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Search results for: SPME/GC
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Determination of non-steroidal anti-inflammatory drugs in natural waters using off-line and on-line SPE followed by LC coupled with DAD-MS
PublicationOpisano dwie metody pozwalające na jednoczesne oznaczanie zawartości niesterydowych leków przeciwzapalnych (difluisal, diklofenak, naproksen, tolmetin, fenoprofen, ibuprofen) w próbkach wodnych. Próbki przygotowywano do analizy z użyciem techniki ekstrakcji do fazy stałej (off-line i on-line). Natomiast oznaczeń końcowych dokonano z użyciem LC-DAD-MS. Sprawdzono kilka różnych kolumienek ekstrakcyjnych i wybrano RP-18 jako najlepsze...
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Terahertz investigations on some bi-heterocyclic compounds
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Autoimmunity and Cancer—Two Sides of the Same Coin
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Module structure in Conley theory with some applications
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Antioxidant activities and bioactive components in some berries
PublicationThe objective of this study was to evaluate the antioxidant and binding effects of gooseberry, a less-stud-ied berry, and to compare with blueberry and cranberry in the model of interaction with human serum albumin (HSA). The relationship between the scavenging properties of dietary polyphenols of the selected berries and their affinities for HSA were investigated by fluorescence anal- ysis. In order to perform the extraction and...
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Some applications of thermophiles and their enzymes for protein processing
PublicationPrzedstawiono charakterystykę, właściwości oraz możliwości zastosowań enzymów proteolitycznych wytwarzanych przez termofile. Zaletą tych biokatalizatorów jest między innymi duża odporność na działanie rozpuszczalników organicznych, detergentów i innych czynników denaturujących białka oraz mała wrażliwość na zmiany pH. Dokonano też przeglądu czynników powodujących dużą stabilność proteaz z termofili.
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Some application of neutron activation analysis: A Review
PublicationW pracy przedstawiono podstawowe informacje dotyczące neutronowej analizy aktywacyjnej. Przedstawiono również zastosowanie neutronowej analizy aktywacyjnej w badaniu próbek środowiskowych i biologicznych wraz z krótkim omówieniem wyników. Poruszono także aspekt zapewnienia jakości i kontroli wyników analitycznych otrzymywanych tą metodą.
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EUDEM2: Overview and some early findings Issue
PublicationW publikacji prezentowany jest projekt EUDEM2 oraz wyniki prowadzonych prac.
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Some approaches to the determination of saw blade stiffness.
PublicationW nowoczesnych zakładach przerobu drewna obserwuje się tendencję do redukcji rzazu w celu ograniczenia strat surowca. Jednakże, cienkie piły są bardziej wrażliwe na odziaływanie sił odporowych (bocznych). Dlatego też, znajomość sztywności statycznej pozwala użytkownikowi prognozować zachowanie się piły podczas pracy. W pracy przedstawiono metodykę wyznaczania sztywności statycznej początkowej i roboczej pił trakowych oraz taśmowych....
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Some aspects surface cooling by impinging jet
PublicationW pracy przedstawiono wyniki badań wymiany ciepła, uskoku hydraulicznego i stabilności podczas napływu strugi na powierzchnię ciała stałego.
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Curves of thermodynamic states in some fluids with dispersion
Publicationvariations in the thermodynamic state of a dispersive medium, caused by sound, are studied. A bubbly liquid and a Maxwell fluid are considered as examples. Curves in the plane of thermodynamic states are plotted. They are in fact pictorial images of linear relations of excess pressure and excess density in the acoustic wave which reflect irreversible attenuation of the sound energy. The curves account for the nonlinear generation...
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Reliability Modeling for SPMD and DAC Applications in MERPSYS
PublicationIn this chapter we shall see a method for modeling of reliability of application execution in the MERPSYS system, and the results of reliability simulation of the same SPMD and DAC application which we have previously presented in this book. Unlike energy usage modeling and modeling of execution efficiency we could not compare the reliability model and simulation results to real experiment just because the experiment would last too...
