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Search results for: MASA BITUMICZNA
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Modeling and control of a redundantly actuated variable mass 3RRR planar manipulator controlled by a model-based feedforward and a model-based-proportional-derivative feedforward–feedback controller
PublicationIn the paper, dynamics of a complex mechatronics system is considered. A redundantly actuated planar manipulator is the base of the mechanical part of it. It is a 3RRR 1 platform based parallel manipulator. To control its trajectory, a model-based feedforward controller is employed. Three aspects are fundamental in the presented investigations. The first focus is on development of an accurate numerical model used to solve the inverse...
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Determination of eight artificial sweeteners and common Stevia rebaudiana glycosides in non-alcoholic and alcoholic beverages by reversed-phase liquid chromatography coupled with tandem mass spectrometry.
PublicationThe method for the determination of acesulfame-K, saccharine, cyclamate, aspartame, sucralose, alitame, neohesperidin dihydrochalcone, neotame and five common steviol glycosides (rebaudioside A, rebaudioside C, steviol, steviolbioside and stevioside) in soft and alcoholic beverages was developed using high-performance liquid chromatography and tandem mass spectrometry with electrospray ionisation (HPLC-ESI-MS/MS). To the best of...
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Dispersive solid-phase extraction using multi-walled carbon nanotubes combined with liquid chromatography–mass spectrometry for the analysis of β-blockers: Experimental and theoretical studies
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High performance super-twisting sliding mode control for a maritime autonomous surface ship (MASS) using ADP-Based adaptive gains and time delay estimation
PublicationThis research addresses two kinds of problems related to optimal trajectory tracking of a Maritime Autonomous Surface Ship (MASS): those caused by the time-varying external disturbances including winds, waves and ocean currents as well as those resulting from inherent dynamical uncertainties. As the paper shows, an accurate and robust optimal controller can successfully deal with both issues. An improved Optimal Adaptive Super-Twisting...
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Przemówienie wygłoszone 16 maja 2017 roku podczas inauguracji konferencji naukowej "Obszary fennistyki: język – kultura – naród" na Uniwersytecie Gdańskim (Konferenssin terveliaispuhe)
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Determination of parent and methylated polycyclic aromatic hydrocarbons in water samples by dispersive liquid–liquid microextraction–two dimensional gas chromatography–time-of-flight mass spectrometry
PublicationPolycyclic aromatic hydrocarbons (PAHs) are contaminants frequently found in environmental waters. Owing to their toxic effects, it is important to develop analytical methodologies that allow their fast and reliable determination. Dispersive liquid–liquid microextraction (DLLME) allows a quick extraction of analytes with little organic solvent consumption. The best results regarding sample preparation are obtained when 40 mL of...
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Stabilities of bisphenol A diglycidyl ether, bisphenol F diglycidyl ether, and their derivatives under controlled conditions analyzed using liquid chromatography coupled with tandem mass spectrometry
PublicationBisphenol A diglycidyl ether (BADGE), bisphenol F diglycydyl ether (BFDGE), and their related compounds are widely used as precursors in production of epoxy resins. The high reactivity of these compounds makes the development of analytical methodologies that ensure appropriate metrological accuracy crucial. Consequently, we aimed to determine whether and to what extent the composition of the solution and storage conditions affect...
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Comparison of hydrophilic interaction and reversed phase liquid chromatography coupled with tandem mass spectrometry for the determination of eight artificial sweeteners and common steviol glycosides in popular beverages
PublicationHydrophilic interaction liquid chromatography (HILIC) coupled with tandem mass spectrometry (MS/MS) was used to separate artificial and natural sweeteners approved for use in European Union (EU). Among three tested HILIC columns (BlueOrchid PAL-HILIC, Ascentis Express Si and Acclaim™ Trinity™ P2) the last one was selected for the development of HILIC method due to the best results obtained with it. Early eluting and coeluting compounds...
