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Search results for: wax crystals
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Preparation of platinum modified titanium dioxide nanoparticles with the use of laser ablation in water
PublicationWe report on the preparation method of nanocrystalline titanium dioxide modified with platinum by using nanosecond laser ablation in liquid (LAL). Titania in the form of anatase crystals has been prepared in a two-stage process. Initially, irradiation by laser beam of a titanium metal plate fixed in a glass container filled with deionized water was conducted. After that, the ablation process was continued, with the use of a platinum...
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Optimization of Polycrystalline CVD Diamond Seeding with the Use of sp³/sp² Raman Band Ratio
PublicationThe influence of various nanodiamond colloids used for seeding nondiamond substrates in microwave plasma enhanced chemical vapour deposition diamond process was investigated. Colloids based on deionized water, isopropanol alcohol and dimethyl sulfoxide (DMSO) were used with different grain size dispersion: 150, 400 and 35 nm, respectively. The influence of growth time was also taken into consideration and bias enhanced nucleation....
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Influence of chloroform on crystalline products yielded in reactions of 5,10,15,20-tetraphenylporphyrin with HCl and copper(II) salts
PublicationStwierdzono, że chloroform wbudowuje się do sieci krystalicznej dichlorowodorku 5,10,15,20-tetrafenyloporfiryny, oraz że powoduje krystalizację nowej, jednoskośnej odmiany polimorficznej porfirynianu miedzi(II), CuTPP. W pracy opisano strukturę krystaliczną solwatu dichlorowodorku porfiryny z ośmioma cząsteczkami chloroformu, C44H32N42+·2Cl-·8CHCl3, i porównano ją...
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(2,2'-Bipyridine)bis(tri-tert-butoxysilanethiolato-kS)lead(II) and (4,7-diphenyl-1,10-phenanthroline-k2N,N')bis(tri-tert-butoxysilanethiolato-kS)lead(II) benzene hemisolvate
PublicationWyznaczono i opisano struktury rentgenowskie tytułowych związków. Atom ołowiu w obu przypadkach wykazuje koordynację typu zniekształconej piramidy kwadratowej o rdzeniu PbON2S2 w której jeden z atomów siarki leży w pozycji osiowej. Struktury są stabilizowane przez oddziaływania międzycząsteczkowe typu pi-pi oraz C-H...pi.
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Supramolecular structures of bis-thionooxalamic acid esters derived from (±)-cyclohexane-1,2-diamine and (±)-1,2-diphenylethylenediamine
PublicationZsyntezowano dwa racemiczne estry kwasu bis(tiooksamowego) i zbadano ich sposób upakowania w sieci krystalicznej. Analiza rentgenograficzna monokryształów badanych związków wykazała, że organizują się one w jednowymiarowe struktury, które tworzone są przez molekuły o przeciwnej chiralności, połączone za pomocą trójcentrowych wiązań wodorowych C=S...NH...O=C. Powstające agregaty są dodatkowo stabilizowane przez słabe oddziaływania...
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The 2:1 cocrystal of benzamide and pentafluororbenzoic acid
PublicationKrystaliczna struktura centrosymetrycznej supermolekuły składa się z czterech cząsteczek benzamidu oraz dwóch kwasu karboksylowego, które powiązane są ze sobą za pomocą wiązań wodorowych typu O-H...O oraz N-H...O.
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The first compound with an unusual type of anion, [Li(SR)2]-:bis(µ2-aqua-d2)tetrakis(aqua-d2)]dilithium(I)bis[bis(tri-tert-butoxysilanethiolato-k2O,S)lithate(I)]dihydrate-d2
PublicationTytułowy związek [Li2(D2O)6][Li(C9H27SSiO3)2]2*2D2O, jest pierwszym związkiem z wiązaniem S-M (M-metal alkaliczny), zawierającym niespotykany typ anionu litanowego: [Li(SR)2]-,gdzie R=Si{OC{CH3)3}3. Centrum symetrii związku znajduję się pośrodku pierścienia Li2O2 wchodzącego w skład kationu. Wszystkie atomy litu budujące rdzenie kationów - LiO4 i anionów - LiO2S2, są czterokoordynacyjne. Jednoujemne aniony [Li(SR)2]- są dobrze...
