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Search results for: LIGNIN EXTRACTION
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Charakterystyka wad w szynach kolejowych wykrytych na linii kolejowej nr 131 Chorzów Batory - Tczew ze szczególnym uwzględnieniem wad 227 squat
PublicationDiagnostyka szyn kolejowych ma istotne znaczenie przy ocenie stanu technicznego nawierzchni kolejowej. Rosnąca liczba wykrywanych wad kontaktowo-zmęczeniowych stawia przed diagnostami nowe wyzwania. W artykule scharakteryzowano wady 227 squat obserwowane na odcinku doświadczalnym zlokalizowanym na linii kolejowej nr 131 Chorzów Batory - Tczew. Wskazano czynniki wpływające na ich powstawanie i rozwój. Porównano wyniki prowadzonych...
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An in situ derivatization – dispersive liquid–liquid microextraction combined with gas-chromatography – mass spectrometry for determining biogenic amines in home-made fermented alcoholic drinks
PublicationA novel dispersive liquid–liquid microextraction (DLLME) gas chromatography mass-spectrometry(GC–MS) method was developed for the determination of 13 biogenic amines in home-made wine sam-ples. The method allows to simultaneous extraction and derivatization of the amines providing a simpleand fast mode of extract enrichment. During the study, two different procedures were examined. Sta-tistical analysis was performed to choose...
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Ionogel sorbent coatings for determining organophosphorus and pyrethroid insecticides in water and fresh juice samples by headspace-solid phase microextraction
PublicationThe sol–gel method yielded three different ionogel sorbent coatings that were obtained based on a silica material containing ionic liquids (ILs) immobilized in its pores. Two ILs, triethylsulfonium bis(trifluoromethylsulfonyl) imide [Set3][TFSI] and 1-butyl-1-methylpiperidinium bis(trifluoromethylsulfonyl)imide [C4C1Pip][TFSI], as well as their equimolar mixture [Set3/C4C1Pip], were used to obtain ionogel fibers. The developed...
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Head-Space SPME for the Analysis of Organophosphorus Insecticides by Novel Silica IL-Based Fibers in Real Samples
PublicationThis work demonstrates the suitability of a newly developed ionic liquid (IL)-based silica SPME fiber for the determination of seven organophosphorus insecticides in cucumber and grapefruit samples by headspace solid-phase microextraction (HS-SPME) with a gas chromatography–flame ionization detector (FID). The sol-gel method released four different sorbent coatings, which were obtained based on a silica matrix containing ILs immobilized...
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Green chemical and hybrid enzymatic pretreatments for lignocellulosic biorefineries: Mechanism and challenges
PublicationThe greener chemical and enzymatic pretreatments for lignocellulosic biomasses are portraying a crucial role owing to their recalcitrant nature. Traditional pretreatments lead to partial degradation of lignin and hemicellulose moieties from the pretreated biomass. But it still restricts the enzyme accessibility for the digestibility towards the celluloses and the interaction of lignin-enzymes, nonproductively. Moreover, incursion...
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Microstrip line with short-circuited edge as a high-pass filter operating up to millimeter-wave frequencies
PublicationPrzedstawiono prosty planarny filtr górnoprzepustowy wykorzystujący linię mikropaskową ze zwartym brzegiem. Układy zaprojektowano w taki sposób, aby pasmo przepustowe rozpoczynało się w zakresie K lub Ka. Wykonano dwa prototypy: na podłożu w postaci warstwy dielektrycznej wykonanej z ceramiki alundowej oraz na podłożu organicznym o niskiej przenikalności elektrycznej. Wykazano dużą zgodność teoretycznych i pomierzonych charakterystyk...
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Analysis of the Capability of Deep Learning Algorithms for EEG-based Brain-Computer Interface Implementation
PublicationMachine learning models have received significant attention for their exceptional performance in classifying electroencephalography (EEG) data. They have proven to be highly effective in extracting intricate patterns and features from the raw signal data, thereby contributing to their success in EEG classification tasks. In this study, we explore the possibilities of utilizing contemporary machine learning algorithms in decoding...
