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Wyniki wyszukiwania dla: ion-selective electrodes · multisensor system · potenctiometric measurements · reference electrode
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Monika Wilamowska-Zawłocka dr hab. inż.
OsobyDr hab. inż. Monika WILAMOWSKA-ZAWŁOCKA jest absolwentką Wydziału Chemicznego Politechniki Gdańskiej. Studia doktoranckie ukończyła w 2011 r., następnie odbyła roczny staż na Technicznym Uniwersytecie w Darmstadt w Niemczech. Pracuje w Politechnice Gdańskiej od 2013 r., od 2019 r. na stanowisku profesora uczelni. Specjalność –materiały elektrodowe w zastosowaniu do ogniw litowo-jonowych, sodowo-jonowych, kondensatorów elektrochemicznych...
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Verification of multiband system for non-contact emissivity measurements
PublikacjaW pracy przeprowadzono weryfikację wielopasmowej pasywnej metody pomiaru emisyjności obiektu na drodze eksperymentalnej. W oparciu o zrealizowane stanowisko pomiarowe dokonano pomiarów emisyjności wybranych obiektów. Uzyskano dobrą zgodność wyników pomiarów z wynikami wcześniejszej komputerowej analizy systemu. Potwierdziło to przydatność wielopasmowej metody do pomiaru emisyjności w warunkach roboczych.
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Camera-based Automatic System for Tool Measurements and Recognition
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Pitting corrosion characterization by electrochemical noise measurements on asymmetric electrodes. [DOI 10.1007/s10008-008-0643-y]
PublikacjaObecność korozji wżerowej może być wykryta na podstawie występowania charakterystycznych przebiegów prądu płynącego między dwiema elektrodami, których wyprowadzenia są zwarte. Autorzy proponują nową metodę, która zachowuje informacje o stałej czasowej tych charakterystycznych dla procesów wżerowania przebiegów. Metoda została zastosowana do analizy szumów występujących podczas korozji stali 0H18N9 pod wpływem 1M roztworu FeCl3...
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Optical Bubble Microflow Meter for Continuous Measurements in a Closed System
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Bacterial strains colonizing the sensor electrodes of a continuous glucose monitoring system in children with diabetes
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Corporate social responsibility in reference to environmental statements within EMAS system in small and medium enterprises
PublikacjaAccording to the corporate social responsibility concept, organisations should apply any mechanisms available supporting their business actions contributing i.e. to the improvement of natural environment. Among them is EMAS eco-management and audit scheme. The prove of its implementation is environmental statement and entering the organisation into a national EMAS register. The aim of the statement is informing the society and...
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Harmonic analysis of the current of an electric system simulating the electrode process in conditions of linearly changing potential
PublikacjaAnalizowany był prąd elektrycznego modelu symulującego pierwszorzędową reakcję elektrodową zachodzącą w warunkach liniowo zmieniającego się potencjału z nałożonym sygnałem sinusoidalnym. Pokazano, że transformacja Fouriera nie odzwierciedla zmian amplitudy składowych komponentów w funkcji potencjału. Także matematycznie wykazano, że zastosowanie transformacji Gabora do analizy spektralnej pozwala uzyskać poprawną dekompozycję częstotliwościową....
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The influence of the geographic positioning system error on the quality of ship magnetic signature reproduction based on measurements in sea conditions
PublikacjaIn previous studies, the authors performed the magnetic signature reconstruction of the marine ship Zodiak as part of the measurement campaign focused on recording magnetic data and the relative position of a ship during its passage over a magnetometer immersed on the testing ground. A high degree of representation of the magnetic signature was obtained. However, the recorded measurement data revealed new patterns of the multidipole model...
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Lower rim substituted tert-butylcalix[4]arenes. Part 10. New Pb(II)-selective electrodes based on tetrasubstituted calix[4]arenes amides
PublikacjaOpracowano elektrody selektywne na jony Pb(II) oparte na lipofilowych tetrapodstawionych amidowych pochodnych kaliks[4] arenu. Charakterystyki elektrod mają nachylenie nernstowskie w szerokim zakresie stężeń 10 (-1.3) do 10 (-7.2).
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Electrochemistry from first-principles in the grand canonical ensemble
PublikacjaProgress in electrochemical technologies, such as automotive batteries, supercapacitors, and fuel cells, depends greatly on developing improved charged interfaces between electrodes and electrolytes. The rational development of such interfaces can benefit from the atomistic understanding of the materials involved by first-principles quantum mechanical simulations with Density Functional Theory (DFT). However, such simulations are...
