Wyszukiwarka
Filtry
wszystkich: 28659
-
Katalog
wyświetlamy 1000 najlepszych wyników Pomoc
Wyniki wyszukiwania dla: SEMI-ANALYTICAL METHOD
-
Application of response surface methodology to optimize solid-phase microextraction procedure for chromatographic determination of aroma-active monoterpenes in berries
PublikacjaMost of scientific papers concern the qualitative or semi-quantitative analysis of aroma-active terpenes in liquid food matrices. Therefore, the procedure based on solid-phase microextraction and comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry for determination of monoterpenes in fresh berries was developed. The optimal extraction conditions using divinylbenzene-carboxen-polydimethylsiloxane fiber...
-
Application of Shape From Shading Technique for Side Scan Sonar Images
PublikacjaSide scan sonar (SSS) is one of the most widely used imaging systems in the underwater environment. It is relatively cheap and easy to deploy in comparison with more powerful sensors like multibeam echosounder or synthetic aperture sonar. Although, the SSS does not provide directly the seafloor bathymetry measurements. Its outputs are usually in a form of grey level acoustic images of seafloor. However, the analysis of such images...
-
Uniwersalna metoda projektowania regulacji osi toru z wykorzystaniem pomiarów satelitarnych i optymalizacji
PublikacjaW pracy zwrócono uwagę na ograniczenia stosowanej w naszym kraju metodyki regulacji osi toru związane w głównym stopniu z uzyskiwaną dokładnością określania istniejącego kształtu toru. Jako rozwiązanie alternatywne wskazano opracowaną przez interdyscyplinarny zespół naukowy Politechniki Gdańskiej i Akademii Marynarki Wojennej / Akademii Morskiej w Gdyni i stosowaną od 2009 roku nowatorską technikę mobilnych pomiarów satelitarnych....
-
Model energetyczny łożysk ślizgowych silników spalinowych o zapłonie samoczynnym w aspekcie diagnostyki. XXIV Międzynarodowe Sympozjum Siłowni Okrętowych.
PublikacjaPrzedstawiono zagadnienie tworzenia modelu energetycznego łożysk ślizgowych silników o zapłonie samoczynnym z uwzględnieniem diagnostyki. Wykazano przydatność procesu semi-markowskiego jako modelu zmian stanów technicznych łożysk ślizgowych.
-
Analytical eco-scale for assessing the greenness of analytical procedures
PublikacjaWe propose the analytical eco-scale as a novel comprehensive approach to evaluating the greenness of analytical methodology. It is based on assigning penalty points to parameters of an analytical process that are not in agreement with the ideal green analysis. This approach compares different parameters and different steps of the analytical process. Traditional green chemistry metrics 9e.g. Atom Economy, E-factor and Reaction Mass...
-
Kształtowanie toru zwrotnego rozjazdu z odcinkami krzywizny liniowej
PublikacjaW pracy została przedstawiona analityczna metoda kształtowania toru zwrotnego rozjazdu kolejowego posiadającego na swojej długości odcinki krzywizny liniowej. Odróżnia go to w istotny sposób od rozwiązania typowego, stanowiącego pojedynczy łuk kołowy bez krzywych przejściowych. W metodzie tej dokonano identyfikacji problemu rozkładu krzywizny za pomocą równań różniczkowych. Uzyskane rozwiązania mają charakter uniwersalny; m. in....
-
Synthesis, structure and properties of novel poly(hydroxyurethane)s obtained by non-isocyanate route
PublikacjaNon-isocyanate polyurethanes (NIPUs) can be synthesized by polyaddition of five-membered bis(cyclic carbonate)s and primary diamines. NIPUs are an alternative for the commonly used (in the form of foams, elastomers, coatings or fibers) in the industry polyurethanes obtained using toxic and moisture sensitive diisocyanates, polyols and low-molecular weight chain extenders. The main aim of this work was to synthesize non-isocyanate...
-
Dynamics of cutting power during sawing with circular saw blades as an effect of wood properties changes in the cross section
PublikacjaIn the paper the effect of the method calculation upon the cutting power is presented. In computations were used models in which fracture toughness was incorporated. The comparison concerned models as follows: FM-CM – classic model in which the sum of all uncut chip thicknesses of the simultaneously teeth engaged represented the mean uncut chip thickness, FM-FDM – full dynamical model in which besides variable uncut chip thickness...
