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Search results for: WET SYTHESIS
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Acylic congener of cucurbituril: synthesis and recognition properties.
PublicationZaprezentowano syntezę analogów acyklicznych cucurbiturilu oraz ich zdolności do kompleksowania wybranych 16 amin, dioli, kwasów dikarboksylowych, pochodnych guanidyny oraz pirydyny. Obserwowane tworzenie kompleksów przebiegało około 180 razy słabiej niż dla cucurbiturilu. Wyniki te świadczą o potencjalnych możliwościach zbliżonych do analogów cyklicznych pod względem tworzenia kompleksów i rozpoznawania wyżej wymienionych...
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Robust H- optimal synthesis of FDI systems
PublicationDetekcję błędów występujących w nadzorowanym obiekcie dynamicznym, stanowią-cą podstawę decyzji diagnostycznych, oprzeć można na analizie wektorów resz-towych, generowanych w układzie zawierającym odpowiednio zaprojektowany od-porny estymator stanu danego obiektu. Rozważano tylko zewętrzny aspekt syn-tezy generatora reszt optymalnych ze względu na normę tej przestrzeni H : toznaczy problem odprzęgania wektora resztowego od niemierzalnych...
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Synthesis of autonomous underwater vehicle control system.
PublicationArtykuł dotyczy parametrycznej identyfikacji systemu sterowania autonomicznego pojazdu podwodnego.Badania opierają sie na modelu pojazdu o 4 stopniach swobody, zrealizowanym w środowisku programowym Matlab/Simulink. Zastosowano wielowymiarowy nieliniowy regulator PID. Przedstawiono wyniki symulacji zaprojektowanego układu sterowania.
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Synthesis of Combretastatin A-4 Analogs and their Biological Activities
PublicationCombretastatin A-4 (CA-4) is a natural product, which consists of two phenyl rings, linked by an ethylene bridge. CA-4, inhibitor of polymerization of tubulin to microtubules, possesses a strong antitumor and anti-vascular properties both in vitro and in vivo. Previous studies showed that disodium phosphate salt of CA-4, a water-soluble prodrug is well tolerated at therapeutically useful doses. However, it should be noted that...
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DDQ-mediated synthesis of functionalized unsymmetrical disulfanes
PublicationWe developed a simple and efficient method for the synthesis of functionalized unsymmetrical disulfanes under mild conditions in good yields. The designed method is based on the reaction of bis(5,5- dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)disulfane with thiols in the presence of 2,3-dichloro-5,6-dicyanobenzoquinone (DDQ). The developedmethod allows the preparation of unsymmetrical disulfanes bearing additional hydroxy, carboxy,...
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Optimization of Graphene Oxide Synthesis and Its Reduction
PublicationIn this article, we present the review of the chemical methods of synthesis of graphene oxide and its reduction in order to obtain the so-called reduced graphene oxide (rGO) whose properties are similar to those of pure graphene. We also present our experiments and the results in this field and the comparison of the efficiency of different methods of synthesis as well as the reduction of graphene oxide. To characterize the obtained...
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Functionalized polyolefins, synthesis application and industrial relevance
PublicationPolymers play a key role in our modern life full of technical advances and a continuous request for new materials with tailored properties for a low price. Their excellent mechanical properties, good processability, chemical stability and low price make polyolefins the polymers of choice for most commodity and some more specialized applications. As a result, polyolefins account for over 65% of the total world demand of plastic...
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Synthesis and polymerisation techniques of molecularly imprinted polymers
PublicationMolecularly Imprinted Polymers (MIPs) are materials that has been processed using the molecular imprinting technique which permit to obtain well-defined three-dimensional cavities, with affinity to a template molecule, in the polymer matrix. Technology involves three strategies, i.e., covalent, non-covalent and semi-covalent approach, but the most popular is non-covalent approach. The most important components for the synthesis...
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Introduction to MIP synthesis, characteristics and analytical application
PublicationOne of the trends in analytical chemistry is associated with designing and developing new types of sample preparation techniques, which might significantly increase the efficiency and selectivity of the analytes isolation or/and preconcentration process. One of the most widely employed solutions are selective sorption materials, defined as molecularly imprinted polymers (MIPs), as well as the sorbents with the molecular fingerprint....
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Efficient Synthesis of Functionalized Unsymmetrical Dialkyl Trisulfanes
PublicationWe have developed a convenient method for the synthesis of functionalized unsymmetrical dialkyl trisulfanes under mild conditions in very good yields. The designed method is based on the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)-disulfanyl derivatives with alkyl disulfanyl anions generated in situ from S-acetyl disulfanyl derivatives and sodium methoxide. The developed method allows for the preparation of...