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Measurements of drive system properties of the "Magnetic SpeedLine" ultra-fast robot prototype for IML labeling
Dane BadawczeTests of the drive system of the ultra-fast robot "SpeedLine magnetic" for labeling with the IML method were carried out in order to analyze the influence of the operating parameters of the drive system on the correctness and quality of the drive system.
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Innovative mobile method to determine railway track axis position in global coordinate system using position measurements performed with GNSS and fixed base of the measuring vehicle
PublikacjaThe shape of the railway track axis and its position in the global coordinate system are essential when defining design parameters of the railway. Correct reconstruction of these quantities is vital for both verifying the compliance of real track parameters with the design and for diagnosing, as all track deformations can also be defined as deviations of real parameters from their design values. The measurements of quantities related...
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Improvement of time difference of arrival measurements resolution by using fractional delay filters in a direct sequence-code division multiple access radionavigation system
PublikacjaThis study presents a method of improving time measurements resolution in a direct sequence-code division multiple access receiver by using a fine code tracking loop based on fractional delay filtering of a despreading sequence. It briefly describes the structure of a generic digital code tracking loop and the proposed modification which allows to measure time difference of arrival values with the subsample resolution, together...
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Selected results of measurements carried out in a ship power station with two generators working in parallel with the use of the NI PXIe-1062Q based measurement system
Dane BadawczeThe presented dataset is part of research focusing on the assessment of metrological properties of the instrument, Estimator/Analyzer (A/E v.2), developed and made at the Faculty of Electrical Engineering, Department of Marine Electrical Power Engineering, of Gdynia Maritime University. The attached data set contains the results of measurements made...
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Chromogenic derivatives of new bis(phenylhydrazono-1H-tetrazol-5-yl-acetonitriles) - synthesis and properties
PublikacjaDerivatives of bis(phenylhydrazono-1H-tetrazol-5-yl-acetonitriles) with oxygen and sulphur atoms in the structure of aliphatic chains were successfully synthesised. The correlation between the ligand structure and its complexation properties was investigated by absorption spectroscopy. The formation of complexes of presented compounds with metal cations (Cu2+, Ni2+, Zn2+, Co2+, Fe2+ and Pb2+) was studied. Ligands 5-8 were additionally...
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Study on the Positioning Accuracy of the GNSS/INS System Supported by the RTK Receiver for Railway Measurements
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Measurements of power supply system properties of "Magnetic SpeedLine" ultra-fast robot prototype for IML labeling
Dane BadawczeTests of the power supply system of "SpeedLine magnetic" ultra-fast industrial robot for IML labeling were carried out to analyze the effect of the active power filter (APF) parameters on the power quality. at the target duty cycle. Tests were performed with the target duty cycle. Linear synchronous motors with permanent magnets were used to drive...
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Techniques of interference reduction in probe system for wafer level noise measurements of submicron semiconductor devices.
PublikacjaPrzedstawiono skrótowo system do ostrzowych pomiarów szumów struktur submikronowych. Znaczny wpływ na pomiary ostrzowe mają zakłócenia i szumy własne systemu, zwłaszcza zakłócenia o wysokim poziomie wpraowadzane przez ostrza (fluktuacje rezystancji styków ostrza do struktury powodowane przez wibracje i udary mechaniczne w środowisku pomiarowym)i środowisko elektromagnetyczne. Zakłócenia okresowe powodowane przez wibracje i pola...
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Relieving the Measuring System of the Trailer for Tyre/Road Rolling Resistance Measurements from the Inertia Force
PublikacjaIn the article the principle of measuring of tyre/road rolling resistance tyres in road conditions applied in a special measuring trailer is presented. This trailer was built in Faculty of Mechanical Engineering at Gdansk University of Technology. The construction of two special devices used in this trailer was discussed. These devices eliminate the influence of some chosen confounding measurements factors such as: the inertia...
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The computational methods in the development of a novel multianalyte calibration technique for potentiometric integrated sensors systems
PublikacjaIn recent years, integration and miniaturization of ion-selective electrodes (ISEs) have brought many benefits resulting in the possibility of simultaneous determination of the ions concentration in small volume samples. One of the key problems related to the preparation of potentiometric integrated sensors systems (PISSs) is a calibration procedure due to the necessity to calibrate each particular sensor separately. The main aim...
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Tomasz Wąsowicz dr hab.