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(Di-tert-butylmethylphosphane)(η2-di-tert-butylphosphanylphosphinidene)(triphenylphosphane)platinum(0)
PublicationStruktura krystaliczna tytułowego związku, [(Ph3P)(tBu2PMe)Pt(η2-tBu2PP)], zawiera cztery cząsteczki w części niezależnej nieznacznie różniące się konformacjami. Odległości P-P w ligandzie tBu2PP są zbliżone dla wszystkich czterech cząsteczek [2.0661(13)-2.0678(13)A˚]. Odległości te, wskazują na wielokrotny charakter wiązania P-P w ligandzie tBu2PP. Atom platyny w kompleksie wykazuje koordynację płaską kwadratową. Prezentowana...
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A study of chirality in bis(1,2-dimethoxyethane-κ^2 O,O')sodium bis(tri-tert-butoxysilanethiolato-κ2O,S)sodate
PublicationPraca prezentuje analizę samoorganizacji związku kompleksowego z prostszych jonów na przykładzie silanotiolanosodanu bis(dimetoksyetan)sodu. Stwierdzono, że w anionie (RS)2Na- obie grupy tri-tert-butoksysilanotiolanowe mają tę samą skręcalność - obie (P) lub obie (M). Zjawisko to występuje we wszystkich znanych sodanach i litanach zawierających grupę (tert-BuO)3SiS.
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Two pseudopolymorphs of licl trimers with semicubane structures
PublicationCząsteczki tytułowych związków w ciele stałym przyjmują strukturę semikubanów - jest to pierwsza tego typu struktura dla solwatowanego chlorku litu. Jej budowę można opisać jako kuban [Li4Cl4(OPEt3)4], w którym jedna z cząsteczek LiCl została usunięta. Brak tej cząsteczki, a dokładniej mostkującego atomu Li, powoduje deformację struktury kubanu. Naroża zdeformowanego kubanu stanowią trzy atomy litu pochodzące z LiCl oraz cztery...
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Two isomorphic ZnII/CoII complexes with tri-tert-butoxysilanethiol and histamine, and (4-hydroxymethyl-1H-imidazole-κN)bis(tri-tert-butoxysilanethiolato-κ2O,S)zinc(II)
PublicationOtrzymano dwa izomorficzne kompleksy cynku(II) i kobaltu(II) z tri-tert-butoksysilanotiolem i histaminą oraz kompleks cynku(II) z tri-tert-butoksysilanotiolem i 4(5)-hydroksymetyloimidazolem. Scharakteryzowano strukturę otrzymanych kompleksów w ciele stałym.
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Tetraethylammonium bis(N,N-diethyldithiocarbamato-k2S,S')iodocadmate(II)
PublicationW ramach prezentowanej pracy otrzymano bis-(N,N-dietyloditiokarbaminiano-2S,S')jodokadmian tetraetyloamoniowy, krystalizujący w układzie rombowym, w grupie przestrzennej Pnma. Związek ten posiada kompleksowy anion [Cd(S2NEt2)2I]-, w którym do centralnego atomu Cd przykoordynowane są dwa kleszczowe ligandy ditiokarbaminianowe oraz atom jodu. Centralny rdzeń tego związku, w odróżnieniu od innych układów typu [Cd(dtc)X], posiada...
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10-Methyl- and 9,10-dimethyl acridinium methyl sulfate
PublicationThe title compounds, C(14)H(12)N(+).CH(3)O(4)S(-), (I), and C(15)H(14)N(+).CH(3)O(4)S(-), (II), respectively, crystallize with the planar 10-methylacridinium or 9,10-dimethylacridinium cations arranged in layers, parallel to the twofold axis in (I) and perpendicular to the 2(1) axis in (II). Adjacent cations in both compounds are packed in a 'head-to-tail' manner. The methyl sulfate anion only exhibits planar symmetry in (II)....