-
Application of passive sampling techniques as a usable tool in the field of environmental quality monitoring
PublikacjaAnalysis of literature data published for the past 20 years leads to the conclusion, that passive sampling technique has been developing very quickly and is commonly used in the field of monitoring pollutants in air, water and soil environment. The popularity of application of passive sampling techniques in analytical and environmental chemistry results from its many advantages e.g.: Simplicity in use, low costs of exploitation,...
-
Energetyczny aspekt diagnostyki maszyn
PublikacjaW artykule przedstawiono interpretację wartościującą działania, które jest tu rozpatrywane jako wielkość fizyczna o jednostce miary, nazwanej dżulosekundą. Przedstawiono oryginalną metodę analizy i oceny działania maszyn w ujęciu energetycznym dla potrzeb diagnostycznych. Do uzasadnienia przydatności tak rozumianego działania zastosowano jednorodny proces Poissona i proces semi-Markowa. Procesy te umożliwiły skonstruowanie modelu...
-
MRI-Derived Subcutaneous and Visceral Adipose Tissue Reference Values for Children Aged 6 to Under 18 Years
PublikacjaThe assessment of body composition in pediatric population is essential for proper nutritional support during hospitalization. However, currently available methods have limitations. This study aims to propose a novel approach for nutrition status assessment and introduce magnetic resonance imaging (MRI)-derived subcutaneous and visceral fat normative reference values. A total of 262 healthy subjects aged from 6 to 18 years underwent...
-
Koncepcja i analiza sensora/aktuatora piezoelektrycznego do pomiaru procesu starzenia się ludzkiej skóry
PublikacjaNiniejszy artykuł przedstawia nową koncepcję piezoelektrycznego sensora/aktuatora przeznaczonego do pomiaru właściwości mechanicznych tkanek miękkich a w szczególności skóry ludzkiej. Wyjaśnione jest analityczne podejście z wykorzystaniem schematu zastępczego Mason’a określającego aktuator w stanie rezonansu oraz opis metody impedancji elektromechanicznej wykorzystanej w systemie pomiarowym. Analiza z użyciem metody elementów...
-
Jaroslaw Spychala dr
OsobyOprócz bardzo dobrego wykształcenia osoba posiada również wieloletnie doświadczenie zawodowe, które jest poświadczeniem tego, że potrafi wykorzystać swoją wiedzę teoretyczną w praktycznych działaniach. Doświadczenie zawodowe jest bardzo bogate i rozbudowane. Ze względu na nabyte całkiem nowe umiejętności zwiększa się atrakcyjność doświadczonego pracownika. Są to między innymi kreatywne myślenie, zorientowanie na cel, odporność...
-
Metodyka projektowania i eksploatacji dróg szynowych z wykorzystaniem mobilnych pomiarów satelitarnych
PublikacjaW pracy zostały przedstawione aplikacyjne możliwości metody mobilnych pomiarów satelitarnych w projektowaniu i eksploatacji dróg szynowych. Pokazano wizualizację położenia toru kolejowego, omówiono sposoby oceny odcinków prostych toru i odcinków położonych w łuku oraz tworzenie poligonu kierunków głównych trasy. Szczególną uwagę poświęcono opracowanej analitycznej metodzie projektowania, omawiając jej algorytmy obliczeniowe: projektowania...
-
Application of theory of semi-Markov processes to determining distribution of probabilistic process of marine accidents resulting from colission of ships
PublikacjaIn this paper is presented possible application of the theory of semi-Markov processes to elaborating an eight-state model of the process of occurrence of serviceability state and unserviceability states of sea-going ships making critical manoeuvres during their entering and leaving the ports. In the analysis it was taken into account that sea-going ships are in service for a very long time t (t → ∞). The model was elaborated to...
-
Metrics for green analytical chemistry
PublikacjaGreen analytical chemistry, although not being a new concept, does not have a greenness metrics system. Green chemistry metrics are not suitable for analytical procedure assessment because they often refer to the mass of the product. Some efforts have been made to develop suitable metrics for analytical chemistry. Some are simple to use but do not cover all aspects of analytical methods’ environmental impact. Others are more comprehensive...
-
Smart Innovation Engineering (SIE): Experience-Based Product Innovation System for Industry 4.0
PublikacjaThis paper presents a semi-automatic system capable of facilitating product innovation process. This system, known as Smart Innovation Engineering (SIE) system, helps in decision-making by using the explicit knowledge of formal decision events. The SIE system carries the promise to support the innovation processes of manufactured products in a quick and efficient way. It stores and reuses the past decisional events or sets of experiences...
