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Determination of hormones in water samples using liquid chromatography coupled with tandem mass spectrometry
PublikacjaOver the past few years, many synthetic (ethinylestradiol) and natural (estradiol,estriol, estrone) compounds present in the environment have been affecting the hormonalbalance of humans and animals. Steroid hormones are very often used for medical purposesand have high estrogenic activity what makes them endocrine disrupters. Most hormonalcompounds are released into the water as a result of their incomplete removal in wastewatertreatment...
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Mass Spectrometric Identification of 13C-labeled Metabolites During anaerobic Propanoic Acid Oxidation
PublikacjaBiowaste digestion is a possibility to gain biogas as a renewable fuel source. However, the anaerobic food chain may be disrupted by, e.g., substrate overload or by inhibitors, leading to the accumulation of volatile fatty acids (VFAs), predominantly of propanoic acid (PA). VFA Accumulation may cause a rapid pH decrease, less biogas production, or even a total inhibition. To maintain high biogas productivity or to prevent a collapse...
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Dynamic mass measurement in checkweighers using a discrete time-variant low-pass filter
PublikacjaConveyor belt type checkweighers are complex mechanical systems consisting of a weighing sensor (strain gauge load cell, electrodynamically compensated load cell), packages (of different shapes, made of different materials) and a transport system (motors, gears, rollers). Disturbances generated by the vibrating parts of such a system are reflected in the signal power spectra in a form of strong spectral peaks, located usually in...
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Problem of proper decomposition and initialization of acoustic and entropy modes in a gas affected by the mass force
PublikacjaThe relations connecting perturbations specific for acoustic and entropy modes in an accelerated fluid or in a fluid affected by constant mass force, are derived. They allow to decompose the total vector of perturbations and the overall energy into acoustic and non-acoustic parts uniquely at any instant. In order to do this, three quantities are required, for example total perturbations in entropy, pressure and velocity. The evaluations...
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Mass spectrometric identification of 13C-Labeled metaboloites during anaerobic propanoic acid oxidation
PublikacjaBiowaste digestion is a possibility to gain biogas as a renewable fuel source. However, the anaerobic food chain may be disrupted by, e.g., substrate overload or by inhibitors, leading to the accumulation of volatile fatty acids (VFAs), predominantly of propanoic acid (PA). VFA Accumulation may cause a rapid pH decrease, less biogas production, or even a total inhibition. To maintain high biogas productivity or to prevent a collapse...
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Troubleshooting of the determination of bisphenol A at ultra-trace levels by liquid chromatography and tandem mass spectrometry
PublikacjaDetermination of trace amounts of bisphenol A (BPA) may cause problems mainly related to the presence of BPA in solvents (even in LC-MS grade), laboratory vessels, and plastic equipment used for sample preparation. Variable and sometimes significant amounts of BPA present in the background cause problems in obtaining good repeatability of measurements at the ultra-trace levels. Such observations (i.e., poor repeatability of results)...
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Opracowanie koncepcji oraz programów pilotowych modyfikacji mapy optymalnych prędkości obrotowych wrzeciona
PublikacjaPodczas obróbki przedmiotów o małych gabarytach, dobór najbardziej korzystnej prędkości obrotowej wrzeciona w trakcie obróbki, jest realizowany na podstawie uogólnionego warunku Liao-Younga. Częstotliwość drgań samowzbudnych typu chatter może być różna dla różnych punktów powierzchni obrabianej. Dlatego tworzona jest mapa optymalnych prędkości obrotowych. W przypadku obrabiania przedmiotów ponadgabarytowych, wspomniana wcześniej...
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Direct Analysis of Samples of Various Origin and Composition Using Specific Types of Mass Spectrometry
PublikacjaOne of the major sources of error that occur during chemical analysis utilizing the more conventional and established analytical techniques is the possibility of losing part of the analytes during the sample preparation stage. Unfortunately, this sample preparation stage is required to improve analytical sensitivity and precision. Direct techniques have helped to shorten or even bypass the sample preparation stage; and in this...