OsobyAbsolwent Technikum Elektrycznego w Słupsku (1997 rok) oraz Wydziału Matematyki, Fizyki i Informatyki Uniwersytetu Gdańskiego (2002 rok). W 2006 roku obronił dysertację doktorską z fizyki na WMFiI UG. Pracując już w PG, w 2018 roku uzyskał habilitację. W pierwszym okresie prace badawcze Tomasza Wąsowicza miały związek ze spektroskopią atomową wysokiej zdolności rozdzielczej i koncentrowały się na pomiarze i analizie prawdopodobieństw...
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Experimental verification of multiband system of non coantact temperature measurements. IV Workshop on Atomic and Molecular Physics.
PublikacjaW pracy przedstawiono wielopasmowy optoelektroniczny system do bezkontaktowych pomiarów temperatury wykonane za jego pomocą w zakresie od 250 do 390 stopni Celsjusza. Przeprowadzono dyskusję błędów pomiarowych i porównano otrzymane rezultaty z wynikami modelowania komputerowego.
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A miniaturized atmospheric pressure glow microdischarge system generated in contact with a hanging drop electrode – a new approach to spectrochemical analysis of liquid microsamples
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Flexible dye-sensitized solar cells based on Ti/TiO2 nanotubes photoanode and Pt-free and TCO-free counter electrode system
PublikacjaFlexible dye-sensitized solar cells (DSSCs) are getting more attention compared to standard glass covered DSSCs due to their unique commercial applications (e.g. tents or sail surfaces) and the possibility of rolling up into a small, portable device. In this work, titania nanotubes (TiO2 NT) modified with titania nanoparticles (TiO2 NP) were photoelectrochemically characterized as an anode for flexible dye-sensitized solar cells....
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The influence of chitosan hydrogel coating on different redox probes kinetics
Dane BadawczeThis dataset contains cyclic voltammetry studies of three redox probes: 1 mM K3[Fe(CN)6], [K4Fe(CN)6], C12H14FeO2, and [Ru(NH3)6]Cl2 dissolved in 0.1 M KCl or PBS as the primary electrolyte. The studies are made for glassy carbon electrode (GC) and glassy carbon electrode covered with thin chitosan hydrogel membrane (C2A2). Cyclic voltammograms were...
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Measurements of the mechanical system properties of "SpeedLine magnetic" ultra-fast robot prototype for IML labeling
Dane BadawczeThe mechanical system tests of the high-speed IML labeling robot "SpeedLine Magnetic" were carried out in order to analyze the effects of the drive system's operating parameters on vibration and noise.
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Partial PLA composite surface activation by femtosecond laser ablation
Dane BadawczeThe dataset contains the studies on electrochemical activity of PLA composite (commercially available CB-PLA Protopasta), which was 3D printed in a form of 1x1cm electrodes. The electrodes were submitted to femtosecond laser ablation, etching a certain % of the electrochemically-exposed electrode size. The % value is in the name of each file. The goal...
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Influence of Ni ion site occupancy on laser induced third harmonic generation (THG) studies in Li2SO4–MgO–P2O5 amorphous system
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Locust bean gum as green and water-soluble binder for LiFePO4 and Li4Ti5O12 electrodes
PublikacjaLocust Bean Gum (LBG, carob bean gum) was investigated as an environmentally friendly, natural, and water-soluble binder for cathode (LFP) and anode (LTO) in lithium-ion batteries (Li-ion). For the frst time, we show LBG as an electrode binder and compare to those of the most popular aqueous (CMC) and conventional (PVDF) binders. The electrodes were characterized using TGA/DSC, the galvanostatic charge–discharge cycle test, cyclic...
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Study of Metrological Properties of Voltammetric Electrodes in the Time Domain
PublikacjaMetrological properties of voltammetric electrodes, in the situation where on their surface an electrochemical reaction of oxidizing/reduction takes place, were analyzed in this chapter. The properties of electrodes on which a reaction controlled by ion transport process takes place were taken into consideration. Also, it was analyzed how the electrode’s shape and the voltage polarizing the electrode influence this electrode’s...
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Surface activation by cyclic polarization in 1M HCl and its effects on the electrochemical response of CB-PLA 3D printed electrodes
Dane BadawczeThe dataset contains the electrochemical studies performed for surface activation of the CB-PLA 3D printed electrodes by electrolysis in 1M HCl solution. The studies were performed after treatment at different polarization ranges, as labeled in subfolder names. For each electrode the consecutive studies describe different samples, as labeled in subfolders:...