-
A New Approach to Chemical Recycling of Polyamide 6.6 and Synthesis of Polyurethanes with Recovered Intermediates
PublikacjaA new efficient method for the chemical decomposition of polyamide 6.6 by the glycolysis and amino-glycolysis processes was proposed. The glycolysis was conducted using the mass excess of ethylene glycol (EG) as a decomposing agent in the presence of a catalyst. Also, a mixture of EG and triethylenetetramine was used as another decomposing agent in the amino- glycolysis process. The described process of decomposition did not...
-
Current issues of functional safety and cybersecurity analysis of the industrial and critical infrastructures
PublikacjaThis article addresses some functional safety assessment procedures with cybersecurity aspects in critical industrial installations with regard to the functional safety requirements specified in standards IEC 61508 and IEC 61511. The functional safety management includes hazard identification, risk analysis and assessment, specification of overall safety requirements and definition of safety functions. Based on the risk assessment...
-
“The Guardians of the Truth”: Journalists’ Resistance to the Algorithmization of Journalism
PublikacjaRegardless of the term used, be it “robot journalism,” “automated journalism,” “algorithmic journalism” or “machine-written journalism,” the process of automatic content creation and distribution is progressing in the newsrooms. Meanwhile, exercising control over the creation and distribution of news is considered a fundamental element of journalists’ professional identity. The article presents the results of research on the perception...
-
Green analytical chemistry introduction to chloropropanols determination at no economic and analytical performance costs?
PublikacjaIn this study we perform ranking of analytical procedures for 3-monochloropopane-1,2-diol determination in soy sauces with PROMETHEE method. Multicriteria decision analysis was performed for three different scenarios – metrological, economic and environmental, by application different weights to decision making criteria. All three scenarios indicate capillary electrophoresis – based procedure as the most preferable. Apart from...
-
Analytical chemistry with biosolvents
PublikacjaOne of the current trends in green analytical chemistry is the introduction of green solvents, some of which are biobased. At the same time, the development of the biorefinery concept has allowed more biochemicals to be obtained with increased efficiency and from a wider range of feedstocks. The first examples of the use of biosolvents in analytical applications included extractions performed with alcohols, esters, and terpenes....
-
Limiting distribution of the three-state semi-Markov model of technical state transitions of ship power plant machines and its applicability in operational decision-making.
PublikacjaThe article presents the three-state semi-Markov model of the process {W(t): t 0} of state transitions of a ship power plant machine, with the following interpretation of these states: s1 – state of full serviceability, s2 – state of partial serviceability, and s3 – state of unserviceability. These states are precisely defined for the ship main engine (ME). A hypothesis is proposed which explains the possibility of application...
-
Necessity for and possibility of application of the theory of semi-markov processes to determine reliability of diagnising systems
PublikacjaW opracowaniu uzasadniono konieczność określenia niezawodności systemów diagnozujących (SDG) do sformułowania diagnozy o stanie dowolnego urządzenia technicznego jako systemu diagnozowanego (SDN). Wykazano, że znajomość niezawodności SDG umożliwia określenie wiarygodności diagnozy. Przyjęto, że wiarygodność diagnozy może być określona jako właściwość diagnozy określająca stopień rozpoznania przez system diagnozujący (SDG) rzeczywistego...
-
Wielokryterialna analiza porównawcza lokalizacji źródeł wytwórczych energii elektrycznej
PublikacjaArtykuł przedstawia ranking lokalizacji czterech źródeł wytwórczych energii elektrycznej: biogazowni rolniczej, biogazowni utylizacyjnej oraz dwóch elektrowni fotowoltaicznych, wykonany przy użyciu połączonych metod Analitycznego Procesu Hierarchicznego (AHP) oraz taksonomii numerycznej. Omówiono zalety połączenia metod, przedstawiono przykład zastosowania oraz wskazano kryteria o największym i najmniejszym wpływie na realizację...
-
Developing a methodology for model tests of floating platforms in a towing tank of low depth
PublikacjaThe paper presents two ways to mooring model of semi-submersible platform for research in the small depth towing pool. The tested model was made in the likeness of 1:100 Thunder Horse platform moored in the Gulf of Mexico at a depth of 1,920 m. Its mooring system consisted of 16 semi-taut mooring lines (chain-wire-chain) spaced Star-shape and attached at the bottom to the suction piles. The tests were performed in the towing pool...
