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Wyniki wyszukiwania dla: scanning electrone microscope
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Analysis of Measurement Errors in Rail Vehicles’ Pantograph Inspection System
PublikacjaThe paper presents an approach to evaluation of height measurement errors in laser scanning inspection system. The system, consisting of a laser line generator and a specialized camera, is dedicated to diagnosing carbon contact strips of railway vehicles’ pantographs. While height measurement resolution is easily computable based on system parameters, determining the measurement error is troublesome due to numerous impacts. As...
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Remote sensing in laboratory diagnostics of reinforced concrete elements – current development and vision for the future
PublikacjaContinuous emergence of new concrete types and kinds of reinforcement, as well as technological solutions in the field of structural engineering have made great demand for diagnostic tests of reinforced concrete elements. New challenges and problems facing people require new more efficient tools for laboratory diagnostics than those commonly used. Remote sensing may be the answer to this demand. In this paper the author describes...
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Remote sensing in laboratory diagnostics of reinforced concrete elements – current development and vision for the future
PublikacjaContinuous emergence of new concrete types and kinds of reinforcement, as well as technological solutions in the field of structural engineering have made great demand for diagnostic tests of reinforced concrete elements. New challenges and problems facing people require new more efficient tools for laboratory diagnostics than those commonly used. Remote sensing may be the answer to this demand. In this paper the author describes...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - DISTILLED WATER. Specim. set K07
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DISTILLED WATER. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - DISTILLED WATER. Specim. set K06
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DISTILLED WATER. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K04
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - PARAFFIN OIL. Specim. set K08
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: PARAFFIN OIL. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig:...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - DISTILLED WATER. Specim. set K02
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DISTILLED WATER. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test...
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The morphology of vanadate glasses containing BaTiO3 measured with the use of AFM
Dane BadawczeThe morphology of vanadate glasses doped with BaTiO3 was measured with the use of AFM method. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K05
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K03
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K01
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - PARAFFIN OIL. Specim. set K09
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: PARAFFIN OIL. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig:...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - DISTILLED WATER. Specim. set K06
Dane BadawczeOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DISTILLED WATER. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test...
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Thermal properties of VO2 and V2O3 nanostructures
Dane BadawczeThe DataSet contains the DSC and TG curves of VO2 and V2O3 nanostructures obtained by the sol-gel with different reaction conditions. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The xerogel powder was annealing under argon atmosphere at the selected temperature: 500C, 600C, and 1000C.
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Use of Ginger Nanofibers for the Preparation of Cellulose Nanocomposites and Their Antimicrobial Activities
PublikacjaHere, we report, for the first time, the isolation of ginger nanofibers (GNF) from ginger rhizomes spent by acid hydrolysis and followed by high-pressure homogenization. Scanning electron microscopy was utilized to identify the surface morphology of the GNF and the widths ranged between 130 to 200 nm. Structural analysis of GNF was identified by Fourier transform infrared spectroscopy, Differential scanning calorimetry, and X-ray...
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The microstructure of aluminium alloys AA1050 and AA7075 subjected to anodic polarization at 8V in KOH electrolyte
Dane BadawczeThe dataset contains SEM pictures of the microstructure of aluminum alloy AA1050 and AA7075 exposed in aqueous KOH in the pH range between 14–11. Two sets of samples are presented, revealing the topography of the alloys when exposed to aggressive media under open circuit potential conditions as well as when subjected potentiodynamic polarization ranging...
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High-Temperature Oxidation of Heavy Boron-Doped Diamond Electrodes: Microstructural and Electrochemical Performance Modification
PublikacjaIn this work, we reveal in detail the effects of high-temperature treatment in air at 600 °C on the microstructure as well as the physico-chemical and electrochemical properties of boron-doped diamond (BDD) electrodes. The thermal treatment of freshly grown BDD electrodes was applied, resulting in permanent structural modifications of surface depending on the exposure time. High temperature affects material corrosion, inducing...
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The Optimum Dataset method – examples of the application
PublikacjaData reduction is a procedure to decrease the dataset in order to make their analysis more effective and easier. Reduction of the dataset is an issue that requires proper planning, so after reduction it meets all the user’s expectations. Evidently, it is better if the result is an optimal solution in terms of adopted criteria. Within reduction methods, which provide the optimal solution there is the Optimum Dataset method (OptD)...
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On-line measurement of wood surface smoothness
PublikacjaThe latest progress in the field of optics and microelectronics resulted in development of new generation vision systems capable of scanning surface topography with very high sampling frequencies. The blue color of illuminating light as well as novel systems for controlling ultra-thin laser line thickness allows measurement of the porous surface of wood with a triangulation method. Three alternative sensors were tested here in...
