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Search results for: ptr-ms
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The effects of resistance training experience on movement characteristics in the bench press exercise
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Study of the Effect of Filling Thermoplastic Medical Polyurethane with PVA, PLA or Diatomite on the Relaxation Times Distributions of 1H NMR
PublicationIn this work, to characterize the mobility of diferent sections of the macromole‑ cules of polyurethane (PUR), polyvinyl alcohol (PVA), and polylactic acid (PLA), as well as the density of crosslinks of the polymer chains when using fllers, we used the distributions of spin–lattice and spin–spin relaxation times for the protons. It is shown that the rigidity of the thermoplastic polymers depends on the sizes of the granules of...
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Investigation on air quality of specific indoor environments—spa salons located in Gdynia, Poland
PublicationDue to excessive application of essential oils and scented products in spa salons during aromatherapy and massage sessions, the elevated concentration of total volatile organic compounds (TVOCs), particularly terpenes, which are known as secondary organic aerosol (SOA) precursors, is expected there. This study was aimed at determination of VOCs with a particular regard to terpenes in air samples collected in selected spa salons...
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Comparative investigation of lubricant properties in friction and wear tests
PublicationOpisano porównawcze badania obciążenia zacierania na tribometrze PT3, obciążenia zespawania na aparacie czterokulowym i zużycia frettingowego na stanowisku FRET3, sześciu olejów smarowych i sześciu smarów plastycznych. Próbki do badań na stanowiskach PT3 i FRET3 wykonane były ze stali 35.
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Metody Badań Strukturalnych
e-Learning CoursesI. Podstawy spektroskopii – promieniowanie elektromagnetyczne, poziomy energetyczne w cząsteczce, absorpcja promieniowania, kształt linii, reguły wyboru, zastosowanie transformacji Fouriera w spektroskopii. II. Widma NMR – właściwości magnetyczne jąder atomowych, podstawy fizyczne metody NMR, przesunięcie chemiczne, sprzężenie spinowo-spinowe, anizotropia magnetyczna grup, interpretacja widm 1H NMR, układy spinowe, zależność...
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Mass Spectrometric Identification of 13C-Labeled Metabolites DuringAnaerobic Propanoic Acid Oxidation
PublicationBiowaste digestion is a possibility to gain biogas as a renewable fuel source. However, the anaerobic food chain may be disrupted by, e.g., substrate overload or by inhibitors, leading to the accumulation of volatile fatty acids (VFAs), predominantly of propanoic acid (PA). VFA Accumulation may cause a rapid pH decrease, less biogas production, or even a total inhibition. To maintain high biogas productivity or to prevent a collapse...
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Ekspertyza silnika trakcyjnego tramwaju Dűwag N8C pod kątem wyjaśnienia przyczyny występowania uszkodzeń tego typu silników
PublicationCelem badań było wykonanie ekspertyzy silnika trakcyjnego typu BGK, eksploatowanego w tramwaju Düwag N8C, pod kątem występowania uszkodzeń tych silników. W celu realizacji tego zadania przeprowadzono obserwowaną eksploatację w/w silnika w warunkach rzeczywistych. W tym celu opomiarowano silnik rejestrując w sposób ciągły bieżące wartości prądów i napięć występujących na obu uzwojeniach silnika tj, na uzwojeniu twornika i wzbudzenia....
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Time Synchronization between the eNBs in E-UTRAN under the Asymmetric IP Network
PublicationIn this paper, we present a method for a time synchronization between the two eNodeBs (eNBs) in E-UTRAN (Evolved Universal Terrestrial Radio Access) network. The...
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Mass spectrometric identification of 13C-Labeled metaboloites during anaerobic propanoic acid oxidation
PublicationBiowaste digestion is a possibility to gain biogas as a renewable fuel source. However, the anaerobic food chain may be disrupted by, e.g., substrate overload or by inhibitors, leading to the accumulation of volatile fatty acids (VFAs), predominantly of propanoic acid (PA). VFA Accumulation may cause a rapid pH decrease, less biogas production, or even a total inhibition. To maintain high biogas productivity or to prevent a collapse...