-
A Development of a Capacitive Voltage Divider for High Voltage Measurement as Part of a Combined Current and Voltage Sensor
PublikacjaThis article deals with the development of capacitive voltage divider for high voltage measurements and presents a method of analysis and optimization of its parameters. This divider is a part of a combined voltage and current sensor for measurements in high voltage power networks. The sensor allows continuous monitoring of the network distribution status and performs a quick diagnosis and location of possible network failures....
-
A new tool for the evaluation of the analytical procedure: Green Analytical Procedure Index
PublikacjaA new means for assessing analytical protocols relating to green analytical chemistry attributes has been developed. The new tool, called GAPI (Green Analytical Procedure Index), evaluates the green character of an entire analytical methodology, from sample collection to final determination, and was created using such tools as the National Environmental Methods Index (NEMI) or Analytical Eco-Scale to provide not only general but...
-
The Method of Selecting the Interval of Functional Tests Taking into Account Economic Aspects and Legal Requirements
PublikacjaThe article discusses the problem of choosing the optimal frequency of functional tests, taking into account the reliability and law requirements, but also the impact of business aspects in the company. The subject of functional test interval is well described for purposes of the process industry. Unfortunately, this is not the case for the machinery safety functions with low demand mode. This is followed by a presentation of the...
-
Procedure based proactive functional safety management for the risk mitigation of hazardous events in the oil port installations including insurance aspects
PublikacjaThis article addresses selected technical and organization aspects of risk mitigation in the oil port installations with regard to functional safety requirements specified in standards IEC 61508 and IEC 61511. The procedure for functional safety management includes the hazard identification, risk analysis and assessment, specification of overall safety requirements and definition of safety functions. Based on risk assessment results...
-
Usage of Memi-Markov Process in Operation Evaluation of Diesel Engine
PublikacjaIn paper, the proposition of quantitative evaluation of operation using semi-Markov processes theories has been presented. Basic assumptions, essential for creating mathematical model on example of diesel engine were shown. Special attention was given to practical aspects of using established mathematical model. Example of characteristic of analysed process - temporary distribution of probability was assigned.
-
Green analytical chemistry metrics: A review
PublikacjaGreen analytical chemistry encourages reducing the use of toxic chemicals/reagents, using energy-efficient equipment, and generating minimal waste. The recent trends in analytical method development focus on the miniaturization of the sample preparation devices, the development of solventless or solvent-minimized extraction techniques, and the utilization of less toxic solvents. The twelve principles of GAC serve as a basic guideline...
-
ANALYTICAL LETTERS
Czasopisma -
Food Analytical Methods
Czasopisma -
Connections between Mutually Unbiased Bases and Quantum Random Access Codes
PublikacjaWe present a new quantum communication complexity protocol, the promise--Quantum Random Access Code, which allows us to introduce a new measure of unbiasedness for bases of Hilbert spaces. The proposed measure possesses a clear operational meaning and can be used to investigate whether a specific number of mutually unbiased bases exist in a given dimension by employing Semi--Definite Programming techniques.
-
The 12 principles of green analytical chemistry and the SIGNIFICANCE mnemonic of green analytical practices
PublikacjaThe current rapid development of green analytical chemistry (GAC) requires clear, concise guidelines in the form of GAC principles that will be helpful in greening laboratory practices. The existing principles of green chemistry and green engineering need revision for their use in GAC because they do not fully meet the needs of analytical chemistry. In this article we propose a set of 12 principles consisting of known concepts...
-
Piotr Konieczka prof. dr hab. inż.
Osoby -
Optoelectronic properties of curved carbon systems
PublikacjaSystematic investigation of optoelectronic properties of curved carbon systems has been performed and the results have been compared with the representatives of flat carbon systems. Moreover, the application of third order dispersion corrected density functional tight binding method (with third order corrections of self-consistent charges) including Becke-Johnson dumping (DFTB3-D3(BJ)) has been validated in order to obtain reliable...
-
Energetuc aspect of diesel engine operotion
PublikacjaW artykule zaproponowano interpretację wartościującą działania, które (podobnie jak przedstawione mechanice klasycznej działania Hamiltona i Maupertiusa oraz działanie wynikające ze zmiany pędu ciała) jest rozpatrywane jako wielkość fizyczna o jednostce miary zwanej dżulosekundą [dżulsekunda]. Przedstawiono oryginalną metodę analizy i oceny działania silników o zapłonie samoczynnym w ujęciu energetycznym dla potrzeb eksploatacyjnych....
