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Applications of Alkanethiols in Organic Synthesis
PublicationThis manuscript is an update to the earlier Science of Synthesis contribution describing methods for the synthesis of alkanethiols. Thiols can be converted into sulfonic, sulfinic, sulfenic acid and their derivatives, sulfides, disulfides, polysulfides, sulfonium salts, and thiiranes, etc. These transformations are accomplished by nucleophilic displacement or addition, oxidation, condensation, or coupling reactions involving thiol...
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Anna Lisowska-Oleksiak prof. dr hab.
PeopleAnna Lisowska-Oleksiak, born in 1952, has been working at GUT since 1977. Currently is employed at the Faculty of Chemistry as a full professor. She was employed as a research assistant at the University of St Andrews in the group of C. A. Vincent and P.G. Bruce (1991-1994). She completed a two-month research internship in CEA Grenoble (2011). Anna Lisowska-Oleksiak obtained her MSc in chemistry at Nicolaus Copernicus University...
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Beata Krawczyk-Bryłka dr
PeoplePsycholog, doktor nauk humanistycznych w dziedzinie zarządzania, adiunkt w Katedrze przedsiębiorczości. 2018 - 2021: Kierownik projektu NCN: „Efektuacyjny model zespołu przedsiębiorczego. Jak działają przedsiębiorcze zespoły odnoszące sukces" od 2016: Quality Standards Lead filaru People management & personal development na studiach MBA Politechniki Gdańskiej 2008 – 2012: Prodziekan ds kształcenia Wzydziału Zarządzania i Ekonomii...
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Automatic analysis of the aggressive behavior of laboratory animals using thermal video processing
PublicationThe bite detection is very important but difficult element of the social interaction analysis. Standard observation methods like human observer or a camcorder of visible light frequencies fail in this case. However, it is possible to discern cooler spots on the rodent's body that appear after body contact with another individual, and vanish after short time. These spots are assumed to be a saliva trace left on fur after bite. In...
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Cover Feature: Electronic Circular Dichroism Imaging (ECD i ) Casts a New Light on the Origin of Solid‐State Chiroptical Properties (Chem. Eur. J. 4/2022)
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Rengel Cane Sia Doctoral Candidate
PeopleI’m Rengel, born and raised in the Philippines. As an undergraduate I did kinetic modeling on Copper-catalyzed atom transfer radical addition (ATRA). Then I was inspired to do both theoretical and experimental studies, which led me to propose my master’s thesis on Synthesis, Computational, Electrochemical, and Photoconductivity Studies on Naphthalene and its derivatives. This led to a master’s degree in Chemistry in the Mindanao...
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Alkanethiolates of Group 1,2, and 13-15 Metals
PublicationThis manuscript is an update to the earlier Science of Synthesis contribution describing methods for the synthesis of alkanethiolates of group 1, 2, and 13-15 metals. Alkanethiolates can be converted into S-alkyl thiocarboxylic acid esters, 1-thioglycosides, S-alkyl thiosulfinates, tetrahydro-1,4-thiazine-3-ones, sulfides, disulfides, sulfonium salts, dithioacetals and dithioketals, etc. These transformations are accomplished by...
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Binding of anionic Pt(ii) complexes in a dedicated organic matrix: towards new binary crystalline composites
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Między spotkaniem a mijaniem. Rahel Varnhagen, Hannah Arendt, Judith Butler
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«Ciało» na wojnie. Wokół Soli ziemi Józefa Wittlina
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Praktyczne kompetencje cyfrowe
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Rest cure – XIX-wieczna terapia nudą Silasa Weira Mitchella w opowiadaniu „Żółta tapeta” Charlotte Perkins Gilman
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Filip Kutt dr inż.
PeopleFilip Kutt was born in Gdansk, Poland. He received the M.Sc., PhD, degrees in electrical engineering in 2007 and 2013, respectively, all from Gdansk University of Technology (GUT) Poland. He is with GUT since 2007, currently as an Assistant Professor. His main scientific and research interests cover a wide spectrum of mathematical modelling of electrical machines using analytical modelling and FEM-based computations.
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Measurements of angular distribution for photoionization of mercury into the 5d9 2D5/2 ionic state over the energy range from 15 eV to 17 eV
PublicationWykonano pomiary różniczkowych przekrojów czynnych na fotojonizację atomów rtęci do stanu 5d9 2D5/2 jonu w zakresie energii fotonów od 15 eV do 17 eV. Wyznaczono parametr β asymetrii dla stanu 2D5/2 jonu z pomiarów emisji fotoelektronów pod kątami 0˚ i 90˚ stopni względem osi głównej elipsy polaryzacji. Zarejestrowano trzy serie stanów autojonizacyjnych zbieżnych do energii jonizacji do stanu 2D3/2. Badania wykonano w ośrodku synchrotronowym...
