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Search results for: chromatografia wykluczania (gpc/sec)
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Piotr Konieczka prof. dr hab. inż.
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Long-term hindcast simulation of sea level in the Baltic Sea
Open Research DataThe dataset contains the results of numerical modelling of sea level fluctuations over a period of 50 years (1958-2007) in the Baltic Sea. A long-term hindcast simulation was performed using a three-dimensional hydrodynamic model PM3D (Kowalewski and Kowalewska-Kalkowska, 2017), a new version of the M3D model (Kowalewski, 1997). The hydrodynamic model...
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Long-term hindcast simulation of sea ice in the Baltic Sea
Open Research DataThe data set contains the results of numerical modeling of sea ice over a period of 50 years (1958-2007) in the Baltic Sea. A long-term hindcast simulation was performed using a three-dimensional hydrodynamic model PM3D (Kowalewski and Kowalewska-Kalkowska, 2017), a new version of the M3D model (Kowalewski, 1997). A numerical dynamic-thermodynamic model...
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Monthly mean concentration of chlorophyll a on the sea surface of the Baltic Sea
Open Research DataMonthly mean surface concentration of chlorophyll a in the years 2003-2022 calculated on the basis of data from the SatBaltic System (https://satbaltyk.iopan.gda.pl/). Maps of monthly average values with a resolution of 1 km were derived from daily satellite data from the Moderate Resolution Imaging Spectroradiometer (MODIS). Gaps in satellite images...
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Monthly mean sea surface temperature (SST) of the Baltic Sea
Open Research DataMonthly mean sea surface temperature (SST) from 2001 to 2022 calculated from data from the SatBaltic System (https://satbaltyk.iopan.gda.pl/). The spatial resolution of the maps is 1 km. The calculation of monthly mean values at each pixel was based on four SST maps on each day of the month. The primary source of SST information was satellite data collected...
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Validation of the HS-GC-FID method for the determination of ethanol residue in tablets
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Validation of the HS-GC-FID method for the determination of athanol residue in tablets
PublicationW pracy opisano proces walidacji metody oznaczania zawartości pozostałości etanolu w tabletkach. W pomiarach wykorzystano technikę HS-GC-FID. Wyznaczono następujące parametry walidacyjne:- selektywność- liniowość- poprawność- precyzję (powtarzalność i precyzję pośrednią)- granice wykrywalności i oznaczalności- zakres pomiarowy- niepewność
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The difficulties in polybrominated diphenyl ethers identification by GC-EI-MS technique
PublicationAwareness about the harmful effects of brominated flame retardants on living organisms increases mainly due to link their presence in the human environment with health disorders. Therefore is a need to conduct research aimed at content control of these chemicals in the environment. Recent improvements in injection techniques and mass spectrometer ionization methods have led to a variety of options to determine PBDEs in environmental...
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Application of GC-MS/MS technique for the determination of benzodiazepines in blood samples
PublicationAbstract Benzodiazepines (BZD) are widely used as pharmaceuticals in medicine. However, due to psychostimulatory effect of BZD, in the last decade, they are more and more often used as drugs of abuse. These compounds produce similar effects to classical illicit drugs and are sold as “legal” alternatives to them as new psychoactive substances (NPS). Currently new BZD, named designer benzodiazepines (DBZD), are synthesized each year...
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Determination of chlorinated solvents in industrial water and wastewater by DAI- GC-ECD
PublicationA very simple and quick analytical method, basedon direct aqueous injection, for determination of halogenatedsolvents in refinery water and wastewater, is described.There is a need to determine halogenated solvents in refinerywater streams, because they may originate from severalprocesses. There is also a need to develop methods enablingVOX to be determined in samples containing oil fractions.The method described enables simultaneous...
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Critical evaluation of resonaut gc voltage link inventures for electrical drives.
