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Determination of estrogenic endocrine disruptors in environmental samples - a review of chromatographic methods
PublicationWśród związków endokrynnych to estrogeny zarówno naturalne jak i syntetyczne zostały wskazane i opisane jako związki niosące ze sobą największy potencjał aktywności estrogennej. Wysoki potencjał estrogenny jaki posiadają związki z grupy hormonów płciowych potwierdziły badania przeprowadzone zarówno in vitro jak i in vivo. W dużej części (50-95%) próbek ścieków pochodzących z oczyszczalni ścieków zostały wykryte związki z grupy...
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<title>Atom guiding in single mode optical fiber capillary</title>
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Separation of zinc from aqueous samples using a molecular imprinting technique
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An electrochemical interface for direct analysis of amlodipine in tablets and human blood samples
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Novel catalysts for low temperature synthesis of single wall carbon nanotubes
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Reduced diameter distribution of single-wall carbon nanotubes by selective oxidation
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Synthesis and electronic properties of B-doped single wall carbon nanotubes
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Analysis of volatile organic compounds (VOCs) in water samples. Methods and instrumentation
PublicationW pracy przedstawiono stan wiedzy nt. metodyk analitycznych oraz urządzeń kontrolno-pomiarowych, wykorzystywanych w badaniach próbek wody na zawartość lotnych związków organicznych. Szczególną uwagę zwrócono na techniki izolacji i wzbogacania analitów przed etapem oznaczeń końcowych.
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Chapter 13. Immunological determination of the pharmaceutical diclofenac in environmental and biological samples
PublicationOpracowano wysoce specyficzną i czułą metodę immunologiczną oznaczania przeciwzapalnego leku diklofenaku. Jest to jeden z najczęściej wykrywanych farmaceutyków w środowisku. Granicę wykrywalności oraz wartość IC50 określono na poziomie 6 ng/L oraz 60 ng/L dla wody wodociągowej, odpowiednio. W badaniu porównawczym, stosując test ELISA oraz GC-MS określono poziomy stężeń diklofenaku w wodach ściekowych z 21 oczyszczalni ścieków i...
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Quality problems in determination of organic compounds in environmental samples, such as PAHs and PCBs
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Speciation of trace element compounds in samples of biota from marine ecosystems
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Application of GC-MS/MS technique for the determination of benzodiazepines in blood samples
PublicationAbstract Benzodiazepines (BZD) are widely used as pharmaceuticals in medicine. However, due to psychostimulatory effect of BZD, in the last decade, they are more and more often used as drugs of abuse. These compounds produce similar effects to classical illicit drugs and are sold as “legal” alternatives to them as new psychoactive substances (NPS). Currently new BZD, named designer benzodiazepines (DBZD), are synthesized each year...
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Single and Three -Phase PWM AC/AC Converters as Semiconductor Transformers
PublicationAC voltage transformation circuits contain pure or reactance PWM AC/AC converters. These circuits can be treated as AC/AC semiconductor transformers. This paper reviews single-phase and three-phase topologies: both non-isolated and isolated, single as well as two quadrant structure. Additionally, this paper present selected examples of their applications.
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Mechanical exfoliation and layer number identification of single crystal monoclinic CrCl3
PublicationAfter the recent finding that CrI3, displays ferromagnetic order down to its monolayer, extensive studies have followed to pursue new two-dimensional (2D) magnetic materials. In this article, we report on the growth of single crystal CrCl3 in the layered monoclinic phase. The system after mechanical exfoliation exhibits stability in ambient air (the degradation occurs on a time scale at least four orders of magnitude longer than...
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Single crystal growth and physical properties of MCo2Al9 (M= Sr, Ba)
PublicationSingle crystals of SrCo2Al and BaCo2Al9 were grown using a self-flux method. A LeBail analysis of the powder X-ray diffraction patterns show that both compounds crystallize in a hexagonal (P6/mmm) crystal structure with lattice parameters: a = 7.8995(1) Å, c = 3.9159(1) Å for SrCo2Al9, and a = 7.9162(2) Å, c = 3.9702(1) Å for BaCo2Al9 aluminide. The low temperature analysis of the heat capacity measurements give a Sommerfeld...
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Speciation of heavy metal compounds in samples of biota from marine ecosystems
PublicationIt has become increasingly evident that the toxicity, mobility, bioavailability and bioaccumulation of metals are dependent on the particular physico-chemical form in which the element occurs in the environment. Special attention is paid to metals, which are essential for the proper functioning of organisms if present in appropriate amounts but are toxic if in excess (i.e. Se, Cr, Zn), and also to non-essential elements (i.e. Hg,...