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Sample preparation procedure using extraction and derivatization of carboxylic acids from aqueous samples by means of deep eutectic solvents for gas chromatographic-mass spectrometric analysis
PublicationThe paper presents a new procedure for the determination of organic acids in a complex aqueous matrixusing ultrasound-assisted dispersive liquid–liquid microextraction followed by injection port derivati-zation and GC–MS analysis. A deep eutectic solvent (choline chloride: 4-methylphenol in a 1:2 mol ratio)was used both as an extracting solvent and as a derivatizing agent to yield ion pairs which were next con-verted to methyl...
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The preparation and evaluation of core-shell magnetic dummy-template molecularly imprinted polymers for preliminary recognition of the low-mass polybrominated diphenyl ethers from aqueous solutions
PublicationThe design, preparation process, binding abilities, morphological characteristic and prospective field of application of dummy-template magnetic molecularly imprinted polymer (DMMIP) for preliminary recognition of the selected low-mass polybrominated diphenyl ethers (PBDE-47 and PBDE-99) from aquatic environment were investigated. The surface of iron oxide (Fe3O4) nanopowder (50-100 nm particles size) was modified with tetraethoxysilane...
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Novel liquid chromatography method based on linear weighted regression for the fast determination of isoprostane isomers in plasma samples using sensitive tandem mass spectrometry detection
PublicationA simple, fast, sensitive and accurate methodology based on a LLE followed by liquid chromatography–tandem mass spectrometry for simultaneous determination of four regioisomers (8-iso prostaglandin F2α, 8-iso-15(R)-prostaglandin F2α, 11β-prostaglandin F2α, 15(R)-prostaglandin F2α) in routine analysis of human plasma samples was developed. Isoprostanes are stable products of arachidonic acid peroxidation and are regarded as the...
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High performance super-twisting sliding mode control for a maritime autonomous surface ship (MASS) using ADP-Based adaptive gains and time delay estimation
PublicationThis research addresses two kinds of problems related to optimal trajectory tracking of a Maritime Autonomous Surface Ship (MASS): those caused by the time-varying external disturbances including winds, waves and ocean currents as well as those resulting from inherent dynamical uncertainties. As the paper shows, an accurate and robust optimal controller can successfully deal with both issues. An improved Optimal Adaptive Super-Twisting...
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Ultrasound assisted solvent extraction of porous membrane-packed samples followed by liquid chromatography-tandem mass spectrometry for determination of BADGE, BFDGE and their derivatives in packed vegetables
PublicationThe problem of the presence of trace organic pollutants in food is of growing importance due to increasing awareness about their impact on newborns, infants and adults of reproductive age. Despite the fact that packaged food products offer many advantages, packaging can be a source of contamination for stored food. Thus, monitoring such pollution in food is of high importance. In this work, a novel methodology based on the solvent...
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Rapid ion-exchange matrix removal for a decrease of detection limits in the analysis of salt-rich reservoir waters for fluorobenzoic acids by liquid chromatography coupled with tandem mass spectrometry
PublicationA matrix removal procedure with ion-exchange resin prior to analysis for 18 fluorinated benzoic acids (FBAs) tracers in saline (>25% salt) reservoir water was optimized. The elimination of >98% of salt and the simultaneous matrix sample cleanup allowed the direct analysis using the supernatant by liquid chromatography coupled with tandem mass spectrometry (LC-MS/MS). This resulted in a gain in detection limits for most of the tracers...
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Characterization of GM3 Gangliosides in Human Milk throughout Lactation: Insights from the Analysis with the Use of Reversed-Phase Liquid Chromatography Coupled to Quadrupole Time-Of-Flight Mass Spectrometry
PublicationGangliosides are complex lipids found in human milk that play important structural and biological functions. In this study, we utilized reversed-phase liquid chromatography coupled to quadrupole time-of-flight mass spectrometry to evaluate the molecular distribution of GM3 in human milk samples collected at distinct lactation stages, ranging from colostrum to advanced lactation samples. Throughout lactation, GM3 d40:1 emerged as...