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Determination of Metals Content in Wine Samples by Inductively Coupled Plasma-Mass Spectrometry
PublicationKnowledge about the metal content of wine is very important, for many reasons. Depending on the element, its quantity varies in wine from ng/L to mg/L. Despite the fact that metals are not directly connected to the taste and aroma of the wine, their content should be determined and controlled, because excess is undesirable, and in some cases prohibited, due to potential toxicity. Several analytical procedures for metal determination...
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Presence of antibiotics in the aquatic environment in Europe and their analytical monitoring: Recent trends and perspectives
PublicationThe presence of antibiotics and their metabolites in the aquatic environment exerts a negative impact on all organisms. Moreover, the easy migration of these substances to drinking water may also have serious consequences for public health, such as drug resistance. Although antibiotics and their metabolites are detected in surface waters and wastewater, there are still no systemic solutions preventing environmental pollution with...
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Nanomaterials for photothermal and photodynamic cancer therapy
PublicationIn recent years, the role of optically sensitive nanomaterials has become powerful moieties in therapeutic techniques and has become particularly emphasized. Currently, by the extraordinary development of nanomaterials in different fields of medicine, they have found new applications. Phototherapy modalities, such as photothermal therapy (PTT) by toxic heat generation and photodynamic therapy (PDT) by reactive oxygen species, are...
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Genotyping and characterization of virulence factors in Escherichia coli strains isolated from patients from Polish hospital
PublicationZakażenia układu moczowego (UTIs - ang. urinary track infections) są jedną z najczęstszy infekcji, za które w 85% przypadków odpowiedzialne są bakterie Escherichia coli. Infekcje układu moczowego mogą prowadzić do groźnych powikłań m. in. odmiedniczkowego zapalenia nerek. Śmiertelność wśród tej grupy pacjentów wynosi 1-3%. Zakażenia układu moczowego występują również u ok. 7% kobiet ciężarnych. W pracy przebadano 82 szczepy E....
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Preliminary studies comparing the chemical composition of goitschiteand Saxonian succinite = Wstępne badania dotyczące porównania chemicznego składu goitszytu i sukcynitu saksońskiego
PublicationChemiczny skład goitszytu i sukcynitu saksońskiego porównano metodą spektroskopową (FTIR). Dalsza analiza została przeprowadzona z ekstraktów niepolarnych za pomocą chromatografii gazowej sprzężonej ze spektrometrią mas (GC-MS). Potwierdzono podobieństwo składu chemicznego bursztynu bitterfeldzkiego i sukcynitu z regionu Morza Bałtyckiego. Substancje zidentyfikowane w ekstrakcie goitszytu mogą sugerować jego genetyczne podobieństwo...
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Solid Phase Microextraction: Apparatus, Sorbent Materials, and Application.
Publicationhe primary objective of this review article is to strategically screen and highlight the advancements in the area of solid phase microextraction (SPME). The plenty of review articles have been written on different aspects of SPME, this review is dedicated to provide the brief but clear overview of the research footprints so produced from SPME. Some of the key advancements in types and designs, coating materials, coating strategies,...
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Analysis of volatile fraction of hybrid fruit pulp using Proton Transfer Reaction - Time-Of-Flight Mass Spectrometry
PublicationFruits and vegetables are important ingredients in human diet. Because of this, it is very important to know their exact composition and to control their quality. Based on the aroma of food products, it is possible to pre-evaluate their quality and freshness. The aim of this work was to characterize the volatile fraction of the hybrid fruit ‘sweetie’ using the modern analytical device PTR-TOFMS. Hybrid fruit samples are human-made...
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Marta Kuc-Czarnecka dr
PeopleMarta Kuc-Czarnecka is the deputy head of the Department of Statistics and Economics at the Faculty of Management and Economics of the Gdańsk University of Technology. She also serves as the Dean's proxy for AMBA accreditation. She is a co-founder of Rethinking Economics Gdańsk and a member of the Foundation Edward Lipiński for the promotion of pluralism in economic sciences. In 2018-2022, she was Eurofound’s quality of life and...
