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Standing Waves and Acoustic Heating (or Cooling) in Resonators Filled with Chemically Reacting Gas
PublikacjaStanding waves and acoustic heating in a one-dimensional resonator filled with chemically reacting gas, is the subject of investigation. The chemical reaction of A ! B type, which takes place in a gas, may be reversible or not. Governing equations for the sound and entropy mode which is generated in the field of sound are derived by use of a special mathematical method. Under some conditions, sound waves propagating in opposite...
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Propagation of initially sawtooth periodic and impulsive signals in a quasi-isentropic magnetic gas
PublikacjaThe characteristics of propagation of sawtooth periodic and impulsive signals at a transducer are analytically studied in this work. A plasma under consideration is motionless and uniform at equilibrium, and its perturbations are described by a system of ideal magnetohydrodynamic equations. Some generic heating/cooling function, which in turn depends on equilibrium thermodynamic parameters, may destroy adiabaticity of a flow and...
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Impact of Boundary Conditions on Acoustic Excitation of EntropyPerturbations in a Bounded Volume of Newtonian Gas
PublikacjaExcitation of the entropy mode in the field of intense sound, that is, acoustic heating, is theoreticallyconsidered in this work. The dynamic equation for an excess density which specifies the entropy mode,has been obtained by means of the method of projections. It takes the form of the diffusion equation withan acoustic driving force which is quadratically nonlinear in the leading order. The diffusion coefficient isproportional...
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Gas Turbine Cycle with External Combustion Chamber for Prosumer and Distributed Energy Systems
PublikacjaThe use of various biofuels, usually of relatively small Lower Heating Value (LHV), affects the gas turbine efficiency. The present paper shows that applying the proposed air by-pass system of the combustor at the turbine exit causes tan increase of efficiency of the turbine cycle increased by a few points. This solution appears very promising also in combined gas/steam turbine power plants. The comparison of a turbine set operating...
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Inlet air fogging of marine gas turbine in power output loss compensation
PublikacjaThe use of inlet air fogging installation to boost the power for gas turbine engines is widely applied in the power generation sector. The application of fogging to mechanical drive is rarely considered in the literature [1]. This paper will cover some considerations relating to its application to gas turbines in ship drive. There is an important evaporative cooling potential throughout the world when the dynamic data is evaluated,...
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Radioisotope measurements of the liquid-gas flow in the horizontal pipeline using phase method
PublikacjaThe paper presents application of the gamma-absorption method to a two-phase liquid-gas flow investigation in a horizontal pipeline. The water-air mixture was examined by a set of two Am-241 radioactive sources and two NaI(Tl) scintillation probes. For analysis of the electrical signals obtained from detectors the cross-spectral density function (CSDF) was applied. Results of the gas phase average velocity measurements for CSDF...
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Decomposition of Acoustic and Entropy Modes in a Non-Isothermal Gas Affected by a Mass Force
PublikacjaDiagnostics and decomposition of atmospheric disturbances in a planar flow are considered in this work. The study examines a situation in which the stationary equilibrium temperature of a gas may depend on the vertical coordinate due to external forces. The relations connecting perturbations are analytically established. These perturbations specify acoustic and entropy modes in an arbitrary stratified gas affected by a constant...
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Balance of pesticides mass in gas, liquid and solid phase after their chemical degradation.
PublikacjaOpisano metodę usuwania pestycydów z wody przy zastosowaniu fotodegradacji (UV) i katalizatora (TiO2). Efektywność procesu usuwania pestycydów była kontrolowana przy zastosowaniu chromatografu gazowego z detektorem wychwytu elektronów. Oznaczano zawartość pestycydów w wodzie, a także zaadsorbowanych na powierzchni stałej, oraz w fazie gazowej. Największa zawartość pestycydów znajdowała się na fazie stałej, następnie w cieczy i...
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Piecewise continuous distribution function method in the theory of wave disturbances of inhomogeneous gas
PublikacjaUkład równań typu hydrodynamicznego dla warstwowych gazów w polu grawitacyjnym pochodzi od równania BGK metodą częściowej ciągłej funkcji dystrybucji. Otrzymany system równań uogólnia układ Naviera-Stokesa w dowolnych liczbach Knudsena.
