sensor based on a biomimetic peptide
PublicationThere is an increasingly popular trend aimed at improvement of fundamental metrological parameters of sensors via implementation of materials mimicking biological olfactory systems. This study presents investigation on usefulness of the peptide mimicking HarmOBP7 region as a receptor element of the piezoelectric sensor for selective analysis of long-chain aldehydes. Identification of odorant binding proteins creates new possibilities...
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DSC study of polyurethanes obtained from 4,4´bis(10-hydroxydecaoxy) biphenyl.
PublicationW naszych badaniach nad poliuretanami segmentowymi i sztywno segmentowymi, otrzymanymi z 4,4`-bis(6-hydroksyheksyloksy)bifenylu (BHHBP), diizocyjanianu4,4`-dicykloheksylometanu (HMDI) i oligo(adypinianu 1,6-heksylenu) stwierdziliśmy, że poliuretany otrzymane z HMDI o składzie 16% trans, trans-, 52%cis, trans- i 32% cis, cis-HMDI charakteryzują się znacznie niższymi temperaturami przejść fazowych, niż te otrzymane z frakcji...
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Density functional LCAO calculations of vibrational modes and phonon density of states in the strained single-layer phosphorene
PublicationThe paper presents an investigation of phosphorene under axial strain on the phonon density of states and vibrational modes. The studies were performed by means of density functional theory (DFT) within the linear combination of atomic orbitals (LCAO). The strained models were constructed using optimised supercell techniques. The vibrational mode spectra were estimated for strains applied for both the zigzag and armchair directions...
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Two isomorphic ZnII/CoII complexes with tri-tert-butoxysilanethiol and histamine, and (4-hydroxymethyl-1H-imidazole-κN)bis(tri-tert-butoxysilanethiolato-κ2O,S)zinc(II)
PublicationOtrzymano dwa izomorficzne kompleksy cynku(II) i kobaltu(II) z tri-tert-butoksysilanotiolem i histaminą oraz kompleks cynku(II) z tri-tert-butoksysilanotiolem i 4(5)-hydroksymetyloimidazolem. Scharakteryzowano strukturę otrzymanych kompleksów w ciele stałym.
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Thermal stability analysis of poly(lactic acid)-carbon black-nanodiamond composite
Open Research DataThis dataset contains thermal stability tests carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques include: thermogravimetric analysis (TGA)...
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Detection of Water on Road Surface with Acoustic Vector Sensor
PublicationThis paper presents a new approach to detecting the presence of water on a road surface, employing an acoustic vector sensor. The proposed method is based on sound intensity analysis in the frequency domain. Acoustic events, representing road vehicles, are detected in the sound intensity signals. The direction of the incoming sound is calculated for the individual spectral components of the intensity signal, and the components...
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LOW COST MEASUREMENT MODULE FOR MATRIX OF AMPEROMETRIC GAS SENSOR
PublicationThis paper describes an amperometric sensor module for gas concentration measurement. A module can be used for many types of electrochemical gas sensors without major hardware changes. Device is based on AVR ATmega8 microcontroller. As signal processing circuit a specialized integrated circuit LMP9l000 configurable via I2C interface is used. The concept of a measuring system composed of several modules dedicated for a gas sensors...
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Lower Rim Substituted tert-Butyl Calix[4]arenes (Part IV). Calix[4]arene-Crown Ethers as Ionophores in Plasticized PVC-membrane electrodes.
PublicationPrzedstawiono syntezę i charakterystykę trzech p-tert-butylokaliks[4]aren-koron-4, -5, -6 (związki 2 - 4 o różnej długości łańcucha polyoksaetylenowego łączącego distalne grupy OH). Syntezowane związki wykazują wysoką selektywność na kationy sodu, potasu lub cezu. Badano zależność pomiędzy stereochemiczną strukturą tych ligandów, a wyznaczonymi potencjometrycznie współczynnikami selektywności oraz wyznaczonymi stałymi trwałości...
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Photocatalytic and Self-Cleaning Properties of Ag-Doped TiO2~!2009-10-16~!2009-10-30~!2010-01-27~!
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Support for Employees with ASD in the Workplace Using a Bluetooth Skin Resistance Sensor–A Preliminary Study
PublicationThe application of a Bluetooth skin resistance sensor in assisting people with Autism Spectrum Disorders (ASD), in their day-to-day work, is presented in this paper. The design and construction of the device are discussed. The authors have considered the best placement of the sensor, on the body, to gain the most accurate readings of user stress levels, under various conditions. Trial tests were performed on a group of sixteen...