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Energy Consumption Modeling in SPMD and DAC Applications
PublicationIn this chapter, we show a study of energy consumption during execution of SPMD and DAC application – the same applications which time of execution we modeled in the previous two chapters. We measured an average power usage at a single node of the GALERA+ cluster during application execution and then we modeled the total energy consumption by the application. Next we simulated the applications using MERPSYS and we compared the...
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SOME PROBLEMS OF SUPPORTING OFFSHORE WIND TURBINES
PublicationBasic problems of foundations of sea wind turbines are considered in this paper. This aims to search for solutions to optimize supporting of the offshore turbines with a size greater than 10 MW. The types of foundations, their basic features, including most important dimensions, applications as well as general design considerations are discussed. Numerical model of the offshore turbine and some preliminary computations for a case...
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On some open questions for Ramsey and Folkman numbers
PublicationWe discuss some of our favorite open questions about Ramsey numbers and a related problem on edge Folkman numbers. For the classical two-color Ramsey numbers, we first focus on constructive bounds for the difference between consecutive Ramsey numbers. We present the history of progress on the Ramsey number R(5,5) and discuss the conjecture that it is equal to 43.
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Module structure in Conley theory with some applications
PublicationA multiplicative structure in the cohomological versjon of Conley index is described . In the case of equivariant flows we apply the normalization procedure known from equivariant degree theory and we propose a new continuation invariant. The theory is then applied to obtain a mountain pass type theorem. Another application is a result on multiple bifurcations for some elliptic PDE.
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SOME CONVERGENCE PROPERTIES OF THE SUM OF GAUSSIAN FUNCTIONALS
PublicationIn the paper, some aspects of the convergence of series of dependent Gaussian sequences problem are solved. The necessary and sufficient conditions for the convergence of series of centered dependent indicators are obtained. Some strong convergence results for weighted sums of Gaussian functionals are discussed.
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Some remarks on the Euler ring U(G)
PublicationNiech G będzie zwartą grupą Liego i niech U(G) oznacza pierściń Eulera G skonstruoawany przez tom Diecka w [5,6]. Główny wynikpracy (Twierdzenie 4.1) opisuje homomorfizm pierścienia U(SO(3)) w pierścień U(SO(2))indukowany przez włożenie grupy SO(2) w grupę SO(3).
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Some kind of joints in composite polymer bridges
PublicationContemporary, polymer composites bridge structures are of two types: truss or arch structures(with many joints along the length) and beam structures with limited number of joints. Both of them have special types of composite polymer decks. An ideal solution is to join advantages of two types of structuresdescribed below and create long span FRP beam bridge structure system using joints along the length. Theproblem is to find the...
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Some Security Features of Selected IoT Platforms
PublicationIoT (Internet of Things) is certainly one of the leading current and future trends for processing in the current distributed world. It is changing our life and society. IoT allows new ubiquitous applications and processing, but, on the other hand, it introduces potentially serious security threats. Nowadays researchers in IoT areas should, without a doubt, consider and focus on security aspects. This paper is aimed at a high-level...
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On some accuracy limiting factors in wood sawing
PublicationPrzedstawiono szczegółową klasyfikację czynników determinujących dokładność przecinania drewna piłami. Uwzględniono w niej również pozorną utratę dokładności wynikającą z anatomicznej budowy drewna i metody pomiaru (wykorzystywanie lasera). Występujące błędy przecinania zobrazowano szeregiem przykładów z badań doświadczalnych.
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Head-Space SPME for the Analysis of Organophosphorus Insecticides by Novel Silica IL-Based Fibers in Real Samples
PublicationThis work demonstrates the suitability of a newly developed ionic liquid (IL)-based silica SPME fiber for the determination of seven organophosphorus insecticides in cucumber and grapefruit samples by headspace solid-phase microextraction (HS-SPME) with a gas chromatography–flame ionization detector (FID). The sol-gel method released four different sorbent coatings, which were obtained based on a silica matrix containing ILs immobilized...