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Phytoplankton in the Kashubian Lakes – microscopic photo archive
Dane BadawczePhytoplankton is a group of microscopic plant organisms passively floating in water. The organisms included in the phytoplankton of lakes include the following main taxonomic groups: cyanobacteria (Cyanobacteria), green algae (Chlorophyta), dinoflagellates (Dinophyta), diatoms (Bacillariophyceae), cryptophytes (Cryptophyta), chrysophytes (Chrysophyceae)...
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Structure and optical measurements of Eu doped tellurium oxide thin films
Dane BadawczeThin films were deposited by magnetron sputtering method and simultaneously heated at 200 oC. Presence of Eu ions and their valence states was confirmed by X-ray photoemission spectroscopy measurements. The structure of the films as well as the influence of europium dopant on crystalline structure of the films was examined by X-ray diffraction method. ...
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The SEM micrographs of the synergistic action between cavitation erosion and pitting corrosion on stainless steel 304
Dane BadawczeThe dataset contains Scanning Electron Micrographs of stainless steel AISI304 samples made after cavitation erosion-corrosion exposure using a vibratory transducer (in accordance with ASTM G32). The micrographs compare the topography of samples subjected to either cavitation erosion (in deionized water), pitting corrosion (in 8% FeCl3 solution, without...
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Deformation Analysis of a Composite Bridge during Proof Loading Using Point Cloud Processing
PublikacjaRemote sensing in structural diagnostics has recently been gaining attention. These techniques allow the creation of three-dimensional projections of the measured objects, and are relatively easy to use. One of the most popular branches of remote sensing is terrestrial laser scanning. Laser scanners are fast and efficient, gathering up to one million points per second. However, the weakness of terrestrial laser scanning is the...
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Modified nanodiamond particle size studies by means of dynamic light scattering technique
PublikacjaThe Methods Utilizing the Phenomena of Light Scattering to Measure Particle Size distribution in different solvent, such as deionise water and alcohol and also to study the various structural formation when nanodiamond solution is placed on silicon surface. The purpose of this research project is divided into two parts to configure the measurement units for examining modified nanodiamond particles, examination...
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Modified nanodiamond particle size studies by means of dynamic light scattering technique
PublikacjaThe Methods Utilizing the Phenomena of Light Scattering to Measure Particle Size distribution in different solvent, such as deionise water and alcohol and also to study the various structural formation when nanodiamond solution is placed on silicon surface. The purpose of this research project is divided into two parts to configure the measurement units for examining modified nanodiamond particles, examination...
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Topography measurement methods evaluation for entire bending-fatigued fracture surfaces of specimens obtained by explosive welding
PublikacjaIn this paper, the methods of compensation of differences in the results of entire bending-fatigued fracture surface topographies were presented. The roughness evaluation was performed with a focus variation microscope and confocal surface topography measurement techniques. The differences in the ISO 25178 roughness parameters were investigated and procedures for their compensation were studied. It was found that various types...
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Recovering Evaluation of Narrow-Kerf Teeth of Mini Sash Gang Saws
PublikacjaSash gang saws with narrow-kerf saw blades are used in the production of glued laminate flooring elements in plants where dry technology is applied. This means that boards or friezes are sawn into top layer lamellae in dry conditions (moisture content of about 10–12%) from expensive wood species, often exotic. The object of this research was stellite-tipped teeth of narrow kerf saw blades sharpened under industrial conditions....
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High-conducting Bi4V2-xFexO11-δ ceramics containing Fe2O3 nanocrystals: Structure and properties
PublikacjaThe topography, structure, thermal, magnetic, and electrical properties of Bi4V2-xFexO11-δ ceramics substituted with x = 0.5 and 0.7 Fe were studied. The microscope analysis showed the presence of iron-rich nanocrystals formed on the Bi-Fe-V-O grains. The X-ray diffraction studies confirmed that grains are built mostly of tetragonal Bi4V1.5Fe0.5O10.5 phase. Thermal properties analysis showed an order-disorder type γ ↔ γʹ phase...
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Prototype design and development of low-load-roof photovoltaic modules for applications in on-grid systems
PublikacjaFour prototypes of lightweight photovoltaic modules for applications in on-grid systems have been designed, developed, manufactured and tested for compliance with relevant IEC standards. Selected, commercially available materials characterized by thermogravimetry, differential scanning calorimetry, dilatometry, scanning electron microscopy and nanoindentation technique were used in frameless, adhesively-bonded sandwich-structures...