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Green aspects of techniques for the determination of currently used pesticides in environmental samples
PublicationPesticides are among the most dangerous environmental pollutants because of their stability, mobility and long-term effects on living organisms. Their presence in the environment is a particular danger. It is therefore crucial to monitor pesticide residues using all available analytical methods. The analysis of environmental samples for the presence of pesticides is very difficult: the processes involved in sample preparation are...
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Pharmacokinetics and bioequivalence of a liquid formulation of hydroxyurea in children with sickle cell anemia
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Shape Restoration of Deformed Egg-Shaped Single Layer Space Frames
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Losses Model of the WPT System with Single-Phase T-Type Inverter
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Barkhausen noise properties measured by different methods for deformed Armco samples
PublicationPorównano właściwości sygnału napięciowego efektu Barkhausena (BN) uzyskanego za pomocą 'sondy punktowej' (użytecznej dla badań przemysłowych) oraz cewki otaczającej badany materiał. W pierwszej metodzie mierzono trzy wielkości: V1 - napięcie skuteczne, Nc - liczba impulsów, V2 - napięcie kontrolne z cewki. W drugiej metodzie z napięcia indukowanego w cewce wyznaczano pętlę histerezy B(H), obwiednie z napięcia skutecznego a także...
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Capillary Electrophoresis in determination of short - chain carboxylic acids in aqueous samples
PublicationAnalysis of pollution is extremely important especially in areas directly adjacent tothe residential district. Studies show that short- chain carboxylic acids are a group ofcompounds widespread around sewage treatment plants, landfills, livestock farms. The mostcommon techniques for determination of short - chain carboxylic acids are chromatographictechniques, especially gas chromatography, whose main limitation is that only volatilemonocarboxylic...
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Mechanical Properties of Single-Walled Carbon Nanotubes with AIREBO Force-Filed
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Iron filled single-wall carbon nanotubes – A novel ferromagnetic medium
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Renal Regulation of Calcium-Phosphate Metabolism in Single- and Twin Pregnant Goats
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Simulation of the remanence influence on the transient states in a single-phase multiwinding transformer
PublicationThis paper presents the mathematical model of a single-phase multi-winding core type transformer taking into account magnetic hysteresis phenomenon based on the feedback Preisach model (FPM). The set of loop differential equations was developed for a K-th winding transformer model where the flux linkages of each winding includes flux Φ common to all windings as a function of magneto motive force Θ of all windings. The first purpose...
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Genetic and biochemical characterization of yeasts isolated from Antarctic soil samples
PublicationThe Polish Arctowski Station is situated in the maritime Antarctic on the western shore ot' Admiralty Bay and encompasses terrestrial habitats which are not perma-nently covered by ice, in contrast to morę than 90% of the island's surface area. Over the past several decades, stud-ies exploring the soils of those habitats have revealed a considerable diversity of bacteria, filamentous fungi, and, to a lesser extent, yeasts; however,...
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New kinematic systems in single-sided lapping and their influence on lap wear
PublicationPrevious studies on one-sided lapping allow to state that not only parameters of lapping elements (i.e. properties of workpiece, abrasive grains and lapping plate) impact on a lapping efficiency. Influential are also kinematics and dynamics of the process. It is crucial to control an average velocity of lapping (v), a distribution of tangential acceleration (at), a nominal pressure (p), a lapping time (t) and disposal of workpiece...
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Nonlinear impedance in oxide glasses containing single and mixed alkali ions
PublicationThe aim of the present was to find more clues on the nonlinearities in impedance of oxide glasses. The first family of researched glasses has a composition of FeO-P2O5-Na2O. Oxide glasses containing iron and alkali are well known for a very low alkali ion mobility and may be considered purely polaron conducting. These glasses show no detectable nonlinearities in the impedance spectra. The second was a family of ionic conducting...
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The speciation of organotin compounds in sediment and water samples from the port of Gdynia
PublicationOrganotin compounds (OTC) are toxic towards all living organisms. The application of organitin-based antifouling systems is becoming the main source of OTC in the ocean. Harbor sediments and water contain large deposits of organotin compounds due to application of antifouling systems in the shipping industry. OTC contamination presents a potential risk to the marine environment. Sediment and water samples were collected in 2009...
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Numerical single-phase modeling of turbulent flow and heat transfer of nanofluids
PublicationIn this work, Nusselt number and friction factor are calculated numerically for turbulent pipe flow (6 000< Re < 12 000) with constant heat flux boundary condition using nanofluids. The nanofluid is modelled with the single-phase approach and the simulation results are compared with published experimental data.