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Electrochemically Induced Synthesis of Triphenylamine-based Polyhydrazones
PublicationTriphenylamine-based hydrazones were subjected to electropolymerization process that gave well conductive hydrazone based polymers. The first example of polyhydrazone formation during the electrochemical process was shown. The estimation of polymer structure was demonstrated using IR spectroelectrochemistry. The EPR spectroelectrochemistry allowed to explain why in some cases dimer couldn’t be formed. The results of electrochemical,...
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SYNTHESIS AND PROPERTIES OF OLIGOMERS WITH HYDROXY END-GROUPS
PublicationMethods of oligomers (polymers) with hydroxy end-groups obtaining are examined. The synthesis of hydroxy-containing oligomers based on epoxy resins is of special attention. The molecules of mentioned oligomers apart from free primary and secondary hydroxy groups contain epoxy, peroxy, carboxy or acrylic groups.
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Analysis and synthesis of structural system dimensional deviations
PublicationBłedne zasady określania dopuszczalnych odchyłek wymiarowych stalowych elementów konstrukcyjnych lub wręcz ich brak często powodują trudności w czasie montażu konstrukcji. W każdym układzie konstrukcyjnym można wyróżnić tzw. Koordynacyjne Wymiary Montażowe (KWM). Odchyłki wymiarowe (tolerancje) KWM decydują o zachowaniu poprawnej geometrii ustroju budowlanego po jego zamontowaniu na placu budowy. KWM tworzą zamknięte ciągi wymiarowe,...
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Intramolecular Proton Transfer in the Radical Anion of Cytidine Monophosphate Sheds Light on the Sensitivities of Dry vs Wet DNA to Electron Attachment-Induced Damage
PublicationSingle-strand breaks (SSBs) induced via electron attachment were previously observed in dry DNA under ultrahigh vacuum (UHV), while hydrated electrons were found not able to induce this DNA damage in an aqueous solution. To explain these findings, crossed electron-molecular beam (CEMB) and anion photoelectron spectroscopy (aPES) experiments coupled to density functional theory (DFT) modeling were used to demonstrate the fundamental...
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ITM Web of Conferences
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ADVANCED SYNTHESIS & CATALYSIS
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CURRENT ORGANIC SYNTHESIS
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We are in touch
PublicationIn Touch - opis pracy „Dłonie stanowią część indywidualnej osobowości i charakteru, ale wykonują również swoje niezależne działania, i jako wyposażone we własny język, mają kluczowe znaczenie dla ludzkiej komunikacji.” Myśląca dłoń, J. Pallasmaa Obraz In Touch powstał z potrzeby zbudowania metafory czasu, którego aktualnie doświadczamy. Popularny w języku angielskim, wyrażający intencję pozostania w kontakcie, zwrot we are in...
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Anna Zielińska-Jurek prof. dr hab. inż.
People2018 DSc in technical sciences in the field of chemical technology Chemical Faculty, Gdansk University of Technology, Title: “Functionalized titanium(IV) oxide as a photocatalyst for environmental purification” 2011 Ph. D. in technical sciences in the field of chemical technology Chemical Faculty, Gdansk University of Technology, Title of the dissertation:...
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Scanning Electron Microscopy images of nanocubes suspension 1 month after synthesis
Open Research DataThis dataset contains the SEM images of the gold nanocubes suspension in citrate buffer. The goal of the study was to evaluate the size of the synthesized nanocubes, their stability one month after the synthesis process, and to verify the optimal conditions regarding nanocubes concentration for the SEM analysis. Solutions with two different AuNC concentrations...
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Wykorzystanie Web 2.0 oraz architektury informacji w pracy brokera informacji = TAKING ADVANTAGE OF WEB 2.0 AND THE INFORMATION ARCHITECTURE IN THE INFORMATION BROKER’S WORK
PublicationThe development of information and communication technologies, dissemination of access as well as unlimited increase of publications result in the uncontrolled growth of knowledge resources. Looking up for the relevant information becomes increasingly difficult, especially when time plays a role. Such process requires vast knowledge, practical experience in obtaining and providing information and also analytical...
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A novel architecture of Web-GIS for mapping and analysis of echinococcosis in Poland
PublicationEchinococcosis is an infectious disease transferred through ingestion of food or water which have been contaminated with eggs of the Echinococcus tapeworm, which are spread by intermediate parasite hosts. Because the latter are primarily territorial, research related to diagnosis and prevention of echinococcosis requires investigation of environmental factors, which can be supported with the use of a Geographical Information System...
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Smart Innovation Engineering Using Set of Experience and Decisional DNA
PublicationKnowledge-based Engineering Systems are founded upon integration of knowledge into computer systems and are one of the core requirements for the future Industry 4.0. Since the fourth industrial revolution is passing through the developing phase, implementation of Cyber-Physical Production Systems require more realistic approach. Knowledge Management and Knowledge Engineering plays an important role in manufacturing industries facing...
