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Search results for: PLASTICS SEPARATION
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Alternative Methods of Preparation of Soluble Keratin from Chicken Feathers
PublicationHuge amount of keratinous waste, especially birds’ feathers, demands more value-added application instead of dumping. The present work reports the results of experiments aimed at preparing soluble keratin useful for novel bioproduct formation. The effect of thermo-chemical treatments with various reducing agents, i.e. 2-mercaptoethanol, dithiothreitol, sodium m-bisulphite, and sodium bisulphite, as well as sodium hydroxide, on...
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Sample preparation and recent trends in volatolomics for diagnosing gastrointestinal diseases
PublicationThe analysis of the human volatilome can be successfully used for rapid and non-invasive diagnostics of gastrointestinal diseases. However, the introduction of techniques based on detection of volatiles is limited, among other factors, by difficulties which arise during the sampling stage and instrumental analysis. The aim of this article was to review and discuss medical and analytical literature on the analysis of volatiles in...
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Convenient and Efficient Diastereoselective Preparation of Functionalized Z -Alkenyl Sulfides
PublicationWe have developed an efficient and convenient regio‐ and stereoselective reduction of the alkynyl sulfides with pinacolborane in the presence of copper(I) chloride to produce (Z)‐alkenyl sulfides in good and very good yields. The functionalized alkynyl sulfides are readily available based on the reaction of lithium acetylides with thiotosylates under mild conditions.
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Manganese Phosphatizing Coatings: The Effects of Preparation Conditions on Surface Properties
PublicationManganese phosphate coating could be used to protect the surface of steel products. However, it is essential to determine the effects which process parameters, as well as the types of additives used, have on the efficiency of coating deposition. Thus, we present here a process of phosphatization of low-alloy steel (for 15 min at 95 ◦C) in manganese/nickel baths followed by a passivation process with the use of a silicon and zircon...
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AN ORIGINAL APPROACH IN THE FIELD OF PREPARATION REFERENCE MATERIALS OF VOLATILE ANALYTES
PublicationStandard gas mixtures (SGM) are indispensable reference materials for ensuring the reliability of analytical work. Reference materials are an excellent tool for the quality control and assurance of analytical results. Standard gas mixtures are unique among reference materials. The rapid progress of SGM production is connected with the instability of gaseous analytes which make them difficult to obtain. The use of standards with...
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Sample preparation techniques for determination of pesticide residues in food samples
PublicationPesticides are very important in increasing the efficiency and quality of agricultural production. They are applied in many spheres of life, not only in agriculture, and their applications are expanding. Despite their numerous merits, pesticides are some of the most toxic substances contaminating our environment and have a negative impact on the human health. Properties of pesticides such as stability, ability to bioaccumulation...
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Use of Ginger Nanofibers for the Preparation of Cellulose Nanocomposites and Their Antimicrobial Activities
PublicationHere, we report, for the first time, the isolation of ginger nanofibers (GNF) from ginger rhizomes spent by acid hydrolysis and followed by high-pressure homogenization. Scanning electron microscopy was utilized to identify the surface morphology of the GNF and the widths ranged between 130 to 200 nm. Structural analysis of GNF was identified by Fourier transform infrared spectroscopy, Differential scanning calorimetry, and X-ray...
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Group 11 complexes with a phosphanylphosphaalkene ligand: preparation and stability study
PublicationThe reactivities of two selected phosphanylphosphaalkenes, Ph2C=P-PtBu2 (1a) and (p-MeO-Ph)2C=P-PtBu2 (1b), toward CuCl, AgCl and (tht)AuCl (tht = tetrahydrothiophene) were investigated. As a result, new phosphanylphosphaalkene dimeric and monomeric complexes were formed (Cu and Ag dimeric and Au monomeric). All obtained products were air and moisture stable and light insensitive.
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Surfactants application in sample preparation techniques: Insights, trends, and perspectives
PublicationSince the implementation of Green Chemistry into analytical practice, significant efforts have been made to improve the sustainability of chemical analysis. These include reducing the use of hazardous chemicals and solvents, minimizing waste, and improving energy efficiency. Surfactants can be applied in chemical analysis as an environmentally friendly alternative to conventional solvents and chemicals. The use of surfactants can...
