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Wyniki wyszukiwania dla: FTIR spectrum of CO2
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Spectroscopic and cytotoxic characteristics of (p-cymene)Ru(II) complexes with bidentate coumarins and density functional theory comparison with selected Pd(II) complexes
PublikacjaThis paper presents the synthesis of two new (p-cymene)-ruthenium(II) complexes with the bidentate coumarin ligands. Both complexes were characterized by FTIR spectroscopy, 1H NMR, 13C NMR, MS, elemental analysis and DFT calculations. The X-ray structure of complex 3a was also solved. The cytotoxic properties of both complexes were examined on human leukemia NALM-6 and HL-60 cells and melanoma WM-115 cells. The complexes possess...
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WPŁYW METODY SYNTEZY NA WŁAŚCIWOŚCI STRUKTURALNE I KATALITYCZNE ZWIĄZKU Ce0.9Pr0.1O2-δ PODCZAS WYSOKOTEMPERATUROWEJ PRACY W BIOGAZIE
PublikacjaTlenkowe ogniwa paliwowe zasilane biogazem degradują się pod wpływem węgla osadzającego się na anodzie. Aby wyeliminować ten efekt, szuka się warstw katalitycznych, które nałożone na anodę powstrzymują osadzanie się węgla i zmniejszają straty wydajności ogniwa. Związkiem użytym w tym celu jest Ce0,9Pr0,1O2-δ wytworzony dwiema metodami: Pechiniego i metodą strącania z odwróconej emulsji. Aby zbadać wpływ metody syntezy na właściwości...
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Functionalization of graphene oxide coatings with phosphorus atoms and their corrosion resistance in sodium chloride environment
PublikacjaIn this work, we compared corrosion resistance of graphene oxide, and phosphorus functionalized reduced graphene oxide coatings obtained as a result of electrophoretic deposition on the copper substrate. Doping graphene oxide with phosphorus atoms was performed by a hydrothermal method in the presence of different amounts of phosphoric acid. Structural studies confirmed the insertion of phosphorus atoms into the graphene oxide...
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FUNKCJONALIZOWANE ADSORBENTY WĘGLOWE DO EFEKTYWNEGO USUWANIA JONÓW METALI Z WODY
PublikacjaW niniejszej pracy zbadano skuteczność adsorpcyjnego usuwania jonów Hg2+, Sr2+ z roztworów wodnych, z wykorzystaniem funkcjonalizowanych materiałów węglowych. Jako adsorbenty zastosowano nanorurki węglowe, tlenek grafenu oraz węgiel aktywny. Oprócz często stosowanej praktyki jaką jest wykorzystanie materiałów węglowych które na swojej powierzchni zawierają tlenowe grupy funkcyjne, zaproponowano aby na powierzchnię materiałów węglowych...
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Electrochemical behavior of a composite material containing 3D-structured diatom biosilica
Publikacja3D-structured diatom biosilica mixed with conducting carbon black was investigated as an active electrode material for lithium-ion batteries. Diatom biosilica was obtained by cultivation of the selected diatom species under laboratory conditions. Several instrumental techniques (XRD, FTIR, Raman, SEM-EDX, TGA) were used to characterize the physicochemical properties of applied biosilica. It was evidenced that the prepared new composite...
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Determination of phenylbutazone, sulfamethazine, carbendazim and linuron using a novel pine bark biosorbent for solid-phase extraction (SPE) with high-performance liquid chromatography (HPLC)
PublikacjaThe paper presents a novel pine bark based biosorbent for solid-phase extraction (SPE). The morphology and composition of the pine bark were characterized using Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM). The biosorbent was used for the preparation of wastewater for the determination of phenylbutazone, sulfamethazine, carbendazim, and linuron by high performance liquid chromatography with...
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Distance measurement by the low coherent interferometer
Dane BadawczeThe obtained data was acquired by the interferometric fiber-optic sensor of distance. The setup was constructed of a broadband light source working at the central wavelength of 1560 nm, an optical spectrum analyzer and a fiber-optic 2x1 coupler (with the power split 50:50). All elements were connected by standard single-mode optical fibers. The measurement...
