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Effect of conventional cooking on changes in the contents of basic composition and glucosinolates in kale
PublikacjaBrassica vegetables have been strongly recommended as part of human diet because of its high content of bioactive sulphur compounds, eg glucosinolates. The nutrient and health promoting compounds in kale are significantly affected by traditional cooking. The study investigated changes in the levels of dry mass, ash, fat, total protein, dietary fibre as well as total and individual glucosinolates in the kale due to the traditional...
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The electronic characterization of the cubic Laves-phase superconductor CaRh2
PublikacjaWe present the synthesis and experimental characterization of the electronic properties of the cubic Laves phase superconductor CaRh2. Its crystal structure was confirmed by powder X-ray diffraction and its ambient temperature lattice parameter (a = 7.5326(6) Å) is in good agreement with the literature. Magnetization, resistivity and heat-capacity measurements indicate that CaRh2 is a moderate-coupling type-II superconductor (λe-p = 0.89)...
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Pomiary i analiza dźwięku w filmie oraz w reklamach filmowych z wykorzystaniem modelu głośności LKFS .
PublikacjaCelem niniejszej pracy był pomiar dźwięku filmie, zapowiedziach filmów oraz reklamach poprzedzających projekcję filmu. W referacie w pierwszej kolejności przywołano problemy związane z pomiarem dźwięku, rekomendacje, które wskazują na dopuszczalne poziomy projekcji filmowej oraz przywołano jednostki, które są wykorzystywane w określaniu głośności projekcji. Następnie przedstawiono pomiary, kalibrację sprzętu pomiarowego oraz analizę...
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Molecular geometry and optical activity of helically chiral N-nitrosamines derived from 1,2,3,4-tetrahydro- and 1,2,3,4,7,8,9,10-octahydro-1,10-phenanthroline
PublikacjaX-ray crystallographic analysis of the title N-nitrosamines revealed that they assume helical conformations in the solid state. Nitrosamines 1b and 2b were resolved by inclusion crystallization with optically active diols (TADDOLs). The absolute configuration of the guest molecules in the complexes 1b·3b and 2b·3b was assigned as M. The optical activity of the resolved compounds is manifested by their solid state CD spectra, which...
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Rapid multi-objective simulation-driven design of compact microwave circuits
PublikacjaA methodology for rapid multi-objective design of compact microwave circuits is proposed. Our approach exploits point-by-point Pareto set identification using surrogate-based optimization techniques, auxiliary equivalent circuit models, and space mapping as the major model correction method. The proposed technique is illustrated and validated through the design of a compact rat-race coupler. A set of ten designs being trade-offs...
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KTaO3-based nanocomposites for air treatment
PublikacjaA series of single semiconductors and their nanocomposites combination (such as KTaO3 + CdSe + SrTiO3; KTaO3 + CdS +WO3; KTaO3 + CdS + MoS2) were prepared using hydrothermal route. Photocatalytic activity of as-prepared nanocomposites was estimated by photocatalytic degradation of toluene in the gas phase using light-emitting diodes (LEDs, 375 nm) in four subsequent cycles. The nanocomposites were characterized by scanning electron...
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Self-Organizing Map representation for clustering Wikipedia search results
PublikacjaThe article presents an approach to automated organization of textual data. The experiments have been performed on selected sub-set of Wikipedia. The Vector Space Model representation based on terms has been used to build groups of similar articles extracted from Kohonen Self-Organizing Maps with DBSCAN clustering. To warrant efficiency of the data processing, we performed linear dimensionality reduction of raw data using Principal...
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Reactions of Lithiated Diphosphanes R2P-P(SiMe3)Li (R = tBu, iPr, iPr2N, Et2N) with [Cp2WCl2]. Syntheses and Structures of the First Terminal Phosphanylphosphido Complexes of Tungsten(IV)
PublikacjaReactions of R2P−P(SiMe3)Li (R = tBu, iPr, iPr2N, Et2N) with [Cp2WCl2] yield terminal phosphanylphosphido complexes [Cp(C5H4P-PR2)WH] or [Cp{C5H4P-PR2}-W(SiMe3)] by way of a hydrogen or SiMe3 migration to tungsten. The solid-state structures of [Cp(C5H4P−PtBu2)-WH] and [Cp(C5H4P-PNEt2)WH] were established by singlecrystalX-ray diffraction. Two stereoisomers of [Cp(C5H4P−PtBu2)WH] were identified by solution NMR spectroscopy. Reaction...