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Organic and conventional kiwifruit myths versus reality: antioxidant, antiproliferative and health effects
PublicationComparison between organic and conventional kiwifruit cultivars ''Hayward'' and ''Bidan'', which was done by four redical scavenging assays, ESI-MS, and DSC measurements, showed significant differences between cultivars. Such results were not estimated in kiwifruit growing under organic and conventional conditions. The extraction of bioactive compounds was done by two different methods: sequential extraction with ethyl acetate...
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Elektryczne zespoły zasobnikowe jako alternatywa dla elektryfikacji nowych linii w Trójmieście = Electric Multiple Units With Energy Storage – Alternative to Electrification of New Lines in Three City
PublicationRozważono zastosowanie nowoczesnych zespołów trakcyjnych na liniach pasażerskich Trójmiasta. Zaproponowano budowę linii Gdańsk Śródmieście - Orunia Górna oraz odtworzenie komunikacji do północnych dzielnic Gdyni. Przeanalizowano trójmiejski układ komunikacyjny dla ruchu pociągów z zasobnikami energii. Zaproponowano trasę Orunia Górna - Wrzeszcz - Osowa - Chylonia - Port Oksywie z naprzemiennie występującymi odcinkami zelektryfikowanymi...
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Measurement accuracy evaluation of transmission line earthings by impulse tests
PublicationUziemienia słupów linii energetycznych powinny być sprawdzane okresowo. Pomiary rezystancji takich uziemień przy pomocy metody niskoczęstotliwościowej wymaga wyłaczania linii i odkręcania przewodów odprowadzających od konstrukcji słupa. Metoda udarowa jest znacznie łatwiejsza w tej aplikacji i nie wymaga wyłaczania linii na czas pomiarów. W pracy oszacowano wpływ uziemień sąsiednich słupów na dokładność pomiarów metodą udarową.
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Screening of potential inhibitors for COVID-19 main protease from phytoconstituents of Tectona grandis Linn: application of molecular modeling studies
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Implementation of multicriteria decision analysis in design of experiment for dispersive liquid-liquid microextraction optimization for chlorophenols determination
PublicationA novel and efficient approach to optimization of extraction step prior the chromatographic determination of nine chlorinated phenols is described. It is based on the combination of design of experiments and multicriteria decision analysis. Such an approach is used to optimize dispersive liquid-liquid microextraction procedure for the determination of 9 chlorophenols in water samples. Three parameters are optimized – sample volume,...
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Determination of volatile organic compounds using solventless sample preparation techniques and gas chromatography
PublicationIn this paper the latest advances in the determination of volatile organic compounds using solvent-free extraction techniques in the sample preparation step are presented. A paper is focus mainly on one of the most popular sample preparation technique: solid-phase microextraction technique (SPME) combined with different detection systems and its applications to sampling of VOCs from the samples with different matrices. This paper...
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Surfactants application in sample preparation techniques: Insights, trends, and perspectives
PublicationSince the implementation of Green Chemistry into analytical practice, significant efforts have been made to improve the sustainability of chemical analysis. These include reducing the use of hazardous chemicals and solvents, minimizing waste, and improving energy efficiency. Surfactants can be applied in chemical analysis as an environmentally friendly alternative to conventional solvents and chemicals. The use of surfactants can...
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Zastosowanie wysokosprawnej kolumnowej chromatografii cieczowej w odwróconych układach faz (RP-HPLC) do rozdzielania i wstępnej identyfikacji składników hydrofilowych mieszanin po hydrolizie zasadowej biomasy ligno-celulozowej (BMLC)
PublicationWzrost konsumpcji paliw kopalnych, ich pozyskiwanie oraz eksploatacja niesie ze sobą wiele zagrożeń dla środowiska, dlatego alternatywnym źródłem energii stają się biopaliwa, w tym bio-wodór pozyskiwany w konwersji biomasy ligno-celulozowej, która poddawana jest obróbce wstępnej. Najczęściej wykorzystywaną metodą obróbki wstępnej jest hydroliza alkaliczna, podczas której powstaję bardzo dużo produktów ubocznych, nieprzydatnych...
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Comparison of High Performance Liquid Chromatography Methods with Different Detectors for Determination of Steroid Hormones in Aqueous Matrices
PublicationThis paper presents the development and comparison of procedures for the qualitative and quantitative determination of five estrogenic compounds (17-a-ethynylestradiol, estrone, estradiol, estriol, and progesterone) in drinking water and wastewater samples. Five extraction columns and two disks were tested for their efficiency. The C18 columns were superior on the basis of cost for solid phase extraction of drinking water or sewage....