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UV-Light-Induced Fluctuation Enhanced Sensing by WO3-Based Gas Sensors
PublikacjaWO3-based gas sensors were investigated under UV-light irradiation and at different working temperatures with the object of achieving superior sensitivity and selectivity. Resistance fluctuations in the WO3 layer were studied together with dc resistance measurements. The data were taken in synthetic air, ethanol, nitrogen dioxide, and mixtures of these gases. We conclude that UV irradiation can easily be applied to enhance the...
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Nickel Oxide Thin Film Sensor for Fluctuation-Enhanced Gas Sensing of Formaldehyde
PublikacjaNanocrystalline nickel-oxide-based thin films were prepared by advanced reactive gas deposition, and the response of these films to formaldehyde was studied by fluctuationenhanced sensing. Morphological and structural analyses showed porous deposits of nickel oxide particles with face-centered cubic structure. Resistance fluctuations were measured upon exposure to ethanol, formaldehyde and methane at 200 °C. Power density spectra...
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Fluctuation-enhanced and conductometric gas sensing with nanocrystalline NiO thin films: A comparison
PublikacjaNanocrystalline thin films of NiO were prepared by advanced reactive gas deposition, and their responses to formaldehyde, ethanol and methane gases were studied via fluctuation-enhanced and conductometric methods Thin films with thicknesses in the 200–1700-nm range were investigated in as-deposited form and after annealing at 400 and 500 °C. Morphological and structural analyses showed porous deposits with NiO nanocrystals having...
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The role of centrifugal partition chromatography in the removal of β-asarone from Acorus calamus essential oil
PublikacjaΒ-asarone is a phenylpropane derivative present in the rhizomes of Acorus calamus, that was proved to exhibit toxic effects in humans. Because of its presence the whole plant that is commonly used in traditional medicine for its sedative, anti-inflammatory, neuroprotective and other properties has limited application nowadays. In the study, qualitative and quantitative analysis of a collection of nine essential oil (EO) samples...
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The application of gradient reversed-phase high-performance liquid chromatography to the pKa and determination of polyprotic analytes
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The study of salting-out thin-layer chromatography and their application on QSRR/QSAR of some macrolide antibiotics
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Quantitative determination of diazepam, nitrazepam and flunitrazepam in tablets using thin-layer chromatography–densitometry technique
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Comprehensive methodology for Staphylococcus aureus lipidomics by liquid chromatography and quadrupole time-of-flight mass spectrometry
PublikacjaStaphylococcus aureus is a common pathogen known to cause relatively minor infections as well as severe disorders in humans. Although there is fair amount of published data concerning various aspects of its biology, epidemiology, genetics, etc., there is still a scarce amount of data presenting reliable and thorough investigations regarding high-throughput analysis of total S. aureus lipid content. Therefore, the aim of this study...
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Solid phase microextraction combined with chromatography - a powerful tool for determination of warfare agents and related compounds
PublikacjaOpisano zastosowanie mikroekstrakcji do fazy stacjonarnej do izolacji wzbogacania środków bojowych i produktów ich degradacji w powietrzu, wodzie i glebie oraz próbkach bilogicznych. Na etapie oznaczeń końcowych stosuje się najczęściej chromatografię gazową. Anality można pobierać przez bezpośrednie zanurzenie włókna w próbce ciekłej i gazowej oraz w fazie nadpowierzchniowej. Stosując SPME-GC można osiągnąć niskie granice oznaczalności...
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The Analysis of the distribution of available mesopores in cellulosic pulp, using Inverse Size Exclusion Chromatography-ISEC
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Application of chiral chromatography for enantiomeric separation of currently used pesticides from various chemical groups
PublikacjaChiral pesticides account for more than 25 % of currently used pesticides and this ratio is still increasing. According to the number of chiral centers in the structure, a pesticide may consist of two or multiple enantiomers or stereoisomers. Studies into the stereoselective behaviour of pesticides started in the early 1990s and most research efforts focused on understanding the environmental fate and effects of these pesticides....