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Potential Alternative to Styrene–Butadiene–Styrene for Asphalt Modification Using Recycled Rubber–Plastic Blends
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Evaluation of the impact of geometry and plastic deformation on the stray magnetic field around the bone shaped sample
PublicationInfluence of two factors: the variable cross-section and the localized plastic deformation, which affect the stray magnetic field profile of a ferromagnetic sample have been studied. Evaluation of an effect size is based on the analysis of the stray magnetic field component which is tangential to the longest dimension of a sample. However, in order to describe the nature of the stray magnetic field, the normal component (perpendicular...
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Selective H2 production from plastic waste through pyrolysis and in-line oxidative steam reforming
PublicationThis study deals with the proposal of pyrolysis and in-line oxidative steam reforming (P-OSR) for plastic waste valorization and assesses the potential of this strategy for the selective production of H2. Overall, the study aims at progressing towards the fine-tuning of the pyrolysis-reforming technology by co-feeding O2. Thus, a multi-point O2 injection system has been developed to ensure a suitable O2 distribution in the reforming...
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Highly efficient conversion of waste plastic into thin carbon nanosheets for superior capacitive energy storage
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The Dominant Influence of Plastic Deformation Induced Residual Stress on the Barkhausen Effect Signal in Martensitic Steels
PublicationThe paper presents the results of investigation of the influence of plastic deformation on the magnetic properties of martensitic steel (P91 grade). The properties of the hysteresis loops as well as of the Barkhausen effect (BE) signal are analysed for both tensile and compressive loading up to ε = 10% of plastic deformation. The choice of the steel and of the deformation range is unique, since for such combination one can expect...
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An experimental assessment on a diesel engine powered by blends of waste-plastic-derived pyrolysis oil with diesel
PublicationThe utilization of plastic solid wastes for sustainable energy production is a crucial aspect of the circular economy. This study focuses on pyrolysis as an effective method to convert this feedstock into renewable drop-in fuel. To achieve this, it is essential to have a comprehensive understanding of feedstock composition, pyrolysis process parameters, and the physicochemical characteristics of the resulting fuel, all correlated...
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An elasto-plastic constitutive model with non-local softening and viscosity to describe dynamic concrete behaviour.
PublicationW artykule zaproponowano model do opisu betonu podczas dynamicznego obciążenia. Przyjęto model sprężysto-plastyczny z degradacją sztywności i nielokalnym osłabieniem rozszerzony o lepkość. Obliczenia MES dla elementów betonowych pod obciążeniem dynamicznym o różnej prędkości obciążenia porównano z doświadczeniami.
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Green chromatography
PublicationAnalysis of organic compounds in samples characterized by different composition of the matrix is very important in many areas. A vast majority of organic compound determinations are performed using gas or liquid chromatographic methods. It is thus very important that these methods have negligible environmental impact. Chromatographic techniques have the potential to be greener at all steps of the analysis, from sample collection...
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Light‐Driven Multi‐Charge Separation in a Push‐Pull Ruthenium‐Based Photosensitizer – Assessed by RASSCF and TDDFT Simulations
PublicationThe performance of photosensitizers in the field of, for example, solar energy conversion, relies on their light-harvesting efficiency in the visible region, population of long-lived charge separated intermediates, as well as their charge-accumulation capacity amongst other properties. In this computational study, we investigate the photophysical properties of a bis(bipyridyl)ruthenium(II)-based black dye (Ru) incorporating a chromophoric...
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Usefulness of separation techniques for identification and determination of Oxygenated Volatile Organic Compounds used in process analytics of water and wastewater
PublicationW pracy przedstawiono przegląd i porównanie metodyk identyfikacji i oznaczania Lotnych Związków Tlenoorganicznych (LZT). Porównano metodyki klasyczne umożliwiające oznaczanie wybranej grupy związków chemicznych należących do LZT lub dokonywanie oznaczeń sumarycznej zawartości z metodykiami wykorzystującymi techniki rozdzielania. Lotne związki tlenoorganicze, do których zaliczane są aldehydy, alkohole, ketony, estry, etery oraz...