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The new silica-based coated SPME fiber as universal support for the confinement of ionic liquid as an extraction medium
PublicationThe new silica-based SPME fiber coating is reported for the first time as universal support purposed to confinement of ionic liquid as an extraction medium. Fiber coating was prepared by the sol-gel process, using potassium silicate (K2SiO3) as a precursor and dimethylformamide (DMF) as a pore-forming medium. The concept of synthesis assumes obtaining a solid porous material on the surface of the glass rod and, being characterized...
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Gas chromatography-olfactometry (GC-O), electronic noses (e-noses) and electronic tongues (e-tongues) for in vivo food flavour measurement
PublicationThe capter revies two types of artificial olfaction instrumentation, i.e. gas-chromatography-olfactometry (GC-O) and chemical sensor technologies (electronic nose and tongue), combined with multivariate data processing methods as promising approaches for rapid analysis of food. The chapter also includes examples of specific applications for the detection of food flavour and volatile components.
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Application of electronic nose based on fast GC for comparison of aroma profiles of homemade cherry "Nalewka" made with addition of different amount of sugar
PublicationNalewka is a traditional Polish homemade spirit beverage and there are many different recepies for the production of nalewkas. However, it is not knownwhat amount of sugar can have influence of their aroma profiles. There is little information on the comparison of aroma profiles of Polish cherry nalewkas made with addition of different amount of sugar. For this purpose electronic nose based on fast GC has been used. Electronic...
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Application of electronic nose based on fast GC for comparison of aroma profiles of homemade cherry "Nalewka" made with addition of different amount of sugar
PublicationNalewka is a traditional Polish homemade spirit beverage and there are many different recepies for the production of nalewkas. However, it is not knownwhat amount of sugar can have influence of their aroma profiles. There is little information on the comparison of aroma profiles of Polish cherry nalewkas made with addition of different amount of sugar. For this purpose electronic nose based on fast GC has been used. Electronic...
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Simultaneous determination of ibuprofen and its metabolites in complex equine urine matrices by GC-EI-MS in excretion study in view of doping control
PublicationA novel assay for the simultaneous determination of ibuprofen (IBU) and its four probable metabolites, 1-hydroxyibuprofen (1-OH IBU), 2-hydroxyibuprofen (2-OH IBU), 3-hydroxyibuprofen (3-OH IBU) and carboxyibuprofen (CBX IBU) in equine urine samples with the application of Gas Chromatography-Electron Ionization-Mass Spectrometry (GC-EI-MS) has been developed and elaborated. The new approach for sample preparation including minimizing...
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Monitoring of occupational exposure to volatile organohalogen solvents (VOXs) in human urine samples of dry-cleaner workers by TLHS-DAI-GC-ECD procedure
PublicationChlorinated hydrocarbon solvents are often used for dry-cleaning clothes in the laundry industry. The object of this study was to monitor the occupational exposure of dry-clean employees coming into contact with VOXs. 25 workers collected their urine samples before the work shift, after 4 hours of work and after the work shift. The analyses of urine samples and solvents used in dry-cleaning were performed using TLHS-DAI-GC-ECD....
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Identyfikacja lotnych składników ścieków z instalacji oksydacji asfaltów z wykorzystaniem chromatografii gazowej sprzężonej ze spektrometrią mas (GC-MS)
PublicationW pracy przedstawiono wyniki badań nad identyfikacją lotnych związków organicznych występujących w ściekach z instalacji oksydacji asfaltów. Ścieki poddano deemulgacji, w celu usunięcia fazy organicznej, a następnie ekstrakcji dichlorometanem, w celu wyizolowania pozostałych w ściekach związków organicznych. Zidentyfikowano 30 związków organicznych oraz szereg n-alkanów, które pozostały w ściekach pomimo zastosowanej deemulgacji....