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General route for the synthesis of terminal phosphanylphosphido complexes of Zr(IV) and Hf(IV): Structural investigations of the first zirconium complex with a phosphanylphosphido ligand
PublikacjaReactions of R2P-P(SiMe3)Li with [Cp2MCl2] (M = Zr, Hf) in hydrocarbons yield the related terminal phosphanylphosphidocomplexes [Cp2M(Cl){(Me3Si)P-PR2-jP1}] (R = iPr and tBu). The solid state structures of [Cp2M(Cl){P(SiMe3)-PiPr2-jP1}] (M = Zr, Hf) were established by single crystal X-ray diffraction studies. The phosphido-P atoms adopt almost planar geometries and the phosphanyl P atoms adopt pyramidal geometries. The reaction...
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Synthesis and Spectroscopic Properties of New Bis-tetrazoles
PublikacjaSyntheses of N,N'-phenyltetrazole podands link with aliphatic chains containing oxygen, nitrogen and sulphur atoms, are described. The complexing properties of these compounds towards metal cations (Fe2+, Cu2+, Zn2+, Co2+, Ni2+) were investigated by absorption and infrared spectroscopy. The UV-Vis titrations were performed to estimate the stability constant values of the respective complexes with Cu2+ ion. Changes in UV-Vis absorption...
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Synthesis and Characterization of Monometallic (Ag, Cu) and Bimetallic Ag-Cu Particles for Antibacterial and Antifungal Applications
PublikacjaIn this paper, the experimental studies are concerned with the effect of the synthesis parameters on the formation of monometallic Ag and Cu nanoparticles (NPs). We consider the synthesis strategies verification for the bimetallic core-shell and alloy particles preparation. It was successfully obtained by chemical reduction method. The obtained colloidal solution is characterized by the transmission electron microscopy (TEM) with...
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Wykorzystanie wybranych wskaźników makroekonomicznych do oceny efektywności gospodarek krajów Unii Europejskiej
PublikacjaProces integracji Europy, w którym uczestniczy aktywnie nasz kraj, spowodował konieczność ustawicznej oceny jej efektywności na tle wybranych krajów UE. Zarówno w okresie przedakcecyjnym, jak i po przystąpieniu Polski do struktur UE podjęto działania w celu zmniejszenia dystansu w zakresie konkurencyjności, innowacyjności, nowoczesności struktury gospodarki polskiej oraz ograniczenia skali bezrobocia. Celem niniejszego opracowania...
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Effects of La Content on the Densification, Microstructure, and Conductivity of Doped La10−x Ge6 O26±δ Electrolytes
PublikacjaIn this study, the influence of La content on the characteristics of Nb-, Mo-, and W-doped LaxGe6O26±δ electrolytes was investigated through sintering study, X-ray diffraction, scanning electron microscopy, and conductivity measurement. The densification of LaxGe5.5Nb0.5O26±δ and LaxGe5.5W0.5O26±δ was retarded as the x reached 9.75, while that of LaxGe5.5Mo0.5O26±δ improved with increasing La content. The average grain size slightly...
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The Role of Proteins in Food
PublikacjaThis chapter describes the effect of proteins on the sensory attributes and the biological value and safety of foods. The role of proteins depends on their amino acid composition and structure, on changes due to storage and processing, as well as on interactions with other food components. The effect on the sensory quality of foods is brought about by hydrophobicity, solubility, water holding capacity, gelling, film formation,...
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Experimental evaluation of estimator mean square error curve for cognitive tracking radar
PublikacjaTo make decisions, cognitive radar must rely on predictions of its own performance. In the literature, these predictions are usually based on some form of Cram\'er-Rao lower bound. This approach is scientifically sound, but it also brings a possibility of the cognitive controller overestimating radar performance. It therefore makes sense to back theoretical predictions with careful experiments which will verify their applicability....
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Asynchronous Method of Simultaneous Object Position and Orientation Estimation with Two Transmitters
PublikacjaThis paper proposes an object location method for all types of applications, including the Internet of Things. The proposed method enables estimations of the position and orientation of an object on a plane or in space, especially during motion, by means of location signals transmitted simultaneously from two transmitters placed on the object at a known distance from each other. A mathematical analysis of the proposed method and...
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Simple colorimetric copper(II) sensor – spectral characterization and possible applications
PublikacjaNew o-hydroxyazocompound L bearing pyrrole residue was obtained in the simple synthetic protocol. The structure of L was confirmed and analyzed by X-ray diffraction. It was found that new chemosensor can be successfully used as copper(II) selective spectrophotometric regent in solution and can be also applied for the preparation of sensing materials generating selective color signal upon interaction with copper(II). Selective colorimetric...