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Separation of Volatile Oxygen-containing Organic Compounds by Gas Chromatography - selectivity comparison of different polarity stationary phases
PublicationThis paper present a results of the separation of 36 reference compounds belonging to the group of Volatile Oxygen-Containing Organic Compounds (OVOCs) using capillary gas chromatography with flame ionization detector (GC-FID) and three stationary phases of different polarity. A selectivity has been studied regarding to OVOCs and n -alkanes. The most useful for the separation of the group OVOCs is a polar ionic liquid stationary...
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Effective Gap Size Index for Determination of Optimum Separation Distance Preventing Pounding between Buildings during Earthquakes
PublicationSeismic excitations may lead to collisions between adjacent civil engineering structures causing major damage. In this paper, an effective equation for calculating the gap size index is proposed so as to provide the optimum separation distance preventing structural pounding during different earthquakes. Evaluation of the best prediction of the required separation distance between two adjacent buildings was carried out by using...
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The Impact of Operational Parameters on Polypropylene Membrane Performance during the Separation of Oily Saline Wastewaters by the Membrane Distillation Process
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Bulky ligands shape the separation between the large spin carriers to condition field-induced slow magnetic relaxation
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The Influence of the Morphology and Mechanical Properties of Polymer Inclusion Membranes (PIMs) on Zinc Ion Separation from Aqueous Solutions
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Multi-DBD plasma actuator for flow separation control around NACA 0012 and NACA 0015 airfoil models
PublicationIn this paper application of innovative multi-DBD plasma actuator for flow separation control is presented. The influence of the airflowgenerated by this actuator on the flow around NACA 0012 and NACA 0015 airfoil models was investigated. The results obtained from 2D PIVmeasurements showed that the multi-DBD actuator with floating interelectrode can be attractive for leading and trailing edge separation control.
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Zr‐Based Metal‐Organic Framework UiO‐66/Ultem® 1000 Membranes for Effective CO2/H2 Separation
PublicationMixed-matrix membranes (MMMs) using UiO-66 nanofillers as dispersing inorganic phase and polyetherimide (PEI) as continuous polymeric matrix were synthesized. Different UiO-66 loadings of 10, 20, and 30 wt % were applied. The morphology and UiO-66 dispersion over the prepared MMMs were examined. Gas separation measurements were performed for H2/CO2 gas mixture to evaluate the influence of UiO-66 on the separation yield of resulting...
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On time-dependent nonlinear dynamic response of micro-elastic solids
PublicationA new approach to the mechanical response of micro-mechanic problems is presented using the modified couple stress theory. This model captured micro-turns due to micro-particles' rotations which could be essential for microstructural materials and/or at small scales. In a micro media based on the small rotations, sub-particles can also turn except the whole domain rotation. However, this framework is competent for a static medium....
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On continuity conditions at the phase interface of two-phase elastic shells
PublicationW pracy rozwinięto ogólną nieliniową teorię powłok sprężystych podlegających przejściom fazowym typu martenzytowego. Przedstawione sformułowanie oparte jest na statycznie i kinematycznie ścisłym modelu powłokowym. Uwzględniono gęstośc energii odkształcenia, jak również siły i momenty zadane wzdłuż krzywoliniowego przejścia fazowego. W szczególności otrzymano statyczne warunki ciągłości wzdłuż koherentnego połączenia oraz połączenia...
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Anti-plane waves in an elastic thin strip with surface energy
PublicationWe consider anti-plane motions of an elastic plate taking into account surface energy within the linear Gurtin–Murdoch surface elasticity. Two boundary-value problems are considered that describe complete shear dynamics of a plate with free faces or with free and clamped faces, respectively. These problems correspond to anti-plane dynamics of an elastic film perfectly or non-perfectly attached to a rigid substrate. Detailed analysis...
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Differential cross section minima in elastic scattering of electrons fromzinc
PublicationZostały obliczone położenia minimów różniczkowych przekrojów czynnych na sprężyste rozpraszanie elektronów na atomach cynku. Metoda obliczeniowa oparta jest na równaniach relatywistycznej mechaniki kwantowej. Wyniki obliczeń zostały porównane z ostatnimi danymi doświadczalnymi grupy z Uniwersytetu Belgradzkiego.