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4-methyl-1-nitroacridine derivative C-1748 induces apoptosis, mitotic catastrophe or senescence in human colon carcinoma HCT116 cells depending on p53 status
PublicationPrzeprowadzone badania miały na celu określenie zdolności pochodnej 4-metylo-1-nitroakrydyny C-1748 do uruchomienia apoptozy, katastrofy mitotycznej lub procesu starzenia komórek ludzkiego raka okrężnicy HCT116 posiadających dziki gen p53 oraz podlinii nie posiadającej tego genu. Wykazano, że pochodna C-1748 indukuje apoptozę w komórkach obu linii HCT116 w sposób zależny od czasu inkubacji, przy czym komórki HCT116 p53+/+ wykazują...
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Lokal zamienię od zaraz : przenoszeie aplikacji do środowiska operacyjnego solaris 10.
PublicationProblem przeróbki aplikacji do funkcjonowania w nowej wersji systemu operacyjnego może okazać się niebagatelny. Nawet jeśli same zmiany w aplikacji nie są skomplikowane, przejście przez stosowną część cyklu jej rozwoju zajmuje czas.Niestety, nierzadko oprócz przerabiania kodu samej aplikacji typu enterprise, trzeba uwzględnić jej integrację z nowym środowiskiem operacyjnym: nowe metody startowania, zmiany niektórych komend systemu...
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Is 9-acridinamine anion a dispersion-bound anion?
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2-Methylphenyl 2-methoxyacridine-9-carboxylate
PublicationThe title compound, C22H17NO3, crystallizes in the monoclinic space group P21/c with four molecules per unit cell. The molecules are arranged in centrosymmetric pairs, joined via the C and attached H atoms in the meta position relative to the methoxy group. These pairs are bonded in the crystalline phase as a result of non-specific dispersive interactions, and through a network of C—H⋯O interactions involving the non-bonded O...
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9 - Solid oxide fuel and electrolysis cells
PublicationIn this chapter, the fundamental reactions, the geometrical designs, the material requirements, and the status of SOFCs and SOECs are presented. In the following seven chapters, the most important components of an SOC are described and the chapter ends with a summary and outlook. The described components are: (i) oxygen-ion conductors (electrolyte), (ii) anode materials for SOFCs (cathode in SOEC mode), (iii) cathode materials...
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A New Approach to Capacitive Sensor Measurements Based on a Microcontroller and a Three-Gate Stable RC Oscillator
PublicationA complete smart capacitive sensor solution basedA complete smart capacitive sensor solution based on a microcontroller was developed. This approach includes the development of both the hardware and software. The hardware part comprises an 8-bit microcontroller equipped with two timers/counters and a three-gate stable RC relaxation oscillator. The software part handles system configuration, measurement control, communication control,...
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Preparation and HPLC evaluation of a new 1,3-alternate 25,27-bis-[p-chlorobenzyloksy]26,28-bis-[3-propyloxy]-calix[4]arene silica bonded stationary phase
PublicationPrzeprowadzono syntezę nowej fazy stacjonarnej HPLC na bazie pochodnej 25,27-bis-[p-chlorobenzyloksy]26,28-bis-[3-propyloksy]-kaliks[4]arenu zablokowanego w konformacji 1,3-naprzemianległej. Zbadano selektywność i sprawność fazy w stosunku do aromatycznych izomerów pozycyjnych, alkilobenzenów, WWA, sulfonamidów i niesterydowych leków przeciwbólowych.
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A measurement method for capacitive sensors based on a versatile direct sensor-to-microcontroller interface circuit
PublicationIn the paper, there is presented a new time-domain measurement method for determining the capacitance values of capacitive sensors, dedicated, among others, to capacitive relative humidity sensors. The method is based on a versatile direct sensor-to-microcontroller interface for microcontrollers with internal analog comparators (ACs) and with precision voltage reference sources, e.g. digital-to-analog converters (DACs). The reference...
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Rheology studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains rheology measurements carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques was performed by melt mass-flow rates (MFR)....
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Mechanical studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains mechanical tests carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques was dynamic mechanical analysis (DMA). The measurements...
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Electrochemical studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains electrochemical investigation on electrodes 3D printed using a new composite composed of poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The presented results contain:1. electrochemical characterisation...
