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Pyrolysis of RDF and Catalytic Decomposition of the Produced Tar in a Char Bed Secondary Reactor as an Efficient Source of Syngas
PublikacjaOne of the technical limitations of refuse-derived fuel (RDF) pyrolysis is the high content of tar in its gas products. In order to resolve this problem, a two-stage RDF pyrolysis with a catalyst based on char from RDF pyrolysis is proposed. This paper presents the results of municipal waste pyrolysis beginning in an oven heated to 480 °C and ending with catalytic tar cracking carried out in the temperature range from 800 to 1000...
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Pyrolysis Combined with the Dry Reforming of Waste Plastics as a Potential Method for Resource Recovery—A Review of Process Parameters and Catalysts
Publikacja: Emissions of greenhouse gases and growing amounts of waste plastic are serious environmental threats that need urgent attention. The current methods dedicated to waste plastic recycling are still insufficient and it is necessary to search for new technologies for waste plastic management. The pyrolysis-catalytic dry reforming (PCDR) of waste plastic is a promising pro-environmental way employed for the reduction of both CO2 and...
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Experimental and theoretical investigation of the reactivity of [(BDI*)Ti(Cl){η2-P(SiMe3)-PiPr2}] towards selected ketones
PublikacjaIn this work, we report a new type of reactivity of [(BDI*)Ti(Cl){η2-P(SiMe3)-PiPr2}] (1) towards ketones (BDI* = 2,6-diisopropylphenyl-β-methyldiketiminate ligand). In the reaction of 1 with acetone, cyclopentanone or cyclohexanone, a ketone moiety is inserted into Ti–Pphosphanyl or Ti–Pphosphido bonds to form complexes with a new C–P–P moiety, providing [(BDI*)Ti(Cl){η2-P(SiMe3)-PiPr2-C(Me)2O}] (2a), [(BDI*)Ti(Cl){η2-OC(Me)2P(SiMe3)-PiPr2}]...
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Enhancement of self-trapped excitons and near-infrared emission in Bi3+/Er3+ co-doped Cs2Ag0.4Na0.6InCl6 double perovskite
Dane BadawczeErbium (Er) complexes are used as optical gain materials for signal generation in the telecom C-band at 1540 nm, but they need a sensitizer to enhance absorption. Na+ substitution for Ag+ and Bi3+ doping at the In3+ site is a possible strategy to enhance the broadband emission of Cs2AgInCl6, which could be used as a sensitizer for energy transfer to...
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Durban szansą rozwoju energetyki gazowej w Polsce?
PublikacjaOpisano konferencję klimatyczną w Durbanie (17 COP ONZ). Podano determinnaty polityki energetycznej Polski w kontekście rozwoju gazownictwa.
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Optical recognition elements. Macrocyclic imidazole chromoionophores entrapped in silica xerogel
PublikacjaNowe chromojonofory zawierające fragment eteru koronowego i resztę azolu zostały unieruchomione w krzemionkowej matrycy żelowej metodą zol-żel i zbadane jako optyczne elementy rozpoznające kationy Li+,Cs+, Cu2+. Elementy optyczne oparte na 21-członowych pochodnych imidazolu i 4-metyloimidazolu rozpoznawały jony Li+ w roztworze wodnym. Wyznaczono parametry g i A na podstawie badań EPR dla kompleksów 18-członowej i 21-członowej pochodnej...
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La 0.6 Sr 0.4 Co 0.2 Fe 0.8 O 3-δ oxygen electrodes for solid oxide cells prepared by polymer precursor and nitrates solution infiltration into gadolinium doped ceria backbone
PublikacjaInfiltration is a method, which can be applied for the electrode preparation. In this paper oxygen electrode is prepared solely by the infiltration of La0.6Sr0.4Co0.2Fe0.8O3‐δ (LSCF) into Ce0.8Gd0.2O2-δ (CGO) backbone. The use a polymer precursor as an infiltrating medium, instead of an aqueous nitrate salts solution is presented. It is shown that the polymer forms the single-phase perovskite at 600 °C, contrary to the nitrates...