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Characterization and properties of LDPE/(ground tire rubber)/crosslinked butyl rubber blends
PublicationIn recent years, interest in used rubber recycling, mainly focusing on the utilization of end-of-life tires, has heightened. This interest, is owing to the activities related to environmental protection and economic factors, which both stimulate companies to reuse the high-quality rubber present in ground rubber scrap. In this study, the application of crosslinked butyl rubber in thermoplastic compositions of low-density polyethylene...
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Tuning of microstructure in engineered poly (trimethylene terephthalate) based blends with nano inclusion as multifunctional additive
PublicationImmiscible blends and their composites are heterogeneous and have variable morphology due to variation in mesophase regions. Tuning, i.e. controlling the phase dimension is important, thereof we report a “super-combo” effect of multiwalled carbon nanotubes (MWCNTs) in poly (trimethylene terephthalate)/polypropylene (PTT/ PP) blend system. MWCNTs act as a good reinforcing agent and compatibilizer in the otherwise immiscible PTT/...
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Gospodarka przestrzenna GIK 2022-2023
e-Learning CoursesKurs z przedmiotu Gospodarka Przestrzenna dla studentów kierunkuGeodezja i Kartografia VI sem. Prosimy, aby zapisać się do zespołu na MS TEAMS Gospodarka przestrzenna GIK z wykorzystaniem kodu ...
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Konsultacje on-line dr Anny Baj-Rogowskiej
e-Learning CoursesZapraszam państwa na konsultacje on-line, które odbywać się będą w semestrze zimowym 2020/2021 w każdą środę w godz. 10:45 - 11:30 na platformie MS Teams. Zalecana przeglądarka to najnowsza wersja Microsoft EDGE lub Google Chrome.
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Fawad Ahmed PhD Scholar
PeopleI am Ph.D. Scholar in Faculty of Mechanical Engineering at Gdansk University of Technology, Poland. My research focuses on improving the thermal management of batteries that are used in Electric Vehicles. I received my MS in Thermal Energy Engineering from the National University of Sciences and Technology, Pakistan. My MS thesis was related to the application of thermal energy storage systems for space heating. I tried to improve...
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Path Loss Modelling for Location Service Applications
PublicationThe aim of this paper is the path loss modeling for the radiolocation services in radiocommunication networks, particularly in cellular networks. The main results of the measurements obtained in the physical layer of the UMTS are introduced. A new method for the utilization of the multipath propagation phenomenon to improve the estimation of the distance between the mobile station (MS) and the base station (BS) is outlined. This...
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Thermal analysis of copper(II) complexes of general formula [Et4N]2[CuBrnCl4-n]
PublicationBadano dekompozycję termiczną związków składających sie z anionów: [CuBrnCl4-n]2- (n=0-4) i kationów tetrametyloamoniowych. Stosowano następujące metody badawcze: TG-FTIR, TG-MS, DTA i DTG. Pomiary przeprowadzono w atmosferze argonu i powietrza w zakresie temperatur od 293 K do 1073 K. Produkty dekompozycji identyfikowano metoda spektroskopii w podczerwieni (IR i FIR) oraz metodą dyfrakcji promieniowania rentgenowskiego.
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Cyanobacterial toxins in fresh and brackish waters of Pomorskie Province (Northern Poland)
PublicationPraca dotyczy oznaczania toksyn należących do grupy hepatotoksycznych peptydów cyklicznych oraz neurotoksycznych alkaloidów. Są one odpowiedzialne za uszkodzenia ryb i ptaków, które powstają w wyniku zakwitu glonów. Badano zakwity w wodach słodkich Pomorza. Oznaczano hepatoksyny, mikrocysty oraz nodularynę. Opracowano w tym celu warunki analityczne przy zastosowaniu techniki HPLC-DAD. Do identyfikacji anatoksyny-A użyto techniki...