-
Developing Methodology for Model Tests of Floating Platforms in Low -Depth Towing Tank
PublikacjaThe paper presents two different methods of physical modeling of semi-submersible platform mooring system for research in low depth towing tank. The tested model was made in the scale of 1:100 resembling the "Thunder Horse" platform moored in the Gulf of Mexico at a depth of 1,920 m. Its mooring system consisted of 16 semi-taut mooring lines (chain-wire-chain) spaced starshape and attached at the bottom to suction piles. The tests...
-
Customizing nano-chitosan for sustainable drug delivery
PublikacjaChitosan is a natural polymer with acceptable biocompatibility, biodegradability, and mechanical stability; hence, it has been widely appraised for drug and gene delivery applications. However, there has been no comprehensive assessment to tailor-make chitosan cross-linkers of various types and functionalities as well as complex chitosan-based semi- and full-interpenetrating networks for drug delivery systems (DDSs). Herein, various...
-
An updated method identifying collision-prone locations for ships. A case study for oil tankers navigating in the Gulf of Finland
PublikacjaTo ensure the risk level associated with continuously increasing maritime traffic through particularly sensitive sea areas remains at acceptable level, a periodic risk assessment needs to be carried out by the relevant authorities. As a part of such assessment, allowing for proactive countermeasures to mitigate risk, the frequency of accidents is estimated along with the assessment of geographical locations where the accidents...
-
Analytical Chemistry_GT
Kursy Online -
AGREE—Analytical GREEnness Metric Approach and Software
PublikacjaGreen analytical chemistry focuses on making analytical procedures more environmentally benign and safer to humans. The amounts and toxicity of reagents, generated waste, energy requirements, the number of procedural steps, miniaturization, and automation are just a few of the multitude of criteria considered when assessing an analytical methodology’s greenness. The use of greenness assessment criteria requires dedicated tools. We...
-
Projektowanie układów geometrycznych toru z zastosowaniem optymalizacji wielokryterialnej
PublikacjaW pracy przedstawiono metodę projektowania odcinków trasy kolejowej położonych w łuku, dostosowaną do techniki mobilnych pomiarów satelitarnych. Rozwiązanie problemu projektowego wykorzystuje zapis matematyczny i polega na wyznaczeniu uniwersalnych równań opisujących całość układu geometrycznego. Odbywa się to sekwencyjnie, obejmując kolejne fragmenty tegoż układu. Procedura projektowania ma charakter uniwersalny, gdyż w ogólnym...
-
Sensitive Demonstration of the Twin-Core Couplers including Kerr Law Non-Linearity via Beta Derivative Evolution
PublikacjaTo obtain new solitary wave solutions for non-linear directional couplers using optical meta-materials, a new extended direct algebraic technique (EDAT) is used. This model investigates solitary wave propagation inside a fiber. As a result, twin couplers are the subject of this study. Kerr law is the sort of non-linearity addressed there. Because it offers solutions to problems with large tails or infinite fluctuations, the resulting...
-
A SHORT REVIEW OF BLOOD FLOW MODELLING METHODS: FROM MACRO- TO MICROSCALES
PublikacjaThe aim of this paper it to review various scale approaches to the blood flow modelling. Blood motion may be described by three types of mathematical models according to the observed scales or resolutions, namely microscopic, mesoscopic and macroscopic descriptions. The above approaches are discussed together with their advantages and disadvantages. Several results of mesoscopic simulations are presented with particular attention...
-
Finite Element Method
Kursy OnlineItem Name : Finite Element Method- Abaqus learning Field of study : Civil Engineering Faculty : Faculty of Civil and Environmental Engineering Education level : Second degree studies Form of studies : Full-time studies Year of studies : 1 Study semester : 2 Start of the semester : November 2021 Academic year of the course : 2021/2022 Form of classes : Lecture, Laboratory
-
Manufacture and research of TPS/PE biocomposites properties
PublikacjaIn this paper the process of native starch preparing for modification by extrusion and manufacture of biocomposites is presented. The first aim of this study was to determine the mixing and granulating condition of native starch to obtain granulated native starch. For mixing and granulation of native starch Intensive Mixer manufactured by Maschinenfabrik Gustav Eirich was used. Mixing and granulation in a single process is a new...
-
Low cost set-up for supercapacitors parameters evaluation
PublikacjaSupercapacitors are capable to store relatively high amount of energy comparing to its mass. Growing number of these devices applications requires development of new testing methods. Standard methods of evaluation of supercapacitor parameters, as cycling voltammetry, CV, galvanostatic cycling with potential limitation, GCPL, impedance measurements, require equipment of high cost...