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Quantification of key red blood cell folates from subjects with defined MTHFR 677C>T genotypes using stable isotope dilution liquid chromatography/mass spectrometry
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Determination of tributyltin (TBT) in marine sediment using pressurised liquid extraction–gas chromatography–isotope dilution mass spectrometry (PLE–GC–IDMS) with a hexane–tropolone mixture
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Determination of tributylotin (TBT) in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry (PLE-GC-IDMS) with a hexane-tropolone mixture
PublicationOpracowano metodę oznaczania zawartości tributylocyny w próbkach osadu morskiego. Na etapie izolacji zastosowano technikę przyspieszonej ekstrakcji za pomocą roztworu tropolonu w heksanie.Na etapie oznaczeń końcowych wykorzystano technikę chromatografii gazowej, stosując metodę spektrometrii mas rozcieńczenia izotopowego. Wyznaczono parametry walidacyjne opracowanej metody: granicę wykrywalności, precyzję, poprawność i niepewność.
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Sprawozdanie z międzynarodowej konferencji naukowej A Lost World? Jewish International Lawyers and New World Orders (1917–1951), Jerozolima, 24–25 maja 2021 r.
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Surface characteristics of glass fibres covered with an aluminum layer after a chemical modification process using secondary ion mass spectrometry (SIMS) and atomic force microscopy (AFM)
PublicationPrzedstawiono wyniki z badań powierzchni modyfikowanych włókien szklanych (przed i po procesie chemicznej modyfikacji ich powierzchni), które są kandydatem na przyszły oryginalny bezmatrycowy materiał odniesienia lotnych analitów etenu (C2H4) metodami spektrometrii mas jonów wtórnych oraz mikroskopii sił atomowych. Badania miały na celu obserwację zmian oraz procesów, jakie zaszły na powierzchni włókien szklanych pokrytych...
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain monocarboxylic acids in cattle farm wastewater and waste landfill leachates
PublicationZaproponowano metodykę oznaczania krótkołańcuchowych kwasów monokarboksylowych w ściekach z hodowli bydła i odciekach ze składowisk zawierających organiczne odpady, oparta na technice mikroekstrakcji do fazy stacjonarnej z fazy nadpowierzchniowej próbek ciekłych, w połączeniu ze sprzężonym układem GC-MS.
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Green, simple analytical method for biogenic amines determination in fruit juice samples using salting-out assisted liquid-liquid microextraction and gas chromatography-mass spectrometry
PublicationSalting-out assisted liquid-liquid microextraction (SALLME) was integrated with the derivatization procedure to establish a one-step sample pre-treatment approach for rapid analysis of 14 biogenic amines (BAs) in fruit juices. The methodology consists of salting-out of analytes, derivatization with ethyl chloroformate (ECF), extraction with ethyl acetate (EtAc), and the analysis of the derivatized BAs using gas chromatography-mass...
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A nontargeted approach to determine the authenticity of Ginkgo biloba L. plant materials and dried leaf extracts by liquid chromatography-high-resolution mass spectrometry (LC-HRMS) and chemometrics
PublicationThe lack of stringent regulations regarding raw materials for herbal supplements used for medicinal purposes has been a constant challenge in the industry. Ginkgo biloba L. leaf extracts attract consumers because of the supposed positive effect on mental performance and memory. Supplements are produced using dried leaf materials and standardized leaf extracts such as EGb 761. Adulteration of Ginkgo biloba L. plants and extracts...
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Simultaneous analysis of non-steroidal anti-inflammatory drugs and estrogenic hormones in water and wastewater samples using gas chromatography–mass spectrometry and gas chromatography with electron capture detection
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Application of gas flow headspace liquid phase micro extraction coupled with gas chromatography-mass spectrometry for determination of 4-methylimidazole in food samples employing experimental design optimization
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Marta Kuc-Czerep, Niemieckojęzyczni mieszkańcy Warszawy. Droga do obywatelstwa w osiemnastowiecznej Rzeczypospolitej, Wydawnictwo Instytutu Historii Polskiej Akademii Nauk, 2021, ss. 444 + mapa.