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Potentiometric Oxygen Sensor with Solid State Reference Electrode
PublicationThe concentration or the partial pressure of oxygen in an environment can be determined using different measuring principles. For high temperature measurements of oxygen, ceramic-based sensors are the most practical. They are simple in construction, exploration and maintenance. A typical oxygen potentiometric sensor consists of an oxygen ion conducting solid electrolyte and two electrodes deposited...
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an intelligent image processing sensor - the algorithm and the hardware implementation
PublicationW artykule przedstawiono algorytm przeznaczony do rozpoznawania obiektów ruchomych w obrazie do celu analizy ruchu pojazdów. Algorytm został zrealizowany w układzie FPGA.Ang.: This paper describes the idea and theimplementation of the robust algorithm dedicated toextraction of moving vehicles from real-time cameraimages for the evaluation of traffic parameters, suchas the number of vehicles, their direction of movementand their...
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Morphology and properties of nanotubular oxide layer on the Ti13Zr13Nb alloy
PublicationThe Ti13Zr13Nb alloy in solid and porous form was oxidised. The constant voltage 20 V, oxidation time 0.5 and 1 h, and 1 M H3PO4 (orthophosphoric acid) with addition of HF (hydrofluoric acid) as a test solution were applied. SEM (Scanning Electron Microscope) examinations of surface, EDS (Energy Dispersive X-ray Spectroscopy) chemical analysis, nanohardness and nano-scratch tests, and corrosion potentiokinetic tests at various...
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Structural and Dynamic Properties of Water within the Solvation Layer around Various Conformations of the Glycine-based Polypeptide
PublicationSeveral conformations of the solvated glycine-based polypeptides were investigated using molecular dynamics simulations. Some properties of water in the neighboring space around these molecules were investigated. It was found that water forms a well-defined layer—the first solvation shell—around the peptide molecule, and thickness of this layer is independent of the peptide structure and is equal to approximately 0.28 nm. Within...
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Electrochemical sensor for measurement of volatile organic compounds employing square wave perturbation voltage
PublicationThe paper presents the results of investigation on a prototype sensor for measurement of benzaldehyde in air. Sensitivity and limit of quantification of the sensor were determined for different internal electrolyte using the square wave voltammetry (SWV) as a detection technique. The working and counter electrodes were made of platinum. Ionic liquids 1-hexyl, 3-methylimidazolium chloride,1-hexyl, 3-methylimidazolium bis (trifluoromethanesulfonyl)...
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Mechanika ruchu pojazdów - W-10/Ć-10/L-10/P-0, WIMiO, MiBM, II st., sem. 02, niestacjonarne (PG_00057463), semestr zimowy 2022/2023, ZIMA
e-Learning CoursesWspółczynnik przyczepności. Hamowanie pojazdu dwuosiowego. Hamowanie przednią osią. Hamowanie tylą osią. Rozkład sił hamowania. Hamowanie na wzniesieniu i spadku. Opóźniene hamowania. Zjawisko bocznego znoszenia opon. Ruch pojazdu na zakręcie bez zjawiska bocznego znoszenia opon. Ruch pojazdu na zakręcie ze zjawiskiem bocznego znoszenia opon. Samochód: nadsterowny, neutralny i podsterowny. Wpływ bocznego wiatru na stateczność poprzeczną...
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4-Point beam tensile test on a soft adhesive
PublicationAn adhesive butt joint with a soft bondline has been studied. A series of experiments was conducted on test pieces constituted of aluminium adherends bonded with a low modulus epoxy adhesive, ScotchWeld™ 2216. The joint was subjected to four point bending, in tension/compression loading, under constant deflection rate, with the bondline being parallel to the applied load. The objective was to examine and evaluate crack nucleation...
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Identification of volatile compounds based on the electrocatalytic gas sensor responses
PublicationMeasured response in case of electrocatalytic gas sensors is in form of a voltamperometric characteristic. Current-voltage (I-V) response shape depends on the gas type and its concentration. Such response contains significantly more information comparing with typical electrochemical sensors, but is quite difficult to analyze. When I-V curve contains current peaks, position of such peaks can be used...
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Influence of sensor design and optical properties of tissue on the photoplethysmographic signal
PublicationPhotopletysmography and an associated technique called pulse oximetry are still explored due to the expectations that they give a lot of information about the state of the patient and, also, due to the fact that they are non invasive. Knowledge about the impact of various parameters on the measured signal leads to a faster and a more reliable way of analyzing measurement results and finding the dependencies between the involved...
