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Search results for: MAGNETIC SORBENT
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JOURNAL OF MAGNETIC RESONANCE
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Bulletin of the Ancient Orient Museum (of Tokyo)
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The Journal of the Economic and Social History of the Orient
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Physicochemical Properties and Application of Silica-Doped Biochar Composites as Efficient Sorbents of Copper from Tap Water
PublicationThis article concerns research on new sorption materials based on silica-doped activated carbon. A two-stage synthesis involved pyrolysis of plant material impregnated in a water glass solution , followed by hydrothermal activation of the pyrolysate in KOH solution. The resulting composite can be used as a sorbent in drinking water filters. The proposed method of synthesis enables the design of materials with a surface area...
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Effective assessment of biopolymer-based multifunctional sorbents for the remediation of environmentally hazardous contaminants from aqueous solutions
PublicationPersistent contaminants in wastewater effluent pose a significant threat to aquatic life and are one of the most significant environmental concerns of our time. Although there are a variety of traditional methods available in wastewater treatment, including adsorption, coagulation, flocculation, ion exchange, membrane filtration, co-precipitation and solvent extraction, none of these have been found to be significantly cost-effective...
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Curing epoxy with ethylenediaminetetraacetic acid (EDTA) surface-functionalized Co Fe3-O4 magnetic nanoparticles
PublicationIn this work, the bulk and surface composition of Fe3O4 supermagnetic nanoparticles were modified for efficient epoxy curing. The bare, ethylenediaminetetraacetic acid (EDTA) capped, and cobalt (Co)-doped EDTA capped Fe3O4 nanoparticles were synthesized electrochemically. The crystalline structure and phase information, surface capping, morphology and magnetization behavior of nanoparticles were studied by X-Ray diffraction (XRD),...
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Magnetic properties of Co/Pd multilayered films on porous Al2O3 templates with developed cell substructure
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Structural and Magnetic Properties of Co‒Mn Codoped ZnO Nanoparticles Obtained by Microwave Solvothermal Synthesis
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Evaluation of the impact of geometry and plastic deformation on the stray magnetic field around the bone shaped sample
PublicationInfluence of two factors: the variable cross-section and the localized plastic deformation, which affect the stray magnetic field profile of a ferromagnetic sample have been studied. Evaluation of an effect size is based on the analysis of the stray magnetic field component which is tangential to the longest dimension of a sample. However, in order to describe the nature of the stray magnetic field, the normal component (perpendicular...
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Recent advances on magnetic carbon-related materials in advanced oxidation processes of emerging pollutants degradation
PublicationRecently, carbon-related materials have been proposed to improve the charge separation of the photogenerated carriers in the semiconductor matrices’ and surface properties. Carbon-related materials may act as co-catalysts, enhancing the pollutants adsorption on the surface, improving the charge carriers separation and photocatalyst stability and providing more active centres for photocatalytic reactions. This review summarizes...
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Minimization of a ship's magnetic signature under external field conditions using a multi-dipole model
PublicationThe paper addresses the innovative issue of minimizing the ship's magnetic signature under any external field conditions, i.e., for arbitrary values of ambient field modulus and magnetic inclination. Varying values of the external field, depending on the current geographical location, affect only the induced part of ship's magnetization. A practical problem in minimizing the ship signature is separating permanent magnetization...
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coincidence investigation of inelastic electron-atom collisions with magnetic selection of scattering angle - feasibility study
PublicationOpisana została nowa aparatura do badania zderzeń elektronów z atomami metodą koincydencji z wykorzystaniem techniki lokalnego pola magnetycznego. Połączenie obu metod umożliwia wyznaczenie parametrów koincydencji w pełnym kącie rozproszenia. W pracy zaprezentowano pierwsze widma energii straconej oraz widma koincydencji.
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Magnetic Field Influence on the Superconducting Transition in Granular (BiPb)-Sr-Ca-Cu-O Superconductors
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Microscopic impact of creep damage incipience and development on the magnetic properties of ferromagnetic Cr-Mo steel
PublicationPokazano wyniki badań emisji magneto-akustycznej (EMA0 oraz magnetostrykcji dla stali P22 w stanie dostawy i po ekploatacji. Wyniki te pokazują, że maksimum EMA jest skorelowane z maksimum pochodnej magnetostrykcji. Badania morfologii wydzieleń w granicach ziarn i w ich wnętrzu potwierdzają tezę, iż te pierwsze są główną przyczyną zmniejszania natężenia EMA. Zaproponowano prosty model tłumaczący ilościowo funkcję zmian natężenia...