PublicationPrzedstawiono wyniki modelowania i symulacji falowników z centralnym obwodem rezonansowym dla zastosowań w napędzie elektrycznym. Porównano struktury ukladów z rezonansowym równoległym obwodem pośredniczącym o ograniczonej wartości szczytowej i uasi-rezonansowych. Dla potrzeb projektowania tych układów, wobec przeciwstawnych funkcji celu dokonano ich wielokrytycznej oceny.
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Solvent residue determination in Uncaria Tomentosa Bark by HS-GC technique
PublicationPrzedstawiono wyniki oznaczeń pozostałości rozpuszczalników organicznych w preparacie uzyskanym z kory liany U. Tomentosa, wykorzystywanej do produkcji farmaceutyków i dodatków do żywności. 1,1,2-trichloroeten oraz dichlorometan są powszechnie stosowane do usunięcia z kory kilku grup alkaloidów o znanych właściwościach biologicznych, co umożliwia zbadanie pozostałych jej związków. Ilościowe oznaczanie tych rozpuszcalników jest...
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Determination of SCFAs in water using GC-FID. Selection of the separation system
PublicationIn the present study, an analytical procedure was developed for the determination of short-chain fatty acids (SCFAs) in landfill leachate and municipal wastewater employing injection of aqueous samples to gas chromatograph with flame ionization detector (GC-FID). Chromatographic conditions such as a separation system, injection volume, oven temperature program were investigated and selected. With two columns, one with a polar (polyethylene...
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Comparison of GC–MS and MEKC methods for caffeine determination in preworkout supplements
PublicationIn this study, GC–MS- and MEKC-based methods for determination of caffeine (CAF) in preworkout supplements were developed and validated. The proposed protocols utilized minimal sample preparation (simple dilution and syringe filtration). The developed methods achieved satisfactory validation parameters, i.e. good linearity (R2 0.9988 and R2 0.9985 for GC–MS- and MEKC-based method, respectively), satisfactory intraand interaccuracy...
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FTIR spectra of gas mixtures from the methanation chamber filled with 50-50wt.% NiO-GDC
Open Research DataThe dataset includes the FTIR spectra collection of the outlet gas mixtures (CO2, CO, CH4) from reactor chamber filled with 50/50 wt.% NiO-GDC (Gadolinia Doped Ceria 20mol.%Gd2O3) catalyst for perfoming methanation reaction. The inlet gas mixture was composed of 3:1 by vol. H2:CO. Spectra were collected using PerkinElmer FTIR every 1 min.
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High resolution model for assessment of contamination by chemical warfare agents dumped in the Baltic Sea
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Distribution and extent of benthic habitats in Puck Bay (Gulf of Gdańsk, southern Baltic Sea)
PublicationThe majority of the southern Baltic Sea seabed encompasses homogenous soft-bottom sediments of limited productivity and low biological diversity, but shallow productive areas in the coastal zone such as wetlands, vegetated lagoons and sheltered bays show a high variety of benthic habitat types offering favourable biotopic conditions for benthic fauna. Within Polish marine areas, semi-enclosed Puck Bay (the western part of the...
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Studies of kicking of three targets – does sex differentiate the velocity of the taekwondo front kick?
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Mercury in suspended matter of the Gulf of Gdańsk: Origin, distribution and transport at the land–sea interface
PublicationThe coastal regions of inland seas are particularly vulnerable to Hg pollution. An important carrier of toxic Hg in the marine environment is suspended matter originating from multiple sources. The present study was conducted in the Gulf...
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Fluoride content in the hair in dependence of the place of residence, sex, dietary habits and anthropometric data
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Mesh-based internet on the Baltic sea for improving e-navigation services. A case study
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Mercury in the Polish part of the Baltic Sea: A response to decreased atmospheric deposition and changing environment
PublicationOur review of the literature showed that since the beginning of the socio-economic transformation in Poland in the 1990s, the downward trend in Hg emissions and its deposition in the southern Baltic Sea was followed by a simultaneous decrease in Hg levels in water and marine plants and animals. Hg concentrations in the biota lowered to values that pose no or low risk to wildlife and seafood consumers. However, in the first decade...