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ARRAY OF MINIJETS – THERMAL AND HYDRAULIC PHENOMENA IN BOUNDARY LAYER
PublicationPresented work considers flow and thermal phenomena occurring in the system consisting of minijets array and heated with constant heat flux surface. Numerical analyses, based on the mass, momentum and energy conservation laws, were conducted. Focus was placed on the proper model construction, in which turbulence and boundary layer modelling was crucial. Calculations were done for various mass flow rates. The main calculations were...
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Degradation of Gel-Coat Layer in Glass/Polyester Laminate in Seawater Environment
PublicationGlass/polyester laminate coated with gelcoat layer of different thickness 0,5; 1,5; 3 mm was studied in terms of blistering behaviour and water sorption in hot water environment. Blistering was found to be accelerated for thin (0,5 mm) gel-coat layer compared to the thick (1,5; 3 mm), however no significant difference in blistering behaviour was observed between the laminates with gel-coat thickness 1,5 and 3 mm which may suggest...
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Ocena efektywności 4-węzłowych elementów powłokowych.
PublicationW ramach nieliniowej sześcioparametrowej teorii powłok wprowadzono rodzinę 4-węzłowych elementów skończonych klasy C0. W pracy analizuje się wrażliwość tychże elementów na zjawisko blokady/zakleszczenia (ang. locking effect). Rozważania ograniczone są do liniowej statyki. Formułuje się zasadę prac wirtualnych i zasadę wariacyjną Hu-Washizu, z których wynikają postaci macierzy elementowych. Następnie w przykładach analizuje się...
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Measurement spectrum obtained with the use of ZnO coated microsphere-based fiber-optic sensor - microsphere inspection s.2
Open Research DataApplication of a microsphere-based fiber-optic sensor with 200 nm zinc oxide (ZnO) coating, deposited by Atomic Layer Deposition (ALD) method, for temperature measurements between 100°C and 300°C, is presented. The main advantage of integrating a fiber-optic microsphere with a sensing device is the possibility of monitoring the integrity of the sensor...
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Measurement spectrum obtained with the use of ZnO coated microsphere-based fiber-optic sensor - microsphere inspection s.1
Open Research DataApplication of a microsphere-based fiber-optic sensor with 200 nm zinc oxide (ZnO) coating, deposited by Atomic Layer Deposition (ALD) method, for temperature measurements between 100°C and 300°C, is presented. The main advantage of integrating a fiber-optic microsphere with a sensing device is the possibility of monitoring the integrity of the sensor...
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Application of Multiplicative Drift Correction and Component Correction methods on simulated gas sensor array responses
PublicationSensor response drift is one of the most challenging problems in gas-analyzing systems. Such systems, commonly called electronic noses, are expected to be reliable and reproducible in the long term. Due to the drift phenomena, electronic noses usability is limited to the relatively short period of time, and frequent recalibrations of device are required. Because it is very hard to fabricate sensors without drift, this phenomenon...
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Determination of toxic gases based on the responses of a single electrocatalytic sensor and pattern recognition techniques
PublicationA response from an electrocatalytic gas sensor contains fingerprint information about the type of gas and its concentration. As a result, a single gas sensor can be used for the determination of different gases. However, information about the type of gas and its concentration is hidden in the unique shape of the current–voltage response and it is quite difficult to explore. One of the ways to get precise information about the measured...
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Singlet Exciton Diffusion in Vacuum-Evaporated Films of Amine-Based Materials as Studied by Photocurrent and Photoluminescence Quenching Methods
PublicationThe singlet exciton diffusion lengths are determined by the photoconductivity as well as the luminescence surface quenching technique, in vacuum‐evaporated layers of (4,4′,4″‐tris(N‐(3‐methylphenyl)‐N‐phenylylamino) triphenylamine) (m‐MTDATA), 4,4′,4″‐tris[2‐naphthyl(phenyl)amino] triphenylamine (2TNATA), and N,N′‐diphenyl‐N,N′‐bis(3‐methylphenyl)‐[1,1′‐biphenyl]‐4,4′‐diamine (TPD) which are frequently used for fabrication of electroluminescent...