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Relationships and bioaccumulation of chemical elements in the Baikal seal (Phoca sibirica)
PublicationOznaczono stężenia w próbkach wątroby foki bajkalskiej, planktonu i zoobentosu ryb stanowiących źródło pokarmu dla fok. Badania przeprowadzono z wykorzystaniem technik ICP-MS oraz ICP-AES. Zbadano wpływ czynników wewnętrzynch i zewnętrznych (środowiskowych) na proces bioakumulacji z wykorzystaniem technik wielowymiarowych (ANOVA, analiza czynników) oraz analizy korelacyjnej. Stwierdzono istotny wpływ płci oraz wieku na proces akumulacji...
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Load test of new European record holder in span length among extradosed type bridges
PublicationThe article presents acceptance load tests of a newly built extradosed MS-3 bridge located along the national road DK-16 near Ostróda (Poland). The structure features significant dimension in European reference scale. It is a new record holder in span length regarding this distinct bridge category. Its length ranges 206 m. Static and dynamic load tests were performed here. The program was extended by entire structural laser scanning...
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The contingent nature of warehouse flexibility
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Family Tree for Aqueous Organic Redox Couples for Redox Flow Battery Electrolytes: A Conceptual Review
PublicationRedox flow batteries (RFBs) are an increasingly attractive option for renewable energy storage, thus providing flexibility for the supply of electrical energy. In recent years, research in this type of battery storage has been shifted from metal-ion based electrolytes to soluble organic redox-active compounds. Aqueous-based organic electrolytes are considered as more promising electrolytes to achieve “green”, safe, and low-cost...
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Energy Losses Due to Imperfect Payment Infrastructure and Payment Instruments
PublicationOne of the strategic objectives of the European Union is a reduction in greenhouse gas emissions and improvement of energy efficiency by at least 32.5% in different areas of the economy by 2030. However, little is known about the impact of payment in retail on energy consumption. The purpose of this paper is to assess the chain of losses of time and energy, and therefore financial losses, that occur due to the imperfection of payment...
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Budesonide treatment of professional athletes and anti-doping testing- case studies
PublicationAccording to the World Anti-Doping Agency (WADA) Prohibited List, glucocorticosteroids are prohibited in competition and only when administered by oral, intravenous, intramuscular or rectal routes. Up to now, in order to differentiate whether glucocorticosteroids were administered by one of the prohibited routes or not, a specific reporting limit for urinary concentrations of parent compounds and their metabolites was established...
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Development of a liquid chromatography–tandem mass spectrometryprocedure for determination of endocrine disrupting compounds infish from Mediterranean rivers
PublicationA new, sensitive and rapid method based on QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe)approach followed by ultra high performance liquid chromatography coupled with tandem mass spec-trometry (UHPLC–MS/MS) was developed for the determination of nineteen endocrine disruptors (EDCs)and related compounds belonging to different classes in various fish species. Matrix effect on the analyti-cal performance was evaluated,...
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Mass Spectrometric Identification of 13C-labeled Metabolites During anaerobic Propanoic Acid Oxidation
PublicationBiowaste digestion is a possibility to gain biogas as a renewable fuel source. However, the anaerobic food chain may be disrupted by, e.g., substrate overload or by inhibitors, leading to the accumulation of volatile fatty acids (VFAs), predominantly of propanoic acid (PA). VFA Accumulation may cause a rapid pH decrease, less biogas production, or even a total inhibition. To maintain high biogas productivity or to prevent a collapse...
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Polychlorinated biphenyls (PCBs) and polychlorodibenzo-p-dioxins (PCDDs) determination in disposable baby diapers with the application of natural deep eutectic solvent
PublicationIn this work a new method involving solvent extraction of porous membrane-packed solid samples (SE-PMSS) coupled to gas chromatography-mass spectrometry (GC–MS) has been developed for the determination of six polychlorinated biphenyls (PCBs) and five polychlorodibenzo-p-dioxines (PCDDs) in disposable baby diapers. In that aim, a terpenoid-based natural deep eutectic solvent (NADES) composed of carvone and camphor in a 1:1 M ratio...
