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Wyniki wyszukiwania dla: mass%20spectrometry
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Vacuum ultraviolet photoionization and ionic fragmentation of the isoxazole molecules
PublikacjaThe photofragmentation of the isoxazole molecules producing ionized atomic and molecular fragments was investigated in the photon energy range of 9e32 eV, using synchrotron radiation excitation combined with ion time-of-flight spectrometry. Twenty-one well resolved cations were identified in the mass spectra of the isoxazole, and their appearance energies were determined. The yield curves of these cations were obtained in the photon...
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Dissociative multi-photon ionization of isolated uracil and uracil-adenine complexes
PublikacjaRecent multi-photon ionization (MPI) experiments on uracil revealed a fragment ion at m/z 84 that was proposed as a potential marker for ring opening in the electronically excited neutral molecule. The present MPI measurements on deuterated uracil identify the fragment as C3H4N2O+ (uracil+ less CO), a plausible dissociative ionization product from the theoretically predicted open-ring isomer. Equivalent measurements on thymine...
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High performance super-twisting sliding mode control for a maritime autonomous surface ship (MASS) using ADP-Based adaptive gains and time delay estimation
PublikacjaThis research addresses two kinds of problems related to optimal trajectory tracking of a Maritime Autonomous Surface Ship (MASS): those caused by the time-varying external disturbances including winds, waves and ocean currents as well as those resulting from inherent dynamical uncertainties. As the paper shows, an accurate and robust optimal controller can successfully deal with both issues. An improved Optimal Adaptive Super-Twisting...
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The preparation and evaluation of core-shell magnetic dummy-template molecularly imprinted polymers for preliminary recognition of the low-mass polybrominated diphenyl ethers from aqueous solutions
PublikacjaThe design, preparation process, binding abilities, morphological characteristic and prospective field of application of dummy-template magnetic molecularly imprinted polymer (DMMIP) for preliminary recognition of the selected low-mass polybrominated diphenyl ethers (PBDE-47 and PBDE-99) from aquatic environment were investigated. The surface of iron oxide (Fe3O4) nanopowder (50-100 nm particles size) was modified with tetraethoxysilane...
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High performance super-twisting sliding mode control for a maritime autonomous surface ship (MASS) using ADP-Based adaptive gains and time delay estimation
PublikacjaThis research addresses two kinds of problems related to optimal trajectory tracking of a Maritime Autonomous Surface Ship (MASS): those caused by the time-varying external disturbances including winds, waves and ocean currents as well as those resulting from inherent dynamical uncertainties. As the paper shows, an accurate and robust optimal controller can successfully deal with both issues. An improved Optimal Adaptive Super-Twisting...
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Sample preparation procedure using extraction and derivatization of carboxylic acids from aqueous samples by means of deep eutectic solvents for gas chromatographic-mass spectrometric analysis
PublikacjaThe paper presents a new procedure for the determination of organic acids in a complex aqueous matrixusing ultrasound-assisted dispersive liquid–liquid microextraction followed by injection port derivati-zation and GC–MS analysis. A deep eutectic solvent (choline chloride: 4-methylphenol in a 1:2 mol ratio)was used both as an extracting solvent and as a derivatizing agent to yield ion pairs which were next con-verted to methyl...
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Modeling and control of a redundantly actuated variable mass 3RRR planar manipulator controlled by a model-based feedforward and a model-based-proportional-derivative feedforward–feedback controller
PublikacjaIn the paper, dynamics of a complex mechatronics system is considered. A redundantly actuated planar manipulator is the base of the mechanical part of it. It is a 3RRR 1 platform based parallel manipulator. To control its trajectory, a model-based feedforward controller is employed. Three aspects are fundamental in the presented investigations. The first focus is on development of an accurate numerical model used to solve the inverse...