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9-(Trichloroacetylimino)acridine monohydrate
PublicationThe title compound, alternatively called N-acridin-9(10H)-ylidene-2,2,2-trichloroacetamide monohydrate, C15H9Cl3N2O·H2O, crystallizes in space group P21/c with Z = 4. The acridine moieties are arranged in layers, tilted at an angle of 15.20 (4)° relative to the ac plane, while adjacent molecules pack in a head-to-tail manner. Acridine and water molecules form columns along the b axis held in place by a network of hydrogen...
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Bis(diisopropylammonium) thiosulfate and bis(tert-butylammonium) thiosulfate
PublicationTwo new dialkylammonium thiosulfates, namely bis(diisopropylammonium) thiosulfate, 2C6H16N+S2O3 2-, (I), and bis(tert-butylammonium) thiosulfate, 2C4H12N+S2O3 2-, (II), have been characterized. The secondary ammonium salt (I) crystallizes with Z = 4, while the primary ammonium salt (II), with more...
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Video traffic data - Interchange Sulno (S1-94), Poland
Open Research DataThe data includes video traffic data registered with 8 video cameras at weaving area (weaving section type A) of the Sulno interchange within S1 expressway in Poland (interchange of expressway S1 and national road 94), located in the Silesian Agglomeration. The data covers the two days: 12.09.2017 (expressway S1) and 13.09.2017 (road 94).
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Module of priorities for public transport vehicles in the TRISTAR system
PublicationOne of the most important elements of the intelligent traffic control systems is the ability to control movement in such a way as to privilege the selected users movement, in particular public transport vehicles. Implemented at the Tri-City the TRISTAR system will also have a module for prioritizing public transport vehicles. The article presents a characteristics of the priority action system: the way of communication with the...
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Collaborative approach to WordNet and Wikipedia integration
PublicationIn this article we present a collaborative approach tocreating mappings between WordNet and Wikipedia. Wikipediaarticles have been first matched with WordNet synsets in anautomatic way. Then such associations have been evaluated andcomplemented in a collaborative way using a web application.We describe algorithms used for creating automatic mappingsas well as a system for their collaborative development. Theoutcome enables further...
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L'Italie. Gagner à tout prix. L'industrie de l'armenent italien pendant la Grande Guerre
PublicationThe chapter outlines the economic and technological transformations of the Italian armament industry during the First World War
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Guitar String Sound Retrieved from Moving Pixels
PublicationThe aim of this study was to develop a method of visual recording and analyzing the vibrations of guitar strings using high-speed cameras and dedicated video processing algorithms. The recording of a plucked string reveals the way in which the deformations propagate, composing the standing and travelling wave. The paper compares the results for a few selected models of classical and acoustic guitars, and it involves processing...
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Nowy wewnątrzbudynkowy algorytm wyznaczania położenia obiektów
PublicationW referacie zaprezentowano nowy wewnątrzbudynkowy algorytm wyznaczania położenia obiektów WAP. W algorytmie tym uwzględnia się właściwości środowiska propagacyjnego, dzięki czemu dokładność estymat położenia obiektów wyznaczonych algorytmem WAP jest większa niż wyznaczonych znanymi algorytmami Chana oraz Foy’a. W referacie przedstawiono wyniki analizy porównawczej tych trzech algorytmów z użyciem rzeczywistych pomiarów odległości...
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Navigational decision support system during approach manoeuvre in emergency STS transfer operation
PublicationThe paper is concerned with the problem of safe trajectory planning for approaching during emergency STS (Ship to Ship) transfer operation with oil spill. The safe trajectory means that the way points does not cross in the area of the environment with the static and dynamic obstacles and at the same time satisfies ship's stopping and speed deceleration performance. The evolutionary path planning algorithm is used to determine trajectory...
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Przewodnik Architektoniczny=Architectural Guide=Architekturführer. Gdynia
PublicationGdynia is a unique city that is particularly interesting for architects due to its homogeneous architecture. The city, based on the structure of an earlier fishing village, was entirely designed and built from scratch in the interwar period, as was the case later for cities such as Brasilia and Chandigarh. Today, Gdynia is a modern port town that forms the Tri-City metropolitan area together with Gdańsk, the city of amber, and...
