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Search results for: ARBUZOV REACTION
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In-situ FTIR study of reaction mechanism and chemical kinetics of a Xundian lignite during non-isothermal low temperature pyrolysis
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Solvent effects for proton transfer reaction from dimethyl(4-nitrophenyl)malonate to cis 1,2-bis(diethylaminomethyl)cyclohexane
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The reaction of substituted N-phenacyl-pyridinium bromides in the pyridine ring with DABCO and DBU in water and DMSO. Kinetics and DFT studies
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Red phosphorus as self-template to hierarchical nanoporous nickel phosphides toward enhanced electrocatalytic activity for oxygen evolution reaction
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Surface-orientated platinum nanoparticles electrodeposited on a carbon substrate as a high performance electrocatalyst for glucose oxidation reaction in alkaline media
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Robust and highly efficient electrocatalyst based on ZIF-67 and Ni2+ dimers for oxygen evolution reaction: In situ mechanistic insight
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Tuning of eg electron occupancy of MnCo2O4 spinel for oxygen evolution reaction by partial substitution of Co by Fe at octahedral sites
PublicationTo study the effect of partial Co substitution by Fe in the B site of MnCo2O4 spinel on its physicochemical and electrochemical properties, a series of MnCo2-xFexO4 powders (x=0.125; 0.250; 0.500; 0.750; 1.000) were synthesized by means of the sol-gel method. The produced powders were characterized by powder X ray diffraction (pXRD), scanning and transmission electron microscopy (SEM & TEM) coupled with energy dispersive spectroscopy...
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Online Volatile Compound Emissions Analysis Using a Microchamber/Thermal Extractor Coupled to Proton Transfer Reaction-Mass Spectrometry
PublicationIndoor air is a complex and dynamic mixture comprising manifold volatile organic compounds (VOCs) that may cause physiological and/or psychological discomfort, depending on the nature of exposure. This technical note presents a novel approach to analyze VOC emissions by coupling a microchamber/thermal extractor (μ-CTE) system to a proton transfer reaction-mass spectrometer (PTR-MS). This configuration provides an alternative to...
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Non-Coaxially Rotating Motion in Casson Martial along with Temperature and Concentration Gradients via First-Order Chemical Reaction
PublicationThe effect of non-coaxial rotation on the transport of mass subjected to first-order chemical reaction is studied analytically. The effects of thermal radiation, buoyancy, constructive and destructive chemical reactions along with Casson fluid in rotating frame are discussed. Time evolution of primary and secondary velocities, energy and solute particles are analyzed. The behavior of flow under the variation of intensity of magnetic...
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The Effect of Cobalt Incorporation into Nickel–Iron Oxide/(oxy)hydroxide Catalyst on Electrocatalytic Performance Toward Oxygen Evolution Reaction
PublicationThis work presents a study on the influence of the addition of cobalt into state-of-the-art nickel–iron (NiFe) mixed oxides/hydroxides/(oxy)hydroxides on their structural and morphological properties, and oxygen evolution reaction (OER) catalytic activity. A one-step electrodeposition process is performed without any additives to fabricate NiFe and x cobalt-doped nickel/iron (xCoNiFe) layer-double-hydroxide catalysts directly on...
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Solvent Impact on the Diversity of Products in the Reaction of Lithium Diphenylphosphide and a Ti(III) Complex Supported by a tBu2P–P(SiMe3) Ligand
PublicationWe present two important trends in the reactivity ofthe titanium complex [MeNacNacTi(Cl){η2-P(SiMe3)-PtBu2}](MeNacNac− = [Ar]NC(Me)CHC(Me)N[Ar]; Ar = 2,6-iPr2Ph)with nucleophilic reagents RLi (R = Ph2P,tBuO, (Me3Si)2N, andtBu2N) depending on the reaction medium. Reaction in nonpolarsolvent (toluene) leads to three main products: via an autoredoxprocess and nucleophilic substitution at the Ti-atom to afford theTi(IV) complex [MeNacNacTi(R){η2-P-PtBu2}]...
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On-line assessment of oil quality during deep frying using an electronic nose and proton transfer reaction mass spectrometry
PublicationWe describe a novel method for the quality assessment of oil utilized for deep frying. The method is based on the analysis of frying fumes using a custom electronic nose. The quality score could be obtained after less than 3 min of analysis and without interrupting the frying process or sampling the oil directly. The obtained results were correlated with the peroxide value using a multivariate linear regression model. The most...