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Simple adaptive cubic spline interpolation of fluorescence decay functions
PublicationZaproponowano prostą metodę interpolacji funkcji zaniku fluorescencji. W pierwszym kroku interpolowany zanik jest całkowany za pomocą adaptacyjnego algorytmu wykorzystującego kwadratury Newtona-Cotesa. Uzyskiwana w ten spoób siatka wartości czasu jest używana w drugim kroku polegającym na typowej interpolacji za pomocą funkcji sklejanych trzeciego stopnia.
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The Hanseatic City Challenge
EventsSee more at www.hanseaticcitychallenge.com
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Powder x-ray diffraction pattern of polycrystalline Cu(IO3)2*xH2O
Open Research DataHydrated copper(II) iodate sample was prepared in water solution by reacting copper(II) sulfate and potassium iodate, following the method described by Peterson (J. Chem. Educ. 1957, 34, 12, 612). The sample was subsequently dried at various temperatures in order to produce an anhydrous Cu(IO3)2:
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Imaging of morphological and physicochemical changes occuring in the structure of austenitic steel due to the thermal sensitization
Open Research DataIn polycrystalline materials, grain boundaries are always where phenomena such as surface diffusion, sedimentation and corrosion occur. They have a significant impact on the macroscopic properties of the construction material [1]. In addition to inhomogeneities such as manganese sulphide inclusions formed during the metallurgical process, interfacial...
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abiotic degradation of chlorinated ethanes and ethenes in water
PublicationIntroduction Chlorinated ethanes and ethenes are among themost frequently detected organic pollutants of water. Theirphysicochemical properties are such that they can contaminateaquifers for decades. In favourable conditions, they canundergo degradation. In anaerobic conditions, chlorinatedsolvents can undergo reductive dechlorination.Degradation pathways Abiotic dechlorination is usuallyslower than microbial but abiotic dechlorination...
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Forster energy transfer from nonexponentially decaying donors
PublicationPrzedyskutowano niezbędne modyfikacje stałej szybkości transferu foersterowskiego w sytuacji, kiedy zanik fluorescencji donora w nieobecności akceptora jest nieeksponencjalny. Stwierdzono, że najbardziej przydatna modyfikacja wynika założenia jednakowej wartości stałej zaniku radiacyjego dla wszystkich molekuł donora.
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Site-to-site distance distribution in flexible molecules: theoretical evaluation of the donor and/or acceptor fluorescence decay function
PublicationPrzedstawiono wyrażenie teoretyczne opisujące zależność funkcji zaniku fluorescencji od rozkładu odległości P(r) pomiędzy donorami i akceptorami w giętkich molekułach dwuchromoforowych. Wyrażenie uwzględnia wiekoeksponencjalny zanik izolowanych donorów i akceptorów, a także możliwość niekompletnego oznakowania molekuł akceptorami. Przyjęto, że względne zmiany odległości donorów i akceptorów w czasie życia fluorescencji donora mogą...
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Evaluation of La 2 Ni 0.5 Cu 0.5 O 4+δ and Pr 2 Ni 0.5 Cu 0.5 O 4+δ Ruddlesden-Popper-type layered oxides as cathode materials for solid oxide fuel cells
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THERMION-C2S_10 Ionic thermoelectri effect in the phase transition in Cu2Se
Open Research DataThe dataset contains results of measurements of the ionic thermoelectric effect in copper selenide with Cu1.99Se and Cu1.8Se compositions. X-Ray diffraction data, SEM images and EDX spectra of the samples are also in the dataset.
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Imaging and chemical investigation of silver coating
Open Research DataThe recovery of silver from materials such as plates, still used in clinical radiography [1], or scrap jewelery is still very popular. The subject of the research, part of which was microscopic imaging, was to recreate the behavior of an electrochemically deposited silver coating. The copper electrodes were covered with a layer of silver obtained from...
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The impact of cooking method on the phenolic composition, total antioxidant activity and starch digestibility of rice (Oryza sativa L.)
PublicationThis study investigated changes in the phenolic composition, total antioxidant activity (TAA) and starch digestibility in white and brown rice due to three different cooking procedures, and subsequent reheating of cooked rice after storage. Among the analyzed samples, brown rice showed the highest TAA and phenolic content (622.5 mg kg-1 DW). All cooking methods resulted in significant decrease of phenolic content and TAA of rice...