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Supramolecular structures of bis-thionooxalamic acid esters derived from (±)-cyclohexane-1,2-diamine and (±)-1,2-diphenylethylenediamine
PublicationZsyntezowano dwa racemiczne estry kwasu bis(tiooksamowego) i zbadano ich sposób upakowania w sieci krystalicznej. Analiza rentgenograficzna monokryształów badanych związków wykazała, że organizują się one w jednowymiarowe struktury, które tworzone są przez molekuły o przeciwnej chiralności, połączone za pomocą trójcentrowych wiązań wodorowych C=S...NH...O=C. Powstające agregaty są dodatkowo stabilizowane przez słabe oddziaływania...
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Remote Monitoring System for Impedance Spectroscopy using Wireless Sensor Network
PublicationThe architecture of a miniaturized impedanceanalyser with wireless communication module for remoteImpedance Spectroscopy (IS) of anticorrosion coatings ondifficult-to-reach objects (e.g. on the steel construction ofthe bridge) is described in this paper. Some practical aspectsof implementation of a Wireless Sensor Network (WSN) arealso discussed. A low scale, middle range, WSN networkcomposed of a Base Station (BS) with a Personal...
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Modeling of Ozonation of Reactive Black 5 Through a Kinetic Approach
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Synchronization helps robots to detect black holes in directed graphs
PublicationPraca zawiera nowe wyniki dla problemu poszukiwania czarnej dziury w grafie skierowanym przez zbiór agentów. Czarna dziura jest węzłem niszczącym wszystkich wchodzącej do niej agentów. Pokazano, że w przypadku, gdy stopień wejściowy czarnej dziury wynosi D, do przeszukania grafu skierowanego w modelu synchronicznym wystarcza O(D 2^D) agentów. Wartość ta jest bliska znanemu z literatury oszacowaniu dolnemu Omega (2^D). W pracy pokazano...
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Sarmaci znad Morza Czarnego [Sarmatians from the Black Sea]
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Scene Segmentation Basing on Color and Depth Images for Kinect Sensor
PublicationIn this paper we propose a method for segmenting single images from Kinect sensor by considering both color and depth information. The algorithm is based on a series of edge detection procedures designed for particular features of the scene objects. RGB and HSV color planes are separately analyzed in the first step with Canny edge detector, resulting in overall color edges mask. In depth images both clear boundaries and smooth...
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Determination of Odor Air Quality Index (OAQII) Using Gas Sensor Matrix
PublicationThis article presents a new way to determine odor nuisance based on the proposed odor air quality index (OAQII), using an instrumental method. This indicator relates the most important odor features, such as intensity, hedonic tone and odor concentration. The research was conducted at the compost screening yard of the municipal treatment plant in Central Poland, on which a self-constructed gas sensor array was placed. It consisted...
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Optimized photodegradation of palm oil agroindustry waste effluent using multivalent manganese–modified black titanium dioxide
PublicationThis article presents a methodological approach to use manganese (Mn3+Mn7+)-modified black titanium dioxide (Mn/BTiO2) as a photocatalyst to optimize and improve visible-light-driven photodegradation of treated agro-industrial effluent (TPOME). A modified wet chemical process was used to prepare BTiO2. The BTiO2 was then wet impregnated with Mn and calcined at 300 °C for 1 h to produce Mn/BTiO2. The activity of Mn/BTiO2 was investigated...
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Вестник Московского университета. Серия 9. Филология
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Multiple sound sources localization in free field using acoustic vector sensor
PublicationMethod and preliminary results of multiple sound sources localization in free field using the acoustic vector sensor were presented in this study. Direction of arrival (DOA) for considered source was determined based on sound intensity method supported by Fourier analysis. Obtained spectrum components for considered signal allowed to determine the DOA value for the particular frequency independently. The accuracy of the developed...
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Multiple sound sources localization in real time using acoustic vector sensor
PublicationMethod and preliminary results of multiple sound sources localization in real time using the acoustic vector sensor were presented in this study. Direction of arrival (DOA) for considered source was determined based on sound intensity method supported by Fourier analysis. Obtained spectrum components for considered signal allowed to determine the DOA value for the particular frequency independently. The accuracy of the developed...
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Chemical characterization of wild populations of Brassica oleracea complex species (n=9) for the content of their bioactive compounds
PublicationThe wild species belonging to Brassica oleracea complex species (n=9) are widespread in the Mediterranean basin and represent the relative species of several vegetable crops, such as broccoli, cauliflower, kale, cabbage. They are characterized by the high level of bioactive compounds, such as glucosinolates (GLSs), known for their benefits for human health. Four accessions were evaluated: B. macrocarpa (BM) from Favignana (Trapani),...