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The luminescence study of Sr2−xSrxPN3:Eu2+ nitridophosphate.
Dane BadawczeIn this work, a series of Ca2−xSrxPN3:Eu2+ nitridophosphate phosphors through a solid-solution strategy involving a hot isostatic press was developed by collaborators from National Taiwan University. Unexpected dual emissions in the red and infrared regions are observed, different from previous research results. The unique change in red and near-infrared...
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Electrochemical impedance spectroscopy measurements - conductivity vs. temperature and conductivity vs. oxygen partial pressure - BaCe0.6Zr0.2Y0.1Tb0.1O3-δ
Dane BadawczeThe dataset consists of two main catalogs consisting of measurement data: of the electrical conductivity of the BaCe0.6Zr0.2Y0.1Tb0.1O3-δ (BCZYTb) sample as a function of temperature and of the electrical conductivity as a function of oxygen partial pressure (pO2). Measurements as a function of temperature were carried out in dry and wet air (pH2O ~...
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Studies on origin of Polish honeys by two-dimensional gas chromatography Ocena pochodzenia surowcowego polskich miodów przy użyciu dwuwymiarowej chromatografii gazowej
PublikacjaPolish acacia, linden, rapessed and buckwheat-derived honeys and a honydew were analysed for presence of hydrocarbons, alcs., ketones and esters by 2-dimensional gas chromatog. to establish the markers for the honey origin. PrOH was found characteristic for acacia honey, Me(CH2)11OH for linden honey, Me(CH2)6CHOMe for honeydew and Me(CH2)8COOEt for the rapeseed honey. Wykorzystano technikę dwuwymiarowej chromatografii gazowej sprzężonej...
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Electricity generation from rapeseed straw hydrolysates using microbial fuel cells
PublikacjaRapeseed straw is an attractive fuel material for microbial fuel cells (MFCs) due to its high content of carbohydrates (more than 60% carbohydrates). This study has demonstrated that reducing sugars can be efficiently extracted from raw rapeseed straw by combination of hydrothermal pretreatment and enzymatic hydrolysis followed by utilization as a fuel in two-chamber MFCs for electrical power generation. The most efficient method...
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Multibeam data processing for 3D object shape reconstruction
PublikacjaThe technology of hydroacoustic scanning offers an efficient and widely-used source of geospatial information regarding underwater environments, providing measurement data which usually have the structure of irregular groups of points known as point clouds. Since this data model has known disadvantages, a different form of representation based on representing surfaces with simple geometric structures, such as edges and facets,...
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Jacek Krenz : City in my eyes
PublikacjaSketch City: Tips and Inspiration for Drawing on Location is the companion for any creative traveler, urban explorer, or budding artist. 50 artists scattered around the globe have been brought together to share tips about their favorite urban settings, including locations in South America, Europe, Canada, Asia, and beyond. Citified sketchers are guiding through techniques for capturing frenetic street scenes as well as the rare...
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Comparison of the coordination geometries of Zn(II) and Cd(II) ions in complexes with water, methanol and bulky aryloxysilanethiolate ligands
PublikacjaZinc and cadmium complexes containing silanethiolate anions and methanol or water were synthesized and characterized by X-ray diffraction, FT-IR and NMR spectroscopy, and DFT calculations. Contrary to zinc, the cadmium ion utilizes very weak donors to complete its coordination sphere; it forms contacts to phenyl rings of the silanethiolate ligand. Two zinc analogs of the general formula [Zn{SSi(OAr)3}2(L)2] where L = CH3OH (2)...
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A structure and simulation-driven design of compact CPW-fed UWB antenna
PublikacjaIn this letter, a structure of a miniaturized ultra-wideband CPW-fed antenna and its design proce-dure are presented. The antenna is a modified version of the design previously proposed in the literature, with additional degrees of freedom introduced in order to improve the structure flexibility. The small size is achieved by executing a rigorous optimization procedure that consists of two stages: (i) smart random search carried...