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Transparent thin films of Cu-TiO2 with visible light photocatalytic acitivity
PublicationThin films of Cu–TiO2 with a high level of transparency were prepared by a dip-coating procedure on the glass surface. CuCl2 was used as a copper precursor added during sol – gel synthesis of TiO2. The extension of optical absorption into the visible region of as-prepared thin films was indicated by UV/Vis spectroscopy. Only the anatase phase was detected by X-ray di ffraction analysis (XRD). The presence of copper in the structure...
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A concerted evolution of supramolecular interactions in a {cation; metal complex; π-acid; solvent} anion-π system
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Bibliografie cyfrowe
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Alcohol Potentiates Orthostatic Hypotension
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Zmiany w instalacjach stacjonarnych a spełnienie wymagań emisji przewodowej
PublicationW pracy przedstawiono wyniki pomiarów emisji przewodowej przeprowadzonych w zakładowym laboratorium EMC obwodów zasilania instalacji alarmowych na zgodność z wymaganiami normy EN 55022 (dla urządzeń klasy B) w których nastąpiła zmiana zasilacza AC/AC względem zalecanej przez producenta konfiguracji. Uzyskane wyniki wskazują, że stosunkowo niewielkie odstępstwo od zalecanej konfiguracji instalacji skutkują przekroczeniem poziomów...
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Performance Evaluation of a 650V E-HEMT GaN Power Switch
PublicationGaN power switches have better characteristics compared to the state-of-the-art Si power transistors. These devices offer high operating temperature and current densities, fast switching and low on-resistance. However, currently only a few producers offer technology of high voltage GaN transistors. Immaturity of this technology is the reason why experimental evaluation of GaN parameters must be performed to properly exploit their...
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Performance‐driven modeling of compact couplers in restricted domains
PublicationFast surrogate models can play an important role in reducing the cost of EM-driven design closure of miniaturized microwave components. Unfortunately, construction of such models is challenging due to curse of dimensionality and wide range of geometry parameters that need to be included in order to make it practically useful. In this letter, a novel approach to design-oriented modeling of compact couplers is presented. Our method...
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Jan Hupka prof. dr hab. inż.
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The effect of surfactants mixtures composition on wetting of different solid materials
PublicationThe wetting properties of surfactants mixtures were investigated. Three types of compounds were used: nonionic gemini α, α'-[2,4,7,9-tetramethyl-5-decyne-4,7-diyl]bis[ω-hydroxyl-olioxyethylene] (S-10), anionic sodium dodecyl sulphates (SDS) and cationic dodecyl trimethyl ammonium bromide (DTAB). The materials used in wetting experiments were steel and methyl polymethacrylate. These materials differ...
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Understanding the capacitance of thin composite films based on conducting polymer and carbon nanostructures in aqueous electrolytes
PublicationIn this work electrochemical performance of thin composite films consisted of poly(3,4-ethylenedioxythiophene) (PEDOT), graphene oxide (GOx) and oxidized multiwalled carbon nanotubes (oxMWCNTs) is investigated in various sulphates (Li2SO4, Na2SO4, K2SO4, MgSO4) and acidic (H2SO4) electrolytes. Capacitance values, rate capability and cycling stability achieved for the composite layers are correlated with the electrolytes’ properties...
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Physicochemical and photocatalytic data of Cu-TiO2/Ti3C2 composites
Open Research DataIn this dataset, we include the data regarding the physicochemical properties (XRD, DR/UV-vis, photoluminescence, electrochemistry) and photocatalytic activity of TiO2/Ti3C2 and Cu-TiO2/Ti3C2 composites in the reaction of carbamazepine degradation. Herein we present the results for pure TiO2/Ti3C2 and composites modified with copper particles (0.25%,...
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Size Reduction of Microwave Couplers by EM-Driven Optimization
PublicationThis work addresses simulation-driven design optimization of compact microwave couplers that explicitly aims at circuit footprint area reduction. The penalty function approach allows us to minimize the area of the circuit while ensuring a proper power division between the output ports and providing a sufficient bandwidth with respect to return loss and isolation around the operating frequency. Computational cost of the optimization...
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Dariusz Mikielewicz prof. dr hab. inż.
PeopleProfessor Dariusz Mikielewicz – born on February 6, 1967. in Gdansk. Here in 1974 he enrolled first to the Elementary School No. 17, and then in the Grammar School No. 5, named after Stefan Żeromski in Gdansk-Oliwa. After graduating from the Secondary School, with honors, in 1985 he successfully passed the entrance exams to the Faculty of Mechanical Engineering of Technical University of Gdansk, where he graduated with a very good...