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INNOVATIVE THERMODYNAMICAL CYCLES BASED ON ENHANCEMENT MASS, MOMENTUM, ENTROPY AND ELECTRICITY TRANSPORT DUE TO SLIP, MOBILITY, TRANSPIRATION, ENTROPY AND ELECTRIC JUMPS AS WELL AS OTHER NANO-FLOWS PHENOMENA
PublicationIn our work, a further development of the authors model of thermo-chemical flow of fuel, air, oxygen, steam water, species, ionic and electron currents within nano channels and nano-structures of novel devices is presented. Different transport enhancement models are taken into account -among them the most important are: the velocity slip connected with complex external friction, the Darcy mobility and the Reynolds transpiration....
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Mobility Oriented Development (MOD): Public-Private Partnership in Urban Parking & Traffic Management with the Use of Autonomous Automobiles, Car-Sharing, Ridesharing Modes of Transport & Mobility as a Service (MaaS)
PublicationThe focus of the following research are relations between mobility technologies and metropolitan (urban and suburban) spatial structures. In this paper the author discusses various urban modes of transport (automobile, mass transit) in the context of emerging technical (autonomous vehicles, self-driving cars and driverless shuttles) and organizational (carpooling, ridesharing, car-sharing, on-demand mobility) solutions for " mobility...
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The presence of polycyclic aromatic hydrocarbons in disposable baby diapers: A facile determination method via salting-out assisted liquid-liquid extraction coupled with gas chromatography-mass spectrometry
PublicationIn this paper we demonstrate the development of the extraction procedure of polycyclic aromatic hy- drocarbons from baby diapers along with their quantification by gas chromatography-mass spectrometry. Apart from covering plastic foil, disposable baby diapers contain sorbents intended to absorb urine and feces. A hygroscopic, adsorptive, and tough-to-homogenize fibrous sorbent, represents an analytical chal- lenge to analytical...
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Polsko-fiński tezaurus tematyczny. Część I: Ziemia i Kosmos = Puolalais-suomalainen asiasanasto. Osa I: Maa ja Maailmankaikkeus (książka)
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Identyfikacja lotnych składników ścieków z instalacji oksydacji asfaltów z wykorzystaniem chromatografii gazowej sprzężonej ze spektrometrią mas (GC-MS)
PublicationW pracy przedstawiono wyniki badań nad identyfikacją lotnych związków organicznych występujących w ściekach z instalacji oksydacji asfaltów. Ścieki poddano deemulgacji, w celu usunięcia fazy organicznej, a następnie ekstrakcji dichlorometanem, w celu wyizolowania pozostałych w ściekach związków organicznych. Zidentyfikowano 30 związków organicznych oraz szereg n-alkanów, które pozostały w ściekach pomimo zastosowanej deemulgacji....
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Novel analytical approach for real-time monitoring of volatile Maillard reaction products emitted from the sugar-amino acid model system using proton transfer reaction mass spectrometry
PublicationIn the presented research, volatile Maillard reaction products formation in the two sugar-amino acid model systems, namely glucoselysine and ribose-lysine model systems were investigated using proton transfer reaction mass spectrometry. Obtained data were supported by the reference method, i.e., UV/Vis spectrometry. A number of volatile organic compounds were selected based on the correlation of the effect of Maillard reaction...