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Comprehensive two-dimensional gas chromatography and three-dimensional fluorometry for detection of volatile and bioactive substances in some berries
PublikacjaThe volatilefractionsofCapegooseberryandblueberryweredeterminedbyheadspacesolid-phase microextractioncoupledwithcomprehensivetwo-dimensionalgaschromatographywithtime-of-flight mass spectrometry(HS-SPME/GCGC-TOFMS).Thehighestamountofalcohol(51.8%),ester(32.8%)and carboxylicacid(6.9%)wasinblueberryincomparisonwithgooseberryandoppositelyketones(14.7%), aldehydes(9.9%)andterpenes(8%)werefoundingooseberry.Thebioactivecompoundsandantioxidant capacities...
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The EDS elemental maps of reduced LSCNT (SEM)
Dane BadawczeThe dataset includes elemental maps of La, Ce, Ti, O, Sr, Ni in La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s produced using Pechini method sintered at 1200oC under air atmosphere and reduced at 900 for 12 h in wet H2.
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Electron attachment and electron iozization of acetic acid clusters embedded in helium nanodroplets
PublikacjaThe effect of incident electrons on acetic acid clusters is explored for the first time. The acetic acid clusters are formed inside liquid helium nanodroplets and both cationic and anionic productsejected in to the gas phase aredetected by mass spectrometry.
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Jacek Namieśnik prof. dr hab. inż.
OsobyUrodził się 10 grudnia 1949 r. w Mogilnie, zmarł 14 kwietnia 2019 r. w Gdańsku – polski chemik, profesor nauk chemicznych, specjalizujący się w chemii analitycznej i środowiskowej. Rektor Politechniki Gdańskiej w latach 2016–2019. Studia wyższe ukończył w 1972 r. na Wydziale Chemicznym Politechniki Gdańskiej, uzyskując tytuł magistra inżyniera chemika. W 1972 r. rozpoczął pracę na Politechnice Gdańskiej, gdzie w 1978 r. obronił...
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Determination of methylcyclopentadienyl-manganese tricarbonyl in gasoline and water via ionic-liquid headspace single drop microextraction and electrothermal atomic absorption spectrometry
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Solid phase extraction with flame atomic absorption spectrometry for determination of traces of Ca, K, Mg and Na in quality control of white sugar
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Sensitive Determination of Cd in Small-Volume Samples by Miniaturized Liquid Drop Anode Atmospheric Pressure Glow Discharge Optical Emission Spectrometry
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Determination of mercury in mosses by novel cold vapor generation atmospheric pressure glow microdischarge optical emission spectrometry after multivariate optimization
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Development of direct-current, atmospheric-pressure, glow discharges generated in contact with flowing electrolyte solutions for elemental analysis by optical emission spectrometry
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Hanging drop cathode-atmospheric pressure glow discharge as a new method of sample introduction for inductively coupled plasma-optical emission spectrometry
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Functional properties of Cornelian cherry (Cornus mas L.): a comprehensive review
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Technika spektrometrii mas rozcieńczenia izotopowego (IDMS) w analityce chemicznej.
PublikacjaOpisano podstawy teoretyczne techniki spektrometrii mas rozcieńczenia izotopowego. Przedstawiono zalety i wady techniki oraz obszar jej zastosowań.
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Procedura dopuszczenia do eksploatacji maszyn do produkcji mas bitumicznych
PublikacjaW treści artykułu przedstawiono procedury postępowania przy uruchamianiu masbitumicznych. Ponadto opisano wymogi bhp na terenie wytwórni wraz z przeglą-dem aktualnym przepisów związanych z ochroną środowiska w tym odpadami pow-stającymi podczas produkcji, poziomu hałasu w środowisku maszyny i substan-cji zanieczyszczających powietrze.