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Set of Experience and Decisional DNA: Experience-Based Knowledge Structures
PublicationThis chapter presents a description of Set of Experience Knowledge Structure (SOEKS) and Decisional DNA (DDNA), argumentation for a knowledge representation, composition, configuration and metrics. SOEKS is a combination of filtered and amalgamated information obtained from formal decision events. It facilitates effective explicit representation of decisional experience taken from different technologies. SOEKS comprises variables,...
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A numerical analysis of the thermal effects in the jet impingement stagnation zone
PublicationMost of the flows occurring in the engineering systems are turbulent and their accurate numerical analysis is still challenging, especially when combined with the heat transfer. One of the methods of heat transfer enhancement is utilization of the turbulent impinging jets, which were recently applied also in the heat exchangers. Their positive impact on the heat transfer performance was proven, but many questions related to its...
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The potential of web awareness as a determinant of dually defined customer value
PublicationIn the conditions of increasing demand barrier, the enterprise’s basic capital is customers. From an enterprise point of view, this means the need to create a dual perceived and defined customer value which remains related to market value (income and development potential) and customer resource value (reference, information and cooperative potential). The progressing digitisation process transfers business processes, and thus relationships, into...
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Three-dimensional representation of geographic data in a Web-based GIS
PublicationPresenting geographic data in a web environment has been a long standing problem. For many years the low performance of web browsers has limited the visualization of spatial data to only two dimensions. More recently, the introduction of open standards for 3D acceleration of web applications sparked the emergence of new methods of presenting three-dimensional data in a web browser without using third-party extensions. However,...
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Ranking metrics in gene set enrichment analysis: do they matter?
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GlyCulator2: an update on a web application for calculation of glycemic variability indices
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The Comparison of the Web GIS Applications Relevant for 4D Models Sharing
PublicationThe paper presents results of the project: Cultural Heritage Through Time (CHT 2, http://cht2-project.eu) realized accomplished within the framework of the “Joint Programming Initiative in Cultural Heritage” JPI-CH (http://www.jpi-culturalheritage.eu) by an international consortium: Politecnico di Milano (IT), Newcastle University (UK), Salamanca University (ES), and Stanislaw Staszic Scientific Association SSSA (a non-profit...
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Attempts to detect West Nile virus in wild birds in Poland
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BUDOWA I AKTYWNOŚĆ BIAŁEK NALEŻĄCYCH DO RODZINY TET
PublicationBiałka należące do rodziny TET (Tet1, Tet2, Tet3) są enzymami wykazującymi aktywność względem 5-metylocytozyny, która jest ważnym markerem epigenetycznym odgrywającym kluczową rolę w trakcie rozwoju organizmu i mającym istotny wpływ na poziom ekspresji genów. Białka TET przekształcają 5-metylocytozynę do 5-hydroksymetylocytozyny, 5-formylocytozyny i 5-karboksylocytozyny w trakcie następujących po sobie trzech reakcji utleniania....
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Just Let Me Think: Designing Against Acquired Illiteracy.
PublicationThis article concerns the relatively new problem of illiteracy relating to persons previously being literate, which is caused by too intensive using of so-called digital media (TV, computers, tablets, smartphones, e-book readers, portable media players, etc.). The problem has been observed for several years mainly in countries with high economic and technological development. The widespread use of digital media and the ease of...
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Methods for evaluating rated power of diesel-powered generator set
PublicationBasic concepts for evaluating rated power of generator sets powered by combustion engines are presented in this article. A relation between parameters of the engine and the generator are shown. Recommendations contained in the standards and technical literature are systematized. The scheme and methodology for evaluating rated power of the generator set, based on laboratory research, are suggested. Also, the main problems which...
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Applying Web 2.0 Concepts to Creating Energy Planning Portal
PublicationCommunity authorities in Europe are tasked to create Advanced Local Energy Plans (ALEP), which encompasses collecting local data on current energy use and generation, as well as generating future development scenarios. Both the data and the development scenarios must be publicly accessible as a basis for energy-related decisions taken by residents, local companies and other local institutions. The data must partially be collected...
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Introducing the concept of Decisional DNA-Based web content mining
PublicationPrzedstawiono koncepcje zastosowania struktury reprezentacji wiedzy opartej na decyzyjnym DNA w procesie wyszukiwania informacji w internecie. Dokonano analizy eksperymentow tak wspomaganego wyszukiwania oraz sformulowano wnioski na temat przyszlych badan prowadzacych do dalszej integracji procesu wyszukiwania z doswiadczeniami zdobytymi w trakcie tego wyszukiwania.
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Matching Exception Class Hierarchies between .NET, Java Environments
PublicationThe paper presents a methodology of exception classification and matching exception messages between .NET andJava environments. The methodology operates on existing exception class hierarchies and proposes two complementingapproaches: automated and manual matching. The automated matching uses the similarity measure to find associationsbetween exception messages from the two sets of classes for the considered programming languages....