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Reclaimed rubber in-situ grafted with soybean oil as a novel green reactive plasticizer in SBR/silica compounds
PublicationPolymer recycling and biodegradable polymeric materials are two major routes towards the sustainable development of polymer materials which contributes to the management of waste. In this regard, an eco-friendly approach is presented wherein high reclaiming degree of ground tire rubber (GTR) was achieved by low-temperature oxidation under swollen action of soybean oil. In-situ reclaimed GTR with soybean oil was cured into reactive...
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Fragmentation of Hydrographic Big Data Into Subsets During Reduction Process
PublicationThe article presented problems of fragmentation of hydrographic big data into smaller subsets during reduction process. Data reduction is a processing of reduce the value of the data set, in order to make them easier and more effective for the goals of the analysis. The main aim of authors is to create new reduction method. The article presented the first stage of this method – fragmentation of bathymetric data into subsets. It...
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Smart grid technologies in electric traction: Mini inverter station
PublicationThe growing number of trams and trolleybuses equipped with recuperation systems contribute to the increase in the amount of energy recovered during braking. It raises questions about the possibility of its usage. One of such possibilities is the use of smart grid technology. The paper presents a case study of the use of braking energy in the trolleybus system for external loads by implementing mini inverter stations. Analysis is...
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Experimental study on effectiveness of polymer dampers in reduction of structural vibrations
PublicationVibrations of civil engineering structures, generated by dynamic loads, may be very dangerous to the structures themselves as well as may have significant influence on human perception and comfort. A number of different methods have been proposed in order to minimize such situations. This concern newly designed structures as well as those which dynamic properties have to be modified due to problems with excessive vibrations. One...
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Alcohol craving in relation to coping with stress and satisfaction with life in the addicted
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Modeling of Ozonation of Reactive Black 5 Through a Kinetic Approach
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Dynamics of a simplified HPT model in relation to 24h TSH profiles
PublicationWe propose a simplified mathematical model of the hypothalamus-pituitary-thyroid (HPT) axis in an endocrine system. The considered model is a modification of the model proposed by Mukhopadhyay and Bhattacharyya in [10]. Our system of delay differential equations reconstructs the HPT axis in relation to 24h profiles of human in physiological conditions. Homeostatic control of the thyroid-pituitary axis is considered by using...
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Size reduction of ultra-wideband antennas with efficiency and matching constraints
PublicationAntenna design is a multifaceted task that involves handling of various performance figures concerning both electrical performance of the structure as well as its geometry. Simultaneous control of several objectives through rigorous optimization is very challenging and virtually impossible through conventional approaches such as parameter sweeping. In this work, we investigate size reduction of ultra‐wideband antenna structures...
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A study of a reduction of a micro- and nanometric bismuth oxide in hydrogen atmosphere
PublicationA reduction of bismuth oxide in hydrogen atmosphere was investigated. The reaction was performed with a material in various structural forms: powder: with micrometric grains, powder with nanometric grains and powder pressed into pellets. The process was performed in both isothermal and non-isothermal conditions. An activation energy of the reaction calculated with Friedman method was found to be about 85 kJ/mol for the reduction...
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Application of polymer element in reduction of temporary steel grandstand vibrations
PublicationThe numerical analysis focused on reduction of vibrations of a temporary steel scaffolding grandstand has been conducted in this paper. These types of structures are regularly subjected to dynamic loads which, in conjunction with light and quite slender structural members, may induce dangerous vibrations. To increase their safety, temporary steel grandstands are usually strengthened with the diagonal stiffeners of tubular cross...
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Experimental study on the effectiveness of polymer dampers in reduction of structural vibrations
PublicationVibrations of civil engineering structures, generated by dynamic loads, may be very dangerous to the structures themselves as well as may have significant influence on human perception and comfort. A number of different methods have been proposed in order to minimize such situations. This concern newly designed structures as well as those which dynamic properties have to be modified due to problems with excessive vibrations. One...