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Development of chromatographic and mass spectrometry conditions for untargeted lipidomic analysis of human breast milk
PublikacjaHuman breast milk (HBM) is a complex biofluid containing components which are essential for the proper growth of the newborn (for example nutrients such as carbohydrates, proteins, lipids) and also bioactive substances. According to the literature, most of studies involving HBM nutrients investigations focused essentially on the determination of proteins. The molecular composition of lipids in HBM is not well known as the protein...
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Nonlinear planar modeling of massive taut strings travelled by a force-driven point-mass
PublikacjaThe planar response of horizontal massive taut strings, travelled by a heavy point-mass, either driven by an assigned force, or moving with an assigned law, is studied. A kinematically exact model is derived for the free boundary problem via a variational approach, accounting for the singularity in the slope of the deflected string. Reactive forces exchanged between the point-mass and the string are taken into account via Lagrange...
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The impact of mass-media campaigns on physical activity: a review of reviews through a policy lens
PublikacjaBackground This review of reviews aimed to: (1) summarize the evidence from published reviews on the effectiveness of mass-media campaigns to promote physical activity (PA) or PA-related determinants (intermediate psychological and proximal outcomes) and (2) to identify policy-relevant recommendations related to successful PA campaigns. Methods An extensive literature search was performed on 1 March 2021. Reviews that evaluated...
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Influence of Added Water Mass on Ship Structure Vibration Parameters in Virtual and Real Conditions
PublikacjaModelling of ship structures in a virtual environment is now standard practice. Unfortunately, many engineers forget to consideri the influence of added water on the frequency values and the amplitude of natural vibrations. The article presents the effect of water damping on the frequency values of the individual natural vibration modes. The tests were carried out in two stages. First, the mentioned values were determined using...
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FE studies of quasi-static mass flow in bins: the polar elasto-plastic approach
PublikacjaPrzedstawiono wyniki numerycznej analizy zachowania się materiału sypkiego w silosie podczas przepływu quasi-statycznego. Obliczenia wykonano metodą elementów skończonych na bazie mikropolarnego sprężysto-plastycznego prawa materiałowego.
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Bezpośrednia analiza próbek z wykorzystaniem techniki spektrometrii mas. Cz. I. Rozwiązania metodyczne w zakresie spektrometrii mas umożliwiające bezpośrednią analizę próbek
PublikacjaTechnika spektrometrii mas stanowi jedno z najważniejszych narzędzi analitycznych, wykorzystywanych do identyfikacji, określania struktury chemicznej oraz oznaczania stężeń wielu związków chemicznych. Aby zidentyfikować obecne w próbkach rzeczywistych anality, konieczne jest jednak z reguły ich wstępne rozdzielenie, toteż spektrometry mas pełnią najczęściej rolę detektora np. w przypadku technik łączonych, gdy na etapie rozdzielania...
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Bezpośrednia analiza próbek z wykorzystaniem techniki spektrometrii mas. Cz. II. Technika PTR – MS – ciekawe rozwiązanie metodyczne w zakresie spektrometrii mas
PublikacjaTechnika spektrometrii mas stanowi niezwykle istotne narzędzie badawcze, umożliwiające uzyskanie wielu cennych informacji, dotyczących składu chemicznego wielu próbek rzeczywistych pochodzenia biologicznego, farmaceutycznego i spożywczego. Spektrometr mas zazwyczaj pełni role detektora w przypadku stosowania połączenia z urządzeniami chromatograficznymi (GC, LC). Dzięki zastosowaniu pewnych modyfikacji aparaturowych i metodycznych,...
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Effects of safety barrier life cycle cost factors - identification and analysis
PublikacjaThe costs borne by road infrastructure authorities for managing and maintaining road devices such as safety barriers may be very high. This has prompted the need for identifying and analysing in detail all factors that influence the costs of safety barriers throughout their service life. To meet that need, the authors used international experience and field data collected under the LifeRoSE project to define the cost structure...