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Impact resistance of plain and twill fabric in GFRP measured by active thermography
PublikacjaThis paper discusses the impact resistance of glass-fibre reinforced polymer (GFRP) composites depending on the type of reinforcement – plain or twill weave. The values of impact energy were: 3J, 10J and 15J. Specimens featuring twill weave transferred higher force during the impact as compared with plain weave specimens. It was observed that an increase of impact energy was accompanied by an increase of the disproportion in...
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Efficiency of pollutants removal from landfill leachates using Nb/BDD and Si/BDD anodic oxidation
PublikacjaLandfill leachates (LLs) is a complex, refectory and difficult to depurate liquid generated from sanitary landfills. It contains excessive levels of biodegradable and in particular non-biodegradable products (e.g. heavy metals, phenols, sulphide, plasticisers). LLs are among the effluents that may pose major environmental concerns, they can be a dangerous source of pollution e.g. due to infiltration into soil and underlying water....
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Agnieszka Bartoszek-Pączkowska prof. dr hab. inż.
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Electrophoretic co-deposition of Mn1.5Co1.5O4, Fe2O3 and CuO: Unravelling the effect of simultaneous addition of Cu and Fe on the microstructural, thermo-mechanical and corrosion properties of in-situ modified spinel coatings for solid oxide cell interconnects
PublikacjaA systematic microstructural, thermo-mechanical and electrical characterization of simultaneous Fe–Cu doped Mn–Co spinel coatings processed by electrophoretic co-deposition on Crofer 22 APU is here reported and discussed. An innovative approach for the simultaneous electrophoretic deposition of three spinel precursors is designed, conceived and optimised, with the aim of outlining time- and energy-saving spinel modification routes....
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Vibrational excitation of tetrahydrofuran by electron impact in the low energy range
PublikacjaWzbudzenie oscylacyjne cząsteczki tetrahydrofuranu w zderzeniach z elektronami przeprowadzone było w zakresie energii 5-14 eV w szerokim kącie rozproszenia (20°-180°). Pomiary funkcji wzbudzenia oscylacyjnego modów rozciągających w grupie CH2 (wiązania C-H) wykazują obecność struktur dla energii 6.0, 7.9 i 10.3 eV, którym można przypisać formowanie się stanów rezonansowych jonów ujemnych cząsteczki. W pracy wyznaczono także różniczkowy...
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Experience of hybrid constructed wetlands operation in Gdansk region
PublikacjaThe investigation were carried out at five local hybrid constructed wetlands (HCWs), which secured biological treatment of domestic wastewater generated from 15 to 600 pe. Based on over two years monitoring it was indicated that HCWs ensured very effective removal of organic matter from 74.9 to 95.5 COD % in wild range of loadings (1.5 - 17.0g COD/ m3day). Efficiency of total nitrogen removal varied significantly from 23.4 two...
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Tomasz Wąsowicz dr hab.
OsobyAbsolwent Technikum Elektrycznego w Słupsku (1997 rok) oraz Wydziału Matematyki, Fizyki i Informatyki Uniwersytetu Gdańskiego (2002 rok). W 2006 roku obronił dysertację doktorską z fizyki na WMFiI UG. Pracując już w PG, w 2018 roku uzyskał habilitację. W pierwszym okresie prace badawcze Tomasza Wąsowicza miały związek ze spektroskopią atomową wysokiej zdolności rozdzielczej i koncentrowały się na pomiarze i analizie prawdopodobieństw...
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Signature of Oxide-Ion Conduction in Alkaline-Earth-Metal-Doped Y3GaO6
PublikacjaWe have studied alkaline-earth-metal-doped Y3GaO6 as a new family of oxide-ion conductor. Solid solutions of Y3GaO6 and 2% −Ca2+-, −Sr2+-, and −Ba2+-doped Y3GaO6, i.e., Y(3−0.06)M0.06GaO6−δ (M = Ca2+, Sr2+, and Ba2+), were prepared via a conventional solid-state reaction route. X-ray Rietveld refined diffractograms of all the compositions showed the formation of an orthorhombic structure having the Cmc21 space group. Scanning electron...