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Simulation of perovskite-based CuI/CH3NH3PbI3/TiO2 solar cell performance
Dane BadawczeThe presented data set is part of the theoretical research on novel thin-layer lead-halide perovskite solar cells with different inorganic transparent conductive oxides used as charge transport layers. In this study CuI/CH3NH3PbI3/TiO2 model structure (Model 1) was investigated by the use of the SCAPS-1D simulation method (https://scaps.elis.ugent.be/).
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Simulation of perovskite-based CuI/CH3NH3PbI3/SnO2 solar cell performance
Dane BadawczeThe presented data set is part of the theoretical research on novel thin-layer lead-halide perovskite solar cells with different inorganic transparent conductive oxides used as charge transport layers. In this study CuI/CH3NH3PbI3/SnO2 model structure (Model 2) was investigated by the use of the SCAPS-1D simulation method (https://scaps.elis.ugent.be/).
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Simulation of perovskite-based CuI/CH3NH3PbI3/ZnO solar cell performance
Dane BadawczeThe presented data set is part of the theoretical research on novel thin-layer lead-halide perovskite solar cells with different inorganic transparent conductive oxides used as charge transport layers. In this study CuI/CH3NH3PbI3/ZnO model structure (Model 3) was investigated by the use of the SCAPS-1D simulation method (https://scaps.elis.ugent.be/).
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Quantum origins of objectivity
PublikacjaIn spite of all of its successes, quantum mechanics leaves us with a central problem: How does nature create a bridge from fragile quanta to the objective world of everyday experience? Here we find that a basic structure within quantum mechanics that leads to the perceived objectivity is a so-called spectrum broadcast structure. We uncover this based on minimal assumptions, without referring to any dynamical details or a concrete...
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Comparison of three methods of EPR retrospective dosimetry in watch glass
PublikacjaIn this article we present results of our follow-up studies of samples of watch glass obtained and examined within a framework of international intercomparison dosimetry project RENEB ILC 2021. We present three methods of dose reconstruction based on EPR measurements of these samples: calibration method (CM), added dose method (ADM) and added dose&heating method (ADHM). The study showed that the three methods of dose reconstruction...
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Computer-Aided Automated Greenery Design—Towards a Green BIM
PublikacjaContemporary climate challenges are changing the architect’s awareness, which results in a broader spectrum of interest. The available software enables the design of vegetation, but it is often very limited and requires specialist knowledge. The available software allows the creation of individual solutions based on visual algorithms or writing scripts; however, they are still not common methods used in architecture and urban planning....
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Współczynniki podziału lotnych związków organicznych w amoniowych cieczach jonowych
PublikacjaZastosowanie cieczy jonowych jako absorbentów dla lotnych związków organicznych staje się w ostatnich latach obiecującą alternatywą dla tradycyjnych rozpuszczalników stosowanych w tych procesach. W porównaniu z konwencjonalnymi rozpuszczalnikami, ciecze jonowe wykazują szereg zalet, jak rozpuszczają szerokie spectrum związków, posiadają znikomą prężności par, są stabilne termicznie a także istnieje możliwość poprawy ich zdolności...
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The control software of the portable raman spectrometer
PublikacjaThe paper contains a description of the control software of a portable Raman spectrometer which was built in the Department of Optoelectronics and Electronic Systems Faculty of Electronics, Telecommunications and Informatics Gdansk University of Technology. The software has modular structure, which includes the laser control module and the spectrum acquisition module (laser power selection, working mode and data acquisition time)...
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Objectivity in a Noisy Photonic Environment through Quantum State Information Broadcasting
PublikacjaRecently, the emergence of classical objectivity as a property of a quantum state has been explicitly derived for a small object embedded in a photonic environment in terms of a spectrum broadcast form—a specific classically correlated state, redundantly encoding information about the preferred states of the object in the environment. However, the environment was in a pure state and the fundamental problem was how generic and robust...