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Effect of Overloaded Vehicles on Whole Life Cycle Cost of Flexible Pavements
PublikacjaThe phenomenon of vehicle overloading—illegal exceeding of maximum legal weight of vehicles, is a serious problem both in developing and developed countries around the world. Overloaded vehicles occur less frequently in comparison to properly loaded vehicles but due to their greater potential to cause damage they significantly contribute to distress of pavement structure. As studies show, the number of overloaded vehicles increases...
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Diclofenac Alters the Cell Cycle Progression of the Green Alga Chlamydomonas reinhardtii
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Neural Network Application for Recognition of Geometry Degradation of Power Cycle Components
PublikacjaPrzedyskutowano problem rozpoznawania degradacji geometrycznej. Skuteczne zastosowanie wybranego typu sieci neuronowej (SSN) jest prezentowane w referacie. SSN wykrywająca typy degradacji geometrycznej wykazała wysoką jakość. Pokazano pewną możliwość ekstrapolacji takich SSN. Pokazano możliwość wykrywania typów degradacji geometrycznej nawet w przypadku pozyskiwania niepełnych danych pomiarowych.
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Toxicity of cylindrospermopsin in human lymphocytes: Proliferation, viability and cell cycle studies
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THERMODYNAMIC ANALYSIS OF A GENERATION IV SCWR NUCLEAR POWER PLANT CYCLE
PublikacjaThis article presents a flow and thermodynamic analysis of a Generation IV nuclear cycle. An SCWR (Supercritical water reactor) is a high temperature and high pressure reactor that uses water at a temperature above its thermodynamic critical point as the working fluid. The cycle used for the calculations consists of one interstage superheater and 7 regenerative heat exchangers. Division pressure was optimized in view of the cycle efficiency,...
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A space-efficient algorithm for computing the minimum cycle mean in a directed graph
PublikacjaAn algorithm is introduced for computing the minimum cycle mean in a strongly connected directed graph with n vertices and m arcs that requires O(n) working space. This is a considerable improvement for sparse graphs in comparison to the classical algorithms that require O(n^2) working space. The time complexity of the algorithm is still O(nm). An implementation in C++ is made publicly available at http://www.pawelpilarczyk.com/cymealg/.
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Exploration of Creativity Techniques in Software Engineering in Training-Application-Feedback Cycle
PublikacjaCreativity research has proposed about a hundred and fifty creativity techniques. The question is whether they can be applied in software engineering for creativity training or directing creativity in software projects. This paper aims at answering this question via a quasi-experiment conducted in Training-Application-Feedback cycle in which participants express their opinions about selected creativity techniques after training...
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Mechanical exfoliation and layer number identification of single crystal monoclinic CrCl3
PublikacjaAfter the recent finding that CrI3, displays ferromagnetic order down to its monolayer, extensive studies have followed to pursue new two-dimensional (2D) magnetic materials. In this article, we report on the growth of single crystal CrCl3 in the layered monoclinic phase. The system after mechanical exfoliation exhibits stability in ambient air (the degradation occurs on a time scale at least four orders of magnitude longer than...
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Functional properties of Cornelian cherry (Cornus mas L.): a comprehensive review
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Technika spektrometrii mas rozcieńczenia izotopowego (IDMS) w analityce chemicznej.
PublikacjaOpisano podstawy teoretyczne techniki spektrometrii mas rozcieńczenia izotopowego. Przedstawiono zalety i wady techniki oraz obszar jej zastosowań.
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Procedura dopuszczenia do eksploatacji maszyn do produkcji mas bitumicznych
PublikacjaW treści artykułu przedstawiono procedury postępowania przy uruchamianiu masbitumicznych. Ponadto opisano wymogi bhp na terenie wytwórni wraz z przeglą-dem aktualnym przepisów związanych z ochroną środowiska w tym odpadami pow-stającymi podczas produkcji, poziomu hałasu w środowisku maszyny i substan-cji zanieczyszczających powietrze.