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Characterization of single-stranded DNA-binding proteins from the psychrophilic bacteria
PublicationSingle-stranded DNA-binding proteins (SSBs) are indispensable elements in the cells of all living organisms. SSB proteins interact with ssDNAinsequence in an independent manner, preventing them from forming secondary structures and from degradation by nucleases. In this way, SSB-binding proteins participate in all processes involving ssDNA, such as replication, repair and recombination.Although there are differences in amino acid...
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Comparison of single microjet cooling with water, ethanol and HFE7100 as test fluids
PublicationThe paper presents the investigation of a single microjet cooling forming an thin liquid film on the impingement surface of specially designed rig. The basis of microjet technology is to produce laminar jets, which when impinging the surface have a very high kinetic energy at the stagnation point. Applied technology of jet production can result with the size of jets ranging from 20 to 500μm in breadth and 20 to 100μm in width....
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Characterization of single-stranded DNA-binding proteins from the psychrophilic bacteria
PublicationSingle-stranded DNA-binding proteins (SSBs) are indispensable elements in the cells of all living organisms. SSB proteins interact with ssDNA insequence in an independent manner, preventing them from forming secondary structures and from degradation by nucleases. In this way, SSB-binding proteins participate in all processes involving ssDNA, such as replication, repair and recombination. Although there are differences in amino...
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Determination of Surfactants in Environmental Samples. Part III. Non-Ionic Compounds
PublicationNon-ionic surface active agents are a diverse group of chemicals which have an uncharged polar head and a non-polar tail. They have different properties due to amphiphilic structure of their molecules. Commercial available non-ionic surfactants consist of the broadest spectrum of compounds in comparison with other types of such agents. Typically, non-ionic compounds found applications in households and industry during formulation...
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Single and Series of Multi-valued Decision Diagrams in Representation of Structure Function
PublicationStructure function, which defines dependency of performance of the system on performance of its components, is a key part of system description in reliability analysis. In this paper, we compare two approaches for representation of the structure function. The first one is based on use of a single Multi-valued Decision Diagram (MDD) and the second on use of a series of MDDs. The obtained results indicate that the series of MDDs...
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Single-phase power electronics transformer with active functions for smart grid
PublicationThis paper presents the control of one cell of a modular single-phase power electronics transformer with active functions for meeting the smart grid concept. In this way, the converter could be used not only as a conventional transformer but also for grid such as reactive power, harmonic elimination and energy storage. The topology of the cell is composed by a bidirectional converter with three stages: a half bridge in the input...
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Calibration-Free Single-Anchor Indoor Localization Using an ESPAR Antenna
PublicationIn this paper, we present a novel, low-cost approach to indoor localization that is capable of performing localization processes in real indoor environments and does not require calibration or recalibration procedures. To this end, we propose a single-anchor architecture and design based on an electronically steerable parasitic array radiator (ESPAR) antenna and Nordic Semiconductor nRF52840 utilizing Bluetooth Low Energy (BLE)...
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Ionic liquids in extraction techniques: Determination of pesticides in food and environmental samples
PublicationThe intensive use of pesticides in agricultural practices has promoted the appearance of environmentaland public health problems. Due to that, scientists face challenges with developing simple, fast, sensitive,selective, and low-cost methods dedicated to determining pesticide residues in food and environmentalsamples. Following thefifth principle of Green Analytical Chemistry, chemists are searching for greeneralternatives for...
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Comparison of Two Methods for the Determination of Selected Pesticides in Honey and Honeybee Samples
PublicationDeveloped and validated analytical methods for the determination of a wide spectrum of pesticide residues in honey and honeybee samples after the modification of QuEChERS extraction in combination with gas chromatography–tandem quadrupole mass spectrometry (GC-MS/MS) and liquid chromatography–tandem quadrupole mass spectrometry (LC-MS/MS) were discussed and compared. The developed methods were evaluated regarding the utilized equipment...
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Equivalent single-layer models in deformation analysis of laminated multilayered plates
PublicationThe performance of selected Equivalent Single-Layer (ESL) models is evaluated within several classical benchmark tests for linear static analysis of multi-layered plates. The authors elaborated their own Finite Element software based on the first-order shear deformation theory (FOSD) with some modifications incorporated including a correction of the transverse shear stiffness and an application of zig-zag type functions. Seven...