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Assessment of baby disposable diapers application for urine collection and determination of phthalate metabolites
PublicationThe baby disposable diapers were investigated as a sampling material for urine collection and validated for the evaluation of the exposure of children to xenobiotics. Phthalate metabolites detected in urine samples were chosen as proof-of-concept analytes. For the determination of phthalate metabolites in children’s urine samples, high performance liquid chromatography coupled with tandem mass spectrometry (HPLC-MS/MS) was used. Two...
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Closing the loop: Upcycling secondary waste materials into nanoarchitectured carbon composites for the electrochemical degradation of pharmaceuticals
PublicationIn this study, we demonstrated the application of electrochemical oxidation as a safer and cleaner technology for minimizing the impact of pharmaceuticals in wastewaters, simultaneously mediated by upcycled secondary waste materials (SWMs)-derived electrodes, to further reduce their environmental impact. The modularity, scalability, ease of operation and reliability make electrochemical oxidation an ideal process for the destruction...
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Network oscillations modulate interictal epileptiform spike rate during human memory
PublicationEleven patients being evaluated with intracranial electroencephalography for medically resistant temporal lobe epilepsy participated in a visual recognition memory task. Interictal epileptiform spikes were manually marked and their rate of occurrence compared between baseline and three 2 s periods spanning a 6 s viewing period. During successful, but not unsuccessful, encoding of the images there was a significant reduction in...
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Quantification of unconjugated and total ibuprofen and its metabolites in equine urine samples by gas chromatography–tandem mass spectrometry: Application to the excretion study
PublicationIbuprofen (IBU) is a widely used nonsteroidal anti-inflammatory drug (NSAID) in human and also veterinary medicine. NSAIDs are usually highly metabolized compounds in horses; they are often present in equine urine, mostly in their conjugated forms (glucuronides). Thus, hydrolysis to cleave the glucuronide linkage prior to anti-doping analysis is often necessary for improving detection. In this study, unconjugated and total IBU...
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A rapid dispersive liquid–liquid microextraction of antimicrobial onion organosulfur compounds in animal feed coupled to gas chromatography-mass spectrometry
PublicationA rapid analytical procedure is proposed for determining two antimicrobial onion organosulfur compounds, propyl disulfide (PDS) and propyl propane thiosulfonate (PTSO), in animal feed. The use of PTSO as a natural ingredient in animal feed is allowed due to its antimicrobial activity against pathogenic organisms. Two analytical methodologies using gas chromatography coupled to mass spectrometry (GC-MS) are compared. After the extraction...
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Analysis of the reliability of any-hop star network
PublicationZałożono, że sieć ma wielostopniową strukturę gwiaździstą. Jako oceny niezawodności tych sieci przyjęto: 1) średnią liczbę sprawnych par węzłów, które mogą komunikować się wzajemnie; 2) średnią liczbę sprawnych par węzłów, które mogą komunikować się poprzez węzeł centralny; 3) średnią liczbę sprawnych par węzłów, które mogą komunikować się z węzłem centralnym; 4) prawdopodobieństwo zdarzenia, że sprawne węzły mogą komunikować...
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Golden artefacts, resin figurines, body adhesives and tomb sediments from the pre-Columbian burial site El Caño (Gran Coclé, Panamá): tracing organic contents using molecular archaeometry
PublicationThis research aimed to determine the origin of organic residues from funerary contexts in the El Ca~no settlement (Gran Cocl�e area, Panam�a, Central America) by means of multiple molecular probing techniques (GC-MS of organic solvent extracts and pyrolysis-GC-MS, THM-GC-MS and FTIR of solid samples). The samples include particles of precious resin figurines, fillings of golden objects, tomb sediments, plant exudates from extant...
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Involvement of human glutathione S-transferase M1-1 in the glutathione conjugation of the antitumor unsymmetrical bisacridine derivative C-2028.