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Application of dynamic headspace and gas chromatography coupled to mass spectrometry (DHS-GC-MS) for the determination of oxygenated volatile organic compounds in refinery effluents
PublicationThe paper presents a new procedure for the determination of oxygenated volatile organic compounds (O-VOCs) in postoxidative effluents from the production of petroleum asphalt using dynamic headspace coupled to gas chromatography-mass spectrometry in the selected ion monitoring (SIM) mode (DHSGC-MS). Among the GC capillary columns tested, a polar SLB-IL111 column with the ionic liquid stationary phase was found to be superior due...
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Non-volatile molecular composition and discrimination of single grape white of chardonnay, riesling, sauvignon blanc and silvaner using untargeted GC–MS analysis
PublicationThis study developed and applied a GC–MS method aiming at molecular fingerprinting of 120 commercial single grape white wines (Chardonnay, Riesling, Sauvignon Blanc and Silvaner) for possible authentication according to grape variety. The method allowed detection of 372 peaks and tentative identification of 146 metabolites including alcohols, organic acids, esters, amino acids and sugars. The grape variety effect explained 8.3%...
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Determination of Terpene Profile in Cape gooseberry (Physalis peruviana L.) with Use of HS-SPME/GCxGC-TOFMS Method
PublicationFresh fruits and products made of them, especially fruit juice, provide the basic energetic substances (simple and complex sugars) and are a source of health beneficial vitamins, macro and microelements, antioxidants and compounds which are classified together with essential oils (for example terpenes), which positively affect human s health. The terpenes profile of cape gooseberry was determined by headspace solid--phase microextraction...
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HS-SPME-CGC-PID determination of aldehydes in rectified spirits and vodkas after derivatisation with 2,4,6-trichlorophenylhydrazine (TCPH)
PublicationW pracy przedstawiono nową metodę oznaczania aldehydów w spirytusach i wyrobach spirytusowych czystych z zastosowaniem 2,4,6-trichlorofenylohydrazyny (TCPH) jako odczynnika derywatyzującego. Zaproponowana metoda jest co najmniej 100-krotnie tańsza od mikroekstrakcji do fazy stacjonarnej z fazy nadpowierzchniowej (HS-SPME) i chromatografii gazowej z zastosowaniem często zalecanej o-2,3,4,5,6-pentafluorobenzylohydroxyloaminy (PFBHA)....
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Evaluation of polycaprolactone as a new sorbent coating for determination of polar organic compounds in water samples using membrane–SPME
PublicationCommercially available solid-phase microextraction fibers used for isolation of polar analytes are based on the adsorption phenomenon. In consequence, typical limitations bonded with analytes displacement and matrix effects are very frequent. In the present study, alternative solution is described. Polycaprolactone (PCL) was used for the first time as sorbent to isolate polar organic compounds from water samples using the membrane–solid-phase...
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On some ramsey and turan-type numbers for paths and cycles
PublicationUdowodniono, że R(P_3,C_k,C_k)= R(C_k,C_k)= 2k - 1, dla nieparzystych k. Udowodniono, że R(P_4,P_4,C_k) = k + 2 oraz R(P_3,P_5,C_k) = k + 1 dla k > 2.
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Is database a necessary tool in research? Some historical facts
PublicationAutorzy rozważają argumenty za i przeciw używaniu baz danych w badaniach naukowych, a w szczególności w inżynierii. Wnioski z rozważań są jednoznaczne - bazy danych są dziś koniecznością, autorzy podają przykłady zastosowań i pomysły na nowe wdrożenia systemów bazodanowych
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Synthesis of some optically active terpenoid-derived thioamides
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Some Aspects of Potential Measurements in a Stray Current Field
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Some results concerning the complexity of restricted colorings of graphs
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Some results on a trading model in a consensus list coloring
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Propagation of acoustic pulses in some fluids with yield stress
PublicationThis study is devoted to the derivation of approximate equations governing acoustic pulses in flows with yieldstress, including some time-dependent flows with a slow dependence on time of yield stress and apparent viscosity. Themodeling of yield stress and apparent viscosity in the vicinity of a zero deformation rate allows us to consider a thixotropicfluid as a Bingham plastic with coefficients that are dependent on time. The...
