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Spectroscopy properties of 1,8-diazafluoren-9-one (DFO) in PVA polymer for different concentrations
Dane BadawczeSpectroscopy properties: absorption and fluorescence spectra of 1,8-diazafluoren-9-one (DFO) in PVA film for different concentrations of dye.
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Quantification of unconjugated and total ibuprofen and its metabolites in equine urine samples by gas chromatography–tandem mass spectrometry: Application to the excretion study
PublikacjaIbuprofen (IBU) is a widely used nonsteroidal anti-inflammatory drug (NSAID) in human and also veterinary medicine. NSAIDs are usually highly metabolized compounds in horses; they are often present in equine urine, mostly in their conjugated forms (glucuronides). Thus, hydrolysis to cleave the glucuronide linkage prior to anti-doping analysis is often necessary for improving detection. In this study, unconjugated and total IBU...
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JOURNAL OF BIOMATERIALS SCIENCE-POLYMER EDITION
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Electrochemical synthesis of 2D copper coordination-polymers: Layer-stacking deviation induced by the solvent and its effect on the adsorptive properties
PublikacjaA 2D Cu-based Metal-Organic Framework (MOF), namely copper-terephthalate (Cu(1,4-BDC)), was successfully synthesized by electrochemical method for effective methylene blue (MB) sorption from aqueous solutions. The composition, morphology, and the presence of functional groups in the obtained material were verified by Fourier Transform Infrared spectroscopy (FTIR), Powder X-Ray Diffraction (PXRD), Thermal (TGA), and Elemental (EA)...
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Lead(II) coordination polymers with imidazole-4- and pyrazole-3-carboxylate isomeric linkers: Structural diversity and luminescence properties
PublikacjaUsing 1H-imidazole-4-carboxylic acid (4imCOOH) and 1H-pyrazole-3-carboxylic acid (3pyrCOOH) coordination polymers [Pb(4imCOO)2(H2O)]n (1) and [Pb2(3pyrCOO)4]n (2) were constructed. Obtained polymers were characterized via FT-IR, X-ray, PL and TG methods. The coordination polyhedron around Pb(II) in 1 is described as distorted pentagonal pyramid with hemidirected coordination sphere (based on DFT calculations). Compound 2 consists...
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Assessing ecotoxicity, synergic and antagonistic actions of commonly used components of polymerization mixture in molecularly imprinted polymers preparation process
PublikacjaIncreasingly, the challenge is the optimal process of developing a suitable MIP-type sorptive material (taking into account its final form and application area), which is mainly related to the efficiency/effectiveness of the polymerization process. The lack of reaction or its low efficiency generates additional waste and puts it into the environmental cycle. The main aim of the performed research was the estimation of ecotoxicity,...
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Paulina Kosmela dr inż.
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Study on Polymer Elements for Mitigation of Earthquake-Induced Pounding Between Buildings in Complex Arrangements
PublikacjaPounding between neighboring structures during seismic events has been revealed as one of the most commonly observed reasons for severe damage or even total collapse of the adjacent buildings. Therefore, pounding effects have recently become an issue of great interest of many numerical and experimental investigations in many earthquake-prone regions of the world. It has also been observed that the differences in dynamic characteristics...
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Potential applications of by-products from the coffee industry in polymer technology – Current state and perspectives
PublikacjaCoffee is one of the most popular beverages in the world, and its popularity is continuously growing, which can be expressed by almost doubling production over the last three decades. Cultivation, processing, roasting, and brewing coffee are known for many years. These processes generate significant amounts of by-products since coffee bean stands for around 50% of the coffee cherry. Therefore, considering the current pro-ecological...
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How Chain Transfer Leads to a Uniform Polymer Particle Morphology and Prevents Reactor Fouling
PublikacjaABSTRACT: The effect of adding diethyl zinc as a chain transfer agent during the polymerization of propylene in heptane performed at 80 °C was studied. Although it was expected that the chain transfer would stop after precipitation of the polymer, the polymer molecular weight continued to increase throughout the whole of the polymerization. The presence of diethyl zinc had an additional effect that the polymerizations were devoid...
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GOOD HEALTH PRODUCTS AND POLYMER COMPOSITES OBTAINED WITH THE USE OF NATURAL ORIGIN MICRO- AND NANOFIBERS
PublikacjaThe aim of this work was focused on good health products and polymer composites obtained with the use of natural origin micro- and nanofibers. Many different type of the natural plants are used in the production of good health products and polymer processing like curcuma, cellulose, microalgae and others. Often are used as a antioxidants and fillers. In this work the effect of algae and cellulose as a microfillers on the chosen...