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Source-related Wavefields in Fluids and Dielectrics: A new way of Thinking about Medium Dynamics
PublikacjaAcoustic and electromagnetic wave phenomena may seem to have a proper formal representation in field theory dating from the 19th century, founded on the mathematics of complex functions. This paper shows, however, that when replacing the classical spectrum-domain approach related to the assumption of harmonic timeform of signals, with a time-domain approach imposingnorestrictionastotheclassoftimeevolutionofsourceandfieldsignals,...
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Analysis of 2D Feature Spaces for Deep Learning-based Speech Recognition
Publikacjaconvolutional neural network (CNN) which is a class of deep, feed-forward artificial neural network. We decided to analyze audio signal feature maps, namely spectrograms, linear and Mel-scale cepstrograms, and chromagrams. The choice was made upon the fact that CNN performs well in 2D data-oriented processing contexts. Feature maps were employed in the Lithuanian word recognition task. The spectral analysis led to the highest word...
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Daytime Acute Non-Visual Alerting Response in Brain Activity Occurs as a Result of Short- and Long-Wavelengths of Light
PublikacjaVery recent preliminary findings concerning the alerting capacities of light stimulus with long-wavelengths suggest the existence of neural pathways other than melatonin suppression that trigger the nonvisual response. Though the nonvisual effects of light during the daytime have not been investigated thoroughly, they are definitely worth investigating. The purpose of the present study is to enrich existing evidence by describing...
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Poszukiwanie sankcji optymalnej w perspektywie projektu ustawy z dnia 7 lipca 2022 r. o zmianie ustawy Kodeks karny oraz niektórych innych ustaw. The search for the optimal sanction in the perspective of the draft act of 7 July 2022 amending the Penal Code and some other acts.
PublikacjaPolski ustawodawca opublikował w połowie września 2021 r. na stronie Rządowego Centrum Legislacji projekt gruntownej zmiany – między innymi – Kodeksu karnego. W dniu 7 lipca 2022 r. Sejm RP przyjął ww. projekt ustawy (druk sejmowy nr 2024). W zasadniczym stopniu nowelizacja - między innymi - zwiększa wysokość kar grożących za poszczególne przestępstwa. Ustawodawca – poprzez zabiegi legislacyjne –...
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Human-associated bacteria and their mobile genetic elements - important minority in wastewater and wastewater impacted ecosystems
PublikacjaSince human-associated bacteria have been recognized as vectors in two - way gene transmission between the pathogenic and environmental populations, health hazard connected with wastewater discharge requires reevaluation. In this paper the particular attention was given to antimicrobial-resistance of Escherichia coli and enterococci isolated from wastewater and wastewater impacted environments. The obtained results showed that...
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Mono- and bimetallic (Pt/Cu) titanium(IV) oxide core–shell photocatalysts with UV/Vis light activity and magnetic separability
PublikacjaTitanium(IV) oxide is one of the most widely investigated photocatalysts. However, separation of nano-sized particulate titania might result in profitless technologies for commercial applications. Additionally, bare titania is almost inactive under the Vis range of solar spectrum due to its wide bandgap. Therefore, the present study aims to prepare novel coreinterlayer- shell TiO2 magnetic photocatalysts modified with metal nanoparticles...
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Kinetics of Cross-Linking Reaction of Epoxy Resin with Hydroxyapatite-Functionalized Layered Double Hydroxides
PublikacjaThe cure kinetics analysis of thermoset polymer composites gives useful information about their properties. In this work, two types of layered double hydroxide (LDH) consisting of Mg2+ and Zn2+ as divalent metal ions and CO32− as an anion intercalating agent were synthesized and functionalized with hydroxyapatite (HA) to make a potential thermal resistant nanocomposite. The curing potential of the synthesized nanoplatelets in the...
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Spectroscopic studies of Nb-doped tricalcium phosphate glass-ceramics prepared by sol-gel method
PublikacjaCalcium-phosphate based glasses and glass-ceramics play a crucial role in the tissue engineering development. Apart from their high biocompatibility and excellent ability to undergo varying degrees of resorbability1, they exhibit relatively high bioactivity and due to that they are commonly used as bone and dental implants. A substantial research effort is devoted to improve calcium-phosphate materials physico-chemical properties...