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Electrodes array for contactless ECG measurement of a bathing person - a sensitivity analysis
PublikacjaAn applicability of a remote (contactless) electrocardiogram (ECG) measurements in a bathtub is presented in the paper. Possibility of ECG measurements in shallowly filled tube with a water was examined. A bathing person was, both, sitting and lying during experiments performed. The problem became non-trivial when the bathing person was moving in reference to a fixed set of electrodes and located at the longer walls of the bathtub....
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Potentiometric taste sensor application for liquid product taste estimation
PublikacjaThe principles of taste sense and kinds of tastes (sweet, salty, sour, bitter, umami and fat) have been described. Food quality estimation by taste sense: organoleptic testing and sensory analysis has been presented. The principle of operation of potentiometric sensor composed of several Ion Selective Electrodes or All Solid State Electrodes with polymeric membranes and macromolecular chemical compounds sensitive to substances...
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Calix[4]arenes appended with thioamide moieties as powerful tool for heavy metals recognition
PublikacjaSelectivity of new thioamide derivatives was assessed using those ligands as sensor materials in ion-selective membrane electrodes and tested towards Pb2+ - selectivity. The influence of the nature of the thioamide function (linear, branched or cyclic substituents) on their ionophoric properties was investigated. Electrodes based on cyclic thioamide moieties are promising analytical tools for monitoring Pb2+ concentration in natural...
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Performance measurements and optimization of visualization of routes traveled in the distributed dispatcher and teleinformation system for visualization of multimedia data for the Border Guard
PublikacjaMonitoring of country maritime border is an important task of the Border Guard. This activity can be enhanced with the use of the technology enabling gathering information from distributed sources, processing of that information and its visualization. The system presented in the paper is an advancement of the previously developed distributed map data exchange system. The added functionality allows to supplement the map data with...
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TASTE QUALITIES ESTIMATION BY TASTE SENSE AND ELECTROCHEMICAL SENSORS
PublikacjaThe principles of taste sense and kinds of tastes (sweet, salty, sour, bitter, umami and fat) have been described. Food quality estimation by taste sense: organoleptic testing and sensory analysis has been presented. The principle of operation of potentiom etric sensor composed of several Ion Selective Electrodes or All Solid State Electrodes with polymeric membranes and macromolecular chemical compounds sensitive to substances...
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New bis(azobenzocrown)s with dodecylmethylmalonyl linkers as ionophores for sodium selective potentiometric sensors
PublikacjaNovel biscrowns 1 and 2 were synthesized from 13-membered azobenzocrown ethers containing bromoalkylenoxy chains in para position relative to the azo group. The synthesized diester molecules are dodecylmethylmalonic acid derivatives differing by the linker length. The synthesized compounds have the potential of being used as sodium ionophores in ion-selective electrodes. They were characterized and used as ionophores in classic...
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Lower rim substituted p-tert-butyl-calix[4]arene. Part 17. synthesis, extractive and ionophoric properties of p-tert-butylcalix[4]arene appended with hydroxamix acid moieties
PublikacjaThe synthesis and characterization of four p-tert-butylcalix[4]arene-hydroxamic acidc are reported. The dependence of the metal ion binding, assessed by liquid extraction of the metal nitrates from water into dichloromethane in individual and competitive experiments, on the ligand structure, is presented. The results showed that those ligands could be successfully used in separation process of trnasition and heavy metals often...
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Partial PLA composite surface activation by femtosecond laser ablation
Dane BadawczeThe dataset contains the studies on electrochemical activity of PLA composite (commercially available CB-PLA Protopasta), which was 3D printed in a form of 1x1cm electrodes. The electrodes were submitted to femtosecond laser ablation operating with different parameters. These were: gas atmosphere (He or air, data in different subfolders), the percentage...
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The cyclic voltammetry studies of CB-PLA electrode after surface activation by electrolysis in 1M NaOH
Dane BadawczeThe dataset contains the electrochemical studies performed for surface activation of the CB-PLA 3D printed electrodes by electrolysis in 1M NaOH solution. The studies were performed after treatment at an anodic overpotential of 1V, found to be optimal for surface activation. The measurements were carried out with cyclic voltammetry (CV) under different...