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Analytical applications and physicochemical properties of ionic liquid-based hybrid materials: A review
PublicationIonic liquids with their unique properties found so far numerous analytical applications. Among them ionic liquids immobilized on the surface or within the pores of a solid support were successfully utilized in extraction techniques dedicated to preconcentration of the analytes from food, environmental and biological samples. In this review we focus on comprehensive summarizing of available literature data on the examples of ionic...
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Meander microstrip line with defected ground structures
PublicationW artykule omówiono koncepcję miniaturyzacji sekcji linii mikropaskowej poprzez modyfikację brzegu linii oraz warstwy metalizacji masy. W pracy zaprezentowano projekt oraz wyniki eksperymentu sprzęgacza gałęziowego skonstruowanego w oparciu o linię meandrową z zaburzoną warstwą metalizacji masy. Pomierzone charakterystyki transmisyjne potwierdzają atrakcyjność zastosowanych metod redukcji zajmowanej przez układ powierzchni. Osiągnięto...
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Compact microstrip to coplanar standard transformer.
PublicationW pracy zaprezentowano transformator standardu umożliwiający bezodbiciowe połączenie linii mikropaskowej z linią koplanarną. Konstrukcja układu opiera się na założeniu zachowania jednakowej wartości impedancji w każdym przekroju poprzecznym struktury. Zaprojektowano i przebadano dwa rozwiązania z ze skokową i ciągłą zmianą szerokości linii. Do badań numerycznych wykorzystano symulator pełnofalowy Momentum. W symulacjach uwzględniono...
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The influence of fresh cabbage and sauerkraut juices on the activity of protective enzymes in human cell lines
PublicationMechanizmami przeciwrakotwórczego działania związków zawartych w kapuście jest m.in. metaboliczna aktywacja enzymów II fazy detoksykacji, indukcja enzymów naprawczych DNA oraz aktywnośc przeciwutleniająca. Do enzymów II fazy odtruwania należą m.in. S-transferazy glutationowe (GST) oraz oksydoreduktaza chinonowa NQO1 zwana też DT-diaforazą. GST katalizują reakcję sprzęgania glutationu z wieloma różnymi typami ksenobiotyków, ułatwiając...
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Experimental and numerical investigation of crosstalk effect in coupled coplanar waveguides - part II: Multimode coupled line representation
PublicationW pracy przedstawiono metodę analizy nieidealności połączenia poszczegółnych fragmentów rozłożonego ekranu na zjawisko przesłuchu w strukturze sprzężonych falowodów koplanarnych z uziemionym centralnym paskiem. Analiza bierze pod uwagę efekty dyspersji oraz wielorodzajową naturę rozchodzenia się fali elektromagnetycznej w strukturze wieloprzewodowej. Teorię zweryfikowano praktycznie uzyskując bardzo dobrą zgodność pomiędzy wynikami...
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Experimental and numerical investigation of crosstalk effect in coupled coplanar waveguides - part i: bi-mode coupled line representation
PublicationW pracy przedstawiono analizę zjawiska przesłuchu w strukturze sprzężonych falowodów koplanarnych. Analiza wykorzystując metodę przestrzeni widmowej i bazując na dwurodzajowym modelu pary linii sprzężonych uwzględnia efekty dyspersji obserwowane w zakresie wysokich częstotliwośći. Przedyskutowano zagadnienie sposobu definicji impedancji charakterystycznych dla prowadzonych rodzajów pola. Wyniki modelowania numerycznego potwierdzono...
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Modelowanie przepływu powietrza w przewodach pneumatycznych
PublicationW pracy omówiono problem modelowania przepływu powietrza w linii długiej. Postawiono hipotezę, że dla zmian ciśnienia w zbiorniku linia długa może być opisywana jako element o stałych skupionych ze zmiennym współczynnikiem przepływu. Wstępne badania wskazują na poprawność tej hipotezy.