Open Research DataUnsymmetrical bisacridines (UAs) are a novel potent class of antitumor-active therapeutics. The aim of this study was to investigate the possible role of human glutathione S-transferase M1-1 (hGSTM1-1) in the glutathione (GSH) conjugation of a representative UA, C‑2028.
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Research grant applications (W)
e-Learning CoursesSearching for a grant for yourself. Competitions: of the Ministry of Science and Higher Education (MNiSW), of the National Science Center (NCN)' of the Foundation for Polish Science (FNP), of the National Center for Research and Development (NCBiR), European Commission Grants (ERC). Formulation of the application: analysis of the requirements. Description of project issues: purpose, meaning, work plan, and methodology. Reviewer's...
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Two highly thermostable paralogous single-stranded DNA-binding proteins from Thermoanaerobacter tengcongensis
PublicationThe thermophilic bacterium Thermoanaerobacter tengcongensis has two single-stranded DNA-binding (SSB) proteins, designated TteSSB2 and TteSSB3. In a SSB complementation assay in Escherichia coli, only TteSSB3 took over the in vivo function of EcoSSB. We have cloned the ssb genes obtained by PCR and have developed E. coli overexpression systems. The TteSSB2 and TteSSB3 consist of 153 and 150 amino acids with a calculated molecular...
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Ground Tire Rubber Modified by Elastomers via Low-Temperature Extrusion Process: Physico-Mechanical Properties and Volatile Organic Emission Assessment
PublicationIn this paper, low-temperature extrusion of ground tire rubber was performed as a proecological waste tires recycling method. During this process, ground tire rubber was modified with constant content of dicumyl peroxide and a variable amount of elastomer (in the range: 2.5–15 phr). During the studies, three types of elastomers were used: styrene-butadiene rubber, styreneethylene/butylene-styrene grafted with maleic anhydride and...
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Marcin Olszewski dr hab. inż.
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Research Grant Applications (SEM)
e-Learning CoursesSearching for a grant for yourself. Competitions: of the Ministry of Science and Higher Education (MNiSW), of the National Science Center (NCN)' of the Foundation for Polish Science (FNP), of the National Center for Research and Development (NCBiR), European Commission Grants (ERC). Formulation of the application: analysis of the requirements. Description of project issues: purpose, meaning, work plan, and methodology. Reviewer's...
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Wieloobszarowa rozmyta regulacja PIλDµ mocy reaktora jądrowego
PublicationWartykule przedstawiono wieloobszarowy regulator rozmyty z lokalnymi regulatorami PIλDµ niecałkowitego rzędu. Regulator ten ostał zaprojektowany do sterowania mocą reaktora jądrowego typu PWR (Pressurized Water Reactor). Do syntezy wieloobszarowego regulatora PIλDµ wykorzystano model matematyczny reaktora PWR o parametrach skupionych obejmujący procesy generacji i wymiany ciepła oraz efektów reaktywnościowych. Nastawy lokalnych...
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Genotyping of clinical isolates of fluconazole-resistant Candida albicans
PublicationThe aim of the study was to compare the discriminatory power of RAPD-PCR method with using RSD10 primer and microsatellite analysis with using (GACA)4 primer for genotyping clinical isolates of fluconazole-resistant C. albicans. Isolates were received from patients of Children's Memorial Health Institute in Warsaw. However in the case of both tested methods low number of amplified fragments was generated, nine and six different...
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Chemical structures and physical properties of cured segmental polyurethanes
PublicationPrzedmiotem badań były poliuretany (PUR) segmentowe otrzymywane w dwuetapowej syntezie oligomerycznego α,ω-dihydroksy(adypinianu etylenowo-butylenowego) oraz dwóch różnych aromatycznych diizocyjanianów: 4,4'-diizocyjanianu difenylenometanu (MDI) albo MDI modyfikowanego diizocyjanianem karbodiimidu. Na etapie przedłużania łańcucha, oprócz typowo używanego do tego celu 1,4-butanodiolu, stosowano triol - 1,3-dihydroksy-2-(hydroksymetyleno)propan...