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Association between plasma proteome profiles analysed by mass spectrometry, a lymphocyte-based DNA-break repair assay and radiotherapy-induced acute mucosal reaction in head and neck cancer patients
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Struktury oraz mapy przepływu R1233zd w okrągłym minikanale przy średnich i wysokich wartościach ciśnienia zredukowanego [w:] Postępy w badaniach wymiany ciepła i masy
PublicationW wiedzy dotyczącej struktur przepływu niskowrzących czynników roboczych w zakresie wysokich temperatur nasycenia (powyżej 120°C) oraz średnich i wysokich wartościach ciśnienia zredukowanego (0.5-0.9) występuje luka. W literaturze obecne są dane dotyczące podobnych wartości ciśnień zredukowanych, ale dla niższych wartości temperatury nasycenia (głównie z zakresu -20°C do 40°C). Wynika to z dotychczasowych zastosowań chłodniczych...
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Historia we współczesności. Pas Nadmorski w Gdańsku : dobro wspólne na miarę metropolitalną
PublicationW ramach prowadzonych w semestrze letnim 2010/2011 przez Katedrę Historii, Teori Architektury i Konserwacji Zabytków cyklu otwartych wykładów ''Historia we współczesności'', dr Bartosz Macikowski wygłosił 18 maja 2011 r. wykład na temat Pasa Nadmorskiego w Gdańsku. Artykuł w ''Piśmie PG'' poświęcony tematyce poruszonej na wykładzie opracowany został przez autorów części urbanistycznej społecznej koncepcji zagospodarowania Pasa...
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Możliwości zamiany strumieni ciepła odpadowego silników pojazdów na moc efektywną
PublicationW pracy przedstawiono przegląd wybranych pozycji literatury na temat możliwości wykorzystania ciepła odprowadzanego od silnika do otoczenia. Wymieniono głównie nowe nie stosowane seryjnie ale obecnie projektowane i badane układy. Wskazano na niekorzystne cechy takie jak duża masa i koszty układów parowych. Termogeneratory z kolei charakteryzują się małą mocą elektryczną na jednostkę masy. W ostatnim rozdziale wspomniano o akumulacji...
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Study on products of enzymatic hydrolysis of pulp from poplar wood (Populus alba L.) Badanie produktów hydrolizy enzymatycznej masy celulozowej pozyskanej z drewna topoli (Populus alba L.)
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Significant Decrease in Glycated Hemoglobin, 2h-Post-Load Glucose and High-Sensitivity C-Reactive Protein Levels in Patients with Abnormal Body Mass Index after Therapy with Manual Lymphatic Drainage
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Symulacje habitatów marsjańskich.
PublicationW pierwszych misjach załogowych na Marsa ludzie będą mieszkać w prostych metalowych modułach. Ich gabaryty i masa będą niewielkie ze względu na ograniczone możliwości rakiet wynoszących. W programie MARS (Mars Analogue Research Station) zorganizowanym przez stowarzyszenie Mars Society prowadzi się symulacje życia i pracy przyszłych marsonautów. Pomaga to m. in. w ozptymalizowaniu układu funkcjonalnego w module. Trwają poszukiwania...
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Accurate, Direct, and High-Throughput Analyses of a Broad Spectrum of Endogenously Generated DNA Base Modifications with Isotope-Dilution Two-Dimensional Ultraperformance Liquid Chromatography with Tandem Mass Spectrometry: Possible Clinical Implication
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Wpływ stężenia cząstek ciała stałego na szybkość desorpcji amoniaku
PublicationZbadano wpływ stężenia cząstek ciała stałego na szybkość desorpcji amoniaku z fazy ciekłej do przepływającego powietrza. Badania przeprowadzono w kolumnie barbotażowej, stosując zawiesiny tlenku glinu lub celulozy o stężeniach do 6% (mas.) w wodnym roztworze amoniaku o stężeniu 0,4% (mas.). Wyznaczono stopień desorpcji amoniaku oraz objętościowy współczynnik przenikania masy. W zawiesinach tlenku glinu, zarówno stopień desorpcji...
