Search results for: LC THERMOGRAPHY
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,4 V at 420 mA. Sample 103, run #2.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,4 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #2. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 420 mA. Sample 103, run#2.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #2. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103, run #8.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #8. Continuation of experiment at high voltage to accelerate the ageing process.The images were taken with thermographic...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 1281 mA. Sample J51, run #3.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 1098 mA. Sample J51, experiment run #3. The current is extremely high for this type of sample to accelerate ageing processes.The images were taken...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103, run #7.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #7. Continuation of experiment at high voltage to accelerate the ageing process.The images were taken with thermographic...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,0 V at 420 mA. Sample 103, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,0 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #1. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,9 V at 420 mA. Sample 103, run #2.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,9 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #2. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,9 V at 420 mA. Sample 103, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,9 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #1. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 534 mA. Sample J53, run #3.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 534 mA. Sample J53, experiment run #3. The period of images is 30 minutes in order to observe slow temperature fluctuations.The images were taken...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 1281 mA. Sample J51, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 1098 mA. Sample J51, experiment run #1. The current is extremely high for this type of sample to accelerate ageing processes.The images were taken...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 534 mA. Sample J53, run #7.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 534 mA. Sample J53, experiment run #7. The period of images is 30 minutes in order to observe slow temperature fluctuations.The images were taken...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 420 mA. Sample 103, run#1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #1. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,9 V at 420 mA. Sample 103, run #3.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,9 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #3. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 534 mA. Sample J53, run #6.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 534 mA. Sample J53, experiment run #6. The period of images is 30 minutes in order to observe slow temperature fluctuations.The images were taken...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103, run #3.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #3. Continuation of experiment at high voltage to accelerate the ageing process.The images were taken with thermographic...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,4 V at 420 mA. Sample 103, run #1.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,4 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #1. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103, run #2.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103, experiment run #2. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM...
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Prediction of Overall In Vitro Microsomal Stability of Drug Candidates Based on Molecular Modeling and Support Vector Machines. Case Study of Novel Arylpiperazines Derivatives
PublicationOther than efficacy of interaction with the molecular target, metabolic stability is the primary factor responsible for the failure or success of a compound in the drug development pipeline. The ideal drug candidate should be stable enough to reach its therapeutic site of action. Despite many recent excellent achievements in the field of computational methods supporting drug metabolism studies, a well-recognized procedure to model...
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Investigation of the C-1311 glucuronidation: an electrochemical approach
Open Research DataThis study was undertaken to investigate the glucuronidation of the compound C-1311 (5-diethylaminoethylamino-8-hydroxyimidazoacridinone – the model anticancer acridine derivative) using electrochemistry/mass spectrometry (EC/MS) as a complementary technique to in vitro (liver microsomes) and in silico approaches.
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The power spectral density of audible noise and electric disturbances in ship’s electrical drive systems with frequency converters
Open Research DataThe presented dataset is part of research focusing on the impact of the ship's electrical drive systems with frequency converters on vibrations and the level of audible noise on ships.
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Bezpośrednia analiza próbek z wykorzystaniem techniki spektrometrii mas. Cz. II. Technika PTR – MS – ciekawe rozwiązanie metodyczne w zakresie spektrometrii mas
PublicationTechnika spektrometrii mas stanowi niezwykle istotne narzędzie badawcze, umożliwiające uzyskanie wielu cennych informacji, dotyczących składu chemicznego wielu próbek rzeczywistych pochodzenia biologicznego, farmaceutycznego i spożywczego. Spektrometr mas zazwyczaj pełni role detektora w przypadku stosowania połączenia z urządzeniami chromatograficznymi (GC, LC). Dzięki zastosowaniu pewnych modyfikacji aparaturowych i metodycznych,...
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Abuse or contamination? Ratio determination of clenbuterol enantiomers to distinguish between doping use and meat contamination
PublicationClenbuterol has been detected in urine of several athletes during routine doping control in the past years. Athletes claimed that the clenbuterol was ingested by eating contaminated meat. Providing analytical prove for this claim is difficult. clenbuterol consists of two enantiomers, R(-) and S(+)-clenbuterol. Currently available human and veterinary preparations were found to consist of a racemic mixture of both enantiomers. When...
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Retention modeling of some saccharides separated on an amino column.
PublicationUsing an amino column (Supelcosil LC-NH2) and different mixtures of acetonitrile-water, quantitative structure-retention relationship models are discussed. These models are based on computed molecular descriptors representing numerically structured features of some saccharides. The obtained results are underlining the lipophilicity/hydrophilicity balance, and how this is controlling the separation of the saccharides. The resulting...