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A chromatography-free total synthesis of a ferrocene-containing dendrimer exhibiting the property of recognizing 9,10-diphenylanthracene
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The lipophilicity indices of flavonoids estimated by reversed-phase liquid chromatography using different computation methods
PublikacjaDo oceny właściwości chromatograficznych wybranych flawonoidów zastosowano wyskokosprawną chromatografię cieczową z odwróconym układem faz i kolumnami chromatograficznymi typu C-8 i C-18.Lipofilowość wyrażono za pomocą różnych deskryptów lipofilowości.
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Lipophilicity data for some preservatives estimated by reversed-phase liquid chromatography and different copmutation methods
PublikacjaW pracy przedstawiono wyniki badań właściwości chromatograficznych wybranych 12 związków z grupy kopnserwantów. Lipofilowy charakter tych związków był oceniany na podtsawie różnych parametrów retencyjnych (log Kw, log K i inne. Zastosowano narzędzie chemometryczne do zbadania korelacji występujących pomiędzy tymi parametrami retencji chromatogfraficznej.
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Determination of high-intensity sweeteners in beverages by high-performance liquid chromatography with mass spectrometry detection.
PublikacjaThe objective of the present study was to measure the concentration of nine high intensity sweeteners (acesulfame-K, aspartame, alitame, cyclamate, dulcin, neohesperidin dihydrochalcon, neotame, saccharin and sucralose) in different types of beverages available on the polish market. The proposed methodology reported here consists of a extraction with buffer composed of formic acid and N,N-diisopropylethylamine (pH 4.5) followed...
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Determination of isoprostanes in exhaled breath condensate samples by liquid chromatography coupled with tandem mass spectrometry
PublikacjaOxidative stress (OS) is a state of imbalance between continuously generating reactive oxygen species (ROS) during normal cell metabolism and mechanism of detoxifying oxygen radicals through a network of antioxidative enzymes. Isoprostanes are prostaglandin -like substances that are produced in vivo primarily by free radical-induced peroxidation of arachidonic acid. The measurement of isoprostanes in biological fluids and/or tissue...
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A research on the optimal conditions for separation and identyfication of the components from the Droseraceae extracts by column liquid chromatography
PublikacjaThe isolation of the components with anticipated biological properties i.e. antimicrobial, fungicidal, antioxidant and perhaps anticancer activity is for many years a one of the biggest issues of modern separation science. Their obtaining based on the isolation of the components with the biological activity from in vitro cultured plants by extraction techniques is often more difficult than their production by the chemical synthesis.The...
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Assessment of blood–brain barrier permeability using micellar electrokinetic chromatography and P_VSA-like descriptors
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Determination of polyphenolics in extracts of Potentilla species by high‐performance thin‐layer chromatography photodensitometry method
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High-performance liquid chromatography in group-type separation and technical or process analytics of petroleum products
PublikacjaW pracy dokonano przeglądu i poddano krytycznej ocenie metody oznaczania składu grupowego produktów naftowych o różnej lotności, zarówno metody znormalizowane, jak i opisane w literaturze naukowej. W zdecydowanej większości są to metody wykorzystujące technikę chromatografii cieczowej w układzie faz normalnych (NP-HPLC). Na podstawie danych z literatury oraz własnych studiów i badań należy stwierdzić, że im wyższy zakres temperatury...
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Uncertainty of antioxidant profiling in complex mixtures using liquid chromatography involving post-column derivatisation
PublikacjaThe main goal of this paper is to discuss the problems associated with antioxidant profiling in complex samples using a high-throughput HPLC system coupled with post-column derivatisation reactor. Based on the experimental data reported in the literature, we demonstrated that improper optimisation of temperature and/or pH assay conditions performed using an on-line derivatisation reactor may substantially change the antioxidant...