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Income obtained according to particular rates only by taxpayers conducting non-agricultural business activity in 2016
Open Research DataA special form of income taxation addressed to the SME sector is the Lump sum on registered income, which is a simplified form of income tax payment for natural persons conducting business activity.The choice of this form of taxation is optional. In 2016, the tax in this form could be paid by taxpayers who in 2015 obtained income from non-agricultural...
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Le trasformazioni economiche globali
PublicationThe chapter highlights the main economic trasformations of the world economy after the end of Cold War until 2018
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Krzysztof Nowicki dr inż.
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Learning and memory processes in autonomous agents using an intelligent system of decision-making
PublicationThis paper analyzes functions and structures of the memory that is an indispensable part of an Intelligent System of Decision-making (ISD), developed as a universal engine for autonomous robotics. A simplified way of processing and coding information in human cognitive processes is modelled and adopted for the use in autonomous systems. Based on such a knowledge structure, an artificial model of reality representation and a model...
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Sugar Fee in Poland as an Example of New Fiscal Burdens and Stimulation of Consumer Behaviour
PublicationDuring the economic downturn caused by the COVID-19 pandemic, the amount and structure of tax burdens imposed by the state on businesses continue to increase, as shown on the example of the newly introduced sugar fee. A new tax-related burden imposed on businesses and consumers producing and consuming sugar-sweetened beverages appeared at the beginning of 2021. The aim of the paper is to present the fiscal burdens that accompany...
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Learning and memory processes in autonomous agents using an intelligent system of decision-making
PublicationThis paper analyzes functions and structures of the memory that is an indispensable part of an Intelligent System of Decision-making (ISD), developed as a universal engine for autonomous robotics. A simplified way of processing and coding information in human cognitive processes is modelled and adopted for the use in autonomous systems. Based on such a knowledge structure, an artificial model of reality representation and a model...
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Preparation and characterization of Pt/Pd-modified titanium dioxidenanoparticles for visible light irradiation
PublicationSeries of Pt/Pd–TiO2photocatalysts were obtained using the sol–gel method. The Pt/Pd–TiO2nanocom-posites showed significant visible light photoactivity. X-ray diffraction, STEM microscopy, UV–visspectroscopy and BET characterization allowed to conclude that the photocatalysts at the best perfor-mance had the anatase structure, 91 m2/g specific surface area, Pt/Pd alloy structure and 1–4 nm particlesize. The photocatalytic activity...
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Reactions of the Lithiated DiphosphinetBu2P-P(SiMe3)Li with [(η6-C6H6)RuCl2]2in the Presence of Tertiary Phosphines
PublicationtBu2P–P(SiMe3)Li reacted with [(η6-C6H6)RuCl2]2at–40 °C in the presence of PR3(PR3=PEt3,PEt2Ph, PEtPh2) by the nucleophilic addition of the tBu2P–P(SiMe3) moiety to the benzene ring to yield solely the complexes [(R3P)2Ru(Cl)-{η5-C6H6(Me3SiP–PtBu2)}] (1). These products decomposed slowly at ambient temperature to yield benzene, Ru clusters, and small amounts of the dinuclear ruthenium complexes [{(R3P)2Ru}2(μ,η2:2-P2)2Ru(PR3)2](Ru–Ru)(6)....
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Room temperature depinning of the charge-density waves in quasi-two-dimensional 1T-TaS2 devices
PublicationWe report on the depinning of nearly commensurate charge-density waves in 1T-TaS2 thin films at room temperature. A combination of the differential current–voltage measurements with the low-frequency noise spectroscopy provides unambiguous means for detecting the depinning threshold field in quasi-2D materials. The depinning process in 1T-TaS2 is not accompanied by an observable abrupt increase in electric current—in striking contrast...