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Comparison of Volatile Constituents ofAcorus calamusandAsarum europaeumObtained by Different Techniques
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Ab-initio investigations for structural, mechanical, optoelectronic, and thermoelectric properties of Ba2SbXO6 (X Nb, Ta) compounds
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Chromane helicity rule – scope and challenges based on an ECD study of various trolox derivatives
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Correction: Simultaneously improving the thermal stability, flame retardancy and mechanical properties of polyethylene by the combination of graphene with carbon black
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Mass production of hierarchically porous carbon nanosheets by carbonizing “real-world” mixed waste plastics toward excellent-performance supercapacitors
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Simultaneously improving the thermal stability, flame retardancy and mechanical properties of polyethylene by the combination of graphene with carbon black
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On the Disaster Resiliency within the Context of 5G Networks : The RECODIS Experience
PublikacjaNetwork communications and the Internet pervade our daily activities so deeply that we strongly depend on the availability and quality of the services they provide. For this reason, natural and technological disasters, by affecting network and service availability, have a potentially huge impact on our daily lives. Ensuring adequate levels of resiliency is hence a key issue that future network paradigms, such as 5G, need to address. This...
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Superconductivity in the superhard boride WB4.2
PublikacjaWe show that the superhard boride WB4.2 is a superconductor with a Tc of 2.05(5) K. Temperature-dependent magnetic susceptibility, electrical resistivity, and specific heat measurements were used to characterize the superconducting transition. The Sommerfeld constant γ for WB4.2 is 2.07(3) mJ mol−1 K−2 and the ΔC/γTc=1.56, which is somewhat higher than what is expected for weakly coupled Bardeen–Cooper–Schrieffer type superconductors....
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Guanosine Dianions Hydrated by One to Four Water Molecules
PublikacjaIntermolecular interactions such as those present in molecule···water complexes may profoundly influence the physicochemical properties of molecules. Here, we carried out an experimental–computational study on doubly deprotonated guanosine monophosphate···water clusters, [dGMP – 2H]2–·nH2O (n = 1–4), using a combination of negative anion photoelectron spectroscopy (NIPES) with molecular dynamics (MD) and quantum chemical (QM) calculations....
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Surface properties tuning of exfoliated graphitic carbon nitride for multiple photocatalytic performance
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Deep Learning Optimization for Edge Devices: Analysis of Training Quantization Parameters
PublikacjaThis paper focuses on convolution neural network quantization problem. The quantization has a distinct stage of data conversion from floating-point into integer-point numbers. In general, the process of quantization is associated with the reduction of the matrix dimension via limited precision of the numbers. However, the training and inference stages of deep learning neural network are limited by the space of the memory and a...
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In situ spectroelectrochemical and theoretical study on the oxidation of a 4H-imidazole-ruthenium dye adsorbed on nanocrystalline TiO2thin film electrodes
PublikacjaTerpyridine 4H-imidazole-ruthenium(ii) complexes are considered promising candidates for use as sensitizers in dye sensitized solar cells (DSSCs) by displaying broad absorption in the visible range, where the dominant absorption features are due to metal-to-ligand charge transfer (MLCT) transitions. The ruthenium(iii) intermediates resulting from photoinduced MLCT transitions are essential intermediates in the photoredox-cycle...
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π-Stacking attraction vs. electrostatic repulsion: competing supramolecular interactions in a tpphz-bridged Ru(ii)/Au(iii) complex
PublikacjaThe synthesis and characterization of a mixed metal ruthenium(II)/gold(III) complex bridged by tetrapyridophenazine (tpphz) are described. It is isostructural and isoelectronic to the well-known photocatalysts with palladium(II) or platinum(II). Concentration dependent 1H-NMR spectroscopy and XRD studies show that the electrostatic repulsion between the gold(III) moieties exceeds the attractive π-stacking interaction. Theoretical...
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Systemy radionawigacji lotniczej
PublikacjaW artykule przedstawiono rozwiązania systemowe estymacji położenia obiektów w naziemnych systemach radionawigacyjnych dla potrzeb lotniczych: ILS, MLS, VOR, ADF, GPS, DME, RA oraz WAM.
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The resistance of S235JR steel to cavitation erosion
PublikacjaThe erosion resistance of S235JR steel to flow cavitation was investigated. In order to understand an influence of steel properties and cavitation intensities on the degradation mechanisms, low-carbon S235JR steel was tested in the as-received state and after thermal treatment (annealing) under four different flow velocities. Annealing decreased steel hardness, which made S235JR steel less resistant to cavitation erosion. The performed...