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MPSs System monitoringu i obserwacji terenów portowych z wykorzystaniem bezzałogowych mobilnych platform badawczych
ProjektyProjekt realizowany w Katedra Systemów Geoinformatycznych zgodnie z porozumieniem NOR/POLNOR/MPSS/0037/2019-00 z dnia 2021-02-01
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Minimal number of periodic points for C^1 self-maps of compact simply-connected manifolds
PublikacjaNiech f będzie odwzorowaniem gładkiej zwartej i jednospójnej rozmaitości o wymiarze większym lub równym 3. W pracy zdefiniowany został topologiczny niezmiennik będący najlepszym dolnym oszacowaniem liczby punktów periodycznych w klasie gładkich odwzorowań homotopijnych z f.
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A contribution to the moss and liverwort flora of the Reberce Nature Reserve at the Przemyśl Foothills (Western Carpathians, Poland)
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Developing assumptions for the tram noise attenuation passive system using the noise maps analysis method
PublikacjaThe paper presents experimental research carried out to determine the possible actions to reduce thenoise generated by trams in a highly urbanised area. A few design strategies affecting tram ride qualityhave been presented – especially in the aspect of the acoustic phenomena. Main sources of the noisein trams were characterised. The paper includes selected results of comprehensive...
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Custom FBGs inscription using modified phase mask method with precise micro- and nano-positioning
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Landsat 8 Data as a Source of High Resolution Sea Surface Temperature Maps in the Baltic Sea
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Comparison of dry and living Sphagnum palustre moss samples in determining their biocumulative capability as biomonitoring tools
PublikacjaPorównano właściwości suchych i żyjących mchów Sphagnum palustre poprzez wyznaczenie ich zdolności biokumulacyjnych jako narzędzia przy biomonitoringu. Zastosowano dwie formy mchów w celu porównania ich wad i zalet i wybraniu najlepszej. Badania przeprowadzono na terenie zurbanizowanym w celu wyznaczenia głównych źródeł zanieczyszczeń. Przeprowadzono analizę klasterową oraz analizę głównych składowych w celu zidentyfikowania profilu...
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The Application Of A Noise Mapping Tool Deployed In Grid Infrastructure For Creating Noise Maps Of Urban Areas
PublikacjaThe concept and implementation of the system for creating dynamic noise maps in PL-Grid infrastructure are presented. The methodology of dynamic acoustical maps creating is introduced. The concept of noise mapping, based on noise source and propagation models, was developed and employed in the system. The details of incorporation of the system to the PL-Grid infrastructure are presented. The results of simulations performed by...
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Chlorinated solvents in a petrochemical wastewater treatment plant: Anassessment of their removal using self-organising maps
PublikacjaThe self-organising map approach was used to assess the efficiency of chlorinated solvent removal frompetrochemical wastewater in a refinery wastewater treatment plant. Chlorinated solvents and inorganicanions (11 variables) were determined in 72 wastewater samples, collected from three different purificationstreams. The classification of variables identified technical solvents, brine from oil desalting andrunoff sulphates as pollution...
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Voice Maps - portable, dedicated GIS for supporting street navigtion and self-dependent movement of the blind
PublikacjaThe concept and the prototype application of the system supporting the street navigation and independent, outdoor movement of the blind is presented. The system utilises the GIS database of geometric network of the pedestrian paths in the city and is capable of finding the route from the indicated source to destination. Subsequently, the system supports the movement of the blind along the found route. The information on the user's...
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The Influence of the Depth of Cut in Single-Pass Grinding on the Microstructure and Properties of the C45 Steel Surface Layer
PublikacjaThe paper contains the results of a metallographic examination and nanoindentation test conducted for the medium carbon structural steel with low content of Mn, Si, Cu, Cr, and Ni after its grinding to a depth ranging from 2 μm to 20 μm, at constant cutting speed (peripheral speed) of vs = 25 ms−1 and constant feed rate of vft = 1 m/min. Applied grinding parameters did not cause the surface layer hardening, which could generate...
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Doświadczalna i numeryczna analiza wpływu dodatkowej masy na propagację fali w pręcie
PublikacjaW pracy przedstawiono wyniki analizy numerycznej i badań eksperymentalnych mających na celu zbadanie wpływu dodatkowej masy na propagację fali wzdłuznej w pretach izotropowych.