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Structural, magnetic and spectral properties of tetrahedral cobalt(II) silanethiolates: a variety of structures and manifestation of field-induced slow magnetic relaxation
PublikacjaBlue crystals of five heteroleptic cobalt(II) silanethiolates 1–5 have been obtained by the reaction of [Co{SSi (tBuO)3}2(NH3)]2 with aminopyridines and aminomethylpyridines at an appropriate molar ratio and their structural, spectral, thermal and magnetic properties have been established and described. All complexes 1–5 contain Co(II) ions in a tetrahedral CoN2S2 environment formed by (tBuO)3SiS− residues and pyridines and present...
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Bacteriophages as Factories for Eu2O3 Nanoparticle Synthesis
PublikacjaThe use of phage display to identify peptides with an ability to bind and synthesize Eu2O3 nanoparticles is demonstrated in this report. This is the first report of modified phages specifically binding a lanthanide. The peptides exposed on virions revealed very strong binding to Eu2O3 nanoparticles and the ability to catalyze Eu2O3 nanoparticles’ formation from Eu(OH)3 and Eu(NO3)3 solutions. The luminescence emission spectrum...
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Fiber optic displacement sensor with signal analysis in spectral domain
PublikacjaIn this paper, a study of a low-coherence fiber optic displacement sensor is presented. The sensor consisted of a broadband source whose central wavelength was either at 1310 nm or 1550 nm, a sensing Fabry-Pérot interferometer operating in reflective mode and an optical spectrum analyzer acting as the detection setup. All these components were connected by a single-mode fiber coupler. Metrological parameters of the sensor were...
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Response of a fiber-optic Fabry-Pérot interferometer to refractive index and absorption changes – modelling and experiments
PublikacjaThis paper describes how the refractive index and the absorption of investigated substances change the spectrum of the optical radiation at the output of the fiber-optic Fabry-Pérot interferometer. The modeling of the operation of the interferometer takes into account not only the spectra of the refractive index and the absorption of the medium that is inside the cavity, but also spectra of the refractive indices of the core and...
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Applications for investigating therapy progress of autistic children
PublikacjaThe paper regards supporting behavioral therapy of autistic children with mobile applications, specifically applied for measuring the child’s progress. A family of five applications is presented, that was developed as an investigation tool within the project aimed at automation of therapy progress monitoring. The applications were already tested with children with autism spectrum disorder. Hereby we analyse children’ experience...
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Does the low optical band gap of yellow Bi3YO6 guarantee the photocatalytical activity under visible light illumination?
PublikacjaBi3YO6, which is known as an ionic conductor, was tested here as an electrode and photoanode in contact with aqueous electrolytes. Bi3YO6 was deposited onto the Pt substrate and the such prepared electrode was polarized in various aqueous electrolytes. The optical energy band gap of the material equal to 1.89 eV was determined using the Kubelka-Munk function resulting from the UV-Vis spectrum (allowed indirect transition) and also...
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Miniaturization-Oriented Design of Spline-Parameterized UWB Antenna for In-Door Positioning Applications
PublikacjaDesign of ultra-wideband antennas for in-door localization applications is a challenging task. It involves development of geometry that maintains appropriate balance between the size and performance. In this work, a topologically-flexible monopole has been generated using a stratified framework which embeds a gradient-based trust-region (TR) optimization algorithm in a meta-loop that gradually increases the structure dimensionality....
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The role of low-energy electrons in the charging process of LISA test masses
PublikacjaThe estimate of the total electron yield is fundamental for our understanding of the test-mass charging associated with cosmic rays in the Laser Interferometer Space Antenna (LISA) Pathfinder mission and in the forthcoming gravitational wave observatory LISA. To unveil the role of low energy electrons in this process owing to galactic and solar energetic particle events, in this work we study the interaction of keV and sub-keV...