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PELP1 and SRC kinase as important molecules in the estrogen-mediated pathway in human testis and epididymis
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Impact of methane occurrence on iron speciation in the sediments of the Gdansk Basin (Southern Baltic Sea)
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Laboratory measurements of remote sensing reflectance of selected phytoplankton species from the Baltic Sea
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Identification of chemical pollution problems and causes in the Baltic See in relation to socio-economic drivers
PublicationOpisano możliwość wykorzystania nowego narzędzia do zintegrowanej oceny stanu środowiska w akwenie Morza Bałtyckiego. Takie możliwości stwarza narzędzie znane jako DPSIR czyli Drivers (sfery działalności człowieka będące źródłem potencjalnych zznieczyszczeń)-Pressures (ksenobiotyki i specyficzne czynniki szkodliwe emitowane do środowiska)-Stata (stann środowiska)- Impact (efekty niekorzystego oddziaływania na część ożywioną i nieożywioną...
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Impact of hydrotechnical works on outflow of mercury from the riparian zone to a river and input to the sea
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Influence of ice concentration and floe-size distribution on cluster formation in sea-ice floes
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Abnormal features of Macoma balthica (Bivalvia) in the Baltic Sea: alerting symptom of environmental changes?
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Variability of sea ice deformation rates in the Arctic and their relationship with basin-scale wind forcing
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Mean annual and seasonal circulation patterns and long-term variability of currents in the Baltic Sea
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Sea-ice floe-size distribution in the context of spontaneous scaling emergence in stochastic systems
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Mercury in suspended matter of the Gulf of Gdańsk: Origin, distribution and transport at the land–sea interface
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Mercury forms in the benthic food web of a temperate coastal lagoon (southern Baltic Sea)
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Sensitivity, Specificity and Prioritization of Gene Set Analysis When Applying Different Ranking Metrics
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Affymetrix Chip Definition Files Construction Based on Custom Probe Set Annotation Database
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Seagrass vegetation and meiofauna enhance the bacterial abundance in the Baltic Sea sediments (Puck Bay)
PublicationThis study presents the first report on bacterial communities in the sediments of eelgrass (Zostera marina) meadows in the shallow southern Baltic Sea (Puck Bay). Total bacterial cell numbers (TBNs) and bacteria biomass (BBM) assessed with the use of epifluorescence microscope and Norland’s formula were compared between bare and vegetated sediments at two localities and in two sampling summer months. Significantly higher TBNs and...
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Set of Experience and Decisional DNA: Toward Brains for Cyber-physical Systems and Industry of the Future
PublicationThe concept of Decisional DNA is decade old. This article introduces the initial idea of Set of Experience Knowledge Structure, its advancement into Decisional DNA, and its potential for real life applications in divers domains. The most current and future research steps into Industry 4.0 are also presented and discussed
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Set of Experience Knowledge Structure (SOEKS) and Decisional DNA (DDNA): Past, Present and Future
PublicationThis article reviews research work on set of experience knowledge structure (SOEKS)-decisional DNA (DDNA) done in the past, ongoing, and planned for the future. Firstly, the concept of the knowledge representation technique of SOEKS-DDNA is discussed, and then an attempt is made to organize the past research related with it in chronological order. This work focuses on the review on SOEKS-DDNA, its application in different domains,...
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Multilayer coatings based on cerium oxide and manganese cobaltite spinel for Crofer22APU SOC interconnects
PublicationThe current state of the art steel interconnect coating materials are based on critical raw material - Co-oxide spinels. Replacing Co-oxide spinels with alternative, abundant materials can reduce the dependence on the critical raw materials. Cobalt-free coatings with the general formula Mn2-xCuFexO4, where x = 0, 0.1, 0.3, were electrophoretically deposited on a ferritic stainless-steel support and evaluated. Prior to deposition,...