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Sulfonated carbon-encapsulated iron nanoparticles as an efficient magnetic nanocatalyst for highly selective synthesis of benzimidazoles
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Rotating Magnetic Field-Assisted Reactor Enhances Mechanisms of Phage Adsorption on Bacterial Cell Surface
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Effect of Presowing Magnetic Field Stimulation on the Seed Germination and Growth of Phaseolus vulgaris L. Plants
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Biochemical and cellular properties of Gluconacetobacter xylinus cultures exposed to different modes of rotating magnetic field
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Removal of Ni2+ from Aqueous Solutions by Adsorption Onto Magnetic Multiwalled Carbon Nanotube Nanocomposite
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Multi-functional sensor based on photonic crystal fiber using plasmonic material and magnetic fluid
PublicationA unique highly sensitive photonic crystal fiber is investigated based on plasmonic material and magnetic fluid (MF) for the simultaneous measurement of temperature and magnetic field sensor. The designed sensor is explored by tracing the different parameters such as birefringence, coupling length, power spectrum, and the peak wavelength of the transmission intensity. The magnetic field and temperature computation are attained...
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Synthesis of CoFe2O4 Nanoparticles: The Effect of Ionic Strength, Concentration, and Precursor Type on Morphology and Magnetic Properties
PublicationThe present study highlights the effect of metal precursor types (SO4 2¯, Cl¯, and NO3¯), their concentration, and the influence of ionic strength of reaction environment on the morphology, surface, and magnetic properties of CoFe2O4 particles. The magnetic nanoparticles were obtained by chemical coprecipitation in alkaline medium at increasing metal concentration in the range of 0.0425 mol·dm-3 to 0.17 mol·dm-3 and calcination...
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Charge distribution and magnetic interactions in PrBa2Cu3O7 with substitutional defects and oxygen disorder: the ab initio approach
PublicationW artykule zaprezentowano rezultaty kwantowomechanicznych obliczeń ''ab initio: struktury elektronowej układu PrBa2Cu3O7 zawierającego defekty substytucyjne (Pr_Ba) w podsieci barowo-tlenowej oraz wykazującego zaburzoną stechiometrię tlenową (O5). Badane defekty są odpowiedzialne za redystrybucję ładunku w układzie. Defekty Pr_Ba generują silnie zlokalizowane momenty magnetyczne, które oddziałują głównie na płaszczyzny miedziowo-tlenowe.
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Evaluation of time and space distribution of magnetic flux density in a steel plate magnetized by a C-core
PublicationBadano wpływ częstości magnesowania płyty stalowej na rozkład przestrzenny indukcji magnetycznej wewnątrz tej płyty. Rozkład ten oceniano na podstawie pomiaru natężenia emisji magnetoakustycznej a także rozkładu na powierzchni płyty natężenia efektu Barkhausena. Wyniki dyskutowane są ilościowo i porównane z wynikami modelowania metodą elementów skończonych, w której uwzględniono efekt powstawania prądów wirowych.
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Synthesis, characterization and application of cross-linked functional terpolymer through epoxy group as sorbent for extraction of cadmium from waters and foods: Multivariate optimization
PublicationThe purpose of this study was to develop a selective sorbent for cadmium ions (Cd(II)) enrichment in orbital shaker assisted solid phase microextraction (OS-SPME) from different aqueous and food samples. A maleic anhydride-styrene-glycidyl methacrylate (MA-St-GMA) terpolymer was synthesized and characterized in detail. Experimental variables of sample preparation step were optimized using a central composite design (CCD). The final...
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Study on effectiveness of PVC/β-diketone sorbent in removing residue of Zn(II), Cr(III) and Ni(II) from post-galvanic wastewater
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Membrane in tandem with a helical sorbent trap as continuous sampling technique of the polyvinyl chloride thermo-oxidative degradation products for their on-line gas chromatographic monitoring
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Improved finite element method for flow, heat and solute transport of Prandtl liquid via heated plate
PublicationIn the current study, a vertical, 3D-heated plate is used to replicate the generation of heat energy and concentration into Prandtl liquid. We discuss how Dufour and Soret theories relate to the equations for concentration and energy. In order to see how efectively particles, interact with heat and a solvent, hybrid nanoparticles are used. It does away with the phenomena of viscous dissipation and changing magnetic felds. The motivation...
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Controlling the size and morphology of precipitated calcite particles by the selection of solvent composition
PublicationCalcium carbonate particles were obtained in the reaction of calcium hydroxide with carbon dioxide at 65°C. Initial Ca(OH)2 suspensions were prepared in pure water and aqueous solutions of ethylene glycol or glycerol of the concentration range up to 20% (vol.). The course of reaction was monitored by conductivity measurements. Precipitated solids were analyzed by FTIR, XRD, SEM and the particles size distribution was determined...