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A Point Set Connection Problem for Autonomous Mobile Robots in a Grid
PublicationConsider an orthogonal grid of streets and avenues in a Manhattan-like city populated by stationary sensor modules at some intersections and mobile robots that can serve as relays of information that the modules exchange, where both module-module and module-robot communication is limited to a straight line of sight within the grid. The robots are oblivious and move asynchronously. We present a distributed algorithm that, given...
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Equivariant degree of convex-valued applied to set-valued BVP
PublicationW pracy określono stopień ekwiwariantny dla odwzorowań o wartościach zwartych i wypukłych. Zastosowano go do dowodu twierdzenia o istnieniu wielunietrywialnych rozwiązań problemu brzegowego typu Dirichleta dla inkluzji różniczkowych z warunkami wzrostu typu Bernsteina-Nagumo, z dodatkowymi symetriami
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Preparation and Surface Characterization of Chitosan-Based Coatings for PET Materials
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Automatic evaluation of information credibility in Semantic Web and Knowledge Grid
PublicationThis article presents a novel algorithm for automatic estimation of information credibility. It concerns information collected in Knowledge Grid and Semantic Web. Possibilities to evaluate the credibility of information in such structures are much greater than those available for WWW sites which use natural language. The rating system presented in this paper estimates credibility automatically on the basis of the following metrics:...
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Concept of web service for real-time satellite imagery dissemination
PublicationW artykule zaproponowano system upowszechniania obrazów satelitarnych w czasie niemal rzeczywistym realizujący ideę oprogramowania jako usługi. System jest złożony z 4 logicznych modułów - modułu akwizycji danych, zarządzania, serwera Web oraz klienta. Protokół zapytań WCS jest wykorzystywany jako interfejs pomiędzy większością modułów. System tworzony jest z myślą o udostępnianiu danych dla zdalnych użytkowników w formie usługi...
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Web-Based Integrated Timetable Information System for Railways and Airlines
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CFD analysis of jet flows ejected from different nozzles
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Obrazowanie parametryczne w badaniach mózgu metodami MRI/PET
PublicationCelem tej monografii jest przedstawienie technik obrazowania metodami tomografii rezonansu magnetycznego (MRI - Magnetic Resonance Imaging) i pozytonowej tomografii emisyjnej (PET - Positron Emission Tomography) w kontekście badań dynamicznych mózgu, szczególnie w zakresie syntezy obrazów parametrycznych opisujących jakościowo lub ilościowo przepływ mózgowy. Obrazowanie parametryczne określa technikę syntezy obrazów na podstawie...
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Rough set based automatic classification of musical instrument sound
PublicationReferat dotyczy problemu automatycznego rozpoznawania instrumentów muzycznych rozwiązywanego z zastosowaniem, inteligentnych algorytmów decyzyjnych. Wnioski zawarte w referacie dotyczą reprezentacji sygnałów muzycznych, która jest przydatna w procesie automatycznej klasyfikacji instrumentów.
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Urban scene semantic segmentation using the U-Net model
PublicationVision-based semantic segmentation of complex urban street scenes is a very important function during autonomous driving (AD), which will become an important technology in industrialized countries in the near future. Today, advanced driver assistance systems (ADAS) improve traffic safety thanks to the application of solutions that enable detecting objects, recognising road signs, segmenting the road, etc. The basis for these functionalities...
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Electrical properties of ceria films prepared by net shape technology
PublicationW pracy przedtswiono procedurę przygotowania gęstych warstw elektrolitu z wykorzystaniem technologii Net Shpe. Technologia ta na znaczne obniżenie temperatury przygotania tego typu warst. Okresloślono parametry elektryczne warst domieszkowanego ceru przygotowanych w tej technologii.
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WAI-Web Accessibility Initiative. Sieć dostępna dla wszystkich.
PublicationZostały przedstawione podstawowe formy niepełnosprawności i ich wpływ na korzystanie z narzędzi internetowych, w tym głównie ze stron WWW. Tworzenie dostępnego serwisu zostało omówione krok po kroku, uwzględniając przedstawienie dostępnych obecnie technologii wspierających dostępność, narzędzi umożliwiających rozwijanie dostępnych serwisów oraz technik, za pomocą których możliwe jest zaimplementowanie dostępności na stronie. Zostały...
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The potential of Web-GIS and geovisual analytics in the context of marine cadastre
PublicationThe importance of the marine environment to human existence makes it imperative that information models represent the multidimensional nature of reality as closely as possible in order to facilitate good governance. Information regarding jurisdiction, as well as the effects of formal law and community interests on the marine environment (e.g. nature and spatial extents as well as rights, responsibilities, restrictions etc.) would...