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Polymer‐silica additive as a modifier of tribological properties of ecological grease, improvement of fatigue resistance
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Tuning the Wettability of a Thin Polymer Film by Gradually Changing the Geometry of Nanoscale Pore Edges
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Spectral profiling of radicals in polymer degradation based on electron spin resonance imaging (ESRI)
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Catalysis on polymer supports: ESR of molybdenum (V) dispersed in poly(acrylic acid) matrices
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Influence of free carbon on the Young's modulus and hardness of polymer‐derived silicon oxycarbide glasses
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Electrochemical study of lithium insertion into carbon-rich polymer-derived silicon carbonitride ceramics
PublikacjaW pracy przedstawiono materiał ceramiczny, bogaty w węgiel krzemo azotek węgla (SiCN), otrzymany na drodze pirolizy w zakresie temperatur od 1100 do 1700°C. Badania elektrochemiczne insercji litu wykazały, że materiał elektrodowy na bazie SiCN może być obiecujący jako anoda w bateriach litowych. Próbka otrzymana w 1300°C cechuje się pojemnością 392 mAh/g i jest stabilna aktywna elektrochemicznie w trakcie interkalacji i deinterkalacji...
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Determination of the Diffusion Coefficient of Lithium Ions in Graphite Coated with Polymer-Derived SiCN Ceramic
PublikacjaPraca dotyczy wyznaczenia wsółczynnik adyfuzji jonów litu w materiale elektrodowym składającym się z grafitu pokrytego materiałem ceramicznym krzemo-azotkiem węgla (SiCN). Wartość współczynnika dyfuzji zmierzono elektrochemicznie technikami: woltamperometrii cyklicznej (CV), elektrochemicznej spektrodkopii impedancyjnej (EIS) oraz miareczkowania galwanostatycznego (GITT). Materiał otrzymano na drodze pirolizy mieszaniny grafit:polimer...
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Morphology of damage inflicted on brittle polymer in lubricated contact under cyclic static load
PublikacjaIn this article morphology of damage inflicted on the polymethylmethacrylate (PMMA) plate in static point lubricated contact with a ball made of five different materials under cyclic normal load has been presented. It is argued that the counterface material and lubricating film play an important role in the damage process and the extent of damage inflicted in the PMMA plate.
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Influence of surface roughness topography on properties of water lubricated polymer bearings, experimental research
PublikacjaW artykule przedstawiono wyniki badań eksperymentalnych, których celem było zidentyfikowanie wpływu ułożenia chropowatości na powierzchni ślizgowej łożyska smarowanego wodą z polimerową panwią. Badania wykazały, że wpływ ten jest mniejszy niż oczekiwano a na własności łożyska ma wpływ głównie wysokość chropowatości.
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Applications of spin coating of polymer precursor and slurrysuspensions for Solid Oxide Fuel Cell fabrication
PublikacjaW pracy przedstawiono możliwości zastosowania w tlenkowych ogniwach paliwowych metody nanoszenia wirowego prekursorów polimerowych i zawiesin. Przedstawiono przykłady zastosowania tej metody do wytworzenia elektrolitu oraz warstw ochronnych dla stali nierdzewnych.
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Polymer membranes loaded with lipids for taste sensing: electrochemical impedance spedance spectroscopy studies
PublikacjaZcharakteryzowano metodą impedancyjnej spektroskopii elektrochemicznej membrany polichlorku winilu z lipidami zanurzone w roztworze kwasu cytrynowego. Badano membrany elektrod dodatnio naładowanych (heksadecyloamina, chlorek, benzyloheksadecylodimetyloamoniowy) i ujemne naładowanych (kwas elaidynowy, cholesterol, l-dodekonol). Badania impedacyjne pozwoliły na rozróznienie czterech stałych czasowych: rezystancja wysokiej częstotliwości,...
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Swelling process investigation of polymer layer deposited on siliceous materials using SAXS method
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Diffusive properties of solvent molecules in the neighborhood of a polymer chain as seen by Monte-Carlo simulations
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Heterogeneity phantoms for visualization of 3D dose distributions by MRI‐based polymer gel dosimetry
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Characterisation of PRESAGE™: A new 3-D radiochromic solid polymer dosemeter for ionising radiation
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Sensitivity calibration procedures in optical‐CT scanning of BANG®3 polymer gel dosimeters
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Degradation and damage of advanced polymer composites due to environmental effects and low velocity impact
PublikacjaPrzedstawiono zagadnienie wpływu srodowiska wody oraz niskoenergetycznego udaru na właściwości mechaniczne laminatów epoksydowych wzmocnionych włóknami węglowymi, szklanymi, aramidowymi i hybrydowymi. Na tle krótkiego przeglądu literatury na dany temat przedstawiono oryginalne wyniki badań eksperymentalnych autorki.