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Effective assessment of biopolymer-based multifunctional sorbents for the remediation of environmentally hazardous contaminants from aqueous solutions
PublicationPersistent contaminants in wastewater effluent pose a significant threat to aquatic life and are one of the most significant environmental concerns of our time. Although there are a variety of traditional methods available in wastewater treatment, including adsorption, coagulation, flocculation, ion exchange, membrane filtration, co-precipitation and solvent extraction, none of these have been found to be significantly cost-effective...
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Treatment of Odontogenic Maxillary Sinusitis with the Use of Growth Factors in Advanced Platelet-Rich Fibrin for Immediate Closure of Oro-Antral Communication: A Case Report
PublicationChronic odontogenic maxillary sinusitis (COMS), a prolonged inflammation of the maxillary sinus lasting over 12 weeks, is often a result of periapical lesions, marginal periodontitis, and complications like oro-antral communication (OAC) and fistula (OAF). OAC, commonly emerging post-teeth extraction in the lateral maxilla, lacks documented treatments using advanced platelet-rich fibrin (A-PRF). This study evaluates A-PRF’s efficacy...
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MODELLING OF CUTTING BY MEANS OF FRACTURE MECHANICS
PublicationThe suitability of modern fracture mechanic theory was proved for the estimation of the cutting force and the cutting specific resistance. This paper shows modification of Ernst-Merchant theory and its application for determination some other properties of wood sample. This theory is acceptable for evaluation of shear yield stresses and shear plane angle. Sawing by gang saw machine was used as a process similar to the orthogonal...
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THEORETICAL POTENTIAL OF HYDROGEN PRODUCTION FROM TEXTILES WASTES IN POMERANIAN REGION BY MEANS OF DARK FERMENTATION
PublicationModel has been developed for calculating theoretical mass of hydrogen produced from textile wastes by mean of dark fermentation. As vegetable fibres wastes were chosen two mostly used — cotton and linen (flax). As the synthethic carbohydrate rich fiber was chosen viscose. In the background there were introduced: problems of dark fermentation, characteristics of textile material structure. Additionally pathways of the process...
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Recent developments and future trends in solid phase microextraction techniques towards green analytical chemistry
PublicationSolid phase microextraction find increasing applications in the sample preparation step before chromatographic determination of analytes in samples with a complex composition. These techniques allow for integrating several operations, such as sample collection, extraction, analyte enrichment above the detection limit of a given measuring instrument and the isolation of analytes from sample matrix. In this work the information about...
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Plant-based meat substitute analysis using microextraction with deep eutectic solvent followed by LC-MS/MS to determine acrylamide, 5-hydroxymethylfurfural and furaneol
PublicationFor the analysis of plant-based meat substitutes and the determination of Maillard reaction products such as acrylamide, 5-hydroxymethylfurfural and furaneol, a novel and effective procedure based on hydrophobic natural deep eutectic solvent and liquid chromatography coupled with tandem mass spectrometry was developed for the first time. The 49 compositions of the deep eutectic solvents were designed and screened to select the...
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Application of chemometric techniques in studies of toxicity of selected commercially available products for infants and children
PublicationThe goal of the present study is to assess the impact of the experimental conditions for extraction procedures (time of extraction, thermal treatment and type of extraction media) as applied to several baby and infant products checked for their possible ecotoxicological response when tested by various ecotoxicity tests(Microtox®, Ostracodtoxkit F™and Xenoscreen YES/YAS™). The systems under consideration are multidimensional by...
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DETERMINATION OF SURFACTANTS IN ENVIRONMENTAL SAMPLES. PART II. ANIONIC COMPOUNDS
PublicationSurfactants (SAA) with negative charge of polar group are named as anionic compounds. They are main constituent of most products containing synthetic surfactants. The linear alkylbenzene sulfonates (LAS), alkyl ethoxysulfates (AES) and alkyl sulfates (AS) are typically applied from this class of compounds. Those surfactants are ingredients of household detergents and cleaners, laundry detergents, cosmetic. Moreover they can be...