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ANALYSIS OF ENERGY EFFICIENCY IN ELECTRIC DRIVES
PublikacjaIn this paper energy efficiency in electric drives is analysed. This factor strongly depends on energy parameters - efficiency n and power factor k (in special case cos fi)
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Modeling organic nitrogen conversions in activated sludge bioreactors
PublikacjaFor biological nutrient removal (BNR) systems designed to maximize nitrogen removal, the effluent total nitrogen (TN) concentration may range from 2.0 to 4.0 g N/m3 with about 25-50% in the form of organic nitrogen (ON). In this study, current approaches to modeling organic N conversions (separate processes vs. constant contents of organic fractions) were compared. A new conceptual model of ON conversions was developed and combined...
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Characteristics and fate of organic nitrogen in municipal biological nutrient removal wastewater treatment plants
PublikacjaThe aim of this study was to investigate the occurrence and fate of colloidal and dissolved organic nitrogen (CON and DON) across biological nutrient removal (BNR) activated sludge bioreactors. Primary and secondary effluent total nitrogen (TN) measurements and component fractionation, CON and DON concentration profiles across BNR bioreactors, and laboratory batch experiments with the process mixed liquor were carried out at several...
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Statistical evaluation of physical and index properties of Vistula Marshlands deltaic soft soils
PublikacjaThis paper provides statistical evaluation of physical and index parameters of the Vistula Marshlands deltaic soft soils using three datasets. Soft soils from the Vistula Marshlands are grouped into the four categories: (1) silty/sandy loams, (2) organic clays, (3) organic silts and (4) peats. Variability of basic and derivative physical properties as well as Atterberg's limits and plasticity index is studied. It is found that...
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High performance LaNi1-xCoxO3-δ (x = 0.4 to 0.7) infiltrated oxygen electrodes for reversible solid oxide cells
PublikacjaOxygen electrodes prepared by infiltration of yttria stabilized zirconia backbone with Ce0.8Gd0.2O1.95 barrier layer and LaNi1-xCoxO3-δ (x=0.4 to 0.7) catalyst for application in reversible solid oxide cells have been studied. The effect of temperature and Ni:Co ratio on their phase composition, microstructure and electrochemical properties are discussed. It was shown that oxygen electrodes infiltrated with LaNi0.5Co0.5O3-δ had...
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Electrocatalytic oxidation of methanol, ethylene glycol and glycerine in alkaline media on TiO2 nanotubes decorated with AuCu nanoparticles for an application in fuel cells
PublikacjaIn this work, we present the catalytic and photocatalytic activity of AuCu nanostructures obtained on TiO2 nanotubes toward methanol, ethylene glycol and glycerine oxidation. The electrode material is prepared by anodization of Ti foil, thin AuCu layer sputtering and rapid thermal treatment under argon atmosphere. Scanning electron microscopy images confirmed the presence of ordered tubular architecture of TiO2 as well as nanoparticles...
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Nonlinear impedance of vanadate glasses containing BaTiO3
Dane BadawczeThe nonlinear impedance of vanadate glasses doped with BaTiO3 was measured. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on a preheated (573...
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Nonlinear impedance of Bi2VO5.5 glass-ceramic annealed at 423 K was measured with impedance spectroscopy method at high temperature region
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic annealed at 423 K was measured by impedance spectroscopy method.
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Nonlinear impedance of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured with impedance spectroscopy method at high temperature region
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured by impedance spectroscopy method.
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Nonlinear impedance of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured with impedance spectroscopy method at low temperature region
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 glass-ceramic heat-treated at 913 K was measured by impedance spectroscopy method.
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Hybrid constructed wetlands for the National Parks in Poland - a case study, requirements, dimensioning, preliminary results
PublikacjaWater and wastewater management, especially in rural areas, greatly affects loads of nutrients discharged to the Baltic Sea. In Poland, this management is unbalanced because of the dispersed development and in many locations con struction of sewerage system is uneconomic or even impossible. For this reason, a significant part of sewage from single-family houses in rural areas must be discharged into domestic sewage systems. The...