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Transformation of bimetallic Ag–Cu thin films into plasmonically active composite nanostructures
PublicationFormation of plasmonically active silver, copper and composite silver-copper nanostructures were studied in this paper. Metallic nanostructures were fabricated by thermal disintegration, so called dewetting, of the thin films in an argon atmosphere. The formation process of the nanostructures was in-situ observed by a novel method, based on resistance measurements. The influence of the material and thickness of the initial thin...
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Process modeling inside cylinder in an internal combustion engine with heat regeneration
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Optimization of the geometry of the crankshaft for an internal combustion engine with heat regeneration
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Beata Koper dr
PeopleBeata Koper - Ph.D., assistant professor at the University of Opole. Digital Humanities Specialist at the Literary Research Infrastructure Laboratory (Institute of Literary Research, Polish Academy of Sciences), information and documentation specialist, UX designer, and last but not least team member of the Digital Humanities Center at the Institute of Literary Research of the Polish Academy of Sciences. Co-author of the "Polish...
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Obrony prac doktorskich na Wydziale Chemicznym
EventsDn. 26.04.2022 r. o godz. 8.30 w Audytorium 1.4 Wydziału Chemicznego PG (budynek nr 5) odbędzie się w trybie hybrydowym obrona pracy doktorskiej mgr inż. Karoliny Grajewskiej.
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Botanical and geographical origin characterization of polish honeys by headspace SPME-GCxGC-TOFMS
PublicationVolatile organic compounds (VOCs) composition of Polish honeys obtained from various geographical regions was studied. Headspace solid phase microextraction (HS-SPME) using Divinylbenzene/Carboxen/Polydimethylsiloxane-coated fibers was used in combination with comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry (GC× GC-TOFMS) because of the complexity of the samples. Acacia, linden, rapeseed, buckwheat...
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Effect of heat treatment on the diffusion intermixing and structure of the Cu thin film on Si (111) substrate: a molecular dynamics simulation study
PublicationThis work is devoted to the study of the diffusion process at the interface between copper films with a thickness of 2, 3, 4, 7 and 10 atomic monolayers and silicon substrate by molecular dynamics simulation method. For this purpose, the variation of the concentration of copper and silicon along the perpendicular direction to the interface was investigated. An analysis of the density profile along this direction made it possible...
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AN OVERVIEW OF HEAT TRANSFER ENHANCEMENT BASED UPON NANOPARTICLES INFLUENCED BY INDUCED MAGNETIC FIELD WITH SLIP CONDITION VIA FINITE ELEMENT STRATEGY
PublicationThe mathematical model of heat generation and dissipation during thermal energy transmission employing nanoparticles in a Newtonian medium is investigated. Dimensionless boundary layer equations with correlations for titanium dioxide, copper oxide, and aluminium oxide are solved by the finite element method. Parameters are varied to analyze their impact on the flow fields. Various numerical experiments are performed consecutively...
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Depth chemical profile in a CeIr3 sample
Open Research DataThe polycrystalline sample of CeIr3 used in the present studies was synthesized by arc-melting cerium (4N) and iridium (3N5) in an arc furnace on a water-cooled copper hearth using a tungsten electrode under a high purity argon atmosphere. A piece of zirconium was used as an oxygen getter. First, a button of Ir was prepared by arc-melting the iridium...
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Thermodynamic Properties of Inorganic Salts in Nonaqueous Solvents. VI. Apparent Molar Volumes, Expansibilities, and Compressibilities of Divalent Transition Metal Ions in Methanol and Dimethylsulfoxide
PublicationThe temperature dependence of the density of divalent transition metal perchlorates in dimethylsulfoxide as well as cobalt(II), nickel(II) perchlorates, and copper(II) trifluoromethanesulfonate in methanol was determined. Moreover, sound velocities for solutions of cobalt(II), nickel(II) perchlorates, and copper(II) trifluoromethanesulfonate in methanol have been measured at 298.15 K. From these data, the partial molar volumes,...
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Deformation Sweep Test of Cement Bitumen Treated Material Mixture C3E5.5 (field obtained material; over 28 days of curing at 20C)
Open Research DataDataset presents data of results of deformation sweep test determined for cold recycled mixture – cement bitumen treated material mixture with following binding agents: 3% cement and 5.5% emulsion (C3E5.5). Mixture was designed according to Polish requirements for the base course of pavement. Mixture contains 60% of RAP material. Specimen size: f=100...
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Deformation Sweep Test of Cement Bitumen Treated Material Mixture C3E5.5 (field cores; field curing)
Open Research DataDataset presents data of results of deformation sweep test determined for cold recycled mixture – cement bitumen treated material mixture with following binding agents: 3% cement and 5.5% emulsion (C3E5.5). Mixture was designed according to Polish requirements for the base course of pavement. Mixture contains 60% of RAP material. Specimen size: f=100...