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Tworzenie map konceptów dla ontologii opartych na logice opisowej
PublikacjaW poprzednich pracach przedstawiono nową metodę reprezentacji wiedzy nazwaną metodą kartograficzną. Metoda ta pozwala na uchwycenie zależności pomiędzy pojęciami wyznaczonymi w ramach terminologii, jak również na stopniowe (w miarę zwiększania się naszej wiedzy) przyporządkowywanie indywidualnych obiektów tym pojęciom. Zależności te reprezentowane są w postaci tzw. mapy konceptów. Efektywność budowy mapy konceptów stanowi zagadnienie...
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TWORZENIE MAP SIECI KOMPUTEROWYCH Z WYKORZYSTANIEM PROTOKOŁÓW TYPU LLDP
PublikacjaDla administratorów systemów sieciowych niezwykle istot-nym jest posiadanie narzędzia tworzącego dynamicznie mapę sieci do celów zarządzania, diagnostyki, zapobiegania awariom i włamaniom. Artykuł prezentuje protokoły wspierające tworzenie map sieci a także własne badania nad usprawnieniem istniejących algorytmów. Proponowane rozwiązania to: budowa map z użyciem protokołu LLDP i SNMP, odkrywanie wąskich gardeł w sieciach dzięki...
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Prediction of CO2 emissions of a car using the discrete map of the operating conditions
PublikacjaW pracy przedstawiono propozycję opisu warunków eksploatacji pojazdów w wybranej aglomeracji miejskiej z użyciem dyskretnej mapy warunków eksploatacji. Mapa taka umożliwia prognozowanie wybranych parametrów eksploatacyjnych pojazdów dla przyjętych dróg przejazdu oraz różnych jednostek napędowych. Głównymi parametrami wyznaczanymi z użyciem dyskretnej mapy warunków eksploatacji są: całkowita energia przeznaczana do napędu wybranego...
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Deep Features Class Activation Map for Thermal Face Detection and Tracking
PublikacjaRecently, capabilities of many computer vision tasks have significantly improved due to advances in Convolutional Neural Networks. In our research, we demonstrate that it can be also used for face detection from low resolution thermal images, acquired with a portable camera. The physical size of the camera used in our research allows for embedding it in a wearable device or indoor remote monitoring solution for elderly and disabled...
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Main strategies, analytical trends and challenges in LC-MS and ambient mass spectrometry-based metabolomics
PublikacjaA plethora of analytical LC-MS-based methods have been successfully applied to analyses of complex samples of various origin for metabolomics investigations. Over the last ten years, the substantial evolution of ambient mass spectrometry (AMS) techniques has highlighted their tremendous potential in metabolomic studies due to the minimal sample pretreatment requirement and the ability to analyse samples in their native state. This...
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Human sperm proteins identified by 2-dimensional electrophoresis and mass spectrometry and their relevance to a transcriptomic analysis
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A twin study of heritability of plasma lipoprotein-associated phospholipase A2 (Lp-PLA2) mass and activity
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Does Mass Culture Mean a Crisis of Values? Dwight Macdonald's Position and the Issue of Its Topicality
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Towards enhanced heat and mass exchange in adsorption systems: The role of AutoML and fluidized bed innovations
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Perspective Chapter: Reducing the Social Inequality Gaps in Older Ages in Low- and Middle-Income Countries
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THIRD-ORDER EXPONENTIAL INTEGRATOR FOR LINEAR KLEIN–GORDON EQUATIONS WITH TIME AND SPACE-DEPENDANT MASS
PublikacjaAllowing for space- and time-dependance of mass in Klein–Gordon equations re- solves the problem of negative probability density and of violation of Lorenz covariance of interaction in quantum mechanics. Moreover it extends their applicability to the domain of quantum cosmology, where the variation in mass may be accompanied by high oscillations....
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THIRD-ORDER EXPONENTIAL INTEGRATOR FOR LINEAR KLEIN–GORDON EQUATIONS WITH TIME AND SPACE-DEPENDANT MASS
PublikacjaAllowing for space- and time-dependance of mass in Klein–Gordon equations re- solves the problem of negative probability density and of violation of Lorenz covariance of interaction in quantum mechanics. Moreover it extends their applicability to the domain of quantum cosmology, where the variation in mass may be accompanied by high oscillations....