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Hydroxyl and sulfate radical-based degradation of ciprofloxacin using UV-C and/or Fe2+-catalyzed peroxymonosulfate: Effects of process parameters and toxicity evaluation
PublikacjaCiprofloxacin (CIP) is a valuable antibiotic and discharged in huge quantities in aquatic environment. Different •OH and SO4•−-based advanced oxidation technologies (AOTs), e.g., Fe2+/PMS, UV-C/PMS, and UV-C/Fe2+/PMS are developed for treatment of CIP. The removal of CIP by Fe2+/PMS, UV-C/PMS and UV-C/Fe2+/PMS was 63, 77, and 87 %, respectively, under identical conditions which showed better performance of UV-C/Fe2+/PMS. The UV-C/Fe2+/PMS...
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Derivation of motor mean phase currents in PMSM drives operating with low switching-to-fundamental frequency ratio
PublikacjaPulse width modulation (PWM) of inverter output voltage causes the waveforms of motor phase cur-rents to consist of distinctive ripples. In order to provide suitable feedback for the motor current con-trollers, the mean value must be extracted from the currents’ waveforms in every PWM cycle. A com-mon solution to derive the mean phase currents is to sample their value at the midpoint of a symmetrical PWM cycle. Using an assumption...
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Interface layers between electrolyte and cathodes for solid oxide fuel cells
PublikacjaW pracy przebadano możliwość zastosowania warstwy CGO ((CeO2)0.8 (Gd2O3)0.1) w tlenkowych ogniwach paliwowych. Do wytworzenia warstwy użyto pirolizy aerozolowej.
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Marek Czachor prof. dr hab.
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Analytical procedures for determination of cocaine and its metabolites in biological samples
PublikacjaThe dangerous effects and increased usage of illicit drugs have inspired the development of analytical methodologies. We based our review of analytical procedures for determination of cocaine (COC) and its metabolites on literature from the past two decades. Our main aim was to compare the capabilities of different analytical techniques. The diversity of matrices from which COC is determined (e.g., blood, hair, saliva, plasma,...
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Centers of Excellence - initial conception
PublikacjaIn literature, the most basic definition of centers of excellence is " CoE is a team of people that promote collaboration and use best practices around a specific focus area to drive business result". More broadly, center of excellence is defined as " a premier organization providing an exceptional product or service in an assigned sphere of expertise and within a specific field of technology, business, or government, consistent...
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BIOVAC® WASTEWATER TREATMENT PLANTS IN THE MOUNTAIN NATIONAL PARKS.
PublikacjaThis paper presents characteristics of the Biovac® wastewater treatment plants operating in the mountain areas of the Polish national parks (NP): Tatrzanski NP and Babiogórski NP as well as in the West Spitsbergen NP. On the basis of the laboratory tests performed on raw sewage and the final effluent the efficiency of the wastewater treatment plants was evaluated. It was found that high COD values and rather high COD / BOD5 ratios...
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Wykorzystanie fourierowskiej spektroskopii w podczerwieni do badania stężenia gazów wylotowych z tlenkowego ogniwa paliwowego zasilanego biogazem
PublikacjaW dzisiejszych czasach bardzo ważne jest pozyskiwanie energii ze źródeł odnawialnych i bezpiecznych dla środowiska. Jedną z obiecujących technologii są tlenkowe ogniwa paliwowe (ang. Solid Oxide Fuel Cell, SOFC). Stanowią one bezpieczną i ekologiczną alternatywę dla energii uzyskanej z paliw kopalnych. SOFC charakteryzuje się sprawnością energetyczną na poziomie 45-60 %, podczas gdy sprawność klasycznych elektrowni cieplnych nie...