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Raman diagnostics in manufacturing of polymer planar optical waveguides. Optical Fibers and Their Applications VIII.
PublikacjaZastosowano spektroskopię ramanowską do diagnostyki procesu syntezy nowego typu materiałów cienkowarstwowych polimerów hybrydowych, przeznaczonych do wytwarzania światłowodów planarnych. Zbadano poprawność poszczególnych etapów procesu technologicznego oraz strukturę molekularną materiału. Zademonstrowano możliwość kontroli procesu technologicznego w czasie rzeczywistym.
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Advanced super-hydrophobic polymer-based porous absorbents for the treatment of oil-polluted water
PublikacjaThe threat of environmental pollution caused by spilled oil is rapidly increasing along with the expansion of oil exploration, the development of maritime activities and industrial growth. Oil spill incidents usually affect seriously the ecosystem and human life. Therefore, the treatment and recovery of the oil spill have been considered as an ultra-important issue to protect the environment and to minimize its negative impacts...
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Insights into the Thermo-Mechanical Treatment of Brewers’ Spent Grain as a Potential Filler for Polymer Composites
PublikacjaThis paper investigated the impact of twin-screw extrusion parameters on the properties of brewers’ spent grain. The chemical structure, antioxidant activity, particle size, and color properties, as well as the emission of volatile organic compounds during extrusion, were investigated. The main compounds detected in the air during modifications were terpenes and terpenoids, such as α-pinene, camphene, 3-carene, limonene, or terpinene....
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By-Products from Food Industry as a Promising Alternative for the Conventional Fillers for Wood–Polymer Composites
PublikacjaThe present paper describes the application of two types of food-industry by-products, brewers’ spent grain (BSG), and coffee silverskin (ŁK) as promising alternatives for the conventional beech wood flour (WF) for wood–polymer composites. The main goal was to investigate the impact of partial and complete WF substitution by BSG and ŁK on the processing, structure, physicochemical, mechanical, and thermal properties of resulting...
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Recycling of Polyurethanes Containing Flame-Retardants and Polymer Waste Transformed into Flame-Retarded Polyurethanes
PublikacjaThe growing number of polyurethanes (PUs) produced every year has developed methods for their mechanical and chemical recycling which yield valuable products like substitutes for commercial polyols or flame-retardants. PUs can be produced in different shapes and forms (i.e., elastomers, flexible or rigid foams, coatings, etc.) using several different components (i.e., di- or polyisocyanates, ester- or ether-based polyols, low-molecular...
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A facile approach to fabricate load-bearing porous polymer scaffolds for bone tissue engineering
PublikacjaBiodegradable porous scaffolds with oriented interconnected pores and high mechanical are load-bearing biomaterials for bone tissue engineering. Herein, we report a simple, non-toxic, and cost-effective method to fabricate high-strength porous biodegradable scaffolds, composed of a polymer matrix of polycaprolactone (PCL) and water-soluble poly (ethylene oxide) (PEO) as a sacrificial material by integrating annealing treatment,...
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Chitosan/phospholipid coated polyethylene terephthalate (PET) polymer surfaces activated by air plasma
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Characteristics of hybrid chitosan/phospholipid-sterol, peptide coatings on plasma activated PEEK polymer
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Experimental and numerical study on polymer element used for reduction of temporary steel grandstand vibrations
PublikacjaThe purpose of the paper is to analyse the effectiveness of a polymer damper in reduction of a temporary steel grandstand vibrations through the experimental and numerical study. The damper considered in the investigation is constructed out of two L-shape steel members bonded with polymer mass of high damping properties. The element has been installed as a diagonal one at the back part of the structure. The method has been compared...
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Cross-linking of polymer films using phenol-formaldehyde resins with different functional groups
PublikacjaWell-know phenol-formaldehyde resins are used in the production of press-materials, glues, protective coating, mastics. They take a special place among known oligomers because the products based on them are characterized by a low cost and a series of positive properties. Aim of the work: to show the possibility to create polymeric films based on epoxy resins and modified phenol-formaldehyde resins, which contain unsaturated double...
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Experimental investigation of Steel–Concrete–Polymer composite barrier for the ship internal tank construction
PublikacjaTransportation of dangerous cargo by ships demands ensuring an appropriate protection level in case of an accident. Two of the most dangerous accident types resulting in an oil spill are grounding and ship to ship collision. The article presents results of research on a new composite construction for a ship hull that increases structural safety during collision. The concept of semi-elastic Steel–Concrete–Polymer structure is presented....