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Synthesis of isomeric, oxathiolone fuded chalcones and comparison of their activity toward various microorganisms and human cancer cell lines
PublicationIzomeryczne oksationolowe sprzężone chalkony otrzymano w wyniku kondensacji odpowiedniego acetylobenzo[1,3]oksatiolo-2-onu z aldehydem benzoesowym w środowisku kwaśnym. Określono aktywność cytotoksyczną otrzymanych związków wobec komórek linii HeLa, przeciwbakteryjną wobec Micrococcus luteus, Staphylococcus aureus, Salmonella typhimurium, Escherichia coli i Proteus vulgaris, przeciwgrzybową wobec Candida albicans i tuberkulostatyczną...
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Acid-catalysed synthesis of oxathiolone fused chalkones. Comparison of their activity toward various microrganisms and human cancer lines
PublicationOtrzymano podstawione pochodne oksationolowych sprzężonych chalkonów w wyniku kondensacji 4-acetylo-5-metoksy-2-0ksobenz[1,3]oksatiolu z aldehydem benzoesowym w środowisku kwaśnym. Badano właściwości biologiczne otrzymanych związków. Trzy z otrzymanych pochodnych wykazały umiarkowaną aktywność wobec komórek HeLa, dwa były aktywne wobec Micrococcus luteus i Staphylococcus aureus, a jeden wobec Mycobacterium tuberculosis.
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Volatile Organohalogen Compounds Determination with Dispersive Liquid-Liquid Microextraction Applying Solvent Lighter than Water
PublicationBackground: Volatile organohalogen compounds (VOX) are a group of environmental pollutants that risk the quality of drinking water. These compounds are characterized by certain acute and chronic toxicities, possessing mutagenic properties. Because of these potential risks factors that these compounds cause, the maximum allowable concentrations (MACs) have been established by respective organizations. The abundance of VOX, their...
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An image processing approach for fatigue crack identification in cellulose acetate replicas
PublicationThe cellulose acetate replication technique is an important method for studying material fatigue. However, extracting accurate information from pictures of cellulose replicas poses challenges because of distortions and numerous artifacts. This paper presents an image processing procedure for effective fatigue crack identification in plastic replicas. The approach employs thresholding, adaptive Gaussian thresholding, and Otsu binarization...
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Ocena bezpieczeństwa i efektywność jabłczanu sunitynibu w przerzutowych guzach neuroendokrynnych trzustki (NEN G1/G2) w zależności od liczby i rodzaju wcześniejszych linii terapeutycznych — doniesienie wstępne
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Program funkcjonalno-użytkowy i projekt budowlany na potrzeby realizacji projektu"Budowa stacji 220/110 kV Praga(Żerań) wraz z wprowadzeniem linii 220kV Miłosna-Mory" -koreferat
PublicationDokonano oceny PF-U i projektu budowlanego Stacji 220/11- kV Praga na podstawie ok.1000str.dokumentacji projektowej
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A Perspective on Missing Aspects in Ongoing Purification Research towards Melissa officinalis
PublicationMelissa officinalis L. is a medicinal plant used worldwide for ethno-medical purposes. Today, it is grown everywhere; while it is known to originate from Southern Europe, it is now found around the world, from North America to New Zealand. The biological properties of this medicinal plant are mainly related to its high content of phytochemical (bioactive) compounds, such as flavonoids, polyphenolic compounds, aldehydes, glycosides...
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PBDEs in environmental samples: Sampling and analysis
PublicationThe paper reviews the subject literature concerning analytical procedures routinely sed for monitoring polybrominated diphenyl ethers (PBDE) in environmental samples. It describes and summarizes subsequent stages of analytical procedure including sample collection and preparation, extraction, clean-up and final determination. Different approaches with their advantages and limitations are presented. Special attention is drawn to...
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Organic and conventional kiwifruit, myths versus reality: antioxidant, antiproliferative and helth effects
PublicationComparison between organic and conventional kiwifruit cultivars 'Hayward' and 'Bidan', which was done by four radical scavenging assays, ESI-MS, and DSC measurements, showed significant differences between the cultivars. Such results were not estimated in kiwifruit growing under organic and conventional conditions. The extraction of bioactive compounds was done by two different methods: sequential extraction with ethyl acetate...
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Nowe rozwiązania metodyczne i techniczne w zakresie techniki mikroekstrakcji do fazy stracjonarnej
PublicationSample preparation has been recognized as a critical step of the analytical process, being even considered as the bottleneck of the overall process. Enrichment of target compounds, transfer of the analytes into a solvent compatible with the analytical instrumentation, minimization of potential interferences, and efficient sample clean-up, are among the main aims of sample preparation techniques. In this regard, liquid-liquid extraction...