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Badania komunikacji pomiędzy urządzeniami automatyki zabezpieczeniowej zgodnie ze standardem IEC 61850
PublicationW artykule opisano badania modelu sieci SN wyposażonego w przekaźniki REF615 Serii Relion firmy ABB oraz tester zabezpieczeń CMC 256-6 firmy OMICRON. Na stanowisku badawczym na Wydziale Elektrotechniki i Automatyki Politechniki Gdańskiej przeprowadzono badania czasu przesyłania komunikatów GOOSE oraz retransmisji danych za pomocą testera zabezpieczeń CMC 256-6. Wyniki potwierdziły niezawodność oraz powtarzalność czasów przesyłu...
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A framework for accelerated optimization of antennas using design database and initial parameter set estimation
PublicationThe purpose of this paper is to exploit a database of pre-existing designs to accelerate parametric optimization of antenna structures is investigated. Design/methodology/approach The usefulness of pre-existing designs for rapid design of antennas is investigated. The proposed approach exploits the database existing antenna base designs to determine a good starting point for structure optimization and its response sensitivities....
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Trójfazowy 4-gałęziowy falownik SiC w napędzie z wysokoobrotowym silnikiem indukcyjnym
PublicationZastosowanie tranzystorów SiC w falownikach napędów wysokoobrotowych powoduje nowe wyzwania,szczególnie odnośnie generowanego w falowniku napięcia common mode (CM) o wysokiej częstotliwości. Wysokoczęstotliwościowe napięcie CM wchodzi w interakcję z pojemnościami pasożytniczymi falownika, kabla i silnika wymuszając przepływ prądów CM, które są źródłem strat w filtrach pasywnych oraz powodują zakłócenia pomiarów prądów, nieakceptowalne...
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Sources and fate of microplastics in marine and beach sediments of the Southern Baltic Sea—a preliminary study
PublicationMicroplastics’ sources and fate in marine bottom and beach sediments of strongly polluted Baltic Sea have been investigated.Microplastics were extracted using sodium chloride. Their qualitative identification was conducted using micro-Fourier-transform infrared spectroscopy (μFT-IR).
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Model of Nutrient and Pesticide Outflow with Surface Water to Puck Bay (Southern Baltic Sea)
PublicationCoastal basins are particularly exposed to the adverse impact of anthropogenic stress. In many places, despite only the seasonal increase in the number of residents, progressive urbanization and associated changes in the catchment characteristics are noticeable. Puck Bay is part of the Gulf of Gdansk and belongs to the Baltic Sea. Although the area of Puck Bay is covered by the Natura 2000 Network, this has not saved it from eutrophication...
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Effect of sex and menstrual cycle in women on starting speed, anaerobic endurance and muscle power
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Three new records of fishes and their parasite fauna from Pomeranian Bay, Baltic Sea
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Abnormal features of Macoma balthica (Bivalvia) in the Baltic Sea: alerting symptoms of environmental adversity?
PublicationOpisano badania zmian morfologicznych i histopatologicznych populacji mięczaków z Morza Bałtyckiego. Objawy te są związane z niekorzystnymi zmianami w środowisku (obniżenie poziomu stężenia rozpuszczalnego tlenu, występowanie siarkowodoru, podwyższona biodostępność zanieczyszczeń).
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Local properties of the solution set of the operator equation in Banach spaces in a neighbourhood of a bifurcation point.
PublicationW niniejszej pracy badamy problem istnienia bifurkacji w zbiorze rozwiązań równania F(x,p)=0, gdzie F jest odwzorowaniem klasy C^2z iloczynu kartezjańskiego X i R^k do Y, X i Y są przestrzeniami Banacha takimi, że X jest podprzestrzenią liniową Y. Co więcej, dany jest iloczyn skalarny w Y, ciągły względem norm w X i Y. Pokazujemy, że pod pewnymi warunkami (0,p) jest punktem bifurkacji i opisujemyzbiór rozwiązań równania F(x,p)=0...
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Possibilities of detection and identification objects located on the sea bottom by means of a simple sidescan sonar
PublicationPraca zawiera omówienie zagadnień związanych z wykrywaniem i identyfikacją obiektów leżących na dnie przy pomocy sonaru bocznego, umieszczonego na zdalnie sterowanym pojeździe głębinowym.