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Study of pH and temperature effect on lipophilicity of catechol-containing antioxidants by reversed phase liquid chromatography
PublikacjaLipophilicity of selected antioxidant phytochemicals, including flavonoids, phenolic acids and xanthonoids, was determined by reversed phase high performance liquid chromatography with UV detection (RP-HPLC-UV). The analyses run at different temperature and pH conditions in isocratic mode suggested that lipophilicity as distribution coefficient (logD) between aqueous and organic phase decreases with increasing temperature. For...
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Optimization of liquid chromatographic separation of pharmaceuticals within green analytical chemistry framework
PublikacjaThe contribution is aimed at the development of methodology that allows to consider green analytical chemistry criteria during optimization of liquid chromatographic separation with design of experiment. The objectives of the optimization are maximization of peak areas of five non-steroid anti-inflammatory drugs, maximization of resolution between peaks, with simultaneous shortening of chromatographic separation time and minimization...
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New supervised alignment method as a preprocessing tool for chromatographic data in metabolomic studies
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Matrix solid-phase dispersion with sand in chromatographic analysis of essential oils in herbs
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Chromatographic behaviour of ionic liquid cations in view of quantitative structure-retention relationship
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Solid-phase microextraction and ion chromatographic analysis of anions based on polypyrrole electrode
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Classification and fingerprinting of kiwi and pomelo fruits by multivariate analysis of chromatographic and spectroscopic data
PublikacjaThe fingerprinting capacity of two analytical techniques, HPLC and UV-Vis spectroscopy in the case of fruits samples (kiwi and pomelo) has been investigated. The multivariate exploratory techniques were used for sample discrimination according to the fruit species and subspecies. The combination of principal component analysis with linear discriminant analysis is opening new directions in the fingerprinting analysis. The classifications...
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Integration of inertial sensors and GPS system data for underwater navigation
PublikacjaThe Inertial Navigation System (INS) is usually employed to determine the position of an underwater vehicles, like Remotely Operated Vehicles (ROV) and, more recently, Autonomous Underwater Vehicle (AUV). The accuracy of the position provided by the INS, which uses accelerometers and gyroscopes, deteriorates with time. An external aiding sources such as the Global Positioning System (GPS) can be employed to reduce the error growth...
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Electrical responses of nanoporous NiO films for light-activated nitrogen dioxide and acetone gas sensing
Dane BadawczeThe chemoresistive sensor response of nanoporous NiO films prepared by advanced gas deposition was investigated with and without simultaneous light irradiation, to detect nitrogen dioxide and acetone gases. The presented data show electrical responses presented as sensor resistance or relative changes in sensor resistance under selected environment...
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FTIR spectra of gas mixtures from the process of biogas dry reforming using CLO catalyst
Dane BadawczeThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using Ce0.8La0.2O2 nanocatalyst. The specatra were collected every 1 minute.
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FTIR spectra of gas mixtures from the methanation chamber filled with 50-50wt.% NiO-Al2O3
Dane BadawczeThe dataset includes the FTIR spectra collection of the outlet gas mixtures (CO2, CO, CH4) from reactor chamber filled with 50/50 wt.% NiO-Al2O3 catalyst for perfoming methanation reaction. The inlet gas mixture was composed of 3:1 by vol. H2:CO. Spectra were collected using PerkinElmer FTIR every 1 min.
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FTIR spectra of gas mixtures from the methanation chamber filled with 25-75wt.% NiO-Al2O3
Dane BadawczeThe dataset includes the FTIR spectra collection of the outlet gas mixtures (CO2, CO, CH4) from reactor chamber filled with 25/75 wt.% NiO-Al2O3 catalyst for perfoming methanation reaction. The inlet gas mixture was composed of 3:1 by vol. H2:CO. Spectra were collected using PerkinElmer FTIR every 1 min.
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FTIR spectra of gas mixtures from the methanation chamber filled with 50-50wt.% NiO-GDC
Dane BadawczeThe dataset includes the FTIR spectra collection of the outlet gas mixtures (CO2, CO, CH4) from reactor chamber filled with 50/50 wt.% NiO-GDC (Gadolinia Doped Ceria 20mol.%Gd2O3) catalyst for perfoming methanation reaction. The inlet gas mixture was composed of 3:1 by vol. H2:CO. Spectra were collected using PerkinElmer FTIR every 1 min.