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Metabolomic Heterogeneity of Urogenital Tract Cancers Analyzed by Complementary Chromatographic Techniques Coupled with Mass Spectrometry
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Classification of Thyroid Tumors Based on Mass Spectrometry Imaging of Tissue Microarrays; a Single-Pixel Approach
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Discrimination of normal oral mucosa from oral cancer by mass spectrometry imaging of proteins and lipids
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Collaborative planning? Not yet seen in Poland. Identifying procedural gaps in the planning system 2003–2023
PublikacjaCollaborative planning aims to increase the legitimacy of decision-making in spatial development. In this approach, planning involves debate and engagement in discourse, and participation and interaction between actors are thus at the heart of the planning process. This article examines whether the planning system in Poland as defined for the period 2003–2025 provides a level of participation and deliberation and other qualities...
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Mass spectrometry reveals the presence of specific set of epigenetic DNA modifications in the Norway spruce genome
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MARS - BAZA. warsztaty pozaziemskiej architektury ekstremalnej. Warsztaty w ramach Bałtyckiego Festiwalu Nauki
PublikacjaJak przetrwać w różnych warunkach? Czego potrzebujemy, by przeżyć, a czego, by żyć wygodnie? Poszukamy odpowiedzi na te pytania, by stanąć przed nie lada misją: wspólnie podejmiemy się największego wyzwania przyszłości - zbudujemy bazę na Marsie! Budowa schronienia, bazy, domu - troska o zaspokojenie podstawowych potrzeb towarzyszy nam od zawsze, a budowanie jest jednym z pierwszych trwałych działań ludzi, pomagającym spełnić...
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Determination of high-intensity sweeteners in beverages by high-performance liquid chromatography with mass spectrometry detection.
PublikacjaThe objective of the present study was to measure the concentration of nine high intensity sweeteners (acesulfame-K, aspartame, alitame, cyclamate, dulcin, neohesperidin dihydrochalcon, neotame, saccharin and sucralose) in different types of beverages available on the polish market. The proposed methodology reported here consists of a extraction with buffer composed of formic acid and N,N-diisopropylethylamine (pH 4.5) followed...
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Determination of isoprostanes in exhaled breath condensate samples by liquid chromatography coupled with tandem mass spectrometry
PublikacjaOxidative stress (OS) is a state of imbalance between continuously generating reactive oxygen species (ROS) during normal cell metabolism and mechanism of detoxifying oxygen radicals through a network of antioxidative enzymes. Isoprostanes are prostaglandin -like substances that are produced in vivo primarily by free radical-induced peroxidation of arachidonic acid. The measurement of isoprostanes in biological fluids and/or tissue...
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Role of nitrogen in optical and electrical band gaps of hydrogenated/hydrogen free carbon nitride film
PublikacjaWe report the optical and electrical band gap energy of amorphous hydrogenated carbon nitride (a-HCNx) and carbon nitride (a-CNx) as a function of nitrogen concentration (N/C). The optical band gap of a-HCNx and a-CNx films has been determined by means of Ellipsometry and UV-VIS. Both optical and electrical band gaps increase with elevated nitrogen concentration. Experimentally obtained electrical band gap is compared with the...
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Comprehensive methodology for Staphylococcus aureus lipidomics by liquid chromatography and quadrupole time-of-flight mass spectrometry
PublikacjaStaphylococcus aureus is a common pathogen known to cause relatively minor infections as well as severe disorders in humans. Although there is fair amount of published data concerning various aspects of its biology, epidemiology, genetics, etc., there is still a scarce amount of data presenting reliable and thorough investigations regarding high-throughput analysis of total S. aureus lipid content. Therefore, the aim of this study...
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A method of self-testing of analog circuits based on fully differential op-amps with theTCBF classifier
PublikacjaA new approach of self-testing of analog circuits based on fully differential op-amps of mixed-signal systems controlled by microcontrollers is presented. It consists of a measurement procedure and a fault diagnosis procedure. We measure voltage samples of a time response of a tested circuit on a stimulation of a unit step function given at the common-mode reference voltage input of the op-amp. The fault detection and fault localization...