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MARS - BAZA. warsztaty pozaziemskiej architektury ekstremalnej. Warsztaty w ramach Bałtyckiego Festiwalu Nauki
PublikacjaJak przetrwać w różnych warunkach? Czego potrzebujemy, by przeżyć, a czego, by żyć wygodnie? Poszukamy odpowiedzi na te pytania, by stanąć przed nie lada misją: wspólnie podejmiemy się największego wyzwania przyszłości - zbudujemy bazę na Marsie! Budowa schronienia, bazy, domu - troska o zaspokojenie podstawowych potrzeb towarzyszy nam od zawsze, a budowanie jest jednym z pierwszych trwałych działań ludzi, pomagającym spełnić...
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Unsupervised Learning for Biomechanical Data Using Self-organising Maps, an Approach for Temporomandibular Joint Analysis
PublikacjaWe proposed to apply a specific machine learning technique called Self-Organising Maps (SOM) to identify similarities in the performance of muscles around human temporomandibular joint (TMJ). The performance was assessed by measuring muscle activation with the use of surface electromyography (sEMG). SOM algorithm used in the study was able to find clusters of data in sEMG test results. The SOM analysis was based on processed sEMG...
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A ship domain-based model of collision risk for near-miss detection and Collision Alert Systems
PublikacjaThe paper presents a new model of ship collision risk, which utilises a ship domain concept and the related domain-based collision risk parameters. An encounter is here described by five variables representing: degree of domain violation (DDV), relative speed of the two vessels, combination of the vessels’ courses, arena violations and encounter complexity. As for the first three variables, their values can be directly computed...
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Forced vibrations in a dynamic system that is damped by a mechanism that trans-pass through its singular position
PublikacjaIn the paper, vibrations of a hybrid multibody-continuous system are investigated. For all the mechanical devices, effective damping methods are crucial in the design process. To obtain it, installation of viscous dampers or elasto-viscous elements is dominant. In the paper, an alternative method is investigated. It is based on modal disparity. To describe the method briefly, when structural damping is present in continuous systems,...
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Minimal number of periodic points of smooth boundary-preserving self-maps of simply-connected manifolds
PublikacjaLet M be a smooth compact and simply-connected manifold with simply-connected boundary ∂M, r be a fixed odd natural number. We consider f, a C1 self-map of M, preserving ∂M . Under the assumption that the dimension of M is at least 4, we define an invariant Dr(f;M,∂M) that is equal to the minimal number of r-periodic points for all maps preserving ∂M and C1-homotopic to f. As an application, we give necessary and sufficient...
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Mountain pass type periodic solutions for Euler–Lagrange equations in anisotropic Orlicz–Sobolev space
PublikacjaUsing the Mountain Pass Theorem, we establish the existence of periodic solution for Euler–Lagrange equation. Lagrangian consists of kinetic part (an anisotropic G-function), potential part and a forcing term. We consider two situations: G satisfying at infinity and globally. We give conditions on the growth of the potential near zero for both situations.
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Stereo vision with Equal Baseline Multiple Camera Set (EBMCS) for obtaining depth maps of plants
PublikacjaThis paper presents a method of improving the estimation of distances between an autonomous harvesting robot and plants with ripe fruits by using the vision system based on five cameras. The system is called Equal Baseline Multiple Camera Set (EBMCS). EBMCS has some features of a camera matrix and a camera array. EBMCS is regarded as a set of stereo cameras for estimating distances by obtaining disparity maps and depth maps. This...
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Minimization of the number of periodic points for smooth self-maps of closed simply-connected 4-manifolds
PublikacjaLet M be a smooth closed simply-connected 4-dimensional manifold, f be a smooth self-map of M with fast grow of Lefschetz numbers and r be a product of different primes. The authors calculate the invariant equal to the minimal number of r-periodic points in the smooth homotopy class of f.