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On the possible increasing of efficiency of ship power plant with the system combined of marine diesel engine, gas turbine and steam turbine in case of main engine cooperation with the gas turbine fed in parallel and the steam turbine
PublikacjaW pracy przedstawiono koncepcję układu kombinowanego okrętowego dużej mocy złożonego z wiodącego silnika głównego spalinowego silnika tłokowego i skojarzonych z nim turbiny gazowej mocy i układu turbiny parowej, wykorzystujących energię zawartą w spalinach wylotowych głównego silnika spalinowego. Rozpatrzono wariant układu kombinowanego, w którym główny jest silnik tłokowy skojarzony z turbiną gazową mocy i układem turbiny parowej,...
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On the possible increasing of efficiency of ship power plant with the system combined of marine diesel engine, gas turbine and steam turbine in case of main engine cooperation with the gas turbine fed in series and the steam turbine
PublikacjaW pracy przedstawiono koncepcję układu kombinowanego okrętowego dużej mocy złożonego z wiodącego silnika głównego silnika spalinowego tłokowego oraz skojarzonych z nim turbiny gazowej mocy i układu turbiny parowej, wykorzystujących energię zawartą w spalinach wylotowych silnika spalinowego. Rozpatrywano wariant układu kombinowanego, którym turbina mocy jest zasilana szeregowo spalinami wylotowymi. Podano algorytm i obliczenia...
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Waste management in the mining industry of metals ores, coal, oil and natural gas - A review
PublikacjaWaste generated due to mining activity poses a serious issue due to the large amounts generated, even up to 65 billion tons per year, and is often associated with the risk posed by its storage and environmental management. This work aims to review waste management in the mining industry of metals ores, coal, oil and natural gas. It includes an analysis and discussion on the possibilities for reuse of certain types of wastes generated...
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Effects of UV light irradiation on fluctuation enhanced gas sensing by carbon nanotube networks
PublikacjaThe exceptionally large active surface-to-volume ratio of carbon nanotubes makes it an appealing candidate for gas sensing applications. Here, we studied the DC and low-frequency noise characteristics of a randomly oriented network of carbon nanotubes under NO2 gas atmosphere at two different wavelengths of the UV light-emitting diodes. The UV irradiation allowed to sense lower concentrations of NO2 (at least 1 ppm) compared to...
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Design and computational fluid dynamics analysis of the last stage of innovative gas-steam turbine
PublikacjaResearch regarding blade design and analysis of flow has been attracting interest for over a century. Meanwhile new concepts and design approaches were created and improved. Advancements in information technologies allowed to introduce computational fluid dynamics and computational flow mechanics. Currently a combination of mentioned methods is used for the design of turbine blades. These methods enabled us to improve flow efficiency...
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Magnetoacoustic Heating of Plasma Caused by Periodic MagnetosoundPerturbations with Discontinuities in a Quasi-Isentropic Magnetic Gas
PublikacjaThe magnetoacoustic heating of plasma by harmonic or periodic saw-tooth perturbations at a trans-ducer is theoretically studied. The planar fast and slow magnetosound waves are considered. The wavevector may form an arbitrary angleθwith the equilibrium straight magnetic field. In view of variableθand plasma-β, the description of magnetosound perturbations and appropriate magnetosound heatingis fairly difficult. The scenario of...
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Signals Features Extraction in Radioisotope Liquid-Gas Flow Measurements using Autocorrelation Function
PublikacjaKnowledge of the two-phase flow structure is essential for the proper conduct of industrial processes. Description of liquid-gas flow regimes is possible by using of data analysis in time, frequency, or state-space domain. In this research studies, the autocorrelation function is applied for analysis of signals obtained for liquid-gas flow by use gamma-ray absorption. The experiments were carried out on the laboratory hydraulic...