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Greening procedures and analytical parameters. The polychlorinated naphthalenes analysis in complex matrices as proof of concept
PublikacjaDue to the complexity of analytical procedures employed for the determination of wide spectrum of persistent organic pollutants (POPs), it is important to consider the green character of the applied protocols and propose the greenest solutions. In this review, the green aspects of several analytical procedures used for the determination of polychlorinated naphthalenes (PCNs) (as a representatives of POPs) in different types of...
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Theological Intersections: Newman’s ‘Primacy of God’ in Modern Church Discourse
PublikacjaThis article critically examines the Catholic–Anglican theological dialogue, centering on John Henry Newman’s ‘Primacy of God’, Catholic synodality, and Anglican comprehensiveness. It illuminates the interconnectedness of these elements, revealing their potential to enhance ecumenical conversations. Newman’s concept of communal faith and divine primacy resonates across both traditions, advocating a transformative,...
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Resonant ultrasonic spectroscopy in high-voltage varistor spectroscopy
PublikacjaResonant spectroscopy is an effective non-destructive testing method focused on defects in tested objects. The testing procedure, based on the resonant pattern, allows rejection of the tested samples with defects which do not fit the pattern. A sweeping frequency method has been used to measure the spectrum of resonances in high-voltage varistors. As a result we can observe resonances that depend directly on inhomogeneity of the...
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Efficient signal processing in spectroscopic optical coherence tomography
PublikacjaSpectroscopic optical coherence tomography (SOCT) is an extension of a standard OCT technique, which allows to obtain depth-resolved, spectroscopic information on the examined sample. It can be used as a source of additional contrast in OCT images e.g. by encoding certain features of the light spectrum into the hue of the image pixels. However, SOCT require computation of time-frequency distributions of each OCT A-scan, what is...
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Determination of refractive index dispersion using fiber-optic low-coherence Fabry–Perot interferometer: implementation and validation
PublikacjaWe present the implementation and validation of low-coherence Fabry–Perot interferometer for refractive index dispersion measurements of liquids. A measurement system has been created with the use of four superluminescent diodes with different optical parameters, a fiber-optic coupler and an optical spectrum analyzer. The Fabry–Perot interferometer cavity has been formed by the fiber-optic end and mirror surfaces mounted on a micromechanical...
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Spectral measurement of birefringence using particle swarm optimization analysis
PublikacjaThe measurement of birefringence is useful for the examination of both technical and biological objects. One of the main problems is that the polarization state of light in birefringent media changes periodically. Without the knowledge of the period number, the birefringence of a given medium cannot be determined reliably. We propose to analyse the spectrum of light in order to determine the birefringence. We use a Particle Swarm...
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Novel Interpolation Method of Multi-DFT-Bins for Frequency Estimation of Signal with Parameter Step Change
PublikacjaThe IpDFT(Interpolation Discrete Fourier Trans-form) method is one of the most commonly used non-parametric methods. However, when a parameter (frequency, amplitude or phase) step changes in the DFT period, the DFT coefficients will be distorted seriously, resulting in the large estimation error of the IpDFT method. Hence, it is a key challenge to find an IpDFT method, which not only can eliminate the effect of the step-changed...
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Reexamination of the decoherence of spin registers
PublikacjaWe revisit the decoherence process of a multiqubit register interacting with a thermal bosonic bath. We generalize the previous studies by considering not only the register’s behavior but also a part of its environment. In particular, we are interested in information flow from the register to the environment, which we describe using recently introduced multipartite quantum state structures called spectrum broadcast structures....
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Review on Current Status of Echinocandins Use
PublikacjaFungal infections are rising all over the world every year. There are only five medical compound classes for treatment: triazoles, echinocandins, polyenes, flucytosine and allylamine. Currently, echinocandins are the most important compounds, because of their wide activity spectrum and much lower sides effects that may occur during therapy with other drugs. Echinocandins are secondary metabolites of fungi, which can inhibit the...