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Stochastic model of the process of starting combustion engines and practical application of the process
PublicationW atrykule zaproponowano model procesu rozruchu silników o zapłonie samoczynnym w formie procesu semimarkowskiego dyskretnego w stanach i ciągłego w czasie. Zaproponowano również koncepcję zastosowania opracowanego modelu do określenia ilości substancji szkodliwych, jakie są emitowane wraz z spalinami do otoczenia podczas rozruchu każdego silnika. W rozważaniach tych przyjęto, że statystyka zmiennej losowej, rozumianej jako masa...
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“Dilute & Shoot” approach for rapid determination of trace amounts of nicotine in zero-level e-liquids by reversed phase liquid chromatography and hydrophilic interactions liquid chromatography coupled with tandem mass spectrometry-electrospray ionization
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Development of a solventless stir bar sorptive extraction/thermal desorption large volume injection capillary gas chromatographic-mass spectrometric method for ultra-trace determination of pyrethroids pesticides in river and tap water samples
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Koncepcja zapewnienia interoperacyjności w rozproszonych systemach uczelnianychW : Perspektywy Rozwoju e-Uczelni w Kontekście Globalnej Informatyzacji; - e-uczelnia, konferencja krajowa; 14-15 maja 2009, Gdańsk. - [skrypt prezentacji]
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“Dilute & Shoot” approach for rapid determination of trace amounts of nicotine in zero-level e-liquids by reversed phase liquid chromatography and hydrophilic interactions liquid chromatography coupled with tandem mass spectrometry-electrospray ionization
PublicationTwo analytical procedures are proposed where HILIC and RPLC techniques are coupled with tandem mass spectrometry detection for rapid determination of trace amounts of nicotine in zero-level liquids for electronic cigarettes. Samples are prepared on the basis of the approach “dilute & shoot” which makes this important step quick and not complicated. The chromatographic separation was carried out on a Zorbax XDB column (RPLC method)...
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Fast, sensitive and reliable multi-residue method for routine determination of 34 pesticides from various chemical groups in water samples by using dispersive liquid – liquid microextraction coupled with gas chromatography – mass spectrometry
PublicationA simple and efficient dispersive liquid-liquid microextraction technique (DLLME) was developed by using a mixture of two solvents: 40 μL of tetrachlorethylene (extraction solvent) and 1.0 mL of methanol (disperser solvent), which was rapidly injected with a syringe into 10mL ofwater sample. Some important parameters affecting the extraction efficiency, such as type and volume of solvents, water sample volume, extraction time,...
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Właściwości elastomerów poliuretanowych otrzymanych z prepolimerów zawierających glikolizaty
PublicationZaprezentowano wyniki badań elastomerów poliuretanowych otrzymanych z prepolimerów zsyntezowanych z MDI i glikolizatów. Jako przedłużaczy prepolimerów zastosowano dwyfunkcyjne środki chemiczne różniące się masą cząsteczkową. Elastomery poddano badaniom derywatograficznym w których wyznaczono temperatury spadków masy o 5 i 10% oraz scharakteryzowano ich właściwości mechaniczne w warunkach statycznych i dynamicznych (metoda DMA)
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Fundamentals of Communication Networks Resilience to Disasters and Massive Disruptions
PublicationCommunication networks are exposed to a variety of massive failure events following from activities of nature, weather-induced disruptions, technology-implied problems, and malicious human activities. In this chapter, we first highlight the characteristics of these scenarios and discuss example failure events reported during the last three decades. Next, we explain the concept of network resilience and present an overview of major...
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Modelowanie i symulacja ruchu pojazdu zabytkowego podczas hamowania
PublicationOpracowano model samochodu zabytkowego z wykorzystaniem metody masa-sprężyna, służącego do symulacji procesu hamowania pojazdu zabytkowego z możliwością pomiaru drogi hamowania. Konfiguracja sieci połączeń między punktami mas elementów zawieszenia oraz opony okazuje się mieć bardzo duży wpływ na zachowanie symulowanego samochodu podczas hamowania. Poprawność symulacji sprawdzono porównując wyniki uzyskane z symulacji oraz z pomiarów...