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Tuning Electrochemical Performance by Microstructural Optimization of the Nanocrystalline Functional Oxygen Electrode Layer for Solid Oxide Cells
PublikacjaFurther development of solid oxide fuel cell (SOFC) oxygen electrodes can be achieved through improvements in oxygen electrode design by microstructure miniaturisation alongside nanomaterials implementation. In this work, improved electrochemical performance of an La0.6Sr0.4Co0.2Fe0.8O3-d (LSCF) cathode was achieved by the controlled modification of the La0.6Sr0.4CoO3-d (LSC) nanocrystalline interlayer introduced between a porous...
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Influence of the boron doping level on the electrochemical oxidation of the azo dyes at Si/BDD thin film electrodes
PublikacjaIn this study the efficiency of electrochemical oxidation of aromatic pollutants, such as reactive dyes, at boron-doped diamond on silicon (Si/BDD) electrodes was investigated. The level of [B]/[C] ratio which is effective for the degradation and mineralization of selected aromatic pollutants, and the impact of [B]/[C] ratio on the crystalline structure, layer conductivity and relative sp3/sp2 coefficient of a BDD electrode were...
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Application of electrochemical impedance spectroscopy to monitoring discharging process of nickel/metal hydride battery.
PublikacjaThis paper presents the possibility of applying impedance analysis to cell diagnostics. In order to obtain characteristic curves of both electrodes of a NiMH battery simultaneously, a reference electrode was added into the circuit. The authors analysed the cell under three cases, i.e. when its properties are determined only by the state of the positive electrode, only by the state of the negative electrode, or when both electrodes...
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Inhibition of impurities formation in the synthesis of N-alkyltheobromines stimulated by microwave irradiation. Cationic and anionic response of membrane electrodes
PublikacjaN-Alkyltheobromine (1-9) derivatives were obtained by reacting theobromine with appropriate alkyl halide under microwave irradiation at 100-150 W and by conventional synthesis. Formation of by-products of oxygen atom alkylation and 1-N-alkyltheobromine ring opening were considered. The presented compounds 1-5 have been studied as ion carriers in ion-selective membrane electrodes. Selectivity of these membranes was studied towards...
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Electrohydrodynamic Flow Patterns in a Narrow Electrostatic Precipitator with Longitudinal Wire Electrode for Various Electrode Geometries
PublikacjaRecently narrow electrostatic precipitators (ESPs) have become a subject of interest because of their possible application in diesel engines. In this paper results of 2-dimensional (2D) Particle Image Velocimetry (PIV) measurements of the flow patterns in a narrow ESP for a various electrode geometries are presented. The PIV measurements were carried out in the observation plane that is perpendicular to the ESP duct. The ESP was...
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The corrosion studies of 3,4,5-trihydroxybenzoic acid as an effective corrosion inhibitor of low alloy steel
Dane BadawczeThe dataset contains the electrochemical studies evaluating if gallic acid is a corrosion inhibitor for low alloy steel. Three measurements were carried out each case; corrosion potential (label ecorr), electrochemical impedance spectroscopy (label eis) and cyclic polarization (label cp). The measurements were carried out in sodium chloride, acidified...
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Wybrane aspekty oceny jakości produktów żywnościowych
PublikacjaPrzedstawiono wybrane aspekty oceny jakości produk tów żywnościo- wych: pojęcie jakości, wybrane metody oceny jakości ze szczególnym uwzględ- nieniem sztucznych potencjometrycznych sensorów sma ku składających się z szeregu elektrod typu ISE (Ion Selective Electrodes ) oraz ASSE (All Solid State Electrodes). Omówiono działanie sztucznych sensorów smaku. Przedstawiono 10 potencjometryczny sensor wprowadzony do obrotu hand lowego....
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In-situ monitoring of electropolymerization processes at boron-doped diamond electrodes by Mach-Zehnder interferometer
PublikacjaIn this work, the Mach-Zehnder interferometer was designed to monitor the electrochemical processes conducted at boron-doped diamond electrode surface. The diamond electrodes were synthesized via Microwave Plasma-Assisted Chemical Vapor Deposition on optical grade quartz glass. The achieved transmittance in working are of diamond electrodes reached 55 %. A cage system-based Mach-Zehnder interferometer was used which allowed the...
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Influence of titanium layer on counter electrode on electrical parameters of DSSC
PublikacjaIn this paper the influence of the Ti layer thickness at counter-electrode on electrical parameters of DSSCs was examined. The transparent conductive oxide – less (TCO-less) counter electrodes (CE) with titanium layers and platinum as catalyst on Bk7 glass were prepared. Thin metallic films were deposited by means of magnetron sputtering (titanium) and Pulsed Laser Deposition (platinum). The counter electrode with Pt layer on Fluorine...