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Determination of Pesticide Residues in Honeybees using Modified QUEChERS Sample Work-Up and Liquid Chromatography-Tandem Mass Spectrometry
PublicationIncreasing emissions of chemical compounds to the environment, especially of pesticides, is one of factors that may explain present honeybee colony losses. In this work, an analytical method employing liquid chromatography-tandem mass spectrometry (LC-MS/MS) was optimized for the simultaneous screening of 19 pesticides which have not been yet determined in honeybee samples from northern Poland (Pomerania). The sample preparation,...
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Frequency-dependent coupling model for microwave band-pass filter
PublicationThe goal of this work was to create a circuit model which represents frequency-dependent coupling between microwave resonators. Our models are designed for in-line filters. The frequency-dependent coupling enables one to realize a transmission zero which is not possible in classical approach with frequency independent inverters. In addition, the proposed model allows us to observe out-of-band behavior, e.g. spurious resonance....
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3-Monochloropropane-1,2-diol in Infant Foods and Human Breast Milk: Determination by GC-MS
Publication3-Monochloropropane-1,2-diol is one of the food borne contaminants called chloropropanols. Over the last decade plenty of analytical methods was developed in order to determine 3-monochloropropane-1,2-diol in its free and bound form in various foodstuffs with the use of GC-FID, GC-ECD, LC-TOFMS and finally GC-MS, which is now widely used in laboratories. The aim of this research was the determination of 3-monochloropropane--1,2-diol...
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Influence of Diosmin Treatment on the Level of Oxidative Stress Markers in Patients with Chronic Venous Insufficiency
PublicationOxidative stress plays an important role in the pathophysiology of many human disorders, while antioxidants prevent the development of various adverse symptoms. Diosmin is a natural flavonoid applied in vascular system disorders, especially in chronic venous insufficiency (CVI), and it plays a significant part in the alleviation of CVI symptoms. Due to antioxidant activity, it also has the ability to scavenge the oxygen free radicals...
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X-ray and UV Radiation Damage of dsDNA/Protein Complexes
PublicationRadiation and photodynamic therapies are used for cancer treatment by targeting DNA. However, efficiency is limited due to physico-chemical processes and the insensitivity of native nucleobases to damage. Thus, incorporation of radio- and photosensitizers into these therapies should increase both efficacy and the yield of DNA damage. To date, studies of sensitization processes have been performed on simple model systems, e.g.,...
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Sample preparation and chromatographic analysis of acidic herbicides in soils and sediments
PublicationW pracy przedstawiono różne techniki przygotowania próbek i oznaczania herbicydów z grupy pochodnych fenoli i pochodnych kwasów karboksylowych w próbkach gleby. Opisano wybrane metody wzbogacania i izolacji analitów, m. in.: ekstrakcję za pomocą wodnych roztworów zasad i rozpuszczalników organicznych płynem w stanie nadkrytycznym, wodą w stanie podkrytycznym, cieczą pod zwiększonym ciśnieniem, cieczą wspomaganą mikrofalami. Niski...
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Oznaczanie herbicydów kwasowych w próbkach gleby.
PublicationPrzedstawiono różne techniki przygotowania próbek i oznaczania herbicydów z grupy pochodnych fenoli i pochodnych kwasów karboksylowych w próbkach gleby.Opisano wybrane metody wzbogacania i izolacji analitów, m.in: ekstrakcję za pomocą wodnych roztworów zasad i rozpuszczalników organicznych, płynem w stanie nadkrytycznym, wodą w stanie podkrytycznym, cieczą pod zwiększonym ciśnieniem, cieczą wspomaganą mikrofalami. Niski...
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Thermal Images Analysis Methods using Deep Learning Techniques for the Needs of Remote Medical Diagnostics
PublicationRemote medical diagnostic solutions have recently gained more importance due to global demographic shifts and play a key role in evaluation of health status during epidemic. Contactless estimation of vital signs with image processing techniques is especially important since it allows for obtaining health status without the use of additional sensors. Thermography enables us to reveal additional details, imperceptible in images acquired...
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Methods of Assessing Degradation of Supercapacitors by Using Various Measurement Techniques
PublicationThis article presents the qualitative analyses of the construction of supercapacitor samples. The analyses are based on the suggested thermographic measurements as well as the technique of testing the inherent noise of the investigated element. The indicated assessment methods have been referred to the currently used parameters for the qualitative evaluation of supercapacitors. The approach described in this paper, which introduces...