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DETERMINATION OF SURFACTANTS IN ENVIRONMENTAL SAMPLES - PART I. CATIONIC COMPOUNDS = Oznaczanie Surfaktantów W Próbkach Środowiskowych. Część I. Związki Kationowe
PublicationCompounds from the group of cationic surfactants are widely applied in household, industrial, cleaning, disinfectant, cosmetic and pharmaceutical products as their specific properties (antimicrobial, emulsifying, anticorrosion, softening). After use, cationic surfactants are disposed to wastewater-treatment plants and finally with effluent water to surface waters due to their incomplete degradation. Moreover, they can freely circulate...
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Molecular modeling study of tectoquinone and acteoside from Tectona grandis linn: a new SARS-CoV-2 main protease inhibitor against COVID-19
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Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine
PublicationA direct method based on immersion solid phase microextraction (DI-SPME) gas chromatography mass-spectrometry (GC-MS) was optimized and validated for the determination of 16 biogenic amines in Polish wines. In the analysis two internal standards were used: 1,7-diaminoheptane and bis-3-aminopropylamine. The method allows for simultaneous extraction and derivatization, providing a simple and fast mode of extraction and enrichment....
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Investigation of antifungal and antibacterial potential of green extracts of propolis
PublicationPropolis extracts have been used in traditional medicines since ages due to its advantageous complex chemical composition. However, the antibacterial and antifungal activity of poplar propolis extracts prepared in Natural Deep Eutectic Solvent (NADES) are seldom studied. This study investigates suitable alternate for ethanol as a solvent for extraction for Polish poplar propolis. It also attempts to identify suitable extraction...
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Wykonanie ekspertyzy materiałowej w zakresie wytrzymałości betonu oraz składu chemicznego (chlorków) próbek betonowych dla obiektu mostowego w km 191.997 na linii kolejowej nr 7 Lublin-Dorohusk
PublicationCelem opracowania jest przeprowadzenie badań wytrzymałości na ściskanie i określenie klasy betonu wbudowanego w ustrój nośny wiaduktu, a także analiza chemiczna próbek pobranych z konstrukcji.
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Przewidywane kierunki rozwoju technologii utrzymania dróg szynowych z uwzględnieniem linii dużych prędkości. Materiały Ogólnopolskiej Konferencji Naukowo-Technicznej Nowoczesne Technologie i Systemy Usprawniające Zarządzanie w Transporcie Kolejowym.
PublicationOgraniczenie nakładów na utrzymanie przy jednoczesnym zapewnieniu wysokiej jakości drogi kolejowej wymaga minimalizowania ilości podbić realizowanych w ramach napraw interwencyjnych oraz doboru, odpowiednich do warunków Polskich Linii Kolejowych, maszyn torowych
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Experimental examination and modification of chip suction system in circular sawing machine
PublicationThe article presents the results of experimental examination of the wood chip suction system in the existing sliding table saw before and after its modifi cation. The studies focused on the extraction hood of the mentioned system. The methodical experimental research of the pressure distribution inside the hood during wood chip removal for the selected rotational speed of saw blades of 3500 and 6000 min-1 with a diameter of 300...
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Application of modern sample-preparation techniques to the determination of chloropropanols in food samples
PublicationChloropropanols are heat-induced food toxicants that recently caused concern among industrial and scientific experts. World and European organizations related to food safety asked researchers to investigate mitigation strategies regarding these contaminants. The essential objective of this project was development of fast analytical methods enabling reliable determination and quantification of 3-monochloropropane-1,2-diol, 2-monochloropropane-1,3-diol...
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Membrane-SPME the best 'green' sample preparation technique for the gas chromatographic determination polar organic pollutants in polar media
PublicationOne of the most popular technique for sample preparation, which fulfill requirements of green analytical chemistry, is solid phase microextraction (SPME). Because of the undoubted advantages of SPME technique, solvent-free character of the extraction process and the enormous potential in analytical practice, a series of studies has been undertaken to develop new technical solutions, where improving the sensitivity and the extraction...