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Microextraction by packed sorbent: Uncommon detection techniques, sorbents, samples and analytes
PublicationAmong sample preparation approaches, the most desirable are procedures that ensure high efficiency and reproducibility, that are cheap, fast and simple, that minimize the number of operational steps and that require a small amount of sample and solvent and are thus environmentally friendly. Microextraction by packed sorbent (MEPS) is a miniaturized form of solid-phase extraction, the use of which has been continuously expanding...
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Preparation of environmental samples for gas chromatographic determination of selected organic pollutants
PublicationOpisano różne metody izolacji i wzbogacania zanieczyszczeń organicznych z ciekłych, gazowych i stałych próbek środowiskowych. Opisano konstrukcję i testowanie nowych systemów do przygotowania próbek oraz ich zastosowanie w połączeniu z chromatografią gazową do oznaczania zanieczyszczeń organicznych w póbkach rzeczywistych.
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New source of the thermostable alpha-glucosidase suitable for single stepstarch processing
PublicationZbadana wewnątrzkomórkowa termostabilna alfa-glukozydaza z Thermus thermo-philus przejawia największą aktywność w 85 C przy pH 6.2. Aktywność enzymu po 5 h inkubacji w 75 C (pH 6.2) prawie nie ulega zmianie a okres połowicznej inaktywacji w 85 C wynosi 2 h. Właściwości te wskazują na przydatność wymienionego enzymu w jednoetapowej hydrolizie skrobi.
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Derivatisation in gas chromatographic determination of acidic herbicides inaqueous environmental samples.
PublicationW pracy przedstawiono przegląd literaturowy dotyczący wykorzystania derywatyzacji w oznaczaniu herbicydów kwasowych w wodnych próbkach środowiskowych za pomocą chromatografii gazowej. Omówiono główne typy reakcji (transestryfikacja, estryfikacja, sililowanie, alkilacja, alkilacja ekstraktywna i pirolityczna), które powodują utworzenie pochodnych, łatwych do analizy techniką chromatografii gazowej. Scharakteryzowano także...
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A resistivity peak close to Tc in Nd2-xCexCuO4-y single crystals.
PublicationW pracy dyskutowane jest maximum oporu elektrycznego występujące tuż powyżej temperatury przejścia nadprzewodzącego. Maksimum jest obserwowane tylko przy jednej z dwóch możliwych konfiguracji pomiarowych w metodzie van der Pauw.Proponowany, na bazie niejednorodności składu ceru, prosty model wyjaśnia w pełni pochodzenie efektu.
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The effects of growth conditions on superconducting properties of Nd1Ba2Cu3O7-ë single crystals.
PublicationW pracy przedstawiono rezultaty badan wpływu warunków wzrostu kryształów Nd1Ba2Cu3O7-d na ich własności nadprzewodzące. Kryształy hodowano metodą spontanicznego wzrostu z fazy ciekłej. Mikrostruktura kryształów została zbadana skaningowym mikroskopem elektronowym oraz skaningowym mikroskopem tunelowym. Własności nadprzewodzące badano przeprowadzając pomiary momentu magnetycznego w funkcji temperatury.W przypadku badanych kryształów...
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Non-regulated organic compounds (NROC's) in the Odra River water samples.
PublicationW ramach badań opisanych w pracy podjęto próbę identyfikacji lotnych i średniolotnych związków z grupy Non-Regulated Organic Compounds obecnych w próbkach wody rzecznej. Analizie poddano 25 próbek wód pobranych z rzeki Odry w październiku 2000, w trakcie VIII kampanii zorganizowanej w ramach International Odra Project (IOP). W badaniach wykorzystano technikę PT-TD-GC-MS.Komputerowa analiza widm masowych wykazała obecność wielu...
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The ab initio calculations of single nitrogen-vacancy defect center in diamond.
PublicationW artykule zaprezentowano rezultaty kwantowomechanicznych obliczeń ''ab initio'' struktury elektronowej defektu azot-wakans w diamencie. Do obliczeń wykorzystano model złożony z 63 atomów. Otrzymane wyniki zostały porównane z wcześniejszymi pracami teoretycznymi i doświadczalnymi.
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Determining PAHs and PCBs in aqueous samples: finding and evaluating sources of error
PublicationW pracy opisano wyniki badań modelowych (z wykorzystaniem dopowiednich roztworów wzorcowych), których celem było wykrycie źródeł błędów oznaczeń oraz oszacowanie ich wielkości. Przedmiotem badań było oszacowanie wpływu takich procesów jak:- adsorpcja na ściankach naczyń,- adsorpcja na cząstkach materii zawieszonej,- usuwanie nadmiaru rozpuszczalnika (z ekstraktu)na wyniki oznaczeń końcowych.