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Real-time facial feature tracking in poor quality thermal imagery
PublicationRecently, facial feature tracking systems have become more and more popular because of many possible use cases. Especially in medical applications location of the face and facial features are very useful. Many researches have presented methods to detect and track facial features in visible light. However, facial feature analysis in thermography may also be very advantageous. Some examples of using infrared imagery in medicine include...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 64 mA. Sample 91. Image period: 5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 64 mA. Sample 91. Pictures were taken relatively fast, with period of 5 sec in order to examine the fast fluctuations of sample temperature during...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 120 mA. Sample 103. Image period: 0,5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 120 mA. Sample 103. Thermographic pictures were taken relatively fast, with period of 0,5 sec in order to examine the fast fluctuations of sample...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103. Image period: 0,5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 0,5 sec (2 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,4 V at 420 mA. Sample 103. Image period: 0,5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,4 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 0,5 sec (2 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,3 V at 420 mA. Sample 103. Image period: 2 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,3 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken relatively fast, with period of 2 sec in order to examine the fast fluctuations of sample temperature during...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103. Image period: 0,5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 0,5 sec (2 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,5 V at 420 mA. Sample 103. Image period: 0,5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,5 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 0,5 sec (2 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec (1 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec (1 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,4 V at 420 mA. Sample 103. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,4 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec in order to examine the fast fluctuations of sample temperature during charging - discharging...
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Bezpośrednia analiza próbek z wykorzystaniem techniki spektrometrii mas. Cz. I. Rozwiązania metodyczne w zakresie spektrometrii mas umożliwiające bezpośrednią analizę próbek
PublicationTechnika spektrometrii mas stanowi jedno z najważniejszych narzędzi analitycznych, wykorzystywanych do identyfikacji, określania struktury chemicznej oraz oznaczania stężeń wielu związków chemicznych. Aby zidentyfikować obecne w próbkach rzeczywistych anality, konieczne jest jednak z reguły ich wstępne rozdzielenie, toteż spektrometry mas pełnią najczęściej rolę detektora np. w przypadku technik łączonych, gdy na etapie rozdzielania...
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Development of chromatographic and mass spectrometry conditions for untargeted lipidomic analysis of human breast milk
PublicationHuman breast milk (HBM) is a complex biofluid containing components which are essential for the proper growth of the newborn (for example nutrients such as carbohydrates, proteins, lipids) and also bioactive substances. According to the literature, most of studies involving HBM nutrients investigations focused essentially on the determination of proteins. The molecular composition of lipids in HBM is not well known as the protein...
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Determination of Butyltin Species in Sea Water Samples Using Solid Phase Extraction Followed by Liquid Chromatography - Tandem Mass Spectrometry
PublicationReverse phase liquid chromatography (RP-HPLC)-electrospray ionization-tandem mass spectrometry (ESI-MS-MS) was evaluated for the analysis of TBT using solid phase extraction as sample preparation method. TBT was extracted from acidified water samples (spiked with tripropyltin as internal standard) using reversed phase polymeric Strata-X cartridges. Analytes were eluted from cartridges using acetonitrile-water mixture and the volume...
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Profiling of polar ionogenic metabolites in Polish wines by capillary electrophoresis-mass spectrometry
PublicationThe composition of wine is determined by a complex interaction between environmental factors, genetic factors (i.e., grape varieties), and winemaking practices (including technology and storage). Metabolomics using NMR spec-troscopy, GC-MS, and/or LC-MS has shown to be a useful approach for assessing the origin, authenticity, and quality of various wines. Nonetheless, the use of additional analytical techniques with complementary...
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Bisphenols and their derivatives in baby diaper samples.
PublicationMany common products contain and leach hazardous chemicals, including endocrine-disrupting chemicals such as bisphenols that are harmful to human health. For toddlers, this dangerousness is higher because of their not fully developed detoxification system. Due to this, bisphenols content in products such as baby diapers, should be monitored. Baby diapers not only remain in close contact with the skin, but are also used from the...
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Analytical Strategies and Applications in Lipidomics
PublicationLipidomics is a field of study aiming at a comprehensive analysis of a set of lipids in biological systems. This includes both quantitative and qualitative characterization of lipid profiles, comparative studies of lipidomes, and analysis of lipid-protein interactions. Lipids are structurally diversified that make their analysis a challenging task. The constant advances in analytical technologies, especially in the field of high-performance...
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Comparative evaluation of different methods for determining phytochemicals and antioxidant activity in products containing betalains - Verification of beetroot samples
PublicationThis study presents methods that can be used to assess the health quality of products containing betalains. The paper compares and verifies data on the phytochemical composition of three different pigmented beetroot cultivars using spectrophotometric, HPLC-DAD, HPTLC and LC-Q-Orbitrap-HRMS techniques. Additionally, we compared the total antioxidant activity in both the cell-free and cellular systems. Betalain contribution to antioxidant...