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Application of the Optimum Dataset Method in Archeological Studies on Barrows
PublikacjaLight Detection and Ranging (LiDAR) became one of the technologies used in archaeological research. It allows for relatively easy detection of archaeological sites that have their own field form, e.g.: barrows, fortresses, tracts, ancient fields [1]. As a result of the scanning, the so-called point cloud is obtained, often consisting of millions of points. Such large measurement datasets are very time-consuming and labor-intensive...
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Improvement of opipramol base solubility by complexation with β-cyclodextrin
PublikacjaOpipramol (OPI), a tricyclic antidepressant and anxiolytic compound, is administered orally in the form of a dihydrochloride. Salt form of the drug has a higher solubility in water and hence bioavailability and stability. A similar effect can be achieved by closing the hydrophobic part of the drug molecule in the cyclodextrin cavity. The paper presents opipramol inclusion complexes with beta-cyclodextrin (β-CD) in 1:1 molar ratio....
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The time-dependent cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to cancer LNCaP cells
Dane BadawczeThe time-dependent (1, 24, 48, and 72 h) cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to cancer LNCaP cells performed by Confocal Laser Scanning Microscopy (63× magnification; ZEISS LSM T-PMT, Magdeburg, Germany). Based on the fluorescence properties of these compounds, green and orange fluorescence...
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The time-dependent cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to cancer H460 cells
Dane BadawczeThe time-dependent (1, 24, 48, and 72 h) cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to cancer H460 cells performed by Confocal Laser Scanning Microscopy (63× magnification; ZEISS LSM T-PMT, Magdeburg, Germany). Based on the fluorescence properties of these compounds, green and orange fluorescence...
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The time-dependent cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to normal PNT1A cells
Dane BadawczeThe time-dependent (1, 24, 48, and 72 h) cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to normal PNT1A cells performed by Confocal Laser Scanning Microscopy (63× magnification; ZEISS LSM T-PMT, Magdeburg, Germany). Based on the fluorescence properties of these compounds, green and orange fluorescence...
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The SEM micrographs of the cavitation erosion-corrosion process of selected copper alloys degradation
Dane BadawczeThe dataset contains Scanning Electron Micrographs of CuZn40Mn3Fe brass compared with Superston and Novoston bronze after cavitation erosion-corrosion exposure using a vibratory transducer (in accordance with ASTM G32). The micrographs compare the topography of samples subjected cavitation erosion in 3% NaCl at room temperature, leading to the surface...
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The microstructure of AA5754 alloy under corrosion in alkaline media (pH=11) with 20 mM of various carboxylic acids
Dane BadawczeThis dataset contains scanning electron microscopy (SEM) micrographs taken for polished aluminum AA5754 alloy samples, exposed for 100 min in bicarbonate buffer (pH=11) with the addition of 20 mM of carboxylic acids, namely: citric acid, malic acid, maleic acid, succinic acid, tartaric acid, tricarballylic acid and serine. The goal of this study was...
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The microstructure of AA5754 alloy under corrosion in alkaline media (pH=11) with 4.5 mM of various carboxylic acids
Dane BadawczeThis dataset contains scanning electron microscopy (SEM) micrographs taken for polished aluminum AA5754 alloy samples, exposed for 100 min in bicarbonate buffer (pH=11) with the addition of 4.5 mM of carboxylic acids, namely: citric acid, malic acid, maleic acid, succinic acid, tartaric acid, tricarballylic acid and serine. The goal of this study was...
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The effect of cobalt addition on the corrosion behavior of near equiatomic NiTi shape memory alloy in normal saline solution, impedance and microscopic studies
Dane BadawczeThe electrochemical and corrosion (uniform and localized) behavior of a binary Ni52Ti48 shape memory alloy (SMA) and two ternary Ni52Ti48-xCox (x = 1.5 and 4.0 wt.%) SMAs were studied. Measurements were conducted in 0.9% NaCl solution at 37 oC. This dataset contains the results of electrochemical impedance spectroscopy (EIS) studies done on daily basis...
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SEM micrographs of cavitation erosion-corrosion of aluminium alloy 2024 with anodic polarization
Dane BadawczeThe dataset contains Scanning Electron Micrographs of aluminium alloy 2024 samples made after cavitation erosion-corrosion exposure using a vibratory transducer (in accordance with ASTM G32). The experiment duration was 240 min, with cyclic cavitation exposure in on/off cycles 30s:30s. The electrolyte was 0.1 M KNO3 solution. Some samples were anodically...