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Influence of surfactants on interaction forces between polyethylene surfaces in a hydrocarbon solvent.
PublicationPrzeprowadzono bezpośrednie pomiary oddziaływań międzyfazowych pomiędzy cząstkami polietylenowymi w środowisku n-tetradekanu z dodatkiem surfaktantów(kwasu larynowego i dodecyloaminy). Dodatek surfaktantów wpłynął na wzrost oddziaływań odpychających pomiędzy powierzchniami polietylenowymi, szczególnie w przypadku dodecyloaminy. Zaobserwowano obecność wzrostu sferycznych sił odpychających ze wzrostem temperatury.
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Extraction of acidic herbicides from soil by means of accelerated solvent extraction.
PublicationZaprezentowano opracowanie procedury izolacji herbicydów kwasowych z gleby z zastosowaniem urządzenia DIONEX ASE 200. Celem było zoptymalizowanie warunków pracy urządzenia: czasu, temperatury, ciśnienia oraz ilości cykli ekstrakcji. Ostatecznie ekstrakty, po przeprowadzeniu analitów w pochodne metylowe, poddano analizie chromatograficznej (GC).
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Solvent residue determination in Uncaria Tomentosa Bark by HS-GC technique
PublicationPrzedstawiono wyniki oznaczeń pozostałości rozpuszczalników organicznych w preparacie uzyskanym z kory liany U. Tomentosa, wykorzystywanej do produkcji farmaceutyków i dodatków do żywności. 1,1,2-trichloroeten oraz dichlorometan są powszechnie stosowane do usunięcia z kory kilku grup alkaloidów o znanych właściwościach biologicznych, co umożliwia zbadanie pozostałych jej związków. Ilościowe oznaczanie tych rozpuszcalników jest...
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Combined pH/organic solvent gradient HPLC in analysis of forensic material
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Accelerated solvent extraction-gas chromatographic determination of acidic herbicides in soil
PublicationPrzyspieszona ekstrakcja rozpuszczalnikiem z wykorzystaniem wody jako ekstraktanta okazała się skutecznym sposobem izolacji herbicydów kwasowych (MCPP, MCPA, 2,4-D, 2,4,5-T, PCP, dinoseb, dinoterb) z próbek gleby. Wysoka zawartość substancji iłowych powodowała problemy techniczne, które udało się pokonać poprzez zwiększenie stosunku piasku do gleby w celce ekstrakcyjnej. Anality przenoszono z ekstraktu wodnego do rozpuszczalnika...
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Minimal parameter implicit solvent model for ab initioelectronic-structure calculations
PublicationAbstract - We present an implicit solvent model for ab initio electronic-structure calculations which is fully self-consistent and is based on direct solution of the nonhomogeneous Poisson equation. The solute cavity is naturally defined in terms of an isosurface of the electronic density according to the formula of Fattebert and Gygi (J. Comput. Chem., 23 (2002) 662). While this model depends on only two parameters, we demonstrate...
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Solvent extraction of copper ions by 3-substituted derivatives of β-diketones
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Predicting sulfanilamide solubility in the binary mixtures using a reference solvent approach
PublicationBackground. Solubility is a fundamental physicochemical property of active pharmaceutical ingredients. The optimization of a dissolution medium aims not only to increase solubility and other aspects are to be included such as environmental impact, toxicity degree, availability, and costs. Obtaining comprehensive...
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Application of Carbonized Metal–Organic Framework as Efficient Adsorbent of Cationic Dye
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Chemical analysis of low carbon content coals and their applications as dye adsorbent
PublicationCoal is primarily a fuel material but lately it has been utilized as an adsorbent for removing toxic metal ions. However, its usage for removing organic pollutants is not well studied. We report here a systematic study on the use of coal samples of varying carbon contents as adsorbents for removing Basic Blue 41 as a model cationic dye. The coal samples were collected from coal mines and were thoroughly characterized. The concentrations...
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Development of thin film SPME sorbents based on deep eutectic solvents and their application for isolation and preconcentration of endocrine-disrupting compounds leaching from diapers to urine
PublicationIn this study, the thin film solid phase microextraction (TF-SPME) based on a novel sorbent composed of deep eutectic solvent (DES) is proposed. Among several synthesized sorbents the most efficient was DES containing trihexyl(tetradecyl)phosphonium chloride and docosanol mixed with polydimethylsiloxane (PDMS) in a molar ratio 1:3:0.25 to achieve a more stable structure. The proposed sorbent was applied on a fiberglass mesh and...