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Critical minima in elastic scattering of electrons from Ar and Zn.
PublicationDokonano obliczeń różniczkowych przekrojów czynnych na sprężyste rozpraszanie elektronów na atomach argonu i cynku. Otrzymane minimum krytyczne z tych przekrojów porównano z niedawno otrzymanymi danymi doświadczalnymi.
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The high-energy critical minimum in elastic electron scattering by argon.
PublicationZostało zbadane położenie wysokoenergetycznego minimum krytycznego w rozpraszaniu elektronów na argonie. W celu przeprowadzenia dyskusji zachowania się czynnego przekroju różniczkowego w okolicy minimum krytycznego przeprowadzono analizę położenia minimum zarówno dla energii, jak i kątów.
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Damage detection in composite truss structure by application of elastic waves.
PublicationW pracy przedstawiono zastosowanie fal sprężystych do detekcji pęknięć zmęczeniowych w konstrukcjach kompozytowych.
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Thermo-elastic non-linear analysis of multilayered plates and shells
PublicationGeometrically nonlinear FEM analysis of multilayered composite plates and shells is performed in order to resolve the stability problem of the structures being under the influence of temperature field. The Riks-Wempner-Ramm algorithm with a specially modified multi-choice unloading condition has been implemented in authors’ numerical code. As the representation of multilayered medium the Equivalent Single Layer approach with the...
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On effective surface elastic moduli for microstructured strongly anisotropic coatings
PublicationThe determination of surface elastic moduli is discussed in the context of a recently proposed strongly anisotropic surface elasticity model. The aim of the model was to describe deformations of solids with thin elastic coatings associated with so-called hyperbolic metasurfaces. These metasurfaces can exhibit a quite unusual behaviour and concurrently a very promising wave propagation behaviour. In the model of strongly anisotropic...
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On Von Karman Equations and the Buckling of a Thin Circular Elastic Plate
PublicationWe shall be concerned with the buckling of a thin circular elastic plate simply supported along a boundary, subjected to a radial compressive load uniformly distributed along its boundary. One of the main engineering concerns is to reduce deformations of plate structures. It is well known that von Karman equations provide an established model that describes nonlinear deformations of elastic plates. Our approach to study plate deformations...
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Low energy elastic electron scattering from benzonitrile (C6H5CN)
PublicationWe present experimental differential elastic scattering cross sections (DCSs) for low energy electron scattering from benzonitrile along with integral and momentum-transfer cross sections that are determined from these DCSs. The measurements of DCSs are obtained using the relative flow method with helium as the standard gas, in a crossed electron-molecular gas beam arrangement. Our measurements are made at incident electron energies...
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Low energy differential elastic electron scattering from trichloromethane
PublicationExperimental differential cross sections for low energy electron scattering from trichloromethane is measured utilizing a crossed electron-molecular beam experiment via the relative flow method, for the incident electron energies in the range of E = 0.5 eV-30 eV and the scattering angles in the range of θ = 10◦ − 130◦ .
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Damage detection strategies based on propagation of guided elastic waves
PublicationW pracy przedstawiono wyniki symulacji numerycznych oraz badań eksperymentalnych nad wykorzystaniemprowadzonych falsprężystych do wykrywania ilokalizacji uszkodzeń w dwu i trójwymiarowych elementach konstrukcyjnych wykonanych z materiałów izotropowych i kompozytowych.
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Accuracy and parameter estimation of elastic and viscoelastic models of water hammer
PublicationW artykule analizowany jest zagadnienie uderzenia hydraulicznego, stanowiące jeden z najważniejszych problemów nieustalonego przepływu w przewodach pod ciśnieniem. Mimo ponad stuletnich doświadczeń w badaniach zagadnienie to jest ciągle nie w pełni rozpoznane. Może być onio rozpatrywane na dwóch płaszczyznach - praktycznej i teoretycznej. W obu przypadkach na etapie rozwiązania powstają problemy sprawiające, że wyniki nie są satysfakcjonujące....