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Tip-Based Nanofabrication as a Rapid Prototyping Tool for Quantum Science and Technology
PublikacjaTip-Based Nanofabication as a Rapid Prototyping Tool for Quantum Science and Technology discusses the development of cantilevered nanotips techniques of quantum devices prototyping and how they evolved from scanning probe microscopy. Also covered are the advantages and future prospects of atomic resolution capability and how to use this enabling technology as a rapid prototyping tool for quantum science and technology.
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The morphology of vanadate glass-ceramics containing BaTiO3 measured with the use of AFM
Dane BadawczeThe structure of vanadate glass-ceramics doped with BaTiO3 was measured by AFM technique. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on...
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THE STUDY OF WATER POLLUTION OF THE LOWER VISTULA RIVER BY PLASTIC PARTICLES
PublikacjaSince the beginning of widespread use of plastic its consumption and production has been constantly increasing. As a result of human activity part of waste ends up in our environment and is deposited in each of the elements of the biosphere. These impurities can be in the form of large elements, small particles fragmented to macroscopic level (pellets, facial scrub grains) and the microparticles visible under a microscope. Particularly...
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Characterization of volatile compounds, structural, thermal and physico-mechanical properties of cross-linked polyethylene foams degraded thermo-mechanically at variable times
PublikacjaWaste cross-linked polyethylene foam (wXLPE) was thermo-mechanically degraded at variable time using internal batch mixer. The progress of wXLPE degradation has been investigated by using a simultaneous thermogravimetric/differential scanning calorimetry analyzer coupled with Fourier transform infrared spectroscopy, swelling measurements, tensile tests and scanning electron microscopy. Volatile organic compounds generated during...
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Spectroscopic evaluation on pseudopolymorphs of sodium naproxen
PublikacjaThis paper demonstrates the assessment of vibrational spectroscopy methods such as middle infrared, near infrared and Raman spectroscopy (FTIR, FT-NIR, Raman) for the identification of pseudopolymorphic forms of a model active pharmaceutical ingredient (API) - sodium naproxen (NpxNa). NpxNa, in the form of three different pseudopolymorphs, was investigated by methods dedicated for solid state characterization: DSC (differential...
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Comparison of 3D Point Cloud Completion Networks for High Altitude Lidar Scans of Buildings
PublikacjaHigh altitude lidar scans allow for rapid acquisition of big spatial data representing entire city blocks. Unfortunately, the raw point clouds acquired by this method are largely incomplete due to object occlusions and restrictions in scanning angles and sensor resolution, which can negatively affect the obtained results. In recent years, many new solutions for 3D point cloud completion have been created and tested on various objects;...
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Assessment of the impact of bacteria Pseudomonas denitrificans, Pseudomonas fluorescens, Bacillus subtilis and yeast Yarrowia lipolytica on commercial poly(ether urethanes)
PublikacjaThe assessment of the impact of the bacteria Pseudomonas denitrificans, Pseudomonas fluorescens, Bacillus subtilis and yeast Yarrowia lipolytica on commercial poly(ether urethanes) Tecoflex® and Tecothane® is presented. The polyurethane samples were incubated with pure cultures of the microorganisms at 30 °C for five months. The changes in the chemical structure of the polymers were evaluated using loss of weight and contact angle...
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MULTI-OBJECTIVE OPTIMIZATION PROBLEM IN THE OptD-MULTI METHOD
PublikacjaNew measurement technologies, e.g. Light Detection And Ranging (LiDAR), generate very large datasets. In many cases, it is reasonable to reduce the number of measuring points, but in such a way that the datasets after reduction satisfy specific optimization criteria. For this purpose the Optimum Dataset (OptD) method proposed in [1] and [2] can be applied. The OptD method with the use of several optimization criteria is called...
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Fatigue Bending of V-Notched Cold-Sprayed FeCoCrNiMn Coatings
PublikacjaCold-spray coatings were produced by FeCoCrNiMn high-entropy alloy powders deposited on carbon steel substrate. The coatings were realized at intermediate temperature and high pressure (at 1100 °C and 7 MPa). The coating microstructure was characterized by scanning electron microscopy and X-ray diffraction, revealing a very dense deposition and high flattening ratio of the splatted particles. This had a large influence on the...
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The time-dependent cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to cancer Du-145 cells
Dane BadawczeThe time-dependent (1, 24, 48, and 72 h) cellular uptake of C−2028, CD−C−2028, QDgreen−C−2028, and QDgreen−CD−FA−C−2028 conjugates at IC80 value to cancer Du-145 cells performed by Confocal Laser Scanning Microscopy (63× magnification; ZEISS LSM T-PMT, Magdeburg, Germany). Based on the fluorescence properties of these compounds, green and orange fluorescence...