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Testing of the Superconducting Magnets Frequency Characteristics
PublicationPrzedstawiono zagadnienia związane z opracowaniem systemu do wyznaczania impedancji uzwojeń magnesów nadprzewodzących w funkcji częstotliwości. Omówiono strukturę sprzętową systemu, oprogramowanie oraz sposób wyznaczania parametrów badanego uzwojenia. Pokazano przykładowe wyniki uzyskane przy użyciu omawianego systemu w GSI w Darmstadt.
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Ferro- and antiferro-magnetism in (Np, Pu)BC
PublicationTwo new transuranium metal boron carbides, NpBC and PuBC, have been synthesized. Rietveld refinements of powder XRD patterns of {Np,Pu} BC confirmed in both cases isotypism with the structure type of UBC. Temperature dependent magnetic susceptibility data reveal antiferromagnetic ordering for PuBC below T-N = 44 K, whereas ferromagnetic ordering was found for NpBC below T-C = 61 K. Heat capacity measurements prove the bulk character...
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Preparation and characterization of dummy-template molecularly imprinted polymers as potential sorbents for the recognition of selected polybrominated diphenyl ethers
PublicationThe main aim of this work was to conduct the preliminary/basic research concerning the preparation process of a new dummy molecularly imprinted polymer (DMIP) materials. Developed DMIPs were proposed as a sorption material in solid-phase extraction (SPE) technique for recognition of selected low mass polybrominated diphenyl ethers (PBDEs) e PBDE-47 and PBDE-99. Four new DMIPs were synthesized employing bulky polymerization technique...
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Natural/bio-based sorbents as greener extractive materials for endocrine disrupting compounds in samples of different matrix composition
PublicationEndocrine-disrupting compounds (EDCs) are a group of chemicals that interfere with the endocrine system, leading to adverse effects on human health and the environment. Increasing concerns over the EDCs presence in various environmental compartments has driven the search for greener extraction materials. Recently, the use of polymers of natural origin (biopolymers) has been demonstrated to be an effective and promising research...
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MAGNETIC RESONANCE MATERIALS IN PHYSICS BIOLOGY AND MEDICINE
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In-situ synthesis and characterization of biocompatible magnetic ginger nanofiber composites for copper (II) removal from water
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Modular power converter with superconducting magnetic energy storage for electric power distribution system — Analysis and simulation
PublicationThis paper describes selected issues concerning realization of energy storage system (ESS) designed to operate in power distribution system. This paper presents a modular approach of 300 kVA power converter operating with superconducting magnetic energy storage (SMES), which gives high dynamics together with high power and suitable capability for instantaneous energy storage. Analysis and simulation studies of selected power converter...
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Magnetic and capacitive couplings influence on power losses in double circuit high voltage overhead transmission line
PublicationPurpose – The paper aims to discuss problems of power and energy losses in a double-circuit overhead transmission line. It was observed from energymeters’ readings, that in such a line, active power losses can be measured as “negative”. The “negative” active power losses appear when the active power injected to the circuit is lower than the active power received at the circuit end. The purpose of this paper is to explain this phenomenon. Theoretical...
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Evolution of magnetic and transport properties in (Cr1−xMnx)2AlC MAX-phase synthesized by arc melting technique
PublicationHerein we initiate a comeback to the arc melting technique to produce MAX-phase solid solutions. Bulk samples of (Cr1−xMnx)2AlC MAX-phase with X = 0, 0.025, 0.05 and 0.1 were synthesized and studied by means of X-ray diffractometry, scanning electron microscopy in combination with energy-dispersive X-ray spectroscopy. Samples were established to be homogeneous with an incorporation of Cr7C3, AlCr2 and Al2O3 secondary phases which...
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STRUCTURE AND MAGNETIC PROPERTIES OF Bi5Ti3FeO15 CERAMICS PREPARED BY SINTERING, MECHANICAL ACTIVATION AND EDAMM PROCESS. A COMPARATIVE STUDY
PublicationThree different methods were used to obtain Bi5Ti3FeO15 ceramics, i.e. solid-state sintering, mechanical activation (MA) with subsequent thermal treatment, and electrical discharge assisted mechanical milling (EDAMM). The structure and magnetic properties of produced Bi5Ti3FeO15 samples were characterized using X-ray diffraction and Mössbauer spectroscopy. The purest Bi5Ti3FeO15 ceramics was obtained by standard solid-state sintering...
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The Magnetic Fluid Seals Research Results vs. Kelvin-Helmholtz (K-H) instability and Preliminary Conclusions
PublicationIn the article a magnetic-fluid seals durability research and the tests results are presented. The tests were made with three magnetic fluids using various magnets quantity in magnetic assemblies. If values obtained in the repeated test deviated by more than 10 % from results of the first test an additional control test was made for final characteristics. The characteristics are: critical pressure, critical motion velocity and...