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Model Order Reduction for Problems With Dispersive Surface Boundary Conditions
PublicationThis letter proposes a new scheme for reduced-order finite-element modeling of electromagnetic structures with nonlinear, dispersive surface boundary conditions, which optimally exploits the numerically stable and efficient MOR framework for second-order systems provided by SAPOR method. The presented results of numerical experiments for an example of a waveguide filter demonstrate the superior accuracy of the resulting reduced models...
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Bound on Bell inequalities by fraction of determinism and reverse triangle inequality
PublicationIt is an established fact that entanglement is a resource. Sharing an entangled state leads to nonlocal correlations and to violations of Bell inequalities. Such nonlocal correlations illustrate the advantage of quantum resources over classical resources. In this paper, we quantitatively study Bell inequalities with 2 × n inputs. As found in Gisin et al. [Int. J. Quantum. Inform. 05, 525 (2007)], quantum mechanical correlations...
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Evaluation of dampness-induced strength reduction of calcium silicate blocks
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Putative Biological Mechanisms of Efficiency of Substrate Reduction Therapies for Mucopolysaccharidoses
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Moderately Reactive Molecules Forming Stable Ionic Compounds with Superhalogens
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The origin of luminescence accompanying electrochemical reduction or chemical decomposition of peroxydisulfates
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Photocatalytic activity and OH radical formation on TiO2 in the relation to crystallinity
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Double-Wound O-Ring Retraction for Chylothorax Surgery in Dogs
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Abductor and adductor strength relation to sprint performance in soccer players
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Comparing some convolution-based methods for creation of surround sound
PublicationW referacie przedstawiono eksperymenty związane z symulacją dźwięku dookólnego w sali koncertowej. W tym celu wykorzystano splot odpowiedzi impulsowej z danego wnętrza (wielokanałowe nagrania odpowiedzi impulsowej) z nagraniami z komory bezechowej. Uzyskany w ten sposób sygnał został następnie przypisany do odpowiednich kanałów w systemie dookólnym. Uzyskane w ten sposób nagrania były następnie porównywane w testach subiektywnych...
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Review of Research and Development on the Technical Diagnostics in the Field of Electric Traction
PublicationPrzedstawiono funkcje i oprzyrządowanie stanowiska diagnostycznego do badania lokomotyw elektrycznych serii EU07. Zaproponowano nową metodę kontroli charakterystyki statycznej odbieraka prądu. Przedstawiono kompleksowy system diagnostyki sieci jezdnej DST.
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Carbon Nanotubes Derivatized with Mediators for Laccase Catalyzed Oxygen Reduction.
PublicationPrzedstawiono konstrukcję elektrody w której wykorzystano nanorurki modyfikowane znanym mediatorem (ABTS). Cząsteczki mediatora przyłączono do ścian bocznych nanorurek oraz do ich końców. Porównano parametry elektrod zbudowanych w oparciu o nanorurki modyfikowane kowalencyjnie w różny sposób. Zaobserwowano pozytywny wpływ modyfikowanych nanorurek na parametry elektrody.
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Destructive Consequences of PWM Inverter Feeding for Traction AC Motors
PublicationThe electric traction drives with an AC motor fed by a frequency converter are used more and more often nowadays. The most significant side effects, of a converter's output voltage forming PWM method for AC motor windings, are steep voltage changes, which can initiate several destructive phenomena. The paper presents the adverse influence of a converter common mode voltage on the motor windings' increased voltage exposure and the...
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The Method of reduction of aerodynamic forces generated in turbine blade seals
PublicationThe distibution of pressure in the seal gaps does not only affect the so called '' leakage losses'' and the turbine stage overall efficiency but also plays an important role in the generation of aerodynamic forces which may cause self-excited rotor vibrations. The paper describes a chamber seal applied for the reduction of the aerodynamic forces created in shroud seals. This kind of turbine seal was patented and tested.
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C-reactive Protein as a Diagnostic and Prognostic Factor of Endometrial Cancer
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C-reactive protein as a diagnostic and prognostic factor of endometrial cancer
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The Issues of Reactive Power Compensation in High-voltage Transmission Lines
PublicationThis paper discusses the selection of compensation shunt reactors for a double-circuit 400 kV transmission line using the example of the newly built Elk Bis – Alytus transmission line. The analysis takes into account various conditions of the power system. The published results relate to voltage levels in steady states and during switching processes and short circuits.