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Reactive extrusion of bio-based polymer blends and composites – Current trends and future developments
PublikacjaReactive extrusion is a cost-effective and environmentally-friendly method to produce new materials with enhanced performance properties. At present, reactive extrusion allows in-situ polymerization, modification/functionalization of polymers or chemical bonding of two (or more) immiscible phases, which can be carried out on commonly used extrusion lines. Although reactive extrusion has been known for many years, its application...
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Study on polymer elements for mitigation of earthquake-induced pounding between buildings in complex arrangements
PublikacjaPounding between neighbouring buildings during earthquakes has been identified as one of the reasons for substantial damage or even total collapse of colliding structures, so it has been the subject of numerous studies in the recent years. A major reason leading to interactions between adjacent, insufficiently separated structures results from the differences in their dynamic properties. The problem is much more complicated for...
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Experimental and numerical investigation of mercury removal from flue gas by sorbent polymer composite
PublikacjaThis paper presents an experimental and numerical investigation of the performance of a sorbent polymer composite (SPC) material used for removing mercury from the flue gases in a full-scale industrial installation. The investigated material is an attractive alternative to activated carbon, which is commonly used for this purpose. While the application of the SPC is characterized by high capital expenditures, this technology offers...
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Łukasz Piszczyk dr hab. inż.
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On the Equations of the Surface Elasticity Model Based on the Theory of Polymeric Brushes
PublikacjaMotivating by theory of polymers, in particular, by the models of polymeric brushes we present here the homogenized (continual) two-dimensional (2D) model of surface elasticity. A polymeric brush consists of an system of almost aligned rigid polymeric chains. The interaction between chain links are described through Stockmayer potential, which take into account also dipole-dipole interactions. The presented 2D model can be treated...
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Effect of Polymerization Statistics on the Electronic Properties of Copolymers for Organic Photovoltaics
PublikacjaStatistical block copolymers, composed of donor (D) and acceptor (A) blocks, are a novel type of material for organic photovoltaics (OPVs) devices. In particular a new series of polymers based on PBTZT-stat-BDTT-8, recently developed by Merck, offers high solubility in different solvents, and a high power conversion efficiency (PCE) in different device architectures. Although it is known that the electronic properties of these...
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Modeling and Evaluation of Electric Treeing Phenomena in Polymeric Cable Insulation
PublikacjaThis paper investigates the treeing phenomenon in polymeric materials such as crosslinked polyethylene (XLPE) that is widely used in medium and high voltage power cables as primary insulation. The modeling of electrical tree growth in the insulation from its initiation to breakdown is significant research work that illustrates the discharge dynamics and its impact on aging process in polymeric insulation. This study utilizes pulse...
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An analytic approach to the conductance and I-V characteristics of polymeric chains
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Electronic excitation energy migration in partly ordered polymeric films
PublikacjaWieloetapowa migracja energii pomiędzy podłużnymi fluoroforami (karbocyjaniny) w osiowo rozciąganych foliach polimerowych była studiowana na podstawie pomiarów anizotropii emisji i symulacji Monte Carlo. W przeciwieństwie do układów nieuporządkowanych pokazano eksperymentalnie, że stężeniowa depolaryzacja fluorescencji w osiowo orientowanych foliach jest ekstremalnie słaba, mimo tego, że zachodzi zjawisko migracji energii. Opierając...
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Ionophores in polymeric membranes for selective ion recognition; impedance studies
PublikacjaBadania impedancyjne membran zawierających jonofory selektywne na kation Na+ (L1) i Cs+(L2) wykazały, ze stala dielektryczna materiału membrany zależy od typu uzytego plastyfikatora i zmienia się w zakresie od 28 do 60. Rezystancja membran zawierających ligand L1 i L2 wynosi 0.15 -1.4 Mohm w zależności od stężenia elektrolitu zewnnetrznego. Testowona dwa typy elektrod jonoselektywnych: elektrody typu ASS z polimerem przewodzącym...
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Processing, Mechanical and Morphological Properties of GTR Modified by SBS Copolymers
PublikacjaIn this work, ground tire rubber (GTR) was thermo-mechanically treated in the presence of styrene-butadiene-styrene (SBS) copolymers. During preliminary investigation, the effects of different SBS copolymer grades, the variable content of SBS copolymer on the Mooney viscosity, and the thermal and mechanical properties of modified GTR were determined. Subsequently, GTR modified by SBS copolymer and cross-linking agents (sulfur-based...