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Influence of Carbon Sorbent Quantity on Breakthrough Time in Absorbent Filters for Antismog Half Mask Application
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Understanding the formation of metastable furan dication in collisions with ions
PublikacjaThis work relies on complementary theoretical and experimental studies of the processes induced by ion-furan collisions. Results of the Molecular Dynamics simulations and exploration of the energy profiles combined with coincidence mass spectrometry provide complete picture of the fragmentation of furan dication.
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Dehydrogenation in electron-induced dissociative ionization of pyridine molecule
PublikacjaThe electron-impact dissociative ionization of pyridine has been investigated using mass spectrometry. Thirty-two well-resolved mass peaks have been identified in the cation mass spectra and assigned to the most likely ionic molecular fragments. The new sixteen ionic fragments' appearance energies have been determined, and sixteen others remeasured. The total cross-section for electron-impact ionization of pyridine has been measured...
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On the coupling of hydride generation with atmospheric pressure glow discharge in contact with the flowing liquid cathode for the determination of arsenic, antimony and selenium with optical emission spectrometry
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Evaluation of the potential of Microwave Plasma–Atomic Emission Spectrometry for trace elements leaching assessment from the concrete matrix with sewage sludge ash additives
PublikacjaThe management of ash generated during the thermal utilization of sewage sludge is a significant environmental problem requiring an effective technological solution. One alternative way to dispose of sewage sludge is to bind it in concrete as a substitute for part of the aggregate. The properties of the C-S-H phase enable effective immobilization of harmful substances that sewage sludge contains. The amount of individual compounds...
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Dynamics of S-unimodal maps used in population modeling.
Dane BadawczeS-unimodal maps are maps of the interval with negative Schwarzian derivative and having only one turning point (such that the map is increasing to the left of the turning point and decreasing to the right of it). Theory of S-unimodal maps is now a well-developed branch of discrete dynamical systems, including famous Singer theorem which implies existence...
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INNOVATIVE THERMODYNAMICAL CYCLES BASED ON ENHANCEMENT MASS, MOMENTUM, ENTROPY AND ELECTRICITY TRANSPORT DUE TO SLIP, MOBILITY, TRANSPIRATION, ENTROPY AND ELECTRIC JUMPS AS WELL AS OTHER NANO-FLOWS PHENOMENA
PublikacjaIn our work, a further development of the authors model of thermo-chemical flow of fuel, air, oxygen, steam water, species, ionic and electron currents within nano channels and nano-structures of novel devices is presented. Different transport enhancement models are taken into account -among them the most important are: the velocity slip connected with complex external friction, the Darcy mobility and the Reynolds transpiration....
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The Current State-of-the-Art in the Determination of Pharmaceutical Residues in Environmental Matrices Using Hyphenated Techniques
PublikacjaSeveral thousand tons of pharmaceuticals and their transformation products (metabolites and degradation products) are introduced into the environment each year. They affect both human health and the environment, therefore, analytical procedures enabling the determination of a wide range of pharmaceuticals at trace levelswithminimal effort, time, and energy are required. Nowadays, hyphenated techniques are commonly applied in pharmaceutical...
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Emission Profiles of Volatiles during 3D Printing with ABS, ASA, Nylon, and PETG Polymer Filaments
PublikacjaIn this short communication we characterize the emission of volatile organic compounds (VOCs) from fused filament fabrication (FFF) 3D printing using four polymer materials, namely polyethylene terephthalate glycol-modified (PETG), acrylonitrile styrene acrylate (ASA), Nylon, and acrylonitrile butadiene styrene (ABS). Detailed emission profiles are obtained during thermal degradation of the polymers as a function of temperature...
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Minimal number of periodic points for smooth self-maps of two-holed 3-dimensional closed ball
PublikacjaDla ciągłego odwzorowania f przestrzeni określonej w tytule w siebie, które posiada rzeczywiste wartości własne na drugiej grupie homologii, wyznaczona została minimalna liczba punktów r-periodycznych w klasie wszystkich gładkich odwzorowań homotopijnych z f.