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VUV photofragmentation of the six-membered heterocyclic molecules containing oxygen
PublikacjaCancer is a significant public health concern worldwide, which results in millions of deaths each year. The standard cure routine for cancer is surgery, and nowadays, radiotherapy or a hadrontherapy. Depending on the type of cancer, patients may undergo additional treatment, including targeted therapy. A combination of radio- or hadron-therapy with proper drug treatment can inhibit the proliferation of cancer cells and thus can...
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Finite Element Approaches to Model Electromechanical, Periodic Beams
PublikacjaPeriodic structures have some interesting properties, of which the most evident is the presence of band gaps in their frequency spectra. Nowadays, modern technology allows to design dedicated structures of specific features. From the literature arises that it is possible to construct active periodic structures of desired dynamic properties. It can be considered that this may extend the scope of application of such structures. Therefore,...
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Novel 1,2,4-Oxadiazole Derivatives in Drug Discovery
PublikacjaAbstract: Five-membered 1,2,4-oxadiazole heterocyclic ring has received considerable attention because of its unique bioisosteric properties and an unusually wide spectrum of biological activities. Thus, it is a perfect framework for the novel drug development. After a century since the 1,2,4-oxadiazole have been discovered, the uncommon potential attracted medicinal chemists’ attention, leading to the discovery of a few presently...
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Cognitive Systems, Concepts, Processes, and Techniques for the Age of Industry 4.0
PublikacjaThe aim of this Guest Edition of Cybernetics and Systems is to present a wide-ranging scale of concepts and processes being currently researched, developed, and evaluated in real life settings in anticipation of incoming Industry 4.0 era. With the fourth industrial revolution expectation, the broad spectrum of cognitive approaches have emerged as an attempt to mimic and augment, in some way, human intelligence. Intelligence, in...
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Studies on the utilization of post-distillation liquid from Solvay process to carbon dioxide capture and storage
PublikacjaIn this work, a method of precipitated calcium carbonate production from the post-distillation liquid created in the Solvay process and waste carbon dioxide was proposed and investigated. Precipitation was carried out in a model solution of calcium chloride containing ammonia at various molar ratios in relation to Ca2+ ions, while gaseous carbon dioxide was supplied to the reactor as a pure gas or as a mixture with air. It was...
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Effect of Microplastics Pollution on Hydrogen Production from Biomass: A Comprehensive Review
PublikacjaHydrogen production from biomass and organic wastes is considered as a potential alternative energy source and is known as a clean and CO2-free fuel energy carrier. H2 is considered very promising among the other energy sources; therefore, the effective conversion of biomass and organic solid waste to this secondary energy source is urgently sought. As a result, it is of importance to assess the impact of the existence of microplastics...
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The optimization of CuxO microwires synthesis for improvement in photoelectrochemical performance
PublikacjaOne of the most important challenges in the fabrication of CuxO microstructures via the electrochemical method is formation of long, regular and well-packed microwires with good adhesion on the Cu substrate and to achieve better photoelectrochemical properties, which can be potentially applied in solar-driven water splitting and CO2 conversion to light hydrocarbons. In this paper, Cu2O photoelectrode has been fabricated by direct...
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Encapsulation of Cs3Bi2Br9 perovskite photocatalyst with polythiophene for prolonged activity in oxidizing and humid environment
PublikacjaDespite their growing popularity in modern technology, halide perovskites suffer from susceptibility to oxidation, limiting their applications. Our aim was to enhance Cs3Bi2Br9 perovskite's performance in humid environments through polythiophene encapsulation. This extended its lifespan while preserving photocatalytic abilities, as demonstrated in toluene decomposition experiments. We confirmed the stability of Cs3Bi2Br9 encapsulated...
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Fracture susceptibility of high RAP content asphalt concrete in terms of aging
PublikacjaDue to the reduction of CO2 emissions during the production of asphalt mixtures and the decrease in the demand for mineral resources, the addition of reclaimed asphalt pavement (RAP) is becoming indispensable. The durability of asphalt pavements containing a high RAP content may be reduced due to a decrease in the cracking resistance of the material, especially under the influence of operational aging. The article presents the...