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Visualization in Matehmatics Teaching - Some examples of supporting the students'education
PublicationNa całym świecie prowadzi się badania nad wykorzystaniem multimediów w dydaktyce matematyki. Rewolucja cyfrowa jest impulsem do zmiany podejścia do nauczania i metod uczenia się. Oczywiście nowe technologie nie wyeliminują czy nie zastąpią wszystkich tradycyjnych środków nauczania.Studenci, aby zostać dobrymi, konkurencyjnymi na rynku pracy inżynierami, muszą poznać wiele, czasem bardzo zaawansowanych mechanizmów z zakresu matematyki....
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Some mechatronic solutions towards a surveillance of mechanical systems
PublicationCelem artykułu jest przedstawienie nowych rozwiązań związanych z nadzorowaniem systemów mechanicznych. Przedstawia on zmodyfikowaną metodę nadzorowania drgań opartą na sterowaniu modalnym i energetycznym wskaźniku jakości, nadzorowanie drgań z wykorzystaniem zmiennej prędkości obrotowej, nadzorowanie drgań systemu hybrydowego z wykorzystaniem sterowania optymalnego i energetycznego wskaźnika jakosci oraz nadzorowanie ruchu mobilnego...
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Retention modeling of some saccharides separated on an amino column.
PublicationUsing an amino column (Supelcosil LC-NH2) and different mixtures of acetonitrile-water, quantitative structure-retention relationship models are discussed. These models are based on computed molecular descriptors representing numerically structured features of some saccharides. The obtained results are underlining the lipophilicity/hydrophilicity balance, and how this is controlling the separation of the saccharides. The resulting...
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Some Optimization Methods for Simulations in Volunteer and Grid Systems
PublicationIn this chapter, some optimization methods have been presented for improving performance of simulations in the volunteer and grid computing system called Comcute. Some issues related to the cloud computing can be solved by presented approaches as well as the Comcute platform can be used to simulate execution of expensive and energy consuming long-term tasks in the cloud environment. In particular, evolutionary algorithms as well...
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Path dependence, modularity and the offshoring of (some) physician services
PublicationThis paper integrates ideas from modularity and path dependency to explain the potential for and limitations of the offshoring of high value added physician services. While not all medical services are amenable to offshoring, a growing number of physician activities can be viewed as modular components which, at least technically, could be performed remotely. As a result, the presumption that concerns for efficiency dictate how...
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Some problems with operation of engines fueled with landfill biogas
PublicationW referacie przedstawiono wybrane problemy związane z eksploatacją tłokowych silników spalinowych zasilanych biogazem pozyskiwanym z wysypiska śmieci. Biogaz wysypiskowy charakteryzuje się znaczną zmiennością zawartości metanu, co ma istostny wpływ na pracę silników zasilanych tym paliwem. W referacie przedstawiono wyniki badań przeprowadzonych na wysypisku śmieci, w wyniku których zaprezentowano zrówno wielkość zmian zawartości...
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Determination of some off-flavors for vodka quality assessment
PublicationW pracy zostały przedstawione wyniki analizy wybranych związków karbonylowych w wódkach czystych z wykorzystaniem procedury HS-SPME/GC-ECD poprzedzonej derywatyzacją aldehydów za pomocą odczynnika PFBHA. Przeprowadzone badania wykazały, że obecność 2,3-pentanodionu i 2-butenalu skutkuje pogorszeniem jakości analizowanych wódek.
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Some Exact Values of Shannon Capacity for Evolving Systems
PublicationWe describe the notion of Shannon Capacity for evolving channels. Furthermore, using a computer search together with some theoretical results we establish some exact values of the measure.
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Some Aspects of Designing Nozzle Segments of Axial Microturbines,
PublicationIn the paper a multi-stage micro-turbine with partial admission of all the stages is described in detail and the results of the numerical calculations and experimental investigations are presented, followed by an appropriate discussion and conclusions.