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Analiza składu fazy gazowej wytwarzanej podczas fermentacji ciemnej
PublikacjaFermentacja ciemna umożliwia otrzymywanie bio-wodoru z substratów pochodzenia biologicznego, np. z biomasy ligno-celulozowej. Kontrola i właściwe sterowanie przebiegiem procesu fermentacji ciemnej wymaga bieżącego monitoringu składu powstającej fazy gazowej. W niniejszej pracy przedstawiono metodykę analizy składu fazy gazowej z wykorzystaniem techniki GC-TCD-FID. Zaproponowana metodyka umożliwia oznaczenie następujących gazów...
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Hydrogen Production Mechanism in Low-Temperature Methanol Decomposition Catalyzed by Ni3Sn4 Intermetallic Compound: A Combined Operando and Density Functional Theory Investigation
PublikacjaHydrogen production from methanol decomposition to syngas (H2 + CO) is a promising alternative route for clean energy transition. One major challenge is related to the quest for stable, cost-effective, and selective catalysts operating below 400 °C. We illustrate an investigation of the surface reactivity of a Ni3Sn4 catalyst working at 250 °C, by combining density functional theory, operando X-ray absorption spectroscopy, and high-resolution...
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Effect of plasma sprayed and laser re-melted Al2O3 coatings on hardness and wear properties of stainless steel
PublikacjaCommercially available austenic stainless steel substrate was coated with commercially available, raw Al2O3 powder applied by means of plasma spraying method and then re-melted with CO2 laser beam of various parameters. Tribological and mechanical properties of the 120 J/mm and 160 J/mm laser re-melted coatings were compared with the tribological and mechanical properties of the “as-sprayed” coating. The influence of the laser...
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Modelling of the Heat Flux Density Distribution for Laser Beam Welding
PublikacjaGreat interest of the laser beam welding in industry is a new theoretical task, making planning the welding procedure specification and the quality control of welded joints easier. Estimating and calculating the dimensions of a weld pool and temperature distribution near weld mainly concern heat source modelling. In the presented work calculations of welding pool shape and thermal field for cylindrical-powered-normally model of...
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Final report on noise and rolling resistance
PublikacjaWork Package 6 deals with environmental impacts of PERS use, including noise and rolling resistance. This report covers preliminary noise tests performed in the laboratory and at the road test sites. The obtained results indicate that PERS material reduce noise considerably - up to 12 dB in comparison to SMA16 reference surface. Noise reduction properties are especially visible in the case of factory produced PERS slabs supplied...
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The Influence of Selected Parameters of Numerical Modelling on Strains and Stresses at Weld Toe Notch
PublikacjaLatest development in the field of welding technology and prefabrication enabled massive production of thin-walled sandwich structures. Multi-layered sandwich structures are fabricated with the use of high-power CO2 lasers, friction welding, arc welding, hybrid welding, or other technique designed for the special purpose. Steel or aluminium alloy plates with thickness between 1 and 5 mm are connected by internal stiffeners. Strength...
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Permeation and sorption properties of poly(ether-block-amide) membranesfilled by two types of zeolites
PublikacjaThe experimental study of transport properties of mixed matrix membranes (MMMs) based on PEBA-4033 with two types of zeolites is reported. Gas (CO2, O2, N2) and vapor (benzene, toluene, methanol, water) permeation measurements were performed using the differential flow permeameter at temperature of 298.15 K and at atmospheric pressure. Gas/vapor permeation was monitored by measuring the changes of the thermal conductivity of carrier...
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Influence of ethylene glycol on CaCO3 particles formation via carbonation in the gas-slurry system
PublikacjaStrącanie węgalnu wapnia przebiegało w układzie gaz-zawiesina w reakcji wodorotlenku wapnia z dwutlenkiem węgla. Proces precypitacji był prowadzony w obecności glikolu etylenowego. Użyty dodatek organiczny zmieniał lepkość mieszaniny reakcyjnej oraz rozpuszczalność dwutlenku węgla i węgalnu wapnia, co miało wpływ na warunki precypitacji CaCO3. Wzrost stężnia glikolu etylenowego w mieszaninie reakcyjnej powodował większe zużycie...