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Efficient production of B-substituted single-wall carbon nanotubes
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Krytyczne działania i czynniki sukcesu wdrażania projektów informatycznych
PublikacjaCelem niniejszego artykułu jest określenie, jakie działania powinny podjąć organizacje gospodarcze, aby zidentyfikowane krytyczne czynniki sukcesu projektów informatycznych, pozwalające na zwiększenie prawdopodobieństwa pomyślnego zakończenia przedsięwzięcia, zmaterializowały się. Na potrzeby niniejszego artykułu przeprowadzono badania własne. Jako metodę wybrano analizę przypadków. Badanie przeprowadzono w organizacji, która prowadziła...
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Kształtowanie jakości powierzchni powłok Cr2O3 przez docieranie
PublikacjaOmówiono wyniki badań technologicznego docierania powłok ceramicznych Cr2O3, które wykazały przydatność tego procesu w uzyskaniu wysokiej jakości powierzchni, charakteryzującej się niską wartością parametru chropowatości Ra.
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Rapeseed oil methyl ester production in an individual household
PublikacjaFatty acid methyl esters, commonly known as biodiesel, are a cheap and environmental-friendly fuel substitute for diesel engines. Aside from industrial production, individual biodiesel manufacturing is also and important method of fulfilling the requirements of EU Parliament directive no. 2003/30/WE about supporting the use of renewable fuels in transport. Individual FAME production guarantees easy access to the main raw material...
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The role of proteins in food. Chapter 6
PublikacjaStruktura i konformacja wpływają na biologiczne oraz funkcjonalne właściwości białek i na ich rolę w tworzeniu pożądanych cech produktów żywnościowych. Właściwości funkcjonalne to rozpuszczalność w środowisku wodnym o różnej sile jonowej, wodochłonność oraz zdolność żelowania, tworzenia błon, emulgowania lipidów i pienienia się. Białka mięsa, ryb, mleka, jaj, nasion roślin strączkowych, nasion zbóż oraz drobnoustrojów różnią się...
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Application of vertical flow cw for highly contaminated wastewater treatment
PublikacjaBasing on quantitative and qualitative characteristics of reject waters generated during digested sewage sludge dewatering on centrifuges in conventional WWTP (RWC) and municipal landfill leachate (LL), the pilot constructed wetlands for treatment of both types of highly contaminated wastewater were designed. In the paper the characteristics of the pilot plants and assumed treatment efficiencies are presented. According to the...
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Terbium Substituted Lanthanum Orthoniobate: Electrical and Structural Properties
PublikacjaThe results of electrical conductivity studies, structural measurements and thermogravimetric analysis of La1−xTbxNbO4+δ (x = 0.00, 0.05, 0.1, 0.15, 0.2, 0.3) are presented and discussed. The phase transition temperatures, measured by high-temperature x-ray diffraction, were 480 °C, 500 °C, and 530 °C for La0.9Tb0.1NbO4+δ, La0.8Tb0.2NbO4+δ, and La0.7Tb0.3NbO4+δ, respectively. The impedance spectroscopy results suggest mixed conductivity...
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Interrelated shape memory and Payne effect in polyurethane/graphene oxide nanocomposites
PublikacjaWe report the fabrication of graphene oxide (GO) based polyurethane (PU) nanocomposites by a simple method of mixing and their shape memory properties at different temperatures. Both the polymer and the filler were synthesized in the laboratory by simple and easy methods – PU by pre-polymer method and GO by improved graphene oxide synthesis method. High molecular level dispersion of GO platelets within the PU matrix and thus good...
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Synergistic effect of multi walled carbon nanotubes and reduced graphene oxides in natural rubber for sensing application
PublikacjaUtilizing the electrical properties of polymer nanocomposites is an important strategy to develop high performance solvent sensors. Here we report the synergistic effect of multi walled carbon nanotubes (MWCNTs) and reduced graphene oxide (RGO) in regulating the sensitivity of the naturally occurring elastomer, natural rubber (NR). Composites were fabricated by dispersing CNTs alone and together with exfoliated RGO sheets (thermally...
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The effect of processing on the safety and nutritional value
PublikacjaAgricultural crops as well as animal food raw materials are usually somehow processed before being used by humans. Processing should make them more useful, increase their safety and nutritional value, extend the shelf life, and modify the sensory properties. However, changes and interactions of various compounds in the conditions of processing may generate products toxic or otherwise unsafe for the human organism. The food industry...