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On shear correction factors in the non-linear theory of elastic shells
PublicationW pracy wyprowadzono analitycznie wartości korekcyjnych współczynników ścinania dla ścinania poprzecznego oraz dla momentów owinięcia w ramach nieliniowej sześcioparametrowej teorii powłok. Wartości wyprowadzono poprzez odpowiednie sformułowanie komplementarnej energii sprężystej. Na drodze analizy przy pomocy MES, badano wpływ wartości współczynników na położenie punktów bifurkacji, deformacje, całkowitą energię sprężystą układu...
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Fracture Energy of Bonded Joints with 2D Elastic Adhesive Layer
PublicationWhen bonded joint is subjected to mode I fracture loading, the adhesive joints analytical solutions treats the adhesive layer, usually, as not existing or 1D Hooke elastic layer. In the case of 1D elastic layer, represented as Hookes spring element, is acting, only, in direction contrary to the applied load. Basing on the information yielded from sensitive laser profilometry technique, where deflections of bonded part of the joint...
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Elastic Fender-Dolphin Interaction for Economic Design of Berthing Dolphins
PublicationThe study addresses the question of the possible design benefits when considering the interaction between a modern marine modular rubber fender and a steel tubular pile substructure of a berthing dolphin. Absorption of the berthing kinetic energy of the vessel by a dualelasticity pile-fender berthing system is described in detail using the interactive treatment method (ITM). Application of the ITM is illustrated by a calculative...
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Low energy elastic scattering of electrons from hexafluoropropene (C3F6)
PublicationWe present cross sections from a joint experimental and theoretical study on elastic electron scattering from hexafluoropropene (C3F6) in the gas phase. The experimental results, using low energy electron spectroscopy, were obtained at incident electron energies of 0.5, 1, 1.5, 2, 3, 4, 5, 6, 10, 12, 15 and 20 eV, for scattering angles ranging from 10°to 130°. The theoretical method used in the computation of the integral, momentum...
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On refined constitutive equations in the six-field theory of elastic shells
PublicationWithin the resultant six-field shell theory, the second approximation to the complementary energy density of an isotropic elastic shell undergoing small strains is constructed. In this case, the resultant drilling couples are expressed explicitly by the stress resultants and stress couples as well as by amplitudes of the quadratic and cubic distributions of an intrinsic deviation vector. The refined 2D strain-stress and stress-strain...
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Comparison of elastic and viscoelastic analysis of asphalt pavement at high temperature
PublicationThere are many various rheological models which are used for modeling of asphalt layers in flexible pavement structures. It can be expected that the use of various models may affect different results of mechanical pavement calculations and analysis. The paper presents comparison of the use of Burgers’ and Huet-Sayegh’s viscoelastic models and Hooke’s elastic model to calculate pavement deflections and strains at the bottom of asphalt...
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Impulsive lubrication of hip joint for hypo-elastic cartilage model
PublicationPraca rozwiązuje problem smarowania stawu biodrowego człowieka w warunkach niestacjonarnych z uwzględnieniem hypo-sprężystych (pod-sprężystych) właściwości odkształcalnej szkieletu chrząstki stawowej. Prezentowane są rozkłady wartości ciśnienia hydrodynamicznego oraz zmienne w czasie rozkłady wartości sił nośnych.
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Asperities and deformations of hyper elastic joint cartilages in cultivation aspects
PublicationPraca opisuje wyniki badań procesu hodowli chrząstki stawowej w bioreaktorze podczas nieustalonego laminarnego przepływu nienewtonowskiej biologicznej cieczy odżywczej wokół chrząstki spoczywającej na rusztowaniu bioreaktora. Badania takie wymagają eksperymentalnego pomiaru chropowatości powierzchni chrząstki.
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Damage detection in elements of strutures by the elastic wave propagation method.
PublicationW pracy przedstawiono wyniki badań dotyczace wykorzystania fal sprężystych do detekcji uszkodzeń i jedno i dwu wymiarowych elementach konstrukcyjnych.
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One-pot synthesis of core/shell Co@C spheres by catalytic carbonization of mixed plastics and their application in the photo-degradation of Congo red
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