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New σ-phases in the Nb–X–Ga and Nb–X–Al systems (X = Ru, Rh, Pd, Ir, Pt, and Au)
PublicationPreviously unreported σ-phases in the ternary niobium-based systems Nb–X–Ga for X = Ru, Rh, Pd, Ir, Pt, Au, and Nb–X–Al for X = Ir, and Pt are presented, prepared by arc-melting followed by annealing at 1000 °C for 1 week. The phases are primitive tetragonal (P42/mnm, no. 136) with lattice parameters of a = 9.8336(2)–9.9432(1) Å and c = 5.1098(1)–5.1718(1) Å. Refinements of the single crystal X-ray diffraction data for the Ru and...
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Proton transfer and hydrogen bonds in supramolecular, self-assembled structures of imidazolium silanethiolates. X-ray, spectroscopic and theoretical studies
PublicationThe reaction of 1-methylimidazole, 2-ethyl-4-methylimidazole and 2-ethylimidazole with tris(2,6- diisopropylphenoxy)silanethiol (TDST) leads to the formation of three new salts, which have been characterized by elemental analyses, thermogravimetric analyses, FTIR spectroscopy, and their structures were determined by single-crystal X-ray diffraction. Structural analyses indicate that in all three compounds a proton transfer has...
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Synthesis, microstructure and electrical properties of nanocrystalline calcium doped lanthanum orthoniobate
PublicationThe single phase lanthanum orthoniobate with tetragonal structure has been synthesized by the means of mechanosynthesis method. The studies have shown the crystal structure of La0.98Ca0.02NbO4 depends on the synthesis stage. The samples were predominantly in the tetragonal phase with a trace amount of the monoclinic phase. The SEM studies of morphology and microstructure have shown nanocrystallinity of the materials. The Raman...
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Piezoresponse force microscopy and dielectric spectroscopy study of Ba0.6Sr0.4TiO3 thin films
PublicationResearch on synthesis, characterization and determination of processing – structure – property relationships of commercially important ferroelectric thin films has been performed. The sol-gel-type solution deposition technique was applied to produce good quality thin films of Ba0.6Sr0.4TiO3 (BST60/40) chemical composition on the stainless steel substrates. The thin films were characterized in terms of their microstructure, crystal...
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Recycling of photovoltaic modules - legal status, technology, market prospects
PublicationThe increase in the number of manufactured and installed photovoltaic modules and the growing concern about the insufficient supply of pure silicon imply the need to take action to develop infrastructure for recycling PV modules. The article presents a multifaceted analysis of the current state of development of the photovoltaic module recycling sector from a global and national perspective. The essence of the issue was introduced...
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Structure of Microemulsion Formulated with Monoacylglycerols in the Presence of Polyols and Ethanol
PublicationThe influence of polyols as cosurfactants (propylene glycol PG; glycerol G) and short chain alcohol as a cosolvent (ethanol EtOH) on the formation and solubilization capacity of the systems: hexadecane/monoacylglycerols (MAG)/polyol/water:EtOH, at 60C, was investigated. Electrical conductivity measurement, and the DSC method were applied to determine the structure and type of microemulsions formed. The dimension of the droplets...
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Studies on the solid-liquid equilibria and intermolecular interactions Urea binary mixtures with Sulfanilamide and Sulfacetamide
PublicationThe binary phase diagrams of Sulfanilamide-Urea (SN-U) and Sulfacetamide-Urea (SC-U) were measured using differential scanning calorimetry technique (DSC). Both examined mixtures were found to form simple binary eutectics. The limited miscibility in the solid state observed by DSC, proving inability of co-crystallization in new multi-molecular form, was also confirmed using PXRD and FTIR-ATR measurements of solid dispersions...
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Synthesis, Characterization and Biological Investigations of Half-Sandwich Ruthenium(II) Complexes Containing Benzimidazole Moiety
PublicationHalf-sandwich Ru(II) complexes belong to group of biologically active metallo-compounds with promising antimicrobial and anticancer activity. Herein, we report the synthesis and characteri- zation of arene ruthenium complexes containing benzimidazole moiety, namely, [(η6-p-cymene)RuC l(bimCOO)] (1) and [(η6-p-cymene)RuCl2(bim)] (2) (where bimCOO = benzimidazole-2-carboxylate and bim = 1-H-benzimidazole). The compounds were characterized...