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Międzyuczelniany kierunek studiów technologie kosmiczne i satelitarne - edycja trzecia
Publikacjapolitechnika gdańska już po raz trzeci rekrutuje kandydatów na interdyscyplinarny kierunek studiów II stopnia - technologie kosmiczne i satelitarne (TKiS). Jak w latach poprzednich, studia organizowane są we współpracy z Uniwersytetem Morskim w Gdyni oraz Akademią Marynarki Wojennej w Gdyni. Od tego roku akademickiego w przedsięwzięciu weźmie udział także Uniwersytet Gdański. W poprzednich latach studenci osiągnęli wiele sukcesów...
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Influence of dopants on structure of polycrystalline bismuth niobate
PublikacjaBismuth niobate (BiNbO4) has attracted attention as a low-fired ceramics with promising microwave application potential. BiNbO4 ceramics was fabricated by mixed oxide method and sintered at temperature T<1000˚C. As the sintering aids a small amount of CuO oxide was used. The crystalline structure of the ceramic samples was examined by X-ray diffraction method at room temperature. The Rietveld refinement method was used for analysis...
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Crystal structure, chemical bonding, and physical properties of layered AIrSn2 (A = Sr and Ba)
PublikacjaWe report the experimental and theoretical investigation of structure, chemical bonding interactions, and physical properties of new ternary stannides AIrSn2 (A = Sr and Ba). AIrSn2 (A = Sr and Ba) crystallizes in the orthorhombic Re3B-type structure with the space group Cmcm (No. 64). According to single-crystal X-ray diffraction results, the structure of AIrSn2 (A = Sr and Ba) can be considered as a Zintl-type compound with heterogeneous...
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Wyznaczanie parametrów lepkosprężystego modelu Burgersa mieszanek mineralno-asfaltowych na podstawie badania pod obciążeniem dynamicznym
PublikacjaMetoda wyznaczania parametrów reologicznych lepkosprężystego modelu Burgersa dla mieszanek mineralno-asfaltowych bazująca na podstawie wyników badania pełzania pod obciążeniem statycznym bywa często kłopotliwa. Autorzy artykułu przedstawiają, stosowaną przez nich, metodę wyznaczania tych parametrów na podstawie wyników badania próbek pod obciążeniem dynamicznym przy wykorzystaniu programu komputerowego VEROAD. Metoda bazująca na...
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Ekspertyza nr WOiO/II/78/2015 n.t. własności mechanicznych laminatów epoksydowo-bazaltowych
PublikacjaWspółczesne konstrukcje jachtów często wykonywane są z materiałów kompozytowych. Najczęściej stosowane są kompozyty (laminaty), których zbrojenie wykonane jest z włókna szklanego bądź węglowego, przesyconego żywicą (poliestrową, epoksydową, winyloestrową). W przemyśle jachtowym, co raz częściej stosuje się zbrojenia wykonane z włókien bazaltowych. Zleceniodawca dostarczył próbki wykonane z różnych materiałów, w tym m.in ze wspomnianych...
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Smoking: Traditional
PublikacjaSmoking, drying, and salting belong to the oldest methods of food preservation. Meat hung by the fire was preserved by a combination of drying and smoking. Often the raw material was first pickled in brine. In different regions of the world various procedures have been developed, best suited for treating meats and fish for specific purposes. Smoking extended the shelf life and imparted very desirable, new sensory properties to...
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Realizacja zmiany procesu planowania i sterowania produkcją – aspekty metodyczne
PublikacjaKonieczność zapewnienia sprawnej i skutecznej realizacji podstawowego procesu w organizacjach jakim jest proces produkcji wyrobów i usług, wymaga odpowiedniej adaptacji procesu planowania i sterowania produkcją do dynamicznych zmian otoczenia. Dla zagwarantowania efektywnego przebiegu procesu zmiany niezbędne jest nadanie mu właściwych ram i jego systemowe ujęcie. W artykule scharakteryzowano zakres działań i obszary zmian procesu...
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Macro-elements and Model Order Reduction for Efficient Three-Dimensional FEM Analysis
PublikacjaAn efficient model order reduction (MOR) methodology for three dimensional vector finite element method (FEM) is developed to accelerate simulations of the structures containing features that cause strong variations of mesh density. As the result of presented algorithm, FEM subsystems of equations corresponding to the selected refined region are converted into a very compact sets of linear equations, called macro-elements.Numerical...