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Reduction of noise and rolling resistance by horizontal grinding of asphalt pavements
PublicationGrinding of cement concrete pavements to reduce unevenness and noise is common since a long time. Grinding is then made with wheels equipped with diamond blades rotating in the vertical plane. This creates narrow vertical/longitudinal grooves in the pavement. It is not applied to asphalt pavements. In this paper an alternative type of grinding is studied. In this case plates with diamond heads rotate in the same plane as the pavement,...
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Direct reduction of pellets through hydrogen: Experimental and model behaviour
PublicationThis paper presents the hydrogen reduction behaviour of industrial pellets designed for the efficient hydrogen based direct reduction. The pellets were provided with very low non ferrous oxides percentage (0.52 of basicity index) and with the absence on TiO2 oxides. The pellets measured diameters in the range 1.14–1.72 cm and were characterized in terms of porosity, pores size, tortuosity and compression strength. The pellets were...
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Hydrogen direct reduction and reoxidation behaviour of high-grade pellets
PublicationHigh grade pellets with basicity index close to 0.5 were directly reduced in pure hydrogen atmosphere. The reduction experiments were performed in the temperature range 800 e1000 C at the pressure of 8 bar. The pellets internal structure was analysed through micro tomography observations in the unreduced and reduced conditions. After reduction, the pellets showed a variation of porosity up to more than 15% with a remarkable change...
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Pre-treatment of bio fraction waste prior to fermentation processes
PublicationCurrent efforts are taken to increase resource efficiency, close material loops, and improve sustainable waste and by-products management. Thus, networking agro-food by-products and converting them into valuable products completely exhausting the potential of the raw material becomes significant. Model lignocellulosic and starch based biomass were subjected to pre-treatment with the application of acidic compounds, i.e. sulphuric...
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Influence of the improved reduction technique on superconductivity in Nd1.85Ce0.15Cu1+_yO4-z
PublicationW pracy opisano zmodyfikowany proces redukcji próbek ceramicznych NCCO oraz jego wpływ na właściwości nadprzewodzące związku. Uzyskano dobre właściwości nadprzewodzące dla próbek z 2% niedoborem Cu oraz bardzo dobre wyniki dla próbek z 2% nadmiarem Cu.
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An orthogonality relation for the Whittaker functions of the second kind of imaginary order
PublicationPrzeprowadzono dowód ortogonalności funkcji Whittakera drugiego rodzaju rzędu urojonego. Użyto metody analogicznej do tej, którą zaprezentowano we wcześniejszej pracy tych samych autorów [J. Math. Anal. Appl. 365 (2010) 195-197], poświęconej funkcjom Macdonalda rzędu urojonego.
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Drift, wow and flutter measurement and reduction in shrunken movie soundtracks
PublicationReferat przedstawia metodę i algorytmy do oceny i redukcji dryfu, kołysania i drżenia w skurczonych taśmach filmowych. Przedstawione algorytmy działają w oparciu o przetwarzaniu obrazu taśmy filmowej w celu wyznaczenia jej lokalnego skurczu, który jest jednym z powodów powstawania dryfu, kołysania i drżenia. Lokalny skurcz taśmy można wyznaczyć dzięki analizie wysokości: ramki obrazu, perforacji, lub innego, standaryzowanego elementu...
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Application of social relation graphs for early detection of transient spammers
PublicationWczesne wykrywanie społecznych zagrożeń i anomalii jest prawdziwym wyzwaniem w dzisiejszch, dynamicznych społeczeństwach. Ludzie tworzą skoplikowane relacje społeczne, które mogą być przedstawione za pomocą różnych typów grafów, których wierzchołki reprezentować mogą aktorów sieci (konkretne osoby lub organizacje) a krawędzie relacje pomiędzy nimi. Analiza tych dynamicznie zmieniających się relacji może wskazywać na niektóre nadciągające...
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The Method of Reduction of Aerodynamic Forces Generated in Turbine Blade Seals
PublicationOpisano metodę zmniejszania sił wymuszających drgania aerodynamiczne poprzez zastosowanie nowego uszczelnienia nadbandażowego typu komorowego. Efektywność stosowania uszczelnienia komorowego potwierdzono obliczeniami numerycznymi i badaniami eksperymentalnymi.
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Actinidia (Mini Kiwi) Fruit Quality in Relation to Summer Cutting
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