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Polaronic and Mott insulating phase of layered magnetic vanadium trihalide VCl3
PublicationTwo-dimensional (2D) van der Waals (vdW) magnetic 3d-transition metal trihalides are a new class of functional materials showing exotic physical properties useful for spintronic and memory storage applications. In this article, we report the synthesis and electromagnetic characterization of single-crystalline vanadium trichloride, VCl 3 , a novel 2D layered vdW Mott insulator, which has a rhombohedral structure (R3, No. 148) at...
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Arsenic-Based Warfare Agents: Production, Use, and Destruction
PublicationSince the beginning of time, civilizations have looked for more creative ways to dominate and defeat their enemies. The rapid development of the chemical industry just before the Second World War started the era of modern chemical weapon production based on poisons, including toxic arsenic compounds. This paper provides a detailed overview of the production, usage and destruction of this dangerous chemical weapon. Milestones include:...
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Video traffic data - Interchange Zakrzewo (S11-307), Poland
Open Research DataThe data includes video traffic data registered with 8 video cameras at weaving area (weaving section type A) of the Zakrzewo interchange within S11 expressway in Poland (interchange of expressway S11 and regional road 307), located in the Poznan Agglomeration. The data covers the two days: 20.09.2017 (expressway S11) and 21.09.2017 (road 307).
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Catalytic carbonization of polypropylene by the combined catalysis of activated carbon with Ni2O3 into carbon nanotubes and its mechanism
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Fizyka II
e-Learning CoursesKierunek: Gospodarka przestrzenna (WA), I stopnia - inżynierskie, stacjonarne, 2018/2019 - zimowy (obecnie sem. 7)
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Tackling microplastics pollution in global environment through integration of applied technology, policy instruments, and legislation
PublicationMicroplastic pollution is a serious environmental problem that affects both aquatic and terrestrial ecosystems. Small particles with size of less than 5 mm, known as microplastics (MPs), persist in the environment and pose serious threats to various species from micro-organisms to humans. However, terrestrial environment has received less attention than the aquatic environment, despite being a major source of MPs that eventually...
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Mariusz Figurski prof. dr hab. inż.
PeopleMariusz Józef Figurski (born 27 April 1964 in Łasinie, Poland) - Polish geodesist, professor of technical sciences, professor at the Gdańsk University of Technology. Early life and education He passed the matriculation examination in 1983 after he had finished Jan III Sobieski High school in Grudziądz. He graduated the Military University of Technology on an individual mode at the Faculty of Electromechanics and Civil Engineering...
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Testing of Technical Fabrics under Fast Camera Control
PublicationThe dynamic development of measurement and recording techniques has been changing the way one conceives material strength. In this study, two different methods of evaluating the strength of fabrics are compared. The first is the typical and commonly used technique based on the use of a testing machine. The second method uses the so-called “fast camera” to monitor the entire process of the destruction of a fabric sample and analyse...
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Zastosowanie chlorku poliglinu jako sposobu zwalczania bakterii Microthrix parvicella w oczyszczalni ścieków w Kościerzynie
PublicationW pracy przedstawiono wyniki badań nad efektywnością zwalczania bakterii Microthrix parvicella za pomocą chlorku poliglinu (PAX) w miejskiej oczyszczalni ścieków w Kościerzynie. Dozowanie PAX-18 do komór bioreaktora oczyszczalni typu Biooksyblok, w zmniejszającej się dawce od 2,2 do 1,2 g Al/kgsm, okazało się skutecznym sposobem zwalczania pęcznienia i pienienia osadu spowodowanego nadmiernym rozwojem bakterii nitkowatych z rodzaju...
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Mutual Attraction: Siemens Activities in Italy 1855-1968
PublicationThe chapter deals with Siemens investments in Italy between 1855 and 